Lithium fluoride washing and filtering device

By designing a lithium fluoride washing and filtration device with extrusion and descraping components, solid-liquid separation is achieved by using hydraulically driven extrusion plates and sealing plates. This solves the problem of inconvenient solid material cleaning in existing devices and improves separation efficiency and convenience.

CN224194256UActive Publication Date: 2026-05-05INSTITUTE OF APPLIED CHEMISTRY JIANGXI ACADEMY OF SCIENCES +2
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Patent Information

Authority / Receiving Office
CN · China
Patent Type
Utility models(China)
Current Assignee / Owner
INSTITUTE OF APPLIED CHEMISTRY JIANGXI ACADEMY OF SCIENCES
Filing Date
2025-05-09
Publication Date
2026-05-05

AI Technical Summary

Technical Problem

Existing lithium fluoride solid-liquid separation devices are not convenient for cleaning solid materials, which affects production efficiency.

Method used

A lithium fluoride washing and filtration device including an extrusion assembly and a desiccant assembly was designed. The device uses a hydraulic cylinder to drive the extrusion plate and the sealing plate to achieve solid-liquid separation. The liquid material is separated by pressure applied by the extrusion plate, and the solid material is ejected after the sealing is released by the desiccant assembly.

Benefits of technology

Rapid solid-liquid separation of lithium fluoride slurry was achieved, improving production efficiency and convenience, and simplifying the cleaning process of solid materials.

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Abstract

The utility model relates to the technical field of lithium fluoride, in particular to a lithium fluoride washing and filtering device which is characterized in that when the lithium fluoride washing and filtering device is used, a stripping assembly seals the left end of a box body, then materials are injected into the box body through a feeding pipe, a valve is closed, and then an extrusion assembly is operated to extrude the materials, so that the liquid materials are discharged through a filter screen; the solid material stays in the box body, then the stripping assembly relieves sealing of the left end of the box body, the extrusion assembly is operated to eject the solid material staying in the box body out of the box body, and rapid solid-liquid separation of the material is achieved; comprising a box body, a filter screen and supporting legs, the filter screen is arranged at the front end of the box body, the four corners of the bottom end of the box body are each provided with a set of supporting legs, a feeding pipe is arranged at the rear end of the box body, a valve is arranged on the feeding pipe, the device further comprises an extrusion assembly and a stripping assembly, the extrusion assembly is arranged in the box body, and the stripping assembly is arranged at the left end of the box body.
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Description

Technical Field

[0001] This utility model relates to the technical field of lithium fluoride, and in particular to a lithium fluoride washing and filtration device. Background Technology

[0002] Lithium-ion batteries, with their advantages of high energy density, high power density, long cycle life, low self-discharge, and high performance-price ratio, have become the primary choice for rechargeable power sources in today's portable electronic products. The electrolyte is made by dissolving electrolyte salts in a mixed organic solvent. Inorganic electrolytes include lithium perchlorate (used only in primary lithium-ion batteries), lithium tetrafluoroborate, lithium hexafluoroarsenate, and lithium hexafluorophosphate. Among these, lithium tetrafluoroborate and lithium hexafluorophosphate are the most commonly used, while lithium fluoride is the main raw material for the production of lithium tetrafluoroborate and lithium hexafluorophosphate. Currently, the common method for synthesizing battery-grade lithium fluoride is to directly react hydrofluoric acid with a suspension of lithium carbonate and water (or a lithium bicarbonate solution) to obtain lithium fluoride. The main drawback of this method is that the lithium fluoride slurry exhibits severe agglomeration during drying, which affects the screening process and consequently the production quality of lithium tetrafluoroborate and lithium hexafluorophosphate. Some existing lithium fluoride solid-liquid separation devices require solid-liquid separation of the lithium fluoride slurry during processing because the slurry contains solid particles.

[0003] In the prior art, publication number CN221267369U includes: an outer cylinder, a cover, and a liquid injection pipe. The outer cylinder is used to carry lithium fluoride, thereby performing solid-liquid separation of lithium fluoride. The solid-liquid separation mechanism includes a separation cylinder with a filter screen and separation holes. When lithium fluoride enters the interior of the outer cylinder, it is filtered through the separation holes and the filter screen, thereby achieving solid-liquid separation of lithium fluoride. This lithium fluoride solid-liquid separation device, through the solid-liquid separation mechanism, can perform solid-liquid separation of lithium fluoride slurry, thus facilitating subsequent processing of lithium fluoride slurry. The solid-liquid separation mechanism, through the extrusion mechanism, can extrude the lithium fluoride slurry, thereby accelerating the efficiency of solid-liquid separation of lithium fluoride slurry through extrusion.

[0004] During use, it was found that the above device can achieve solid-liquid separation, but the solid remains in the separation cylinder and needs to be cleaned with other tools, which is not very convenient. Utility Model Content

[0005] To solve the above-mentioned technical problems, this utility model provides a lithium fluoride washing and filtration device.

[0006] This utility model discloses a lithium fluoride washing and filtering device, comprising a housing, a filter screen, and support legs. The filter screen is located at the front end of the housing, and a set of support legs is located at each of the four corners of the bottom end of the housing. A feed pipe with a valve is located at the rear end of the housing. The device also includes a squeezing assembly and a descrambling assembly. The squeezing assembly is located inside the housing, and the descrambling assembly is located at the left end of the housing. In use, the descrambling assembly seals the left end of the housing. Then, material is injected into the housing through the feed pipe, the valve is closed, and the squeezing assembly is operated to squeeze the material, causing the liquid material to pass through the filter screen and be discharged, while the solid material remains inside the housing. The descrambling assembly then releases the seal on the left end of the housing, and the squeezing assembly is operated to push the solid material remaining inside the housing out of the housing, achieving rapid solid-liquid separation.

[0007] Preferably, the extrusion assembly includes a first hydraulic cylinder, an extrusion plate, guide rods, and a limiting plate. The first hydraulic cylinder is located at the right end of the housing. The left moving end of the first hydraulic cylinder extends into the housing and is connected to one end of the extrusion plate. The extrusion plate is slidably and sealed inside the housing. Multiple guide rods are provided on the extrusion plate, and each guide rod is slidably connected. A limiting plate is provided at the end of each guide rod away from the extrusion plate. When the first hydraulic cylinder is activated, it extends, thereby pressurizing the material inside the housing under the guidance of the multiple guide rods, thus improving the solid-liquid separation efficiency.

[0008] Preferably, the unloading assembly includes a vertical plate, a horizontal plate, a guide bar, a lifting plate, a sealing plate, a second hydraulic cylinder, and a connecting plate. Two sets of vertical plates are installed at the top of the housing. A set of horizontal plates is installed at the outer ends of the two sets of vertical plates and at the front and rear ends of the housing. A guide bar is installed between the two sets of horizontal plates. A lifting plate is slidably installed on each guide bar. One end of each lifting plate is connected to the right end of the sealing plate. A second hydraulic cylinder is installed at the top of the housing. A connecting plate is installed at the top moving end of the second hydraulic cylinder, and the bottom end of the connecting plate is connected to the top of the sealing plate. During solid-liquid separation, the second hydraulic cylinder is shortened, causing the connecting plate to lower the sealing plate under the guidance of the lifting plate and the guide bar. The sealing plate seals the left end of the housing. When it is necessary to discharge the solid material inside the housing, the second hydraulic cylinder is extended, releasing the seal on the left end of the housing. The first hydraulic cylinder is extended, causing the extrusion plate to discharge the solid material inside the housing.

[0009] Preferably, it also includes a U-shaped clamping plate, a shaft pin, a lead screw, and a wing nut. The bottom end of the sealing plate is provided with a U-shaped clamping plate, and the bottom end of the housing is provided with a shaft pin. The lead screw is hinged to the bottom end of the housing through the shaft pin, and the lead screw is threadedly connected to the wing nut. The sealing plate seals the left end of the housing. The operating lead screw enters the inside of the U-shaped clamping plate, and the wing nut is rotated, so that the wing nut is pressed against the U-shaped clamping plate to seal and reinforce the sealing plate.

[0010] Preferably, it also includes a base, with a base provided at the bottom of each set of legs; multiple sets of legs and multiple sets of bases work together to provide stable support for the equipment and improve stability.

[0011] Preferably, it also includes a flow guide channel, which is installed at the front end of the box; liquid materials pass through the filter screen and are guided through the flow guide channel, improving convenience.

[0012] Preferably, the filter screen is made of stainless steel.

[0013] Compared with the prior art, the beneficial effects of this utility model are as follows: In use, the unloading component seals the left end of the box, then the material is injected into the box through the feed pipe, the valve is closed, and then the extrusion component is operated to extrude the material, so that the liquid material is discharged through the filter screen and the solid material remains inside the box. Then the unloading component releases the seal on the left end of the box, and the extrusion component is operated to push the solid material remaining inside the box out of the box, thereby realizing rapid solid-liquid separation of the material. Attached Figure Description

[0014] Figure 1 This is a schematic diagram of the first isometric structure of this utility model;

[0015] Figure 2 This is a schematic diagram of the second isometric structure of this utility model;

[0016] Figure 3 yes Figure 2 A partially enlarged structural diagram of section A in the middle;

[0017] Figure 4 This is an exploded structural diagram of the present invention;

[0018] Figure 5 This is an enlarged structural diagram of the No. 1 hydraulic cylinder and the extrusion plate, etc.

[0019] The following are labels in the attached diagram: 1. Housing; 2. Filter screen; 3. Hydraulic cylinder No. 1; 4. Extrusion plate; 5. Smooth rod; 6. Limiting plate; 7. Vertical plate; 8. Horizontal plate; 9. Smooth bar; 10. Lifting plate; 11. Sealing plate; 12. Hydraulic cylinder No. 2; 13. Connecting plate; 14. U-shaped clamping plate; 15. Shaft pin; 16. Lead screw; 17. Wing nut; 18. Base; 20. Guide channel; 21. Support leg. Detailed Implementation

[0020] To facilitate understanding of this utility model, a more complete description will be given below with reference to the accompanying drawings. This utility model can be implemented in many different forms and is not limited to the embodiments described herein. Rather, these embodiments are provided to make the disclosure of this utility model more thorough and complete.

[0021] Example 1

[0022] like Figures 1 to 5 As shown, a lithium fluoride washing and filtering device of the present invention includes a housing 1, a filter screen 2 and support legs 21. The filter screen 2 is provided at the front end of the housing 1, and a set of support legs 21 is provided at the four corners of the bottom end of the housing 1. A feed pipe is provided at the rear end of the housing 1, and a valve is provided on the feed pipe. It also includes a squeezing component and a descrambling component. The squeezing component is provided inside the housing 1, and the descrambling component is provided at the left end of the housing 1.

[0023] like Figure 4 and Figure 5 As shown, the extrusion assembly includes a first hydraulic cylinder 3, an extrusion plate 4, a smooth rod 5, and a limiting plate 6. The first hydraulic cylinder 3 is provided at the right end of the housing 1. The left moving end of the first hydraulic cylinder 3 extends into the housing 1 and is connected to one end of the extrusion plate 4. The extrusion plate 4 is slidably and sealed inside the housing 1. Multiple sets of smooth rods 5 are provided on the extrusion plate 4. All smooth rods 5 are slidably connected. A set of limiting plates 6 is provided at the end of the smooth rod 5 away from the extrusion plate 4.

[0024] like Figure 1 , Figure 2 and Figure 3 As shown, the unloading assembly includes a vertical plate 7, a horizontal plate 8, a guide bar 9, a lifting plate 10, a sealing plate 11, a second hydraulic cylinder 12, and a connecting plate 13. The top of the box body 1 is provided with two sets of vertical plates 7. The outer ends of the two sets of vertical plates 7 and the front and rear ends of the box body 1 are respectively provided with a set of horizontal plates 8. A guide bar 9 is provided between the two sets of horizontal plates 8. A lifting plate 10 is slidably provided on each set of guide bars 9. One end of each set of lifting plates 10 is connected to the right end of the sealing plate 11. The top of the box body 1 is provided with a second hydraulic cylinder 12. The top moving end of the second hydraulic cylinder 12 is provided with a connecting plate 13. The bottom end of the connecting plate 13 is connected to the top end of the sealing plate 11.

[0025] In this embodiment, during solid-liquid separation, the second hydraulic cylinder 12 is shortened, causing the connecting plate 13 to lower the sealing plate 11 under the guidance of the lifting plate 10 and the light rod 9. The sealing plate 11 seals the left end of the box 1. Then, the material is injected into the box 1 through the feed pipe. The valve is closed, and the first hydraulic cylinder 3 is extended, causing the extrusion plate 4 to pressurize the material inside the box 1 under the guidance of multiple light rods 5. The liquid material is discharged through the filter screen 2, while the solid material remains inside the box 1. The second hydraulic cylinder 12 is extended, causing the sealing plate 11 to release the seal on the left end of the box 1. The first hydraulic cylinder 3 is extended, causing the extrusion plate 4 to discharge the solid material inside the box 1.

[0026] Example 2

[0027] like Figures 1 to 5As shown, a lithium fluoride washing and filtering device of the present invention includes a housing 1, a filter screen 2 and support legs 21. The filter screen 2 is provided at the front end of the housing 1, and a set of support legs 21 is provided at the four corners of the bottom end of the housing 1. A feed pipe is provided at the rear end of the housing 1, and a valve is provided on the feed pipe. It also includes a squeezing component and a descrambling component. The squeezing component is provided inside the housing 1, and the descrambling component is provided at the left end of the housing 1.

[0028] like Figure 4 and Figure 5 As shown, the extrusion assembly includes a first hydraulic cylinder 3, an extrusion plate 4, a smooth rod 5, and a limiting plate 6. The first hydraulic cylinder 3 is provided at the right end of the housing 1. The left moving end of the first hydraulic cylinder 3 extends into the housing 1 and is connected to one end of the extrusion plate 4. The extrusion plate 4 is slidably and sealed inside the housing 1. Multiple sets of smooth rods 5 are provided on the extrusion plate 4. All smooth rods 5 are slidably connected. A set of limiting plates 6 is provided at the end of the smooth rod 5 away from the extrusion plate 4.

[0029] like Figure 1 , Figure 2 and Figure 3 As shown, the unloading assembly includes a vertical plate 7, a horizontal plate 8, a light bar 9, a lifting plate 10, a sealing plate 11, a second hydraulic cylinder 12, and a connecting plate 13. The top of the box 1 is provided with two sets of vertical plates 7. The outer ends of the two sets of vertical plates 7 and the front and rear ends of the box 1 are respectively provided with a set of horizontal plates 8. A light bar 9 is provided between the two sets of horizontal plates 8. A lifting plate 10 is slidably provided on each set of light bars 9. One end of each set of lifting plates 10 is connected to the right end of the sealing plate 11. The top of the box 1 is provided with a second hydraulic cylinder 12. The top moving end of the second hydraulic cylinder 12 is provided with a connecting plate 13. The bottom end of the connecting plate 13 is connected to the top of the sealing plate 11.

[0030] like Figure 2 and Figure 3 As shown, it also includes a U-shaped clamping plate 14, a shaft pin 15, a lead screw 16 and a wing nut 17. The bottom end of the sealing plate 11 is provided with a U-shaped clamping plate 14, the bottom end of the housing 1 is provided with a shaft pin 15, the lead screw 16 is hinged to the bottom end of the housing 1 through the shaft pin 15, and the lead screw 16 is threadedly connected to the wing nut 17.

[0031] In this embodiment, during solid-liquid separation, the second hydraulic cylinder 12 is shortened, causing the connecting plate 13 to lower the sealing plate 11 under the guidance of the lifting plate 10 and the guide rod 9. The sealing plate 11 seals the left end of the box 1. The screw 16 is inserted into the inside of the U-shaped clamping plate 14, and the wing nut 17 is rotated, causing the wing nut 17 to press against the U-shaped clamping plate 14, thus sealing and reinforcing the sealing plate 11. Then, the material is injected into the box 1 through the feed pipe, the valve is closed, and the first hydraulic cylinder 3 is extended, causing the extrusion plate 4 to pressurize the material inside the box 1 under the guidance of multiple sets of guide rods 5. The liquid material is discharged through the filter screen 2, and the solid material remains inside the box 1. The second hydraulic cylinder 12 is extended, causing the sealing plate 11 to release the seal on the left end of the box 1. The first hydraulic cylinder 3 is extended, causing the extrusion plate 4 to discharge the solid material inside the box 1.

[0032] The filter screen 2, hydraulic cylinder 3, extrusion plate 4, and hydraulic cylinder 12 of the lithium fluoride washing and filtration device of this utility model are commercially available. Technical personnel in this industry only need to install and operate them according to the accompanying instruction manual, without requiring any creative work from those skilled in the art.

[0033] The above description is only a preferred embodiment of the present utility model. It should be noted that for those skilled in the art, several improvements and modifications can be made without departing from the technical principles of the present utility model, and these improvements and modifications should also be considered within the protection scope of the present utility model.

Claims

1. A lithium fluoride washing and filtering device, comprising a housing (1), a filter screen (2), and support legs (21), wherein the filter screen (2) is provided at the front end of the housing (1), a set of support legs (21) is provided at each of the four corners of the bottom end of the housing (1), and a feed pipe is provided at the rear end of the housing (1), and a valve is provided on the feed pipe, characterized in that, It also includes an extrusion assembly and a stripping assembly. The extrusion assembly is provided inside the housing (1), and the stripping assembly is provided at the left end of the housing (1).

2. The lithium fluoride washing and filtering device as described in claim 1, characterized in that, The extrusion assembly includes a first hydraulic cylinder (3), an extrusion plate (4), a smooth rod (5), and a limiting plate (6). The first hydraulic cylinder (3) is provided at the right end of the housing (1). The left moving end of the first hydraulic cylinder (3) extends into the housing (1) and is connected to one end of the extrusion plate (4). The extrusion plate (4) is slidably and sealed inside the housing (1). Multiple sets of smooth rods (5) are provided on the extrusion plate (4). All smooth rods (5) are slidably connected. A set of limiting plates (6) is provided at the end of the smooth rod (5) away from the extrusion plate (4).

3. The lithium fluoride washing and filtering device as described in claim 2, characterized in that, The unloading assembly includes a vertical plate (7), a horizontal plate (8), a light bar (9), a lifting plate (10), a sealing plate (11), a second hydraulic cylinder (12), and a connecting plate (13). The top of the box (1) is provided with two sets of vertical plates (7). The outer ends of the two sets of vertical plates (7) and the front and rear ends of the box (1) are respectively provided with a set of horizontal plates (8). A light bar (9) is provided between the two sets of horizontal plates (8). A lifting plate (10) is slidably provided on each set of light bars (9). One end of each set of lifting plates (10) is connected to the right end of the sealing plate (11). The top of the box (1) is provided with a second hydraulic cylinder (12). The top moving end of the second hydraulic cylinder (12) is provided with a connecting plate (13). The bottom end of the connecting plate (13) is connected to the top of the sealing plate (11).

4. The lithium fluoride washing and filtering device as described in claim 3, characterized in that, It also includes a U-shaped clamp (14), a shaft pin (15), a lead screw (16) and a wing nut (17). The bottom end of the sealing plate (11) is provided with a U-shaped clamp (14), the bottom end of the housing (1) is provided with a shaft pin (15), the lead screw (16) is hinged to the bottom end of the housing (1) through the shaft pin (15), and the lead screw (16) is threadedly connected to the wing nut (17).

5. The lithium fluoride washing and filtering device as described in claim 1, characterized in that, It also includes a base (18), with a base (18) provided at the bottom of each set of legs (21).

6. The lithium fluoride washing and filtering device as described in claim 1, characterized in that, It also includes a flow guide (20), and the flow guide (20) is installed at the front end of the box (1).

7. A lithium fluoride washing and filtering device as described in claim 2, characterized in that, The filter screen (2) is made of stainless steel.

Citation Information

Patent Citations

  • Lithium fluoride solid-liquid separation device

    CN221267369U