Sodium sulfide waste alkali liquor resource recovery device

By installing a circulating flow tank and extension components in the sodium sulfide waste alkali liquid recovery device, combined with scrapers and electric heating, the problem of water vapor carrying away crystalline powder was solved, thus improving the recovery efficiency of sodium sulfide crystals.

CN224279819UActive Publication Date: 2026-05-26ZHANJIANG YUELV ENVIRONMENTAL PROTECTION TECH CO LTD
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Patent Information

Authority / Receiving Office
CN · China
Patent Type
Utility models(China)
Current Assignee / Owner
ZHANJIANG YUELV ENVIRONMENTAL PROTECTION TECH CO LTD
Filing Date
2025-06-16
Publication Date
2026-05-26

AI Technical Summary

Technical Problem

In traditional sodium sulfide waste alkali recovery devices, some of the lighter media are carried away by water vapor during evaporation and crystallization, resulting in low sodium sulfide crystal recovery efficiency.

Method used

A structure including a separator, partition, mounting plate, mounting column and exhaust pipe is designed. By setting up a circulation channel and extension, water vapor circulation is used to make the crystallized powder adhere to the extension for recycling, and it is collected by scraper. Combined with electric heating and exhaust pipe adjustment mechanism, the recycling efficiency is improved.

Benefits of technology

This improved the recovery efficiency of sodium sulfide crystals, reduced the loss of crystallized powder, and achieved more efficient resource recovery.

✦ Generated by Eureka AI based on patent content.

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Abstract

The utility model belongs to the technical field of recycling devices, and discloses a sodium sulfide waste alkali liquor resource recycling device which comprises a recycling box, a bottom cover is installed at the bottom of the recycling box through a thread structure, a feeding pipe is fixedly installed at the top of the recycling box, and a recycling mechanism is arranged in the recycling box. The recycling mechanism comprises a separation frame, a partition plate, a mounting plate, a mounting column and an extension piece, and the separation frame is fixedly mounted in the recycling box; according to the sodium sulfide waste alkali liquid recycling device, water vapor generated in the evaporation process of sodium sulfide waste alkali liquid in the recycling box can circularly flow in the recycling box through the first circulating groove and the second circulating groove by arranging the separation frame, so that the water vapor can be frequently in contact with the mounting columns on the outer side of the separation frame; and the water vapor crystal powder can be attached to the extension piece through the extension piece on the side wall of the mounting column, so that a medium with light mass can be recovered, and the recovery efficiency of the sodium sulfide crystals is higher.
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Description

Technical Field

[0001] This utility model relates to the field of recycling equipment technology, and in particular to a resource recycling device for sodium sulfide waste alkali solution. Background Technology

[0002] Waste alkali solution is a waste liquid containing a large amount of pollutants generated during petrochemical production processes, specifically during the absorption of H2S with NaOH solution, alkali washing of oil products, and cracking of gases. Because it contains inorganic and organic sulfides such as sulfides and thiols, waste alkali solution has a foul, unpleasant odor. The reuse of sodium sulfide waste alkali solution can be achieved in various ways, the most common being evaporation and concentration: by heating and evaporating the water in the waste liquid, the sodium sulfide crystals are recovered after concentration.

[0003] Traditional sodium sulfide waste alkali liquid resource recovery devices usually directly use heating to evaporate water and recover the evaporated sodium sulfide crystals. However, in actual use, when some lighter media are evaporated and crystallized, some crystal powder will be carried away by the water vapor after evaporation, which will affect the recovery efficiency of sodium sulfide crystals. Utility Model Content

[0004] The main purpose of this utility model is to provide a resource recovery device for sodium sulfide waste alkaline solution, which aims to solve the technical problem that when some lighter media are evaporated and crystallized, the crystal powder in the water vapor after evaporation is carried away by the water vapor, thus affecting the recovery efficiency of sodium sulfide crystals.

[0005] In order to achieve the above-mentioned utility model objectives, the first aspect of this utility model proposes a resource recovery device for sodium sulfide waste alkaline solution, including a recovery box, a bottom cover installed at the bottom of the recovery box through a threaded structure, a feed pipe fixedly installed at the top of the recovery box, and a circulation recovery mechanism provided inside the recovery box;

[0006] The recycling mechanism includes a separator, a partition, a mounting plate, a mounting column, and an extension. The separator is fixedly installed inside the recycling bin. The gap between the top of the separator and the inner wall of the recycling bin forms a first flow channel. The partition is fixedly installed on the side wall of the separator. A second flow channel is opened inside the separator and is located at the top of the partition. The mounting plate is installed inside the recycling bin. The mounting column is fixedly installed at the bottom of the mounting plate and is located between one side of the separator and the inner wall of the recycling bin. The extension is fixedly installed on the side wall of the mounting column.

[0007] Furthermore, a plurality of mounting posts and a plurality of extension members are provided.

[0008] Furthermore, the top of the recycling bin is provided with an installation groove, and the installation plate is snapped into the installation groove.

[0009] Furthermore, the mounting column has a mounting component slidably connected to its side wall, the mounting component has an inner wall with a mounting cavity, a spring is fixedly installed on the inner wall of the mounting cavity, and a snap-fit ​​component is fixedly installed on one end of the spring.

[0010] Furthermore, the mounting column has a snap-fit ​​groove on its side wall, which fits into the snap-fit ​​component. A scraper is fixedly installed at the bottom of the mounting component, and the scraper is in contact with the side wall of the mounting column.

[0011] Furthermore, an electric heating wire is fixedly installed on the side wall of the partition, and the electric heating wire is located at the bottom of the partition.

[0012] Furthermore, a mounting rod is fixedly mounted on the top of the mounting plate.

[0013] Furthermore, an exhaust pipe is fixedly installed on the top of the recycling bin, and an adjustment mechanism is provided inside the exhaust pipe.

[0014] Furthermore, the adjustment mechanism includes a bracket, a threaded rod, a movable frame, a connecting rod, a slider, a mounting shaft, a valve disc, and a limiting block. The bracket is fixedly installed on the inner wall of the exhaust pipe, the threaded rod is rotatably connected to the bracket, the slider is fixedly installed on the side wall of the movable frame, the inner wall of the exhaust pipe has a groove that matches the slider, the movable frame is movably connected to the side wall of the threaded rod, the connecting rod is rotatably connected to the side wall of the movable frame via a torsion spring, the mounting shaft is fixedly installed inside the exhaust pipe, the valve disc is rotatably connected to the side wall of the mounting shaft, and the limiting block is fixedly installed on the inner wall of the exhaust pipe.

[0015] Furthermore, a servo motor is fixedly mounted on the top of the bracket, and the threaded rod is fixedly mounted on the output end of the servo motor.

[0016] Beneficial effects:

[0017] The present invention relates to a resource recovery device for sodium sulfide waste alkaline solution, the beneficial effects of which are as follows:

[0018] 1. By setting up a partition frame, the water vapor generated during the evaporation of sodium sulfide waste alkali liquid inside the recovery box can circulate inside the recovery box through the first and second flow channels. This allows the water vapor to frequently come into contact with the mounting columns on the outside of the partition frame. Through the extension of the side wall of the mounting column, the water vapor crystallization powder can adhere to the extension, thereby enabling the recovery of lighter media and making the recovery efficiency of sodium sulfide crystals higher.

[0019] 2. By setting sliders and grooves, the movement direction of the moving frame can be limited to prevent the moving frame from rotating. By setting threaded rods, when the threaded rods rotate, they can drive the moving frame to move inside the exhaust pipe. By moving the moving frame, the position of the connecting rod at the top of the valve disc can be adjusted, thereby limiting the opening angle of the valve disc and thus adjusting the exhaust volume of the exhaust pipe. Attached Figure Description

[0020] Figure 1 This is a schematic diagram of the structure of a resource recovery device for sodium sulfide waste alkaline solution according to an embodiment of this utility model;

[0021] Figure 2 This is a cross-sectional structural schematic diagram of a resource recovery device for sodium sulfide waste alkaline solution according to an embodiment of this utility model;

[0022] Figure 3 This is a schematic diagram of the partition frame structure of a resource recovery device for sodium sulfide waste alkaline solution according to an embodiment of this utility model;

[0023] Figure 4 This is a cross-sectional structural diagram of the installation components of a resource recovery device for sodium sulfide waste alkali liquid according to an embodiment of this utility model;

[0024] Figure 5 This is a cross-sectional view of the exhaust pipe of a resource recovery device for sodium sulfide waste alkali solution according to an embodiment of this utility model.

[0025] in:

[0026] 1-Recycling bin; 2-Mounting plate; 3-Exhaust pipe; 4-Feed pipe; 5-Mounting rod; 6-Separator; 7-First flow channel; 8-Second flow channel; 9-Baffle; 10-Electric heating wire; 11-Bottom cover; 12-Mounting groove; 14-Mounting component; 15-Mounting cavity; 16-Spring; 17-Snap-fit ​​component; 18-Snap-fit ​​groove; 19-Mounting column; 20-Scraper; 21-Extension component; 22-Bracket; 23-Servo motor; 24-Threaded rod; 25-Moving frame; 26-Connecting rod; 27-Slider; 28-Slide groove; 29-Mounting shaft; 30-Valve disc; 31-Limit block.

[0027] The realization of the purpose, functional features and advantages of this utility model will be further explained in conjunction with the embodiments and with reference to the accompanying drawings. Detailed Implementation

[0028] It should be understood that the specific embodiments described herein are merely illustrative of the present invention and are not intended to limit the present invention.

[0029] In the description of this utility model, it should be understood that the terms "center," "longitudinal," "lateral," "length," "width," "thickness," "upper," "lower," "front," "rear," "left," "right," "vertical," "horizontal," "top," "bottom," "inner," "outer," "clockwise," and "counterclockwise," etc., indicating the orientation or positional relationship, are based on the orientation or positional relationship shown in the accompanying drawings and are only for the convenience of describing this utility model and simplifying the description. They do not indicate or imply that the device or element referred to must have a specific orientation, or be constructed and operated in a specific orientation, and therefore should not be construed as a limitation of this utility model. Furthermore, the terms "first" and "second" are used for descriptive purposes only and should not be construed as indicating or implying relative importance or implicitly specifying the number of indicated technical features. Thus, features defined with "first" and "second" may explicitly or implicitly include one or more of the stated features. In the description of this utility model, "a plurality of" means two or more, unless otherwise explicitly and specifically defined.

[0030] In the description of this utility model, it should be noted that, unless otherwise explicitly specified and limited, the terms "installation," "connection," and "joining" should be interpreted broadly. For example, they can refer to a fixed connection, a detachable connection, or an integral connection; they can refer to a mechanical connection, a direct connection, or an indirect connection through an intermediate medium; they can refer to the internal communication of two components or the interaction between two components. Those skilled in the art can understand the specific meaning of the above terms in this utility model according to the specific circumstances.

[0031] In this invention, unless otherwise explicitly specified and limited, "above" or "below" the second feature can include direct contact between the first and second features, or contact between the first and second features through another feature between them. Furthermore, "above," "over," and "on top" of the second feature includes the first feature directly above or diagonally above the second feature, or simply indicates that the first feature is at a higher horizontal level than the second feature. "Below," "below," and "under" the second feature includes the first feature directly below or diagonally below the second feature, or simply indicates that the first feature is at a lower horizontal level than the second feature.

[0032] Reference Figures 1-5 An embodiment of this utility model provides a resource recovery device for sodium sulfide waste alkali liquid, including a recovery box 1, a bottom cover 11 installed at the bottom of the recovery box 1 by a threaded structure, a feed pipe 4 fixedly installed at the top of the recovery box 1, and a circulation recovery mechanism provided inside the recovery box 1.

[0033] The recycling mechanism includes a separator 6, a partition 9, a mounting plate 2, a mounting column 19, and an extension 21. The separator 6 is fixedly installed inside the recycling bin 1. The gap between the top of the separator 6 and the inner wall of the recycling bin 1 forms a first flow channel 7. The partition 9 is fixedly installed on the side wall of the separator 6. A second flow channel 8 is opened inside the separator 6 and is located at the top of the partition 9. The mounting plate 2 is installed inside the recycling bin 1. The mounting column 19 is fixedly installed at the bottom of the mounting plate 2 and is located between one side of the separator 6 and the inner wall of the recycling bin 1. The extension 21 is fixedly installed on the side wall of the mounting column 19.

[0034] Several mounting posts 19 and several extension pieces 21 are provided.

[0035] The top of the recycling bin 1 has an installation groove 12, the installation plate 2 is snapped into the installation groove 12, and the extension 21 is a brush.

[0036] In this embodiment, by setting up a partition frame 6, the water vapor generated during the evaporation process of the sodium sulfide waste alkali liquid inside the recovery box 1 can circulate inside the recovery box 1 through the first flow channel 7 and the second flow channel 8. This allows the water vapor to frequently come into contact with the mounting column 19 on the outside of the partition frame 6. The water vapor crystallization powder can be attached to the extension 21 on the side wall of the mounting column 19, thereby enabling the recovery of lighter media and making the recovery efficiency of sodium sulfide crystals higher. The bottom cover 11 makes it easy to remove the crystals inside the recovery box 1.

[0037] In one embodiment, a mounting member 14 is slidably connected to the side wall of the mounting post 19. The inner wall of the mounting member 14 has a mounting cavity 15. A spring 16 is fixedly installed on the inner wall of the mounting cavity 15. A snap-fit ​​member 17 is fixedly installed at one end of the spring 16. A snap-fit ​​groove 18 is opened on the side wall of the mounting post 19. The snap-fit ​​groove 18 fits with the snap-fit ​​member 17. A scraper 20 is fixedly installed at the bottom of the mounting member 14. The scraper 20 fits against the side wall of the mounting post 19.

[0038] In this example, the spring 16 can support the snap-fit ​​component 17, allowing the snap-fit ​​component 17 to snap into the snap-fit ​​groove 18, and the mounting component 14 to snap onto the side wall of the mounting post 19. At the same time, when the mounting component 14 is pushed hard, the snap-fit ​​component 17 can be disengaged from the snap-fit ​​groove 18, thereby driving the scraper 20 to scrape off the small particles adhering to the side wall of the mounting post 19, making collection convenient.

[0039] In one embodiment, an electric heating wire 10 is fixedly installed on the side wall of the partition 6, the electric heating wire 10 is located at the bottom of the partition 9, and an installation rod 5 is fixedly installed on the top of the mounting plate 2.

[0040] In this example, the electric heating wire 10 can be used to heat the sodium sulfide waste alkali liquid inside the partition rack 6 to evaporate the moisture, and the mounting rod 5 can be used to facilitate the removal of the mounting plate 2.

[0041] In one embodiment, an exhaust pipe 3 is fixedly installed on the top of the recycling bin 1. An adjustment mechanism is provided inside the exhaust pipe 3. The adjustment mechanism includes a bracket 22, a threaded rod 24, a movable frame 25, a connecting rod 26, a slider 27, a mounting shaft 29, a valve disc 30, and a limiting block 31. The bracket 22 is fixedly installed on the inner wall of the exhaust pipe 3. The threaded rod 24 is rotatably connected to the bracket 22. The slider 27 is fixedly installed on the side wall of the movable frame 25. A groove 28 that fits the slider 27 is opened on the inner wall of the exhaust pipe 3. The movable frame 25 is movably connected to the side wall of the threaded rod 24. The connecting rod 26 is rotatably connected to the side wall of the movable frame 25 through a torsion spring. The mounting shaft 29 is fixedly installed inside the exhaust pipe 3. The valve disc 30 is rotatably connected to the side wall of the mounting shaft 29. The limiting block 31 is fixedly installed on the inner wall of the exhaust pipe 3.

[0042] In this example, the moving direction of the movable frame 25 can be limited by setting the slider 27 and the groove 28 to prevent the movable frame 25 from rotating. When the threaded rod 24 rotates, it can drive the movable frame 25 to move inside the exhaust pipe 3. The position of the connecting rod 26 at the top of the valve disc 30 can be adjusted by moving the movable frame 25, thereby limiting the opening angle of the valve disc 30 and thus adjusting the exhaust volume of the exhaust pipe 3.

[0043] In one embodiment, a servo motor 23 is fixedly mounted on the top of the bracket 22, and a threaded rod 24 is fixedly mounted on the output end of the servo motor 23.

[0044] In this example, servo motor 23 can be used to control the rotation of threaded rod 24.

[0045] The above description is only a preferred embodiment of the present utility model and does not limit the patent scope of the present utility model. Any equivalent structural or procedural transformations made based on the content of the present utility model specification and drawings, or direct or indirect applications in other related technical fields, are similarly included within the patent protection scope of the present utility model.

Claims

1. A resource recovery device for sodium sulfide waste alkaline solution, characterized in that, Includes a recycling bin (1), the bottom of which is fitted with a bottom cover (11) via a threaded structure, the top of which is fixedly fitted with a feed pipe (4), and the inside of which is equipped with a recycling mechanism; The recycling mechanism includes a separator (6), a partition (9), a mounting plate (2), a mounting column (19), and an extension (21). The separator (6) is fixedly installed inside the recycling bin (1). The gap between the top of the separator (6) and the inner wall of the recycling bin (1) forms a first flow groove (7). The partition (9) is fixedly installed on the side wall of the separator (6). A second flow groove (8) is opened inside the separator (6). The second flow groove (8) is located at the top of the partition (9). The mounting plate (2) is installed inside the recycling bin (1). The mounting column (19) is fixedly installed at the bottom of the mounting plate (2). The mounting column (19) is located between one side of the separator (6) and the inner wall of the recycling bin (1). The extension (21) is fixedly installed on the side wall of the mounting column (19).

2. The resource recovery device for sodium sulfide waste alkaline solution according to claim 1, characterized in that, The mounting posts (19) are provided in a plurality of units, and the extension members (21) are provided in a plurality of units.

3. The resource recovery device for sodium sulfide waste alkaline solution according to claim 1, characterized in that, The recycling bin (1) has an installation slot (12) on its top, and the installation plate (2) is snapped into the installation slot (12).

4. The resource recovery device for sodium sulfide waste alkaline solution according to claim 1, characterized in that, The mounting column (19) is slidably connected to the side wall of the mounting component (14), and the inner wall of the mounting component (14) is provided with a mounting cavity (15). A spring (16) is fixedly installed on the inner wall of the mounting cavity (15), and a snap-fit ​​component (17) is fixedly installed on one end of the spring (16).

5. The resource recovery device for sodium sulfide waste alkaline solution according to claim 4, characterized in that, The mounting post (19) has a snap-fit ​​groove (18) on its side wall, which fits into the snap-fit ​​part (17). A scraper (20) is fixedly installed at the bottom of the mounting part (14), and the scraper (20) fits into the side wall of the mounting post (19).

6. The resource recovery device for sodium sulfide waste alkaline solution according to claim 1, characterized in that, An electric heating wire (10) is fixedly installed on the side wall of the partition (6), and the electric heating wire (10) is located at the bottom of the partition (9).

7. The resource recovery device for sodium sulfide waste alkaline solution according to claim 1, characterized in that, The mounting plate (2) is fixedly mounted with a mounting rod (5) on its top.

8. The resource recovery device for sodium sulfide waste alkaline solution according to claim 1, characterized in that, The top of the recycling bin (1) is fixedly equipped with an exhaust pipe (3), and an adjustment mechanism is provided inside the exhaust pipe (3).

9. A resource recovery device for sodium sulfide waste alkaline solution according to claim 8, characterized in that, The adjustment mechanism includes a bracket (22), a threaded rod (24), a movable frame (25), a connecting rod (26), a slider (27), a mounting shaft (29), a valve disc (30), and a limiting block (31). The bracket (22) is fixedly installed on the inner wall of the exhaust pipe (3). The threaded rod (24) is rotatably connected to the bracket (22). The slider (27) is fixedly installed on the side wall of the movable frame (25). The inner wall of the exhaust pipe (3) has a groove (28) that matches the slider (27). The movable frame (25) is movably connected to the side wall of the threaded rod (24). The connecting rod (26) is rotatably connected to the side wall of the movable frame (25) via a torsion spring. The mounting shaft (29) is fixedly installed inside the exhaust pipe (3). The valve disc (30) is rotatably connected to the side wall of the mounting shaft (29). The limiting block (31) is fixedly installed on the inner wall of the exhaust pipe (3).

10. A resource recovery device for sodium sulfide waste alkaline solution according to claim 9, characterized in that, A servo motor (23) is fixedly installed on the top of the bracket (22), and the threaded rod (24) is fixedly installed on the output end of the servo motor (23).