An alkylene oxide material mixing device

Abstract

The utility model relates to mixed device technical field, and disclose an epoxy alkane material mixing device, this epoxy alkane material mixing device, including inner kettle, the top end surface of inner kettle is connected with the cover body fixedly, the outer wall of inner kettle is connected with the outer kettle fixedly, the inside of inner kettle is provided with mixing subassembly. This epoxy alkane material mixing device, the mixed arc plate of arc setting pushes the material descending above, and then promotes the sufficient mixing of material above and below, makes the material in the kettle to be scattered and mixed in axial and radial direction, strengthens the stirring efficiency, avoids the stratification, improves the mixed uniformity of initiator and epoxy alkane, and the disturbance arc plate scatters the cooling water, pushes the cooling water ascending below, and then promotes the sufficient mixing of cooling water above and below, improves the uniformity of cooling water temperature, and then reduces the probability of material gasification, and the ethylene oxide after gasification is cooled through condenser again, reduces the loss of ethylene oxide, and improves raw material utilization rate.

Description

Technical Field

[0001] This utility model relates to the field of mixing device technology, specifically to a mixing device for epoxide alkane materials. Background Technology

[0002] Polyepoxides are obtained by initiating the ring-opening reaction of monoepoxides such as epoxides with an initiator. They are liquid at room temperature, and because their cured form remains flexible even at low temperatures, they can be widely used as raw materials for sealing materials, adhesives, etc. In the preparation of polyepoxides, an initiator needs to be added to ensure that the initiator and a certain amount of epoxides coexist. Subsequently, heating is used to enable the catalyst to exhibit polymerization activity. Therefore, in the preparation of polyepoxides, the initiator and epoxides need to be mixed evenly before adding the catalyst.

[0003] However, at higher temperatures, ethylene oxide is prone to significant vaporization during mixing, and the vaporized ethylene oxide is detrimental to subsequent polymerization reactions. Therefore, we propose a mixing device for ethylene oxide materials. Utility Model Content

[0004] The purpose of this invention is to provide an epoxide alkane material mixing device to solve the problems mentioned in the background art.

[0005] To achieve the above objectives, this utility model provides the following technical solution: a mixing device for epoxide alkane materials, comprising an inner vessel, a cover fixedly connected to the top end face of the inner vessel, an outer vessel fixedly connected to the outer wall of the inner vessel, and a mixing assembly disposed inside the inner vessel, the mixing assembly comprising:

[0006] The motor has a rotating shaft fixedly connected to its output end, a stirring rod fixedly connected to the side wall of the rotating shaft, a connecting frame fixedly connected to the side wall of the rotating shaft, a rotating ring fixedly connected to the bottom end of the connecting frame, a mixing arc plate fixedly connected to the top end face of the rotating ring, and a disturbance arc plate fixedly connected to the bottom end face of the rotating ring.

[0007] A condenser, wherein an air inlet pipe is fixedly connected to the top end face of the condenser, a recovery pipe is fixedly connected to the bottom end of the condenser, a water inlet pipe is fixedly connected to the side wall of the condenser, and a water outlet pipe is fixedly connected to the side wall of the condenser.

[0008] Preferably, a thermometer is fixedly connected to the top end face of the cover, the bottom end of the thermometer is located inside the inner vessel, an inlet pipe is provided on the top end face of the cover, and an inlet and an outlet are fixedly connected to the outer wall of the outer vessel.

[0009] Preferably, the motor is fixedly connected to the top end face of the cover, the cross-section of the rotating ring is I-shaped, the inner top surface of the rotating ring is movably connected to the inner bottom surface of the inner vessel, and the inner bottom surface of the rotating ring is movably connected to the outer wall of the inner vessel.

[0010] Preferably, the mixing arc plate is located inside the inner vessel, and the disturbance arc plate is located between the inner vessel and the outer vessel.

[0011] Preferably, the end of the inlet pipe away from the condenser is fixedly connected to the top end face of the cover, and the end of the recovery pipe away from the condenser is fixedly connected to the side wall of the inner vessel, so as to introduce the vaporized ethylene oxide into the condenser.

[0012] Preferably, the end of the water inlet pipe away from the condenser is fixedly connected to the side wall of the outer vessel, and a water pump is fixedly connected to the side wall of the water inlet pipe. The end of the water outlet pipe away from the condenser is fixedly connected to the side wall of the outer vessel. Cooling water between the inner and outer vessels is pumped into the condenser through the water inlet pipe to cool the vaporized ethylene oxide.

[0013] Preferably, the inner wall of the inner vessel is provided with an annular groove, the outer wall of the inner vessel is provided with an annular groove, the annular groove is movably connected to the sealing ring, and the sealing ring is fixedly connected to the inner wall of the rotating ring.

[0014] Compared with the prior art, the present invention provides a mixing device for epoxide alkane materials, which has the following beneficial effects:

[0015] 1. This epoxy alkane material mixing device, through its mixing components, uses an arc-shaped mixing plate to push the material above downwards, thereby promoting thorough mixing of the materials above and below. This ensures that the materials in the reactor are dispersed and mixed in both the axial and radial directions, enhancing stirring efficiency, preventing stratification, and improving the mixing uniformity of the initiator and epoxy alkane. The agitated arc plate disperses the cooling water, pushing the cooling water below upwards, thereby promoting thorough mixing of the cooling water above and below, improving the uniformity of cooling water temperature, and reducing the probability of material vaporization. The vaporized ethylene oxide is then cooled again through a condenser, reducing ethylene oxide loss and improving raw material utilization.

[0016] 2. This epoxy alkane material mixing device, through the setting of a sealing ring, which is embedded in an annular groove to form a sliding sealing structure, ensures that the material does not leak into the jacket space during mixing, thereby improving the system's sealing performance. It is suitable for low-viscosity, high-volatility materials such as ethylene oxide systems, and prevents material leakage. Attached Figure Description

[0017] Figure 1 This is a schematic diagram of the main structure of the present utility model;

[0018] Figure 2 This is a schematic diagram of the cover structure of this utility model;

[0019] Figure 3 This is a schematic diagram of the cross-sectional structure of the inner vessel of this utility model;

[0020] Figure 4 This utility model Figure 4 Schematic diagram of the structure of region A in the middle;

[0021] Figure 5 This is a schematic diagram of the cross-sectional structure of the rotating ring of this utility model;

[0022] Figure 6 This utility model Figure 5 Schematic diagram of the structure of region B in the middle.

[0023] In the diagram: 1. Inner vessel; 2. Cover; 3. Outer vessel; 4. Mixing assembly; 401. Motor; 402. Rotating shaft; 403. Stirring rod; 404. Connecting frame; 405. Rotating ring; 406. Mixing arc plate; 407. Disturbing arc plate; 408. Air inlet pipe; 409. Condenser; 410. Recovery pipe; 412. Water inlet pipe; 413. Water outlet pipe; 5. Thermometer; 6. Sealing ring. Detailed Implementation

[0024] like Figures 1-6 As shown, this utility model provides a technical solution: an epoxy alkane material mixing device, including an inner vessel 1, a cover 2 fixedly connected to the top end face of the inner vessel 1, an outer vessel 3 fixedly connected to the outer wall of the inner vessel 1, and a mixing component 4 arranged inside the inner vessel 1. The mixing component 4 includes a motor 401, a rotating shaft 402, a stirring rod 403, a connecting frame 404, a rotating ring 405, a mixing arc plate 406, a disturbance arc plate 407, an air inlet pipe 408, a condenser 409, a recovery pipe 410, a water inlet pipe 412, and a water outlet pipe 413.

[0025] In one embodiment of this utility model, a motor 401 is fixedly connected to the top end face of the cover 2. A rotating shaft 402 is fixedly connected to the output end of the motor 401. A stirring rod 403 is fixedly connected to the side wall of the rotating shaft 402. A connecting frame 404 is fixedly connected to the side wall of the rotating shaft 402. A rotating ring 405 is fixedly connected to the bottom end of the connecting frame 404. A mixing arc plate 406 is fixedly connected to the top end face of the rotating ring 405. A disturbance arc plate 407 is fixedly connected to the bottom end face of the rotating ring 405. The cross-section of the rotating ring 405 is I-shaped. The inner top surface of the rotating ring 405 is movably connected to the inner bottom surface of the inner vessel 1. The inner bottom surface of the rotating ring 405 is movably connected to the outer wall of the inner vessel 1. The mixing arc plate 406 is located inside the inner vessel 1. The disturbance arc plate 407 is located between the inner vessel 1 and the outer vessel 3.

[0026] An inlet pipe 408 is fixedly connected to the top end face of the condenser 409, a recovery pipe 410 is fixedly connected to the bottom end of the condenser 409, a water inlet pipe 412 is fixedly connected to the side wall of the condenser 409, and a water outlet pipe 413 is fixedly connected to the side wall of the condenser 409. The end of the inlet pipe 408 away from the condenser 409 is fixedly connected to the top end face of the cover 2. The end of the recovery pipe 410 away from the condenser 409 is fixedly connected to the side wall of the inner vessel 1, introducing the vaporized ethylene oxide into the condenser 409. The end of the water inlet pipe 412 away from the condenser 409 is fixedly connected to the side wall of the outer vessel 3, and a water pump is fixedly connected to the side wall of the water inlet pipe 412. The end of the water outlet pipe 413 away from the condenser 409 is fixedly connected to the side wall of the outer vessel 3, drawing cooling water between the inner vessel 1 and the outer vessel 3 into the condenser 409 through the water inlet pipe 412 to cool the vaporized ethylene oxide.

[0027] A thermometer 5 is fixedly connected to the top end face of the cover body 2. The bottom end of the thermometer 5 is located inside the inner vessel 1. An inlet pipe is opened on the top end face of the cover body 2. An inlet and an outlet are fixedly connected to the outer wall of the outer vessel 3.

[0028] Motor 401 drives rotating shaft 402 and stirring rod 403 to rotate, causing stirring rod 403 to mix materials. Stirring rod 403 drives rotating ring 405, mixing arc plate 406 and disturbance arc plate 407 to rotate. Mixing arc plate 406 disturbs the materials inside inner vessel 1. The arc-shaped mixing arc plate 406 pushes the materials above down, thereby promoting full mixing of materials above and below. This makes the materials in the vessel dispersed and mixed in both axial and radial directions, enhancing stirring efficiency, avoiding stratification, and improving the mixing uniformity of initiator and epoxy alkane.

[0029] The cooling water between the outer vessel 3 and the inner vessel 1 cools the material in the inner vessel 1. The agitator plate 407 disperses the cooling water, pushing the cooling water below to rise, thereby promoting thorough mixing of the cooling water above and below, improving the uniformity of the cooling water temperature, and reducing the probability of material vaporization. When vaporized ethylene oxide occurs, it enters the inlet pipe 408 and the condenser 409. The water pump draws cooling water into the condenser 409 to cool the vaporized ethylene oxide. The vaporized ethylene oxide is then cooled again through the condenser 409, reducing ethylene oxide loss and improving raw material utilization.

[0030] In addition, an annular groove is provided on the inner wall of the inner vessel 1 and an annular groove is provided on the outer wall of the inner vessel 1. The annular groove is movably connected to the sealing ring 6, and the sealing ring 6 is fixedly connected to the inner wall of the rotating ring 405. The sealing ring 6 is embedded in the annular groove to form a sliding sealing structure, which ensures that the material does not leak into the jacket space during mixing, improves the system sealing performance, and is suitable for low viscosity and high volatility materials such as ethylene oxide system to prevent material leakage.

[0031] In this invention, during use, the motor 401 drives the rotating shaft 402 and the stirring rod 403 to rotate, causing the stirring rod 403 to mix the materials. The stirring rod 403 drives the rotating ring 405, the mixing arc plate 406, and the disturbance arc plate 407 to rotate. The mixing arc plate 406 disturbs the materials inside the inner vessel 1. The arc-shaped mixing arc plate 406 pushes the materials above down, thereby promoting the full mixing of the materials above and below. This ensures that the materials in the vessel are dispersed and mixed in both the axial and radial directions, enhancing the stirring efficiency and preventing stratification. The cooling water between the outer vessel 3 and the inner vessel 1 cools the materials in the inner vessel 1. The disturbance arc plate 407 disperses the cooling water, pushing the cooling water below up, thereby promoting the full mixing of the cooling water above and below, improving the uniformity of the cooling water temperature, and reducing the probability of material vaporization. The vaporized ethylene oxide is then cooled again by the condenser 409, reducing ethylene oxide loss and improving raw material utilization.

[0032] The present invention has been described in detail above. However, modifications or improvements can be made to it, which will be obvious to those skilled in the art. Therefore, any modifications or improvements that do not depart from the spirit of the present invention are within the protection scope of the present invention.

Claims

1. A mixing device for epoxide alkane materials, comprising an inner vessel (1), wherein a cover (2) is fixedly connected to the top end face of the inner vessel (1), and an outer vessel (3) is fixedly connected to the outer wall of the inner vessel (1), characterized in that: The inner vessel (1) is equipped with a mixing component (4), which includes: A motor (401) is provided, with a rotating shaft (402) fixedly connected to the output end of the motor (401). A stirring rod (403) is fixedly connected to the side wall of the rotating shaft (402). A connecting frame (404) is fixedly connected to the side wall of the rotating shaft (402). A rotating ring (405) is fixedly connected to the bottom end of the connecting frame (404). A mixing arc plate (406) is fixedly connected to the top end face of the rotating ring (405). A disturbance arc plate (407) is fixedly connected to the bottom end face of the rotating ring (405). A condenser (409) is provided with an air inlet pipe (408) fixedly connected to its top end face, a recovery pipe (410) fixedly connected to its bottom end, a water inlet pipe (412) fixedly connected to its side wall, and a water outlet pipe (413) fixedly connected to its side wall.

2. The epoxy alkane material mixing device according to claim 1, characterized in that: A thermometer (5) is fixedly connected to the top end face of the cover (2). The bottom end of the thermometer (5) is located inside the inner vessel (1). An inlet pipe is opened on the top end face of the cover (2). An inlet and an outlet are fixedly connected to the outer wall of the outer vessel (3).

3. The epoxy alkane material mixing device according to claim 1, characterized in that: The motor (401) is fixedly connected to the top end face of the cover (2). The cross-section of the rotating ring (405) is I-shaped. The inner top surface of the rotating ring (405) is movably connected to the inner bottom surface of the inner pot (1). The inner bottom surface of the rotating ring (405) is movably connected to the outer wall of the inner pot (1).

4. The epoxy alkane material mixing device according to claim 1, characterized in that: The mixing arc plate (406) is located inside the inner vessel (1), and the disturbance arc plate (407) is located between the inner vessel (1) and the outer vessel (3).

5. The epoxy alkane material mixing device according to claim 1, characterized in that: The end of the air inlet pipe (408) away from the condenser (409) is fixedly connected to the top end face of the cover (2), and the end of the recovery pipe (410) away from the condenser (409) is fixedly connected to the side wall of the inner vessel (1).

6. The epoxy alkane material mixing device according to claim 1, characterized in that: The end of the water inlet pipe (412) away from the condenser (409) is fixedly connected to the side wall of the outer vessel (3). A water pump is fixedly connected to the side wall of the water inlet pipe (412). The end of the water outlet pipe (413) away from the condenser (409) is fixedly connected to the side wall of the outer vessel (3).

7. The epoxy alkane material mixing device according to claim 1, characterized in that: The inner wall of the inner vessel (1) is provided with an annular groove, and the outer wall of the inner vessel (1) is provided with an annular groove. The annular groove is movably connected to the sealing ring (6), and the sealing ring (6) is fixedly connected to the inner wall of the rotating ring (405).

Images