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38results about How to "Separation fit" patented technology

Online low-pressure, middle-pressure and high-pressure combined two-dimension preparation liquid chromatographic system

InactiveCN101791491AImprove system separation capabilitiesSaves solvent handling stepsIon-exchange process apparatusIon-exchanger regenerationChromatography columnSystem structure
The invention relates to an online low-pressure, middle-pressure and high-pressure combined two-dimension preparation liquid chromatographic system. Two one-dimension low-pressure, middle-pressure and high-pressure preparation liquid chromatographic systems are organically combined through a six-way valve and software. Pressure used by a second dimension system is not lower than pressure used by a first dimension separation system. When the first dimension system and the second dimension system are low-pressure or middle-pressure preparation liquid chromatographic systems, through switching the six-way valve, target compound directly enters a second dimension chromatographic column for second dimension separation after first dimension separation; and when pressure used by a second dimension separation system is higher than pressure used by the first dimension separation system, a trapping column is connected on the six-way valve, the target compound is adsorbed on the head of the trapping column after the first dimension separation, and then the target compound enters the second dimension chromatographic column for second dimension separation. The invention has the advantages that the contradiction between sample injection volume and separation capacity is solved, the large sample injection volume is ensured and the separation capacity of the preparation chromatographic system is greatly improved; the system structure is simple and the establishment is easy; the operation is simple and convenient and the automation can be easily realized; and the application scope is wide.
Owner:SOOCHOW HIGH TECH CHROMATOGRAPHY

Method for detecting quality of senile coughand asthmatablets

The invention relates to the method for detecting the quality of senile cough and cough tablets. The method comprises the following steps: qualitatively distinguishing the active ingredients including radix astragaliseuhedysari, bighead atractylodes rhizome, radix saposhnikoviae, licoriceroot,herbaepimedii andfructuspsoralea in asenile cough and cough tabletpreparation by using a thin layer chromatography, and determining the contents of icariin, psoralen and isopsoralenin the preparation by a UPLC method. The detection method provided by the invention has the advantages of simplifying the sampling steps, having simple operation and high specificity, shortening the content determination time, simultaneously detecting multi-index components, having stabledetection baseline, good resolution, high detection accuracy and good stability, improving efficiency, and being relatively economic and environmentally friendly.
Owner:ZHUZHOU QIANJIN PHARMA

Simple method for separating and preserving ustilaginoidea virens

The invention relates to the technical field of separating and preserving ustilaginoidea virens, in particular to a simple method for separating and preserving the ustilaginoidea virens. The separation method comprises the following steps that fresh yellow, green and black rice false smut ball samples are collected from an attacked rice field, drying is conducted at the room temperature for 7-10 d for standby application; rice false smut balls of which the covering depth of chlamydospore powder is larger than 1 mm are selected in the collected samples and placed on an ultra-clean working table, and sterilization is conducted through an ultraviolet lamp for 30-40 min; single-grain rice false smut balls are taken through tweezers under the aseptic condition, and a small amount of chlamydospore powder on the surfaces of the rice false smut balls is shaken off slightly on a PSA culture medium; 150-200 microliters of sterile water is taken through a pipette and drips on a PSA flat plate containing chlamydospore. By means of the simple method for separating and preserving the ustilaginoidea virens, the ustilaginoidea virens can be separated to the objective strains rapidly and preserved, the problems that time is consumed, and the efficiency is low during separation of the ustilaginoidea virens are solved, and meanwhile the problems that in the preservation process of the strains, the pathogenicity is deteriorated, and the space is occupied and consumed are solved.
Owner:INST OF PLANT PROTECTION SICHUAN ACAD OF AGRI SCI

Extraction system and extraction method of duckweed starch

The invention discloses an extraction system of duckweed starch. The extraction system comprises a lifting device, a grinding device, a slag-slurry separation device, a precipitation device and a spin-drying device, wherein a motor is arranged at the top of the lifting device; a transmission chain is arranged in a bin; multiple groups of collection plates for collecting and lifting duckweed are arranged on the transmission chain; the motor drives the transmission chain to rotate; the slag-slurry separation device is provided with a cylinder, and a strip brush is arranged on a spindle in the cylinder; the spin-drying device is provided with a drum which is connected with a vacuum pump through a vacuum pipeline, and the water-containing starch stuck on the surface of the drum is completely pumped by the vacuum pump; and the lifting device, the grinding device, the slag-slurry separation device, the precipitation device and the spin-drying device are connected in turn. The invention also discloses an extraction method for duckweed starch. Through the invention, current blank of starch extraction technology is filled, continuous and efficient extraction of duckweed starch is facilitated after large-scale culture of duckweed, and later utilization and processing of the duckweed starch are convenient.
Owner:QINGDAO INST OF BIOENERGY & BIOPROCESS TECH CHINESE ACADEMY OF SCI

Gas-liquid separator based on porous media board

The invention discloses a gas-liquid separating device based on a porous dielectric-slab. The device is composed of a filter, a gas-liquid separation container, a pressure adjusting valve and a pipeline; the device is characterized in that the gas-liquid separation container is respectively connected with the filter and the pressure adjusting valve, the filter, the gas-liquid separation container, the pressure adjusting valve and the pipeline are connected by a pipe joint or welding, an inlet is arranged at one end of the filter, an exhausting pipeline is arranged at one end of the pressure adjusting valve, and the filter is used for filtering the solid in the gas-liquid mixed fluid. The gas-liquid separation container comprises a pressure container and a porous dielectric-slab, an exhausting pipeline is arranged at the upper end of the gas-liquid separation container, a lyosorpic phase porous dielectric-slab is arranged at the lower end thereof, and an exhausting pipeline is arranged at one end of the lyosorpic phase porous dielectric-slab. The invention is simple in structure, and convenient in use, can continuously separate gas-liquid mixed fluid in wide loading scope in real time, and can be widely used in gas-liquid separation fields of various pressure and flow ranges.
Owner:INST OF ROCK & SOIL MECHANICS CHINESE ACAD OF SCI

Method for separating Sclerotinia homoeocarpa

The invention discloses a method for separating Sclerotinia homoeocarpa. The method comprises the following steps: collection of disease samples: cutting off a diseased and healthy junction part of a plant having a typical dollar spot symptom and a soil sample as the disease samples; moisturized culture of the disease samples; pathogenic fungi separation: using a transfer needle to pick up filament-shaped spawn growing on the surfaces of the disease samples, putting the filament-shaped spawn on an APDA culture medium, and carrying out culture for 2 days under a dark condition at 22 to 25 DEG C; pathogenic fungi purification: after aerial hyphae grow out, cutting tips of the aerial hyphae on the edge of abacterial colony, putting the tips onto a new APDA culture medium, and carrying out culture for 3 to 5 daysunder a dark condition at 22 to 25 DEG C, so as to obtain target pathogenic bacteria. As moisturized culture pretreatment is conducted on the disease samples, and the acidized PDA culture medium is used, the problem of various non-target fungus contamination in a Sclerotinia homoeocarpa separation process can be solved; the operation is simple; the whole process is free of strict disinfection and sterilization operation. Compared with the traditional Sclerotinia homoeocarpa separation method, the separation efficiency and the success rate of the method disclosed by the invention are improved obviously.
Owner:NANJING AGRICULTURAL UNIVERSITY

Superhydrophilic-superoleophobic particle for oily sewage treatment as well as preparation method and application thereof

The invention relates to a superhydrophilic-superoleophobic particle for oily sewage treatment as well as a preparation method and application thereof. The superhydrophilic-superoleophobic particle comprises a particle core material, a hydrophilic-oleophobic film and a micro-nano secondary coarse structure, wherein the surface of the particle core material is coated with the hydrophilic-oleophobic film, and the micro-nano secondary coarse structure exists on the surface of the film. The hydrophilic-oleophobic film is obtained by coating the surface of the particle material with superhydrophilic-superoleophobic dispersion liquid, and performing drying and curing; the micro-nano secondary coarse structure is obtained by sequentially adding a micron-scale particle material and a nano-scale particle material before a coating liquid coating the surface of the particle core material is dried and cured, and attaching the materials to the surface of the particle core material after drying; and the particle is applied to oil-water separation. Compared with the prior art, the particle has the advantages of simple and quick preparation process, large-scale production, high separation efficiency, convenience in repeated use, flexible application scene and the like, and has the advantages of wide application prospect and the like.
Owner:TONGJI UNIV

Method for extracting, separating and culturing consubstantial xenogeneic liver primary cell

The invention belongs to the technical field of the cell culture, and discloses a method for extracting, separating and culturing consubstantial xenogeneic liver primary cells. The method comprises the following steps: perfusate is in in-situ perfusion through hepatic portal vein; (2) digestive juice is in in-situ perfusion through the hepatic portal vein; (3) the liver is in vitro, the pathologyis torn so as to acquire the cell suspension containing multiple liver primaries through screening; (4), the acquired cell suspension is conventionally centrifuged to acquire parenchyma cell and collected supernatant; (5) the supernatant separates sternzellen and residual submucosa cell suspension through density gradient centrifuging; (6) the residual submucosa cell suspension is incubated with immunomagnetic beads connected with hepatic sinusoidal endothelial cell and kupffer cell specificity, and acquires the hepatic sinusoidal endothelial cell and the kupffer cell through magnetic field sorting. After being separated, the liver primary cell is immediately resuspended in a corresponding and specifically prepared culture medium to culture. The cell yield is high, the separation effect isgood, and a stable cell source is provided for in-vitro construction of a multi-cell liver model.
Owner:DALIAN UNIV OF TECH

Stacked plate separating device and method

The invention discloses a stacked plate separating device and method. The separating device comprises a magnetic assistance module and an air blowing module, the magnetic assistance module comprises a magnet pair, the magnet pair comprises two magnet bases which are horizontally and oppositely arranged, the two magnet bases are horizontally arranged in a spaced mode, and different magnetic poles of the two magnet bases are horizontally and directly opposite. A plate stacking area is arranged between the two magnet bases, the air blowing module comprises an air nozzle, the air blowing direction of the air nozzle faces the plate stacking area, the air nozzle deviates upwards, and the air nozzle is connected with an air supply module. The stacked plate separating device and method have the beneficial effects that a magnetic field exists in the plate stacking area, plates are stacked and placed in the magnetic field, the plates are magnetized, so that magnetic repulsive force exists between every two adjacent plates, the plates are further easily separated under the air flow effect of air blowing of the air nozzle, the influence of the oil sludge adhesion effect on the surfaces of the plates is avoided, and compared with existing equipment, plates can be separated more easily; and in addition, the stacked plate separating device and method can adapt to stacking of the plates of various different shapes and is suitable for separation of the plates of different thicknesses.
Owner:LIAN WEI AUTO PARTS CHONQGING

Special-shaped vibrating screen for separating silvers and tobacco shreds and screening method

The invention discloses a special-shaped vibrating screen for separating silvers and tobacco shreds. The special-shaped vibrating screen is characterized by comprising multiple rows of diversion and organization zones (5) and screen hole zones (6) which are alternatively arranged in the front-back direction, wherein multiple rectangular screen holes (2) are distributed in the screen hole zones (6), a certain distance is reserved between every two adjacent rectangular screen holes (2) and a solid flat plate (7) is limited. Multiple forwards and upwards inclining diversion slope benches (1) aredistributed in the diversion and organization zones (5), a certain distance is reserved between every two adjacent diversion slope benches (1), and an organization groove channel (3) is limited. The special-shaped vibrating screen can solve the problem of silk hanging produced when a traditional screen window type vibrating screen screens a silver and tobacco shred mixture, long-time stable operation can be achieved, and the separating efficiency can be greatly improved.
Owner:CHINA TOBACCO YUNNAN IND

Pain relieving capsule preparation equipment

The invention relates to the technical field of capsule production equipment, and particularly discloses pain relieving capsule preparation equipment which comprises a rack, a venturi tube, a rotary drum, a fixed hopper and a cloth bag, the venturi tube is sequentially divided into an inlet section, a throat part and a diffusion section from bottom to top, and the inlet section of the venturi tube is connected with an air blower; the rotary drum is driven by a driving mechanism to rotate; the lower end of the rotary drum is rotationally sleeved on the periphery of the diffusion section of the venturi tube in a sealing manner; a second through hole is formed in the side wall of the rotary drum; the opening part of the fixed hopper is vertically arranged upwards, the bottom of the fixed hopper is fixedly arranged on the periphery of the inlet section of the venturi tube in a sleeving manner, and the fixed hopper is positioned on the outer side of the rotary drum; the cloth bag is detachably connected to the part, located above the rotary drum, of the rack, the lower portion of the cloth bag is connected with a dust suction pipe, and the dust suction pipe is rotationally connected with the rotary drum in a sealed mode; and the opening of the cloth bag communicates with the outside through an exhaust pipe. The pain relieving capsule preparation equipment aims at solving the problem that the capsule screening efficiency is low due to the fact that wind of a fan is easily blocked by capsules.
Owner:湖南本草制药有限责任公司

A device and method for liquid-liquid extraction and separation of aromatics in diesel oil

The invention provides an apparatus for separating aromatic hydrocarbons in diesel oil through liquid-liquid extraction. The apparatus comprises a liquid-liquid extracting tower (1), a raffinate oil washing tower (2) and a solvent recovery tower (3), wherein a ratio of the diameter D1 of the upper part of the liquid-liquid extracting tower (1) to the diameter D2 of the lower part of the liquid-liquid extracting tower (1) is 0.5 to 0.9, the lower part of the liquid-liquid extracting tower (1) is provided with a raw material feeding pipeline (4), the upper part of the liquid-liquid extracting tower (1) is provided with an extracting solvent feeding pipeline, a top raffinate oil pipeline (7) is connected with the bottom of the raffinate oil washing tower (2), an extract pipeline (11) at the bottom of the liquid-liquid extracting tower (1) is connected with the solvent recovery tower (3), the top of the raffinate oil washing tower (2) is provided with a product discharging pipeline (9), and the bottom of the raffinate oil washing tower (2) is provided with a water draining pipeline (10). The apparatus is used for separating aromatic hydrocarbons in diesel oil through liquid-liquid extraction; through cooperative usage of the apparatus and proper solvents and cosolvents, diesel oil with a high cetane value can be produced, and aromatic hydrocarbons with low alkane content can be obtained.
Owner:CHINA PETROLEUM & CHEM CORP +1

Gas-liquid separator based on porous media board

The invention discloses a gas-liquid separating device based on a porous dielectric-slab. The device is composed of a filter, a gas-liquid separation container, a pressure adjusting valve and a pipeline; the device is characterized in that the gas-liquid separation container is respectively connected with the filter and the pressure adjusting valve, the filter, the gas-liquid separation container, the pressure adjusting valve and the pipeline are connected by a pipe joint or welding, an inlet is arranged at one end of the filter, an exhausting pipeline is arranged at one end of the pressure adjusting valve, and the filter is used for filtering the solid in the gas-liquid mixed fluid. The gas-liquid separation container comprises a pressure container and a porous dielectric-slab, an exhausting pipeline is arranged at the upper end of the gas-liquid separation container, a lyosorpic phase porous dielectric-slab is arranged at the lower end thereof, and an exhausting pipeline is arrangedat one end of the lyosorpic phase porous dielectric-slab. The invention is simple in structure, and convenient in use, can continuously separate gas-liquid mixed fluid in wide loading scope in real time, and can be widely used in gas-liquid separation fields of various pressure and flow ranges.
Owner:INST OF ROCK & SOIL MECHANICS CHINESE ACAD OF SCI

A kind of extraction system and extraction method of duckweed starch

The invention discloses an extraction system of duckweed starch. The extraction system comprises a lifting device, a grinding device, a slag-slurry separation device, a precipitation device and a spin-drying device, wherein a motor is arranged at the top of the lifting device; a transmission chain is arranged in a bin; multiple groups of collection plates for collecting and lifting duckweed are arranged on the transmission chain; the motor drives the transmission chain to rotate; the slag-slurry separation device is provided with a cylinder, and a strip brush is arranged on a spindle in the cylinder; the spin-drying device is provided with a drum which is connected with a vacuum pump through a vacuum pipeline, and the water-containing starch stuck on the surface of the drum is completely pumped by the vacuum pump; and the lifting device, the grinding device, the slag-slurry separation device, the precipitation device and the spin-drying device are connected in turn. The invention also discloses an extraction method for duckweed starch. Through the invention, current blank of starch extraction technology is filled, continuous and efficient extraction of duckweed starch is facilitated after large-scale culture of duckweed, and later utilization and processing of the duckweed starch are convenient.
Owner:QINGDAO INST OF BIOENERGY & BIOPROCESS TECH CHINESE ACADEMY OF SCI

Online low-pressure, middle-pressure and high-pressure combined two-dimension preparation liquid chromatographic system

The invention relates to an online low-pressure, middle-pressure and high-pressure combined two-dimension preparation liquid chromatographic system. Two one-dimension low-pressure, middle-pressure and high-pressure preparation liquid chromatographic systems are organically combined through a six-way valve and software. Pressure used by a second dimension system is not lower than pressure used by a first dimension separation system. When the first dimension system and the second dimension system are low-pressure or middle-pressure preparation liquid chromatographic systems, through switching the six-way valve, target compound directly enters a second dimension chromatographic column for second dimension separation after first dimension separation; and when pressure used by a second dimension separation system is higher than pressure used by the first dimension separation system, a trapping column is connected on the six-way valve, the target compound is adsorbed on the head of the trapping column after the first dimension separation, and then the target compound enters the second dimension chromatographic column for second dimension separation. The invention has the advantages thatthe contradiction between sample injection volume and separation capacity is solved, the large sample injection volume is ensured and the separation capacity of the preparation chromatographic systemis greatly improved; the system structure is simple and the establishment is easy; the operation is simple and convenient and the automation can be easily realized; and the application scope is wide.
Owner:SOOCHOW HIGH TECH CHROMATOGRAPHY
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