Coating debugging and processing control method

By gradually injecting and stirring various raw materials in the coating debugging and processing, and combining real-time monitoring and adjustment of the control system and temperature control system, the problem of lack of item-by-item performance monitoring and high-precision adjustment in the existing technology is solved, and effective monitoring and optimization of coating performance is achieved.

CN115646411BActive Publication Date: 2025-03-07GUANGDONG YUNYI COATING TECH CO LTD
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Patent Information

Application Number
CN202211354694.X
Authority / Receiving Office
CN · China
Patent Type
Patents(China)
Current Assignee / Owner
Filing Date
2022-11-01
Publication Date
2025-03-07
Estimated Expiration
2042-11-01

AI Technical Summary

Technical Problem

During the debugging and processing of existing coatings, there is a lack of item-by-item performance monitoring for different raw material properties, resulting in blurred data adjustment direction and a lack of a sound monitoring system, making it difficult to achieve high-precision adjustment of raw material ratio.

Method used

A coating debugging and processing control method is adopted, and the debugging coating is formed by gradually injecting resin, solvent, emulsifier, wetting and dispersing agent, defoaming agent and pigment into the reactor, and thoroughly stirring and mixing. For unqualified performance indicators, gradually add the corresponding raw materials until the performance is qualified. At the same time, combined with the control system and the temperature control system, the amount of raw materials added and temperature are monitored and adjusted in real time to ensure that the coating layer reaches its best condition.

Benefits of technology

It realizes item by item monitoring and precise adjustment of the various properties of the coating, improves the accuracy of raw material ratio, ensures that the performance of the coating is qualified, and through synchronous monitoring and reverse adjustment, the direction of raw material addition and temperature control is clarified.

✦ Generated by Eureka AI based on patent content.

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Patent Text Reader

Abstract

The invention relates to a coating debugging and processing control method, which comprises the following steps: S1. injecting resin raw material and solvent into a reactor and continuously stirring, and recording the injected mass of the resin raw material as m, and recording the injected mass of the solvent as n; S2. injecting an emulsifier into the reactor through a first feeding mechanism and continuously stirring, and recording the injected mass of the emulsifier as a; S3. injecting a wetting dispersant into the reactor through a second feeding mechanism and continuously stirring, and recording the injected mass of the wetting dispersant as b; S4. injecting a defoaming agent into the reactor through a third feeding mechanism and continuously stirring, and recording the injected mass of the defoaming agent as c; S5. injecting a pigment into the reactor through a fourth feeding mechanism and continuously stirring, and recording the injected mass of the pigment as d; the method performs performance monitoring item by item according to the properties of different raw materials, the monitoring has a strong purpose, and the method of adding raw materials item by item can achieve high-precision adjustment of the raw material ratio.
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Description

Technical Field

[0001] The invention relates to the field of coating processing, in particular to a coating debugging processing control method. Background Art

[0002] The production process of coatings is mainly a physical mixing process. Its main raw materials include resin (film-forming substance) and solvent. In addition, an appropriate amount of additives needs to be added during the mixing process. The additives include emulsifiers, wetting and dispersing agents, defoaming agents and solid coating additives (such as cellulose, pigments), etc. During the physical stirring and mixing of the raw materials, the wetting and dispersing agents mainly play the role of stabilizing the dispersion of solid particles and preventing the tiny particles of solid coatings from aggregating together to form agglomerated particles. The defoaming agent is mainly used to eliminate tiny bubbles in the mixing process. Solid coating additives are mainly used for coating color adjustment, etc.

[0003] During the actual processing and debugging of coatings, the weight of various raw materials added to different types of coatings will also be different. Therefore, when studying new types of coating formulas, it is necessary to debug the amount and proportion of each basic raw material one by one. The current operation method is that people rely on their own operating experience and previous related coating formulas to gradually debug the raw materials that may change in addition in the new coating formula, and then record the added amount of the raw materials that have changed after debugging. If a coating with qualified performance is obtained, it is considered that the debugging is successful. If the coating performance is unqualified, it is considered that the debugging is unsuccessful.

[0004] The current coatings have the following drawbacks during the debugging process: 1. After the current coatings are debugged, the properties of different raw materials are not monitored item by item during the quality monitoring. If the coatings fail to meet the performance requirements at the same time, the addition ratios of the various raw materials need to be arranged and combined. During the debugging process, the target data of each raw material is difficult to find, and the direction of data adjustment is relatively vague.

[0005] 2. After the current paint is debugged, the amount of each raw material added will gradually change. The entire data change process needs to be recorded in real time. The current paint reactor is not equipped with a relatively complete monitoring system. Summary of the invention

[0006] The purpose of the present invention is to solve the defects of the prior art and provide a coating debugging and processing control method.

[0007] In order to achieve the above object, the technical solution adopted by the present invention is as follows:

[0008] The debugging and processing control method of the coating includes the following steps:

[0009] S1. Inject the resin raw material and solvent into the reactor and continue stirring, and record the injected mass of the resin raw material as m, and record the injected mass of the solvent as n;

[0010] S2. injecting an emulsifier into the reactor through the first feeding mechanism and continuously stirring, and recording the injection mass of the emulsifier as a;

[0011] S3. Injecting a wetting and dispersing agent into the reactor through a second feeding mechanism and continuing stirring, and recording the injection mass of the wetting and dispersing agent is b;

[0012] S4. The defoamer is injected into the reactor through a third feeding mechanism and continued stirring, and the injection mass of the defoamer is recorded as c;

[0013] S5. The pigment is injected into the reactor through the fourth feeding mechanism and continued stirring, and the injection mass of the pigment is recorded as d;

[0014] S6. The resin raw material, solvent, emulsifier, wetting dispersant, defoamer and pigment in the reactor are fully stirred and mixed to form a first debugging coating. The first debugging coating is sampled and applied on a sample. The first debugging coating layer on the sample is observed. After the observation is completed, the situation is recorded. The sample coated with the first debugging coating layer is sent to a baking room for a baking experiment. The baking time is 5-10 hours. Then, the appearance change of the first debugging coating layer is observed and the change is recorded.

[0015] S7. Analyze the changes of the first debugging coating layer fed back by S6 one by one;

[0016] S8. If the first debugging coating layer is applied to the surface of the sample, the color depth of the coating layer does not meet the standard, the control system controls the fourth feeding mechanism to intermittently inject pigment into the reactor, and the amount of pigment injected is recorded cumulatively, and the quality data recorded is d1, d2 ... dn;

[0017] Each time the pigment is injected, the reactor is fully stirred and the debug paint is exported. The exported debug paint is applied to a new sample and the color depth is observed. The pigment mass is gradually added many times. Each time the pigment is added, a coating experiment is performed until the color depth reaches the standard. The pigment mass data in the debug paint when the color depth reaches the standard is d k That is the target data;

[0018] S9. After the first debugging coating layer is coated on the surface of the sample, the sample coated with the first debugging coating layer is sent to the baking room for baking experiment. If cracks appear on the surface of the first debugging coating layer, the control system controls the first feeding mechanism to intermittently inject emulsifier into the reactor. When recording the injection amount of the emulsifier, it is cumulatively recorded, and the recorded quality data is a1, a2…an;

[0019] Each time the emulsifier is injected, the reactor is fully stirred, and the debug coating is exported. The exported debug coating is coated on a new sample and a baking test is carried out. The emulsifier is added gradually for many times. Each time the emulsifier is added, a coating test is carried out until the debug coating layer does not crack after the baking test. The quality data of the emulsifier in the debug coating when it meets the standard is a k That is the target data;

[0020] S10. After the first debugging coating layer is coated on the surface of the sample, the sample coated with the first debugging coating layer is sent to the baking room for baking experiment. If particle protrusions appear on the surface of the first debugging coating layer, the control system controls the second feeding mechanism to intermittently inject a wetting and dispersing agent into the reactor. The injection amount of the wetting and dispersing agent is recorded cumulatively, and the recorded quality data is b1, b2...bn;

[0021] Each time the wetting and dispersing agent is injected, the reactor is fully stirred and the debugging paint is exported. The exported debugging paint is coated on a new sample and a baking test is carried out. The wetting and dispersing agent is gradually added many times. Each time the wetting and dispersing agent is added, a coating test is carried out until no particles or protrusions appear in the debugging paint layer after the baking test. The quality data of the wetting and dispersing agent in the debugging paint that meets the standard is b k That is the target data;

[0022] S11. After the first debugging coating layer is coated on the surface of the sample, the sample coated with the first debugging coating layer is sent to the baking room for baking experiment. If there are pores in the cross section of the first debugging coating layer, the control system controls the third feeding mechanism to intermittently inject defoaming agent into the reactor. When recording the injection amount of the defoaming agent, it is cumulatively recorded, and the recorded quality data is c1, c2…cn;

[0023] Each time the defoamer is injected, the reactor is fully stirred and the debug coating is exported. The exported debug coating is coated on a new sample and a baking test is carried out. The defoamer is added gradually for many times. Each time the defoamer is added, a coating test is carried out until no pores appear in the cross section of the debug coating layer after the baking test. The defoamer quality data c in the debug coating that meets the standard k This is the target data.

[0024] According to the technical scheme, the method first injects basic weight portions of resin raw materials, solvents, emulsifiers, wetting and dispersing agents, defoaming agents, and pigments into a reaction kettle, and fully stirs and mixes them to form a first debugging coating. The various properties of the first debugging coating are monitored separately. When a certain property is unqualified, the corresponding raw materials are gradually added for the unqualified performance until the performance monitoring is qualified. Then, the raw materials corresponding to another performance are gradually debugged, and the cycle is repeated until the various properties of the coating are qualified. The method monitors the properties of different raw materials one by one, and the purpose of monitoring is strong. Moreover, the method of adding raw materials one by one can achieve high-precision adjustment of the raw material ratio.

[0025] In addition, this method adopts the synchronous monitoring of the appearance of the coating layer and the use environment, which can not only perform preliminary monitoring of the actual form of the coating, but also monitor the effect of the coating after use. This application combines the real-time performance monitoring of the coating with the coating debugging system. According to the changes in various performance properties of the coating, the addition amount of various raw materials in the coating is reversely changed. The performance monitoring and debugging systems of the coating complement each other, and the adjustment of the raw material addition amount is relatively clear.

[0026] Furthermore, the emulsifier quality data a k , wetting and dispersing agent quality data b k , defoamer quality data c k , Pigment quality data d k After confirmation, the raw materials in the reactor are cleaned. After cleaning, the resin raw material with a mass of m is injected into the reactor again, and the solvent with a mass of n is injected at the same time. At the same time, according to the mass data a k Inject emulsifier, according to quality data b k Injection of wetting and dispersing additive, according to quality data c k Inject defoamer according to quality data d k After the pigment and raw materials are injected, the temperature in the reactor is controlled by the temperature control system, and the temperature environment of the reactor is recorded respectively, and the temperature data are t1, t2…tn;

[0027] After each adjustment of the temperature data, the raw materials in the reactor are fully stirred, that is, a debugging coating is exported, the exported debugging coating is coated on a new sample and a baking experiment is carried out, and the temperature data is gradually adjusted many times. Each time the temperature data is adjusted, a coating experiment is carried out. When the debugging coating layer is in the best state after the baking experiment, the temperature data set in the reactor t k This is the target data.

[0028] Through the above technical solution, after the target data of the addition amount of the resin raw material, solvent, emulsifier, wetting dispersant, defoamer and pigment of the coating are found, the temperature control system gradually controls the temperature of the environment where the reactor is located. Under different temperature environments, the coating processed according to the target data is correspondingly monitored for performance. After the performance monitoring, when the coating layer reaches the optimal state, the temperature data t set in the reactor k That is the target data. The debugging process of raw material addition ratio is independent of the temperature debugging process. In this method, the target data of each raw material is first found through the debugging system, and then the target data of the temperature of the coating processing environment is found through the gradual debugging of the temperature control system. During the coating debugging process, the adjustment direction of each parameter is relatively clear.

[0029] Furthermore, the reaction kettle is connected with a resin raw material supply pipe and a solvent supply pipe, the resin raw material supply pipe is provided with a resin raw material metering pump, and the solvent supply pipe is provided with a solvent metering pump.

[0030] Furthermore, a raw material stirring mechanism is provided in the reactor, and the raw material stirring mechanism includes a first raw material stirring motor installed on the top of the reactor, a reducer connected to the first raw material stirring motor, a first raw material stirring shaft connected to the reducer, and a first raw material stirring blade installed on the first raw material stirring shaft;

[0031] A second raw material stirring motor is provided on one side of the first raw material stirring motor. The second raw material stirring motor is connected to a second raw material stirring shaft. A second raw material stirring blade is installed on the second raw material stirring shaft.

[0032] Further, the first feeding mechanism includes a first feeding box, a first feeding pipe connecting the first feeding box and the reaction kettle, and a first metering pump is installed on the first feeding pipe;

[0033] A first motor is installed on the top of the first feed box, the first motor is connected to a first rotating shaft, a plurality of first paddles are installed on the first rotating shaft, and the first paddles are located in the first feed box. After the equipment is put into use, the first motor is always in a started state to continuously stir the raw materials in the first feed box to prevent precipitation;

[0034] The second feeding mechanism comprises a second feeding box, a second feeding pipe connecting the second feeding box and the reactor, and a second metering pump is installed on the second feeding pipe;

[0035] A second motor is installed on the top of the second feed box, the second motor is connected to the first rotating shaft, a plurality of second paddles are installed on the second rotating shaft, and the second paddles are located in the second feed box. After the equipment is put into use, the second motor is always in the starting state to continuously stir the raw materials in the second feed box to prevent precipitation;

[0036] The third feeding mechanism comprises a third feeding box, a third feeding pipe connecting the third feeding box and the reaction kettle, and a third metering pump is installed on the third feeding pipe;

[0037] A third motor is installed on the top of the third feed box, the third motor is connected to the third rotating shaft, a plurality of third paddles are installed on the third rotating shaft, and the third paddles are located in the third feed box. After the equipment is put into use, the third motor is always in the starting state to continuously stir the raw materials in the third feed box to prevent precipitation;

[0038] The fourth feeding mechanism comprises a fourth feeding box, a fourth feeding pipe connecting the fourth feeding box and the reaction kettle, and a fourth metering pump is installed on the fourth feeding pipe;

[0039] A fourth motor is installed on the top of the fourth feed box, the fourth motor is connected to the fourth rotating shaft, a plurality of fourth paddles are installed on the fourth rotating shaft, and the fourth paddles are located in the fourth feed box. After the equipment is put into use, the fourth motor is always in a started state to continuously stir the raw materials in the fourth feed box to prevent precipitation.

[0040] Furthermore, the temperature control system includes an insulation cover mounted on the outside of the reactor, an insulation chamber is formed between the inner wall of the insulation cover and the outer wall of the reactor, a thermometer, a liquid level gauge and an electric heating tube are arranged in the insulation chamber, the thermometer, the liquid level gauge and the electric heating tube are all installed on the inner wall of the insulation cover and connected to the control system signal, and a water supply valve connected to the insulation chamber is arranged at the bottom of the insulation cover.

[0041] Further, the control system comprises:

[0042] A first execution module, used for controlling the start time of the first metering pump;

[0043] A second execution module, used for controlling the opening time of the second metering pump;

[0044] A third execution module, used for controlling the opening time of the third metering pump;

[0045] A fourth execution module, used for controlling the opening time of a fourth metering pump;

[0046] The fifth execution module is used to control the opening time of the resin raw material metering pump;

[0047] A sixth execution module, used for controlling the opening time of the solvent metering pump;

[0048] The temperature control module is used to control the opening time of the electric heating tube;

[0049] The logic processing unit sends instructions to each execution module to start each metering pump according to the supply amount of raw materials in the reactor;

[0050] A first recording module is used to record the quality data of the material supplied cumulatively by the first metering pump;

[0051] The second recording module is used to record the quality data of the material supplied cumulatively by the second metering pump;

[0052] The third recording module is used to record the quality data of the material supplied cumulatively by the third metering pump;

[0053] A fourth recording module, used for recording the quality data of the material supplied cumulatively by the fourth metering pump;

[0054] The fifth recording module is used to record the quality data of the material supplied cumulatively by the resin raw material metering pump;

[0055] The sixth recording module is used to record the quality data of the material supplied cumulatively by the solvent metering pump;

[0056] The seventh recording module is used to record the parameters of each temperature node of the environment where the reactor is located;

[0057] Through the above technical solution, the control system mainly controls the addition amount of emulsifiers, wetting and dispersing agents, defoaming agents and pigments step by step. The cumulative addition amount of each raw material is recorded in real time by the corresponding recording module. When the addition amount of each raw material changes, the coating formula data in this case can be integrated and exported in time, making data integration convenient.

[0058] Furthermore, a debugging paint sample collection guide device is provided at the bottom of the reactor, and the debugging paint sample collection guide device includes a conveyor belt, a plurality of workstation slots are arranged on the conveyor belt, and a collection bucket is placed in the workstation slots. A first positioner is provided at the bottom of the workstation slots, and a sample export valve is provided at the bottom of the reactor. A second positioner matching the first positioner is provided on the outer side of the sample export valve, and the second positioner and the sample export valve are both connected to the logic processing unit.

[0059] Furthermore, there are multiple samples, which are arranged in a rectangular array on the mounting frame, and the samples and the collection buckets are numbered, and each collection bucket corresponds to one sample;

[0060] A driving trolley is arranged at the bottom of the mounting frame. The driving trolley is placed on a guide rail, and the end of the guide rail extends into the baking room.

[0061] Furthermore, a control panel is provided on the outside of the insulation sleeve, and the control panel is suitable for sending instructions for temperature adjustment and material supply amount adjustment to the control system.

[0062] Through the above technical solution, the control panel is operated by means of a touch screen, and a functional window for adjusting the amount of emulsifier, wetting dispersant, defoaming agent, and pigment added is provided on the control panel, as well as a functional window for adjusting the temperature.

[0063] The beneficial effects of the present invention are as follows: 1. When debugging the formula of the coating, if a certain performance is unqualified, the corresponding raw materials are gradually added for the unqualified performance until the performance is monitored as qualified, and then the raw materials corresponding to another performance are gradually debugged, and the cycle is repeated until all the properties of the coating are qualified. The method monitors the properties of different raw materials one by one, and the purpose of monitoring is strong. Moreover, the method of adding raw materials one by one can achieve high-precision adjustment of the raw material ratio;

[0064] 2. This method uses the synchronous monitoring of the appearance and the use environment of the coating layer, which can not only conduct preliminary monitoring of the actual form of the coating, but also monitor the effect of the coating after use. This application combines the real-time performance monitoring of the coating with the coating debugging system, and reversely changes the addition amount of various raw materials in the coating according to the changes in various properties of the coating. The performance monitoring and debugging system of the coating complement each other, and the adjustment of the raw material addition amount is relatively clear;

[0065] 3. The control system gradually controls the addition amount of emulsifiers, wetting and dispersing agents, defoaming agents and pigments. The cumulative addition amount of each raw material is recorded in real time by the corresponding recording module. When the addition amount of each raw material changes, the coating formula data in this case can be integrated and exported in time, making data integration convenient. BRIEF DESCRIPTION OF THE DRAWINGS

[0066] Figure 1 It is a structural schematic diagram of the processing equipment of the present invention;

[0067] Figure 2 It is a cross-sectional schematic diagram of the reaction kettle of the present invention;

[0068] Figure 3 It is a schematic diagram of the connection between the reaction kettle and each feeding mechanism of the present invention;

[0069] Figure 4 It is a schematic diagram of the principle of the control system of the present invention;

[0070] Figure 5 This is a schematic diagram of the structure of the paint sample collection and guiding device for debugging the present invention.

[0071] Description of reference numerals: 1, reaction kettle; 11, resin raw material supply pipe; 12, solvent supply pipe; 13, resin raw material metering pump; 14, solvent metering pump; 15, first raw material stirring motor; 16, reducer; 17, first raw material stirring shaft; 18, first raw material stirring blade; 19, second raw material stirring motor; 110, second raw material stirring shaft; 111, second raw material stirring blade; 112, sample outlet valve; 113, second positioner;

[0072] 2. Sample; 21. Mounting frame; 22. Driving trolley; 23. Guide rail; 3. Baking room;

[0073] 10. First feeding mechanism; 101. First feeding box; 102. First feeding pipe; 103. First metering pump; 104. First motor; 105. First rotating shaft; 106. First paddle;

[0074] 20. Second feeding mechanism; 201. Second feeding box; 202. Second feeding pipe; 203. Second metering pump; 204. Second motor; 205. Second rotating shaft; 206. Second paddle;

[0075] 30. third feeding mechanism; 301. third feeding box; 302. third feeding pipe; 303. third metering pump; 304. third motor; 305. third rotating shaft; 306. third paddle;

[0076] 40. fourth feeding mechanism; 401. fourth feeding box; 402. fourth feeding pipe; 403. fourth metering pump; 404. fourth motor; 405. fourth rotating shaft; 406. fourth paddle;

[0077] 50. Control system; 501. First execution module; 502. Second execution module; 503. Third execution module; 504. Fourth execution module; 505. Fifth execution module; 506. Sixth execution module; 507. Temperature control module; 508. Logic processing unit; 509. First recording module; 510. Second recording module; 511. Third recording module; 512. Fourth recording module; 513. Fifth recording module; 514. Sixth recording module; 515. Seventh recording module;

[0078] 60. Temperature control system; 601. Insulation sleeve; 602. Insulation chamber; 603. Thermometer; 604. Liquid level gauge; 605. Electric heating tube; 606. Water supply valve;

[0079] 70. Debugging the coating sample collecting guide device; 701. Conveyor belt; 702. Work station slot; 703. Collection bucket; 704. First positioner;

[0080] 80. Control panel. DETAILED DESCRIPTION

[0081] like Figure 1 As shown, the coating debugging and processing control method includes the following steps:

[0082] S1. Inject the resin raw material and solvent into the reactor 1 and continue stirring, and record the mass of the injected resin raw material as m, and record the mass of the injected solvent as n;

[0083] S2. The emulsifier is injected into the reactor 1 through the first feeding mechanism 10 and stirred continuously, and the injection mass of the emulsifier is recorded as a;

[0084] S3. The wetting and dispersing agent is injected into the reactor 1 through the second feeding mechanism 20 and continuously stirred, and the injection mass of the wetting and dispersing agent is recorded as b;

[0085] S4. The defoaming agent is injected into the reactor 1 through the third feeding mechanism 30 and continued stirring, and the injection mass of the defoaming agent is recorded as c;

[0086] S5. The pigment is injected into the reactor 1 through the fourth feeding mechanism 40 and continued stirring, and the injection mass of the pigment is recorded as d;

[0087] S6. The resin raw material, solvent, emulsifier, wetting dispersant, defoamer and pigment in the reactor 1 are fully stirred and mixed to form a first debugging coating. The first debugging coating is sampled and coated on the sample 2. The first debugging coating layer on the sample 2 is observed. After the observation is completed, the situation is recorded, and the sample 2 coated with the first debugging coating layer is sent to the baking room 3 for baking experiment (the temperature in the baking room 3 can be set at 40-60 degrees), the baking time is 5-10 hours, and then the appearance change of the first debugging coating layer is observed and the change is recorded;

[0088] S7. Analyze the changes of the first debugging coating layer fed back by S6 one by one;

[0089] S8. If the first debugging coating layer is applied to the surface of the sample, the color depth of the coating layer does not meet the standard, the control system 50 controls the fourth feeding mechanism 40 to intermittently inject pigment into the reactor 1, and the amount of pigment injected is recorded cumulatively, and the quality data recorded is d1, d2 ... dn;

[0090] Each time the pigment is injected, the reactor 1 is fully stirred and the debugged paint is exported. The exported debugged paint is coated on a new sample 2 and the color depth is observed. The pigment mass is gradually added many times. Each time the pigment is added, a coating experiment is performed until the color depth reaches the standard. The pigment mass data d in the debugged paint when the color depth reaches the standard k That is the target data;

[0091] S9. After the first debugging coating layer is coated on the surface of the sample 2, the sample 2 coated with the first debugging coating layer is sent to the baking room 3 for baking experiment. If cracks appear on the surface of the first debugging coating layer, the control system 50 controls the first feeding mechanism 10 to intermittently inject emulsifier into the reactor 1. When recording the injection amount of the emulsifier, the cumulative record is made, and the recorded quality data is a1, a2…an;

[0092] Each time the emulsifier is injected, the reactor 1 is fully stirred, and the debug coating is exported. The exported debug coating is coated on a new sample 2 and a baking test is carried out. The emulsifier is gradually added for many times. Each time the emulsifier is added, a coating test is carried out until the debug coating layer does not crack after the baking test. The emulsifier quality data a in the debug coating that meets the standard k That is the target data;

[0093] S10. After the first debugging coating layer is coated on the surface of the sample 2, the sample 2 coated with the first debugging coating layer is sent to the baking room 3 for baking experiment. If particle protrusions appear on the surface of the first debugging coating layer, the control system controls the second feeding mechanism 20 to intermittently inject a wetting and dispersing agent into the reactor 1. When recording the injection amount of the wetting and dispersing agent, a cumulative record is made, and the recorded quality data is b1, b2…bn;

[0094] Each time the wetting and dispersing agent is injected, the reactor 1 is fully stirred, and the debug coating is exported. The exported debug coating is coated on a new sample 2 and a baking test is carried out. The wetting and dispersing agent is gradually added for many times. Each time the wetting and dispersing agent is added, a coating test is carried out until no particle protrusions appear in the debug coating layer after the baking test. The quality data of the wetting and dispersing agent in the debug coating when it meets the standard is b k That is the target data;

[0095] S11. After the first debugging coating layer is coated on the surface of the sample, the sample 2 coated with the first debugging coating layer is sent to the baking room 3 for baking experiment. If there are pores in the cross section of the first debugging coating layer, the control system controls the third feeding mechanism 30 to intermittently inject defoaming agent into the reactor. When recording the injection amount of the defoaming agent, it is cumulatively recorded, and the recorded quality data is c1, c2…cn;

[0096] Each time the defoamer is injected, the reactor 1 is fully stirred, and the debug coating is exported. The exported debug coating is coated on a new sample 2 and a baking test is carried out. The defoamer is added step by step for many times. Each time the defoamer is added, a coating test is carried out until no pores appear in the cross section of the debug coating layer after the baking test. The defoamer quality data c in the debug coating that meets the standard k This is the target data.

[0097] Furthermore, the emulsifier quality data a k , wetting and dispersing agent quality data b k , defoamer quality data c k , Pigment quality data d kAfter confirmation, the raw materials in the reactor are cleaned. After cleaning, the resin raw material with a mass of m is injected into the reactor 1 again, and the solvent with a mass of n is injected at the same time. At the same time, according to the mass data a k Inject emulsifier, according to quality data b k Injection of wetting and dispersing additive, according to quality data c k Inject defoamer according to quality data d k After the pigment is injected and the raw material is injected, the temperature in the reactor is controlled by the temperature control system 60, and the temperature environment of the reactor is recorded, and the temperature data are t1, t2 ... tn;

[0098] After each adjustment of the temperature data, the raw materials in the reactor 1 are fully stirred, that is, a debugging coating is exported, and the exported debugging coating is coated on a new sample 2 and a baking experiment is carried out. The temperature data is gradually adjusted many times, and each time the temperature data is adjusted, a coating experiment is carried out. When the debugging coating layer is in the best state after the baking experiment, the temperature data t set in the reactor k This is the target data.

[0099] After finding the target data for the amount of resin raw materials, solvents, emulsifiers, wetting and dispersing agents, defoaming agents, and pigments added to the coating, the temperature control system gradually controls the temperature of the environment where the reactor is located. Under different temperature environments, the coatings processed according to the target data are monitored for performance. After performance monitoring, when the coating layer reaches the optimal state, the temperature data t set in the reactor k That is the target data. The debugging process of raw material addition ratio is independent of the temperature debugging process. In this method, the target data of each raw material is first found through the debugging system, and then the target data of the temperature of the coating processing environment is found through the gradual debugging of the temperature control system. During the coating debugging process, the adjustment direction of each parameter is relatively clear.

[0100] Further, if Figure 1 , Figure 2 As shown, a resin raw material supply pipe 11 and a solvent supply pipe 12 are connected to the reaction kettle 1 . A resin raw material metering pump 13 is provided on the resin raw material supply pipe 11 , and a solvent metering pump 14 is provided on the solvent supply pipe 12 .

[0101] The reactor 1 is provided with a raw material stirring mechanism, which includes a first raw material stirring motor 15 installed on the top of the reactor 1, a reducer 16 connected to the first raw material stirring motor 15, a first raw material stirring shaft 17 connected to the reducer 16, and a first raw material stirring blade 18 installed on the first raw material stirring shaft 17;

[0102] A second raw material stirring motor 19 is disposed on one side of the first raw material stirring motor 15 . The second raw material stirring motor 19 is connected to a second raw material stirring shaft 110 . A second raw material stirring blade 111 is installed on the second raw material stirring shaft 110 .

[0103] Further, if Figure 3 As shown, the first feeding mechanism 10 includes a first feeding box 101, a first feeding pipe 102 connecting the first feeding box 101 and the reactor 1, and a first metering pump 103 is installed on the first feeding pipe 102;

[0104] A first motor 104 is installed on the top of the first feed box 101, and the first motor 104 is connected to a first rotating shaft 105. A plurality of first paddles 106 are installed on the first rotating shaft 105. The first paddles 106 are located in the first feed box 101. After the equipment is put into use, the first motor 104 is always in a started state to continuously stir the raw materials in the first feed box 101 to prevent precipitation;

[0105] The second feeding mechanism 20 comprises a second feeding box 201, a second feeding pipe 202 connecting the second feeding box 201 and the reactor 1, and a second metering pump 203 is installed on the second feeding pipe 202;

[0106] A second motor 204 is installed on the top of the second feed box 201, and the second motor 204 is connected to the first rotating shaft 205. A plurality of second paddles 206 are installed on the second rotating shaft 205, and the second paddles 206 are located in the second feed box 201. After the equipment is put into use, the second motor 204 is always in the starting state to continuously stir the raw materials in the second feed box 201 to prevent precipitation;

[0107] The third feeding mechanism 30 comprises a third feeding box 301, a third feeding pipe 302 connecting the third feeding box 301 and the reactor 1, and a third metering pump 303 is installed on the third feeding pipe 302;

[0108] A third motor 304 is installed on the top of the third feed box 301, and the third motor 304 is connected to a third rotating shaft 305. A plurality of third paddles 306 are installed on the third rotating shaft 306. The third paddles 306 are located in the third feed box 301. After the equipment is put into use, the third motor 304 is always in the starting state to continuously stir the raw materials in the third feed box 301 to prevent precipitation.

[0109] The fourth feeding mechanism 40 comprises a fourth feeding box 401, a fourth feeding pipe 402 connecting the fourth feeding box 401 and the reactor 1, and a fourth metering pump 403 is installed on the fourth feeding pipe 402;

[0110] A fourth motor 404 is installed on the top of the fourth feed box 401, and the fourth motor 404 is connected to the fourth rotating shaft 405. A plurality of fourth paddles 406 are installed on the fourth rotating shaft 405, and the fourth paddles 406 are located in the fourth feed box 401. After the equipment is put into use, the fourth motor 404 is always in a started state to continuously stir the raw materials in the fourth feed box 401 to prevent precipitation.

[0111] Furthermore, the temperature control system 60 includes an insulation sleeve 601 which is sleeved on the outside of the reactor 1. The inner wall of the insulation sleeve 601 and the outer wall of the reactor 1 form an insulation chamber 602. A thermometer 603, a liquid level gauge 604 and an electric heating tube 605 are arranged in the insulation chamber 602. The thermometer 603, the liquid level gauge 604 and the electric heating tube 605 are all installed on the inner wall of the insulation sleeve 601 and are connected to the control system 50 signal. A water supply valve 606 connected to the insulation chamber 603 is arranged at the bottom of the insulation sleeve 601.

[0112] Further, if Figure 4 As shown, the control system 50 includes:

[0113] The first execution module 501 is used to control the start time of the first metering pump 103;

[0114] The second execution module 502 is used to control the opening time of the second metering pump 203;

[0115] The third execution module 503 is used to control the opening time of the third metering pump 303;

[0116] The fourth execution module 504 is used to control the opening time of the fourth metering pump 403;

[0117] The fifth execution module 505 is used to control the opening time of the resin raw material metering pump 13;

[0118] The sixth execution module 506 is used to control the opening time of the solvent metering pump 14;

[0119] The temperature control module 507 is used to control the opening time of the electric heating tube 605;

[0120] The logic processing unit 508 sends instructions to each execution module to start each metering pump according to the supply amount of the raw material in the reactor 1;

[0121] The first recording module 509 is used to record the quality data of the material supplied cumulatively by the first metering pump 103;

[0122] The second recording module 510 is used to record the quality data of the material supplied cumulatively by the second metering pump 203;

[0123] The third recording module 511 is used to record the quality data of the material supplied cumulatively by the third metering pump 303;

[0124] The fourth recording module 512 is used to record the quality data of the material supplied cumulatively by the fourth metering pump 403;

[0125] The fifth recording module 513 is used to record the quality data of the material supplied cumulatively by the resin raw material metering pump 13;

[0126] The sixth recording module 514 is used to record the quality data of the material supplied cumulatively by the solvent metering pump 14;

[0127] The seventh recording module 515 is used to record the parameters of each temperature node of the environment where the reactor is located;

[0128] The control system 50 is mainly used to gradually control the addition amount of emulsifiers, wetting and dispersing agents, defoaming agents and pigments. The cumulative addition amount of each raw material is recorded in real time by the corresponding recording module. When the addition amount of each raw material changes, the paint formula data in this case can be integrated and exported in time, making data integration convenient.

[0129] Further, if Figure 5 As shown, a debugging paint sample collecting guide device 70 is provided at the bottom of the reactor 1, and the debugging paint sample collecting guide device 70 includes a conveyor belt 701, a plurality of workstation slots 702 are arranged on the conveyor belt 701, and a collecting bucket 703 is placed in the workstation slots 702. A first positioner 704 is provided at the bottom of the workstation slots 702, and a sample outlet valve 112 is provided at the bottom of the reactor 1. A second positioner 113 matching the first positioner 704 is provided on the outer side of the sample outlet valve 112, and the second positioner 113 and the sample outlet valve 112 are both connected to the logic processing unit 508.

[0130] There are multiple samples 2, which are arranged in a rectangular array on the mounting frame 21. The samples 2 and the collection barrels 703 are numbered, and each collection barrel 703 corresponds to one sample 2;

[0131] A driving trolley 22 is provided at the bottom of the mounting frame 21 . The driving trolley 22 is placed on a guide rail 23 , and the end of the guide rail 23 extends into the baking room 3 .

[0132] After the paint processing is completed, when sampling is carried out, the conveyor belt 701 drives the empty collecting barrel 703 forward. When the first positioner 704 under the collecting barrel 703 runs to the bottom of the second positioner 113, the first positioner 704 and the second positioner 113 match each other's signals. At this time, the second positioner 113 feeds back the signal to the logic processing unit 508. The logic processing unit 508 controls the sample outlet valve 112 to open. The sample outlet valve 112 introduces a quantitative paint sample in the reactor 1 into the collecting barrel 703. The manual operation at the end of the conveyor belt 701 applies the paint sample in the collecting barrel 703 to the sample 2. During the coating process, the number of the collecting barrel 703 must be consistent with the number of the sample 2.

[0133] Furthermore, a control panel 80 is provided on the outer side of the insulation sleeve 301 , and the control panel 80 is suitable for sending temperature adjustment and material supply quantity adjustment instructions to the control system 50 .

[0134] The control panel 80 is operated by a touch screen, and a functional window for adjusting the amount of emulsifier, wetting dispersant, defoaming agent, and pigment added is provided on the control panel, as well as a functional window for adjusting the temperature.

[0135] Furthermore, when the method is combined with the control system and the temperature control system in actual operation, the specific operation steps are as follows:

[0136] Step 1: Turn on the resin raw material metering pump 13, inject the resin raw material into the reactor 1 through the resin raw material supply pipe 11, turn on the solvent metering pump 14, inject the solvent into the reactor 1 through the solvent supply pipe 12, turn on the first raw material stirring motor 15 and the second raw material stirring motor 19, and continuously stir the basic raw material in the reactor 1. The fifth recording module 513 records the injected mass of the resin raw material as m, and the sixth recording module 514 records the injected mass of the solvent as n;

[0137] Step 2. Manually input the minimum amount of emulsifier added through the function window on the control panel 80 (the amount is determined based on the worker's experience, and ordinary coatings have basic reference standards, and the specific data are not disclosed). After the command is input, the first execution module 501 of the control system 50 controls the first metering pump 103 to open, and the first feed pipe 102 injects the emulsifier into the reactor 1 and continues to stir, and the first recording module 509 of the control system records the injected mass of the emulsifier as a;

[0138] Step 3. Manually input the minimum amount of wetting and dispersing agent added through the function window on the control panel 80. After the command is input, the second execution module 502 of the control system controls the second metering pump 203 to open, and the second feed pipe 202 injects the wetting and dispersing agent into the reactor 1 and continues to stir. The second recording module 510 of the control system records the injection mass of the emulsifier as b;

[0139] Step 4. Manually input the minimum amount of defoaming agent added through the function window on the control panel 80. After the command is input, the third execution module 503 of the control system controls the third metering pump 303 to open, and the third feed pipe 302 injects the defoaming agent into the reactor 1 and continues to stir. The third recording module 511 of the control system records the injection mass of the defoaming agent as c;

[0140] Step 5. Manually input the minimum amount of pigment added through the function window on the control panel 80. After the command is input, the fourth execution module 504 of the control system controls the fourth metering pump 403 to open, the fourth feed pipe 402 injects the pigment into the reactor 1 and continues to stir, and the fourth recording module 512 of the control system records the injected mass of the pigment as d;

[0141] Step 6. Fully stir and mix the resin raw material, solvent, emulsifier, wetting dispersant, defoamer and pigment in the reactor 1 to form a first debugging coating after mixing. Sample the first debugging coating and apply it on the sample 2. Observe the first debugging coating layer on the sample 2. After the observation is completed, record the situation. Drive the trolley to send the sample coated with the first debugging coating layer into the baking room 3 for baking experiment. The baking time is 5-10 hours. Then observe the appearance changes of the first debugging coating layer and record the changes.

[0142] Step 7. Analyze the changes of the first debugging coating layer fed back in step 6 one by one;

[0143] Step eight. If the first debugging coating layer is applied to the surface of the sample, the color depth of the coating layer does not meet the standard, the control system controls the fourth feeding mechanism 40 to intermittently inject pigment into the reactor 1, and the amount of pigment injected is recorded cumulatively, and the quality data recorded is d1, d2 ... dn;

[0144] Each time the pigment is injected, the reactor is fully stirred and the debug paint is exported. The exported debug paint is applied to a new sample and the color depth is observed. The pigment mass is gradually added many times. Each time the pigment is added, a coating experiment is performed until the color depth reaches the standard. The pigment mass data in the debug paint when the color depth reaches the standard is d k That is the target data;

[0145] Step 9. After the first debugging coating layer is coated on the surface of the sample, the sample coated with the first debugging coating layer is sent to the baking room 3 for baking experiment. If cracks appear on the surface of the first debugging coating layer, the control system controls the first feeding mechanism 10 to intermittently inject emulsifier into the reactor 1. The injection amount of the emulsifier is recorded cumulatively, and the recorded quality data is a1, a2…an;

[0146] Each time the emulsifier is injected, the reactor is fully stirred, and the debug coating is exported. The exported debug coating is coated on a new sample and a baking test is carried out. The emulsifier is added gradually for many times. Each time the emulsifier is added, a coating test is carried out until the debug coating layer does not crack after the baking test. The quality data of the emulsifier in the debug coating when it meets the standard is a k That is the target data;

[0147] Step 10. After the first debugging coating layer is coated on the surface of the sample, the sample coated with the first debugging coating layer is sent to the baking room 3 for baking experiment. If particle protrusions appear on the surface of the first debugging coating layer, the control system controls the second feeding mechanism 20 to intermittently inject the wetting and dispersing agent into the reactor 1. The injection amount of the wetting and dispersing agent is recorded cumulatively, and the recorded quality data is b1, b2...bn;

[0148] Each time the wetting and dispersing agent is injected, the reactor 1 is fully stirred, and the debug coating is exported. The exported debug coating is coated on a new sample 2 and a baking test is carried out. The wetting and dispersing agent is gradually added for many times. Each time the wetting and dispersing agent is added, a coating test is carried out until no particle protrusions appear in the debug coating layer after the baking test. The quality data of the wetting and dispersing agent in the debug coating when it meets the standard is b k That is the target data;

[0149] Step 11. After the first debugging coating layer is coated on the surface of the sample, the sample coated with the first debugging coating layer is sent to the baking room 3 for baking experiment. If there are pores in the cross section of the first debugging coating layer, the control system controls the third feeding mechanism 30 to intermittently inject defoaming agent into the reactor 1. When recording the injection amount of the defoaming agent, it is cumulatively recorded, and the recorded quality data is c1, c2...cn;

[0150] After each adjustment of the temperature data, the raw materials in the reactor 1 are fully stirred, that is, a debugging coating is exported, and the exported debugging coating is coated on a new sample 2 and a baking experiment is carried out. The temperature data is gradually adjusted many times, and each time the temperature data is adjusted, a coating experiment is carried out. When the debugging coating layer is in the best state after the baking experiment, the temperature data t set in the reactor k That is the target data;

[0151] Step 12. The data recorded by each recording module is stored by the logic processing unit 508, and the data recorded by the recording module is reset to zero. The raw materials in the reactor 1 are cleaned. After the cleaning is completed, the resin raw material with a mass of m is injected into the reactor again, and the solvent with a mass of n is injected at the same time. At the same time, according to the mass data a k Inject emulsifier, according to quality data b kInjection of wetting and dispersing additive, according to quality data c k Inject defoamer according to quality data d k Inject pigment, the data of each raw material is recorded by the corresponding recording module. After the raw material is injected, the temperature control module 507 of the temperature control system 60 controls the heating time of the electric heater 605, so as to control the temperature in the reactor 1. The thermometer 603 monitors the temperature environment of the reactor 1. The data of each temperature node are t1, t2...tn. The temperature data of each node can be set on the control panel. At the same time, the seventh recording module 515 records the specific values ​​of t1, t2...tn respectively.

[0152] After each adjustment of the temperature data, the raw materials in the reactor 1 are fully stirred, that is, a debugging coating is exported, and the exported debugging coating is coated on a new sample 2 and a baking experiment is carried out. The temperature data is gradually adjusted many times, and each time the temperature data is adjusted, a coating experiment is carried out. When the debugging coating layer is in the best state after the baking experiment, the temperature data t set in the reactor k That is the target data;

[0153] Step 13: After the control system 50 obtains the target data of each raw material and the target data of the temperature, the logic processing unit 508 integrates the target data and sends it to the background system for the background technicians to review and archive.

[0154] In summary, when debugging the formula of the coating, when a certain performance is unqualified, the corresponding raw materials are gradually added for the unqualified performance until the performance monitoring is qualified, and then the raw materials corresponding to another performance are gradually debugged, and the cycle is repeated until all the properties of the coating are qualified. This method monitors the properties of different raw materials one by one, and the monitoring purpose is strong. Moreover, the method of adding raw materials one by one can achieve high-precision adjustment of the raw material ratio;

[0155] This method uses the synchronous monitoring of the appearance and the use environment of the coating layer, which can not only conduct preliminary monitoring of the actual form of the coating, but also monitor the effect of the coating after use. This application combines the real-time performance monitoring of the coating with the coating debugging system, and reversely changes the addition amount of various raw materials in the coating according to the changes in various properties of the coating. The performance monitoring and debugging system of the coating complement each other, and the adjustment of the raw material addition amount is relatively clear;

[0156] The control system gradually controls the addition amount of emulsifiers, wetting and dispersing agents, defoaming agents and pigments. The cumulative addition amount of each raw material is recorded in real time by the corresponding recording module. When the addition amount of each raw material changes, the coating formula data in this case can be integrated and exported in time, making data integration convenient.

[0157] The above shows and describes the basic principles, main features and advantages of the present invention. Those skilled in the art should understand that the present invention is not limited to the above embodiments. The above embodiments and descriptions only describe the principles of the present invention. The present invention may be subject to various changes and improvements without departing from the spirit and scope of the present invention. These changes and improvements fall within the scope of the present invention. The scope of protection claimed by the present invention is defined by the attached claims and their equivalents.

Claims

1. A coating debugging and processing control method, characterized in that: The steps include: S1. Injecting the resin raw material and the solvent into the reactor (1) and stirring continuously, and recording the injected mass of the resin raw material as m, and recording the injected mass of the solvent as n; S2. injecting an emulsifier into the reactor (1) through the first feeding mechanism (10) and continuously stirring, and recording the injected mass of the emulsifier as a; S3. Injecting a wetting and dispersing agent into the reactor (1) through a second feeding mechanism (20) and continuously stirring, and recording the injection mass of the wetting and dispersing agent as b; S4. Defoaming agent is injected into the reactor (1) through a third feeding mechanism (30) and continuously stirred, and the injection mass of the defoaming agent is recorded as c; S5. The pigment is injected into the reactor through the fourth feeding mechanism (40) and continuously stirred, and the mass of the injected pigment is recorded as d; S6. The resin raw material, solvent, emulsifier, wetting dispersant, defoamer and pigment in the reaction kettle (1) are fully stirred and mixed to form a first debugging coating. The first debugging coating is sampled and coated on the sample (2). The first debugging coating layer on the sample (2) is observed. After the observation is completed, the situation is recorded. The sample (2) coated with the first debugging coating layer is sent to the baking room (3) for a baking experiment. The baking time is 5-10 hours. Then, the appearance change of the first debugging coating layer is observed and the change is recorded. S7. Analyze the changes of the first debugging coating layer fed back by S6 one by one; S8. If the first debugging coating layer is applied to the surface of the sample, the color depth of the coating layer does not meet the standard, then the control system controls the fourth feeding mechanism to intermittently inject pigment into the reactor (1), and the amount of pigment injected is recorded cumulatively, and the quality data recorded is d1, d2 ... dn; Each time the pigment is injected, the reaction kettle (1) is fully stirred and the debugged paint is exported. The exported debugged paint is coated on a new sample (2) and the color depth is observed. The pigment mass is gradually added multiple times. Each time the pigment is added, a coating experiment is performed until the color depth reaches the standard. The pigment mass data d in the debugged paint when the color depth reaches the standard is k That is the target data; S9. After the first debugging coating layer is coated on the surface of the sample, the sample (2) coated with the first debugging coating layer is sent to the baking room (3) for baking experiment. If cracks appear on the surface of the first debugging coating layer, the control system (50) controls the first feeding mechanism (10) to intermittently inject emulsifier into the reaction kettle (1). When recording the injection amount of the emulsifier, it is cumulatively recorded, and the recorded quality data are a1, a2...an; Each time the emulsifier is injected, the reactor (1) is fully stirred, and the debug coating is discharged. The discharged debug coating is coated on a new sample (2) and a baking test is carried out. The emulsifier is added gradually for many times. Each time the emulsifier is added, a coating test is carried out until the debug coating layer does not crack after the baking test. The quality data of the emulsifier in the debug coating when it meets the standard is a k That is the target data; S10. After the first debugging coating layer is coated on the surface of the sample (2), the sample coated with the first debugging coating layer is sent to the baking room (3) for baking experiment. If particle protrusions appear on the surface of the first debugging coating layer, the control system (50) controls the second feeding mechanism (20) to intermittently inject a wetting and dispersing agent into the reactor (1). When recording the amount of the wetting and dispersing agent injected, it is cumulatively recorded, and the recorded quality data is b1, b2...bn; Each time the wetting and dispersing agent is injected, the reactor is fully stirred and the debug coating is exported. The exported debug coating is coated on a new sample (2) and a baking test is carried out. The wetting and dispersing agent is added step by step for many times. Each time the wetting and dispersing agent is added, a coating test is carried out until no particles or protrusions appear in the debug coating layer after the baking test. The quality data of the wetting and dispersing agent in the debug coating when it meets the standard is b. k That is the target data; S11. After the first debugging coating layer is coated on the surface of the sample, the sample (2) coated with the first debugging coating layer is sent to the baking room (3) for baking experiment. If there are pores in the cross section of the first debugging coating layer, the control system (50) controls the third feeding mechanism (30) to intermittently inject defoaming agent into the reactor (1). When recording the amount of defoaming agent injected, it is cumulatively recorded, and the recorded quality data is c1, c2...cn; Each time the defoamer is injected, the reactor (1) is fully stirred, and the debug coating is discharged. The discharged debug coating is coated on a new sample (2) and a baking test is carried out. The defoamer is added step by step for many times. Each time the defoamer is added, a coating test is carried out until no pores appear in the cross section of the debug coating layer after the baking test. The defoamer quality data c in the debug coating that meets the standard k This is the target data.

2. The coating debugging and processing control method according to claim 1, characterized in that: Emulsifier quality dataa k , wetting and dispersing agent quality data b k , defoamer quality data c k , Pigment quality data d k After confirmation, the raw materials in the reactor are cleaned. After cleaning, the resin raw material with a mass of m is injected into the reactor again, and the solvent with a mass of n is injected at the same time. At the same time, according to the mass data a k Inject emulsifier, according to quality data b k Injection of wetting and dispersing additive, according to quality data c k Inject defoamer according to quality data d k After the pigment and raw materials are injected, the temperature in the reactor (1) is controlled by the temperature control system (60), and the temperature environment of the reactor is recorded, and the temperature data are t1, t2 ... tn respectively; After each adjustment of the temperature data, the raw materials in the reactor are fully stirred, that is, a debugging coating is exported, and the exported debugging coating is coated on a new sample (2) and a baking experiment is carried out. The temperature data is gradually adjusted many times, and each time the temperature data is adjusted, a coating experiment is carried out. When the debugging coating layer is in the best state after the baking experiment, the temperature data t set in the reactor is k This is the target data.

3. The coating debugging and processing control method according to claim 2, characterized in that: The reaction kettle (1) is connected to a resin raw material supply pipe (11) and a solvent supply pipe (12); the resin raw material supply pipe (11) is provided with a resin raw material metering pump (13); and the solvent supply pipe (12) is provided with a solvent metering pump (14).

4. The coating debugging and processing control method according to claim 3, characterized in that: The reactor (1) is provided with a raw material stirring mechanism, which comprises a first raw material stirring motor (15) installed on the top of the reactor (1), a reducer (16) connected to the first raw material stirring motor (15), a first raw material stirring shaft (17) connected to the reducer (16), and a first raw material stirring blade (18) installed on the first raw material stirring shaft (17); A second raw material stirring motor (19) is provided on one side of the first raw material stirring motor (15); the second raw material stirring motor (19) is connected to a second raw material stirring shaft (110); and a second raw material stirring blade (111) is installed on the second raw material stirring shaft (110).

5. The coating debugging and processing control method according to claim 3, characterized in that: The first feeding mechanism (10) comprises a first feeding box (101), a first feeding pipe (102) connecting the first feeding box (101) and the reaction kettle (1), and a first metering pump (103) is installed on the first feeding pipe (102); A first motor (104) is installed on the top of the first material supply box (101), the first motor (104) is connected to a first rotating shaft (105), a plurality of first paddles (106) are installed on the first rotating shaft (105), and the first paddles (106) are located in the first material supply box (101); The second feeding mechanism (20) comprises a second feeding box (201), a second feeding pipe (202) connecting the second feeding box (201) and the reaction kettle (1), and a second metering pump (203) is installed on the second feeding pipe (202); A second motor (204) is installed on the top of the second material supply box (201), the second motor (204) is connected to the first rotating shaft (105), a plurality of second paddles (206) are installed on the second rotating shaft (205), and the second paddles (206) are located in the second material supply box (201); The third feeding mechanism (30) comprises a third feeding box (301), a third feeding pipe (302) connecting the third feeding box (301) and the reaction kettle (1), and a third metering pump (303) is installed on the third feeding pipe (302); A third motor (304) is installed on the top of the third material supply box (301), the third motor (304) is connected to a third rotating shaft (305), a plurality of third paddles (306) are installed on the third rotating shaft (305), and the third paddles (306) are located in the third material supply box (301); The fourth feeding mechanism (40) comprises a fourth feeding box (401), a fourth feeding pipe (402) connecting the fourth feeding box (401) and the reaction kettle (1), and a fourth metering pump (403) is installed on the fourth feeding pipe (402); A fourth motor (404) is installed on the top of the fourth material supply box (401), the fourth motor (404) is connected to a fourth rotating shaft (405), a plurality of fourth paddles (406) are installed on the fourth rotating shaft (405), and the fourth paddles (406) are located in the fourth material supply box (401).

6. The coating debugging and processing control method according to claim 5, characterized in that: The temperature control system (60) comprises a heat preservation sleeve (601) sleeved on the outside of the reaction kettle (1); a heat preservation chamber (602) is formed between the inner wall of the heat preservation sleeve (601) and the outer wall of the reaction kettle (1); a thermometer (603), a liquid level gauge (604) and an electric heating pipe (605) are arranged in the heat preservation chamber (602); the thermometer (603), the liquid level gauge (604) and the electric heating pipe (605) are all mounted on the inner wall of the heat preservation sleeve (601) and are connected to the control system (50) by signal; and a water supply valve (606) connected to the heat preservation chamber (602) is arranged at the bottom of the heat preservation sleeve (601).

7. The coating debugging and processing control method according to claim 6, characterized in that: The control system (50) comprises: A first execution module (501), used for controlling the start time of the first metering pump (103); A second execution module (502), used for controlling the start time of the second metering pump (203); A third execution module (503), used for controlling the start time of the third metering pump (303); A fourth execution module (504), used for controlling the start time of the fourth metering pump (403); A fifth execution module (505), used for controlling the start time of the resin raw material metering pump (13); A sixth execution module (506), used for controlling the start time of the solvent metering pump (14); A temperature control module (507), used to control the opening time of the electric heating tube (605); The logic processing unit (508) sends instructions to each execution module according to the supply amount of the raw materials in the reactor to start each metering pump; A first recording module (509), used for recording the mass data of the material supplied cumulatively by the first metering pump (103); A second recording module (510) is used to record the mass data of the material supplied cumulatively by the second metering pump (203); A third recording module (511), used for recording the quality data of the material supplied cumulatively by the third metering pump (303); A fourth recording module (512), used for recording the mass data of the material supplied cumulatively by the fourth metering pump (403); A fifth recording module (513), used for recording the quality data of the material supplied cumulatively by the resin raw material metering pump (13); A sixth recording module (514), used for recording the quality data of the material supplied cumulatively by the solvent metering pump (14); The seventh recording module (515) is used to record the parameters of each temperature node of the environment where the reactor (1) is located.

8. The coating debugging and processing control method according to claim 7, characterized in that: A debugging paint sample collecting guide device (70) is provided at the bottom of the reaction kettle (1), and the debugging paint sample collecting guide device (70) comprises a conveyor belt (701), a plurality of workstation slots (702) are arranged on the conveyor belt (701), and a collection bucket (703) is arranged in the workstation slots (702), and a first positioner (704) is provided at the bottom of the workstation slots (702). A sample outlet valve (112) is provided at the bottom of the reaction kettle (1), and a second positioner (113) matching the first positioner (704) is provided on the outer side of the sample outlet valve (112), and the second positioner (113) and the sample outlet valve (112) are both connected to the logic processing unit (508).

9. The coating debugging and processing control method according to claim 8, characterized in that: There are a plurality of the sample plates (2), and the plurality of sample plates (2) are arranged in a rectangular array on the mounting frame (21); the sample plates (2) and the collection barrels (703) are both numbered, and each collection barrel (703) corresponds to a sample plate (2); A driving trolley (22) is provided at the bottom of the mounting frame (21), and the driving trolley (22) is placed on a guide rail (23), and the end of the guide rail (23) extends into the baking room (3).

10. The coating debugging and processing control method according to claim 8, characterized in that: A control panel (80) is provided on the outside of the heat-insulating sleeve (601), and the control panel (80) is suitable for sending temperature adjustment and material supply quantity adjustment instructions to the control system (50).

Citation Information

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