Square steel pipe and its manufacturing method and building structure

By controlling the width of the steel plate and the perimeter of the square-forming frame, and managing the roll forming conditions, the problems of low ductility and toughness of the corners of the square-forming steel pipe are solved, and finished products with a small radius of curvature and a flat plate are achieved, reducing the cost and improving the seismic resistance.

CN116323065BActive Publication Date: 2025-04-08JFE STEEL CORP
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Patent Information

Application Number
CN202180066462.1
Authority / Receiving Office
CN · China
Patent Type
Patents(China)
Current Assignee / Owner
Priority Date
2020-10-05
Filing Date
2021-09-15
Publication Date
2025-04-08
Estimated Expiration
2041-09-15

AI Technical Summary

Technical Problem

The existing roll-formed square steel pipes are severely hardened at the corners during manufacturing, resulting in low ductility and toughness, making it difficult to meet the requirements of building column materials for earthquake resistance. At the same time, heating processes are required during the forming process, which is relatively expensive.

Method used

By controlling the plate width of the raw steel plate and the circumference of the resistance-welded steel pipe of the square-forming frame, the rolling conditions during the forming process are managed, the radius of curvature of the corners is small, the flat plates are flat, and the ductility and toughness of the corners are improved.

Benefits of technology

Square steel pipes with small radius of curvature at the corners, flat plates, excellent corner ductility and toughness are realized, reducing the heating process requirements during the forming process and improving the seismic resistance of the building structure.

✦ Generated by Eureka AI based on patent content.

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Abstract

The present invention provides a square steel pipe and a manufacturing method thereof, and a building structure. The present invention is a square steel pipe having a flat plate portion and a corner portion, wherein when the average wall thickness of the flat plate portion is set to t (mm), the radius of curvature R of the outer side of the corner portion is greater than or equal to 2.0t and less than or equal to 3.0t, the flatness of the outer surface of the flat plate portion is less than or equal to 2.5mm, the uniform elongation E2 at a position 1 / 4t from the outer surface of the corner portion in the wall thickness direction is greater than or equal to 0.60 times the uniform elongation E1 at a position 1 / 4t from the outer surface of the flat plate portion in the wall thickness direction, and the Charpy absorbed energy at -10°C at a position 1 / 4t from the outer surface of the corner portion in the wall thickness direction is greater than or equal to 100J.
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Description

Technical Field

[0001] The present invention relates to a square steel pipe which is particularly suitable for use as a building member in large buildings such as mid-rise buildings, factories, warehouses, etc. having a height greater than 20 m and a method for manufacturing the same. In addition, the present invention relates to a building structure using the square steel pipe of the present invention as a column material. Background Art

[0002] From the viewpoint of earthquake resistance, high ductility and toughness are required for building columns.

[0003] When a square steel pipe having corners and flat portions used as a column is subjected to a large external force such as an earthquake force, the outer surface of the corner portion in particular is greatly deformed. Therefore, the ductility and toughness of the outer surface of the corner portion of the square steel pipe must be sufficiently improved.

[0004] Cold roll-formed square steel pipe (roll-formed square steel pipe) is a square steel pipe widely used as a column material for buildings. The square steel pipe is manufactured by the following method: a steel strip is formed into a cylindrical open pipe by cold roll forming, the butt joint of the open pipe is subjected to resistance welding to form a resistance welded steel pipe, and then, the resistance welded steel pipe is reduced in diameter along the pipe axis direction in a cylindrical state using rollers arranged above, below, left and right of the resistance welded steel pipe, and then formed into a square. In the above-mentioned resistance welding, the butt joint is heated to melt, pressed and solidified, thereby completing the joining.

[0005] However, although the roll-formed square steel pipe has high productivity, on the other hand, the corners are greatly work-hardened during production, so there is a problem that the ductility and toughness of the corners are lower than those of the flat plate.

[0006] In addition, from the perspective of construction site construction and building design, the square steel pipe used for the column is also required to have a smaller curvature radius at the corner. This is because when the area of ​​the flat plate portion of the column is large, the area that can be joined to the beam is large, and a higher degree of freedom in architectural design can be achieved.

[0007] However, for the roll-formed square steel tube, the larger the ratio of the average wall thickness t to the average side length H (i.e., t / H), the greater the circumferential bending strain required for forming the steel strip, and the greater the work hardening amount of the corner. In addition, the smaller the radius of curvature of the corner, the greater the circumferential bending strain required for forming the corner, and the greater the work hardening amount of the corner. Therefore, in the roll-formed square steel tube in which the ratio of the average wall thickness t to the average side length H (t / H) is large and the radius of curvature of the corner is small, the ductility and toughness of the corner are particularly low, and it is difficult to ensure sufficient seismic performance.

[0008] Here, the "average wall thickness t" refers to the average value of the wall thickness (mm) at the center position of the tube circumference of the three flat plate portions excluding the flat plate portion including the welded portion (resistance welded portion). The "average side length H" refers to the average value of the side lengths of the two adjacent flat plate portions sandwiching the corner portion.

[0009] In response to such a demand, for example, square steel pipes described in Patent Documents 1 to 4 have been proposed.

[0010] Patent Document 1 proposes that a semi-formed square steel pipe is formed by bending a steel plate to which vanadium is added as a chemical component, then welding the semi-formed square steel pipe, heating the semi-formed square steel pipe to the vicinity of the A3 transformation point, hot forming the semi-formed square steel pipe, and then cooling the semi-formed square steel pipe. It is disclosed that the square steel pipe has improved endurance and toughness, and has a sharp corner shape.

[0011] Patent Document 2 proposes a square steel pipe obtained by heat-treating a cold-formed portion. It is disclosed that the square steel pipe has improved mechanical properties and weldability of the cold-formed portion.

[0012] Patent Document 3 proposes a square steel pipe in which the toughness and plastic deformation ability of the corners are improved by appropriately controlling the chemical composition of the raw steel plate, the bainite fraction of the metal structure, and the Vickers hardness of the surface layer of the corners.

[0013] Patent Document 4 proposes a square steel pipe in which the toughness of the corners is improved by appropriately controlling the chemical composition of a raw steel plate and the average crystal grain size of the hard phase and ferrite in the metal structure.

[0014] Therefore, for roll-formed square steel pipes, it is also required to establish a technology for improving shape characteristics, especially a technology for achieving both improvement in flatness of the flat plate portion and reduction in the radius of curvature of the corner portion. In response to this requirement, for example, Patent Documents 5 and 6 propose technologies for improving shape characteristics by adjusting manufacturing conditions during roll forming.

[0015] Specifically, Patent Document 5 proposes the following method for forming a square steel pipe: when a steel pipe is formed into a square pipe using three or four stages of square forming rolls and the reduction rate of the final stage roll is kept constant, as the wall thickness / outer diameter ratio of the steel pipe increases, the diameter of the final stage roll is reduced (from convex to concave) to perform forming.

[0016] Patent document 6 proposes a method for manufacturing a structural square tube, which includes: a first forming process, in which when a cylindrical billet tube is roll-formed into a square tube, the outer diameter of the billet tube is set to D, the wall thickness of the billet tube is set to t, and the maximum diameter height is set to H, and the set pressing rate Q defined by Q = (DH) / (Dt) × 100 is maintained in the range of 12 to 23% to form the billet tube into a rectangular cross-sectional shape; and a forming process after the second stage, in which the billet tube formed into a rectangular cross-sectional shape is formed into a target shape.

[0017] Prior art literature

[0018] Patent Literature

[0019] Patent Document 1: Japanese Patent Application Publication No. 2004-330222

[0020] Patent Document 2: Japanese Patent Application Laid-Open No. 10-60580

[0021] Patent Document 3: Japanese Patent No. 5385760

[0022] Patent Document 4: Japanese Patent Application Publication No. 2018-53281

[0023] Patent Document 5: Japanese Patent Application Laid-Open No. 4-224023

[0024] Patent Document 6: Japanese Patent No. 3197661 Summary of the invention

[0025] Problems to be solved by the invention

[0026] However, the square steel pipes described in Patent Documents 1 and 2 require a heating process during or after forming, and therefore are very expensive compared to cold-formed roll-formed square steel pipes. Therefore, it is required to establish a technology for obtaining a desired square steel pipe without requiring a heating process during or after forming.

[0027] Furthermore, the square steel pipes described in Patent Documents 3 and 4 cannot sufficiently suppress a decrease in uniform elongation at the corners due to work hardening during forming, and therefore cannot be said to be able to sufficiently ensure ductility and toughness of the outer surface of the corners.

[0028] Furthermore, the techniques described in Patent Documents 5 and 6 cannot perform forming while suppressing the work hardening of the corners. Therefore, it cannot be said that they are sufficient as a technique for achieving both improved flatness of the flat plate portion of the square steel pipe and reduced curvature radius of the corners, while sufficiently ensuring ductility and toughness of the outer surface of the corners.

[0029] The present invention is completed in view of the above situation, and its purpose is to provide a square steel pipe with excellent shape characteristics, ductility and toughness of the outer surface of the corner and a manufacturing method thereof, and to provide a building structure with excellent earthquake resistance.

[0030] Here, "excellent shape characteristics" in the present invention refers to a square steel pipe having a small radius of curvature at the corners and a flat flat plate portion.

[0031] The above-mentioned “small curvature radius of the corner” means that the curvature radius R of the outer side of the corner is controlled within a specified range. Specifically, when the average wall thickness of the flat plate portion is set to t (mm), the curvature radius R of the outer side of the corner is greater than 2.0t and less than 3.0t.

[0032] The above-mentioned "flat plate portion is flat" means that the flatness of the outer surface of the flat plate portion in the tube axis direction is 2.5 mm or less. Specifically, in the cross section of the plane perpendicular to the tube axis direction, the absolute value represented by the maximum bulge and the maximum depression with respect to the straight line passing through two points at both ends of the circumferential direction on the same side of the outer surface of the flat plate portion is 2.5 mm or less at most (see below). Fig.10 ).

[0033] In addition, the "excellent ductility of the outer surface of the corner" mentioned in the present invention means that when the average wall thickness of the flat portion and the corner is set to t, the uniform elongation E2 at a position 1 / 4t away from the outer surface of the corner in the wall thickness direction is 0.60 times or more relative to the uniform elongation E1 at a position 1 / 4t away from the outer surface of the flat portion in the wall thickness direction.

[0034] In the present invention, “the outer surface of the corner portion has excellent toughness” means that the Charpy absorbed energy of the corner portion at -10°C at a position 1 / 4t from the outer surface of the corner portion in the wall thickness direction is 100 J or more.

[0035] It should be noted that the above-mentioned radius of curvature, flatness, uniform elongation and toughness can be measured by the methods described in the examples described later.

[0036] Methods used to solve problems

[0037] The present inventors have conducted intensive studies to solve the above-mentioned problems, and as a result, have found that by managing the plate width of the raw steel plate and the circumference of the electric resistance welded steel pipe on the inlet side of the square forming stand within an appropriate range relative to the circumference of the square steel pipe on the outlet side of the square forming stand, it is possible to manufacture a square steel pipe having a small radius of curvature of the corner, a flat plate portion, and excellent ductility and toughness of the outer surface of the corner.

[0038] The present invention has been accomplished based on the above-described findings and includes the following gist.

[0039] [1] A square steel pipe having a flat portion and a corner portion, wherein:

[0040] When the average thickness of the flat plate portion is t (mm), the radius of curvature R of the outer side of the corner portion is greater than or equal to 2.0t and less than or equal to 3.0t,

[0041] The flatness of the outer surface of the flat plate portion is less than 2.5 mm.

[0042] The uniform elongation E2 at a position 1 / 4t from the outer surface of the corner portion in the wall thickness direction is 0.60 times or more relative to the uniform elongation E1 at a position 1 / 4t from the outer surface of the flat plate portion in the wall thickness direction,

[0043] The Charpy absorbed energy at -10°C at a position 1 / 4t away from the outer surface of the corner portion in the wall thickness direction is 100 J or more.

[0044] [2] The square steel pipe according to [1], wherein the average wall thickness t is greater than 0.030 times the average side length H (mm) of the flat plate portion.

[0045] [3] The square steel pipe according to [1] or [2], wherein the average wall thickness t is greater than or equal to 20 mm and less than or equal to 40 mm.

[0046] [4] The square steel pipe according to any one of [1] to [3], wherein the yield strength of the flat plate portion is 295 MPa or more, the tensile strength of the flat plate portion is 400 MPa or more, and the yield ratio of the corner portion is 90% or less.

[0047] [5] The square steel pipe according to any one of [1] to [4], wherein the composition of the square steel pipe comprises, in mass%, 0.020 to 0.45% C, 0.01 to 1.0% Si, 0.30 to 3.0% Mn, 0.10% or less P, 0.050% or less S, 0.005 to 0.10% Al, 0.010% or less N, 0.001 to 0.15% Ti, and the balance Fe and inevitable impurities.

[0048] In the steel structure at the center of the wall thickness of the flat plate portion, the total volume fraction of ferrite and bainite is 70% or more and 95% or less relative to the entire steel structure at the center of the wall thickness of the flat plate portion, and the remainder is composed of one or more selected from pearlite, martensite, and austenite.

[0049] When the region surrounded by the boundary where the orientation difference between adjacent crystals is 15° or more is defined as a crystal grain,

[0050] The average grain size of the above-mentioned grains is 15.0 μm or less,

[0051] The total volume ratio of the crystal grains having a grain size of 40 μm or more is 40% or less with respect to the entire steel structure at the center of the thickness of the flat plate portion.

[0052] [6] The square steel pipe according to any one of [1] to [5], which, in addition to the above component composition, further contains, in terms of mass%, one or more selected from the group consisting of Nb: 0.001 to 0.15%, V: 0.001 to 0.15%, Cr: 0.01 to 1.0%, Mo: 0.01 to 1.0%, Cu: 0.01 to 1.0%, Ni: 0.01 to 1.0%, Ca: 0.0002 to 0.010%, and B: 0.0001 to 0.010%.

[0053] [7] A method for manufacturing a square steel pipe, which is the method for manufacturing a square steel pipe according to any one of [1] to [6], wherein:

[0054] The steel plate is cold rolled and both ends of the steel plate in the width direction are resistance welded to form a resistance welded steel pipe. Then, the resistance welded steel pipe is reduced in diameter by a sizing stand and then squared by a square forming stand to produce a square steel pipe.

[0055] The width W of the steel plate is set relative to the circumference C of the square steel pipe at the outlet side of the square forming frame. OUT The ratio satisfies the formula (1), and the circumference C of the electric resistance welded steel pipe at the inlet side of the square forming rack is IN The circumference C of the square steel pipe at the outlet side of the above-mentioned square forming frame is OUT The gap between the rollers of the sizing stand immediately before square forming and the gap between the rollers of the square forming stand are controlled so that the ratio satisfies the formula (2).

[0056] 1.000+0.050×t / H<W / C OUT <1.000+0.50×t / H…Formula (1)

[0057] 0.30×t / H+0.99≤C IN / C OUT <0.50×t / H+0.99…Formula (2)

[0058] Here, in formula (1) and formula (2),

[0059] W: The width of the steel plate as the raw material (mm),

[0060] C IN : The circumference of the electric resistance welded steel pipe on the inlet side of the first section of the square forming rack (mm),

[0061] COUT : The circumference of the square steel pipe at the outlet side of the square forming rack in the final stage (mm), t: The average wall thickness of the flat plate after square forming (mm),

[0062] H: average side length of the flat plate portion after square forming (mm).

[0063] Wherein, in the case of using a square forming frame of one stage to perform square forming, the square forming frame of the first stage and the square forming frame of the final stage refer to the same square forming frame.

[0064] [8] The method for manufacturing a square steel pipe according to [7], wherein the steel plate is obtained by heating a steel raw material to a heating temperature of 1100°C to 1300°C, and then performing hot rolling treatment with a rough rolling end temperature of 850°C to 1150°C, a finish rolling end temperature of 750°C to 900°C, and a total reduction ratio of 50% or more at a temperature below 950°C.

[0065] Next, cooling is performed under the conditions that the average cooling rate is 5°C / s to 30°C / s at the wall thickness center temperature and the cooling stop temperature is 400°C to 650°C.

[0066] Next, coiling is performed at 400°C to 650°C.

[0067] [9] The method for manufacturing a square steel pipe according to [7] or [8], wherein the average wall thickness t is greater than 0.030 times the average side length H of the flat plate portion.

[0068]

[10] The method for producing a square steel pipe according to any one of [7] to [9], wherein the average wall thickness t is greater than or equal to 20 mm and less than or equal to 40 mm.

[0069]

[11] A building structure, wherein the square steel pipe according to any one of [1] to [6] is used as a column material.

[0070] Effects of the Invention

[0071] According to the present invention, it is possible to provide a square steel pipe having excellent shape characteristics and excellent ductility and toughness of the outer surface of the corner portion, a method for manufacturing the same, and a building structure.

[0072] Thus, a cold rolled square steel pipe having a small curvature radius at the corner, a flat flat portion, and excellent ductility and toughness of the outer surface of the corner can be manufactured. In addition, a building structure using the square steel pipe of the present invention as a column material exhibits better earthquake resistance than a building structure using a conventional cold rolled square steel pipe. BRIEF DESCRIPTION OF THE DRAWINGS

[0073] Figure 1 This is a schematic diagram showing a cross section perpendicular to the tube axis direction of the square steel tube of the present invention.

[0074] Figure 2 This is a schematic diagram showing the pipe manufacturing process of the electric resistance welded steel pipe in the present invention.

[0075] Figure 3 Schematic diagram showing the forming process of the square steel pipe of the present invention.

[0076] Figure 4 This is a schematic diagram for explaining the molten solidification portion of a weld portion of an electric resistance welded steel pipe.

[0077] Figure 5 This is a schematic diagram showing an example of the building structure of the present invention.

[0078] Figure 6 This is a schematic diagram showing the positions at which the tensile test specimens at the flat plate portion and the corner portion implemented in the present invention are cut out.

[0079] Figure 7 This is a schematic diagram showing the detailed cutting position of the tensile test piece at the corner implemented in the present invention.

[0080] Figure 8 This is a schematic diagram showing the cutting position of the Charpy test piece of the corner portion implemented in the present invention.

[0081] Fig. 9 This is a schematic diagram showing the detailed cutting position of the Charpy test piece of the corner portion implemented in the present invention.

[0082] Fig.10 This is a schematic diagram for explaining the flatness measurement method implemented in the present invention. DETAILED DESCRIPTION

[0083] The present invention will be described with reference to the accompanying drawings. It should be noted that the present invention is not limited to the embodiments.

[0084] <Square steel pipe>

[0085] The present invention is a square steel pipe having a flat portion and a corner portion, wherein, when the average wall thickness of the flat portion is set to t (mm), the radius of curvature R of the outer side of the corner portion is greater than or equal to 2.0t and less than or equal to 3.0t, the flatness of the outer surface of the flat portion in the pipe axis direction is less than or equal to 2.5mm, the uniform elongation E2 at a position 1 / 4t from the outer surface of the corner portion in the wall thickness direction is greater than or equal to 0.60 times the uniform elongation E1 at a position 1 / 4t from the outer surface of the flat portion in the wall thickness direction, and the Charpy absorbed energy at -10°C at a position 1 / 4t from the outer surface of the corner portion in the wall thickness direction is greater than or equal to 100J.

[0086] Figure 1 2 shows a cross section perpendicular to the tube axis direction of the square steel tube 10 of the present invention.

[0087] In the square steel pipe 10 of the present invention, two or more flat plate portions 11 and corner portions 12 are alternately formed along the pipe circumferential direction. Figure 1 In the example shown, four corner portions 12 and four flat plate portions 11 are sequentially formed along the tube circumferential direction in the square steel tube 10. The square steel tube 10 is rectangular (approximately rectangular) or square (approximately square) in cross section perpendicular to the tube axis. Figure 1 In the embodiment, when the side lengths of two adjacent flat plate portions 11 sandwiching the corner portion 12 are set to H1 and H2, H1>H2, that is, the side length H2 of the flat plate portion opposite to the welded portion (resistance welded portion) 13 described later is shorter than the side length H1 of the adjacent flat plate portion 11. The present invention is not limited to this example, and the relationship may be H1=H2 or H1<H2.

[0088] The square steel pipe 10 is manufactured by forming a blank tube of a resistance welded steel pipe and forming the blank tube into a roll-formed square steel pipe. Therefore, the square steel pipe 10 has a resistance welded portion 13 extending in the tube axis direction, which forms a flat plate portion 11. Although not shown in the figure, the width of the molten solidified portion of the resistance welded portion 13 in the tube circumferential direction is 1.0 μm or more and 1000 μm or less in the total thickness of the tube.

[0089] In the square steel pipe 10 of the present invention, when the average thickness of the flat plate portion is t (mm), the radius of curvature R of the outer side of the corner portion is 2.0 t or more and 3.0 t or less. The average thickness t is a value calculated by the formula (3) described later.

[0090] When the radius of curvature R of the outer side of the corner is less than 2.0t, the circumferential bending strain of the corner increases when the steel strip is formed. As a result, the ductility and toughness targeted by the present invention cannot be obtained at the corner. On the other hand, when the radius of curvature R of the outer side of the corner is greater than 3.0t, the circumferential bending response of the flat plate portion of the square forming machine frame (and the circumferential bending strain of the corner) decreases. As a result, the flatness targeted by the present invention cannot be obtained at the flat plate portion. The above-mentioned radius of curvature R is preferably greater than 2.2t and preferably less than 2.9t.

[0091] It should be noted that in the present invention, as described in the examples described later, when the curvature radius of two or more locations is measured and the maximum and minimum values ​​are within the above range, it is evaluated that the curvature radius R of the outer side of the corner is small. The reason for such evaluation is that the R of the corner of the square steel pipe acts independently on the earthquake resistance and construction performance, not the average value of the four locations.

[0092] The radius of curvature R of the outer side of the corner is, Figure 1As shown, through the corner 12 ( Figure 1 In the example, it is the upper right corner, and the curvature radius of the intersection P of the straight lines (extension lines) L1 and L2 extended from the outer surfaces of the flat plate parts 11 on both sides adjacent to each other, and the intersection B of the straight line L forming an angle of 45° with the extension line L1 or L2 and the curve on the outside of the corner 12.

[0093] The radius of curvature R is measured at the connection point between the extended lines L1, L2 and the flat plate portion 11 and the corner portion 12 ( Figure 1 The radius of curvature is measured within a range of a central angle of 65° centered at the intersection B of the straight line L and the outer surface of the corner 12, which is formed by the points A and A' shown in the figure and the outer surface of the corner 12, and the center is located on the straight line L. The radius of curvature can be measured by, for example, a method of measuring the radius of curvature with a radial measuring instrument that fully matches the outer surface of the corner 12 within the above-mentioned range of the central angle of 65°, but it can also be measured by other methods.

[0094] Furthermore, in the square steel pipe 10 of the present invention, the flatness of the outer surface of the flat plate portion 11 in the pipe axis direction is 2.5 mm or less.

[0095] use Fig.10 Describe the flatness. Fig.10 As shown, the flatness is the value obtained by measuring the maximum bulge and the maximum depression relative to the straight line passing through two points at both ends of the circumferential direction on the same side of the outer surface of the flat plate portion in the cross section of the plane perpendicular to the tube axis direction. It should be noted that the flatness is obtained by the method described in the embodiments described later in the present invention.

[0096] When the above-mentioned flatness is greater than 2.5mm, the compression resistance of the square steel pipe during bending deformation is reduced. As a result, the seismic resistance of the square steel pipe is reduced. In addition, the joint surface with the beam material is greatly bent, so it is difficult to weld and join. As a result, the construction performance is reduced. The smaller the value of flatness, the better. There is no need to specify the lower limit of flatness, and 0.6mm can be allowed as the lower limit of flatness. The lower limit of flatness is preferably 0.2mm, and more preferably 0mm. Preferably, it is less than 2.0mm, and more preferably less than 1.5mm.

[0097] In the square steel pipe 10 of the present invention, the uniform elongation E2 at a position 1 / 4t from the outer surface of the corner portion in the wall thickness direction is 0.60 times or more the uniform elongation E1 at a position 1 / 4t from the outer surface of the flat plate portion in the wall thickness direction.

[0098] When a square steel pipe is subjected to a large external force such as an earthquake force, the outer surface of the corners, in particular, deforms significantly. Therefore, the ductility and toughness of the outer surface of the corners of the square steel pipe must be sufficiently improved.

[0099] When the value of the uniform elongation E2 at a position 1 / 4t from the outer surface of the corner in the wall thickness direction relative to the uniform elongation E1 at a position 1 / 4t from the outer surface of the flat plate in the wall thickness direction (the value of E2 / E1) is less than 0.60, the ductility on the outer surface side of the corner is reduced. As a result, the seismic resistance of the square steel pipe is reduced. The value of E2 / E1 is preferably greater than 0.70, more preferably greater than 0.80, and further preferably greater than 0.82. The upper limit of the value of E2 / E1 is not particularly specified, but is less than 1.00 from the viewpoint that the amount of work hardening during roll forming of the corner is large compared to the flat plate and the uniform elongation is small.

[0100] In addition, in the square steel pipe 10 of the present invention, the Charpy absorbed energy of the corner 12 at -10°C at a position 1 / 4t from the outer surface of the corner 12 in the wall thickness direction is 100 J or more. When the Charpy absorbed energy is less than 100 J, the risk of brittle fracture without plastic deformation when subjected to a large external force such as an earthquake force increases. The above-mentioned Charpy absorbed energy is preferably 150 J or more, and more preferably 200 J or more.

[0101] It should be noted that the square steel pipe 10 of the present invention preferably has the following structure in addition to the above structure.

[0102] When the average thickness of the flat plate portion of the square steel pipe 10 is t (mm) and the average side length of the flat plate portion is H (mm), the average thickness t is preferably set to be greater than 0.030 times the average side length H.

[0103] As described above, in a square steel pipe, as the ratio (t / H) of the average wall thickness t to the average side length H increases and the radius of curvature of the corner decreases, the circumferential bending strain required to form the corner increases, and the bending deformation of the corner increases. As a result, in a square steel pipe with a large ratio (t / H), the ductility and toughness of the corner tend to decrease.

[0104] When the value of the above ratio (t / H) is 0.030 or less, the endurance as a column material is reduced, so the building structures to which it can be applied are limited. Therefore, the above ratio (t / H) is preferably set to be greater than 0.030. It is more preferably 0.035 or more, and further preferably 0.040 or more. On the other hand, in order to ensure the ductility and toughness of the corner, the upper limit of the above ratio (t / H) is preferably 0.10. It is more preferably 0.080 or less.

[0105] Here, the average thickness t (mm) is calculated by the following formula (3).

[0106] t=(t1+t2+t3) / 3…Formula (3)

[0107] In formula (3), t1, t2: the wall thickness (mm) of the two adjacent flat plate portions 11 sandwiching the corner portion 12 relative to the flat plate portion 11 including the weld portion (resistance weld portion) 13 at the center position of the tube circumference, t3: the wall thickness (mm) of the flat plate portion opposite to the flat plate portion including the weld portion (resistance weld portion) at the center position of the tube circumference. That is, the average wall thickness t is the average value of the wall thickness of the three flat plate portions other than the flat plate portion including the weld portion, at the center position relative to the tube circumference (reference Figure 1 ).

[0108] The average side length H (mm) is calculated by the following formula (4).

[0109] H=(H1+H2) / 2…Formula (4)

[0110] In formula (4), H1: the side length of the cross section of any flat plate portion perpendicular to the tube axis direction ( Figure 1 The length of the longitudinal side in (mm), H2: the length of the side of the flat plate portion adjacent to the corner portion of the flat plate portion with a side length of H1 ( Figure 1 That is, the average side length H is the average of the side lengths of the cross sections perpendicular to the tube axis direction of the two adjacent flat plate portions 11 sandwiching the corner.

[0111] In addition, for the square steel pipe 10 of the present invention, in particular, from the viewpoint of being suitable for use in large buildings such as medium-rise buildings, factories, warehouses, etc. with a height greater than 20m, the average wall thickness t is preferably 20mm or more and 40mm or less. From the viewpoint of being suitable for use in medium-rise buildings and large buildings, the yield strength of the flat plate portion 11 is preferably 295MPa or more, and the tensile strength of the flat plate portion 11 is preferably 400MPa or more. From the viewpoint of better earthquake resistance, the yield ratio of the corner portion 12 is preferably 90% or less.

[0112] More preferably, the yield strength of the flat plate portion 11 is 320 MPa or more, the tensile strength of the flat plate portion 11 is 410 MPa or more, and the yield ratio of the corner portion 12 is 89.5% or less. In addition, the yield strength of the flat plate portion 11 is 500 MPa or less, the tensile strength of the flat plate portion 11 is 600 MPa or less, and the yield ratio of the corner portion 12 is 80.0% or more.

[0113] The yield strength, tensile strength and yield ratio can be obtained by performing a tensile test according to JIS Z 2241 as described in the examples below. The Charpy absorbed energy can be obtained by performing a Charpy impact test at a test temperature of -10°C using a V-notch standard test piece according to JIS Z 2242 as described in the examples below.

[0114] Next, from the viewpoint of ensuring the above-mentioned mechanical properties and weldability, preferred ranges of the chemical composition and steel structure of the square steel pipe 10 of the present invention and reasons for their limitation are described.

[0115] First, the composition will be described. The square steel pipe 10 of the present invention preferably has a composition containing, by mass%, C: 0.020-0.45%, Si: 0.01-1.0%, Mn: 0.30-3.0%, P: 0.10% or less, S: 0.050% or less, Al: 0.005-0.10%, N: 0.010% or less, Ti: 0.001-0.15%, and the balance being Fe and inevitable impurities.

[0116] In this specification, "%" indicating the steel composition means "mass %" unless otherwise specified. The following chemical compositions are chemical compositions of the flat plate portion and the corner portion excluding the welded portion of the square steel pipe.

[0117] C: 0.020~0.45%

[0118] C is an element that increases the strength of steel by solid solution strengthening. In addition, C is an element that contributes to the refinement of the structure by lowering the starting temperature of ferrite transformation. In order to obtain such an effect, 0.020% or more of C is contained. In addition, C promotes the formation of pearlite, improves hardenability, contributes to the formation of martensite, and contributes to the stabilization of austenite, so it is an element that also contributes to the formation of hard phases. When the C content is greater than 0.45%, the proportion of hard phases increases, the toughness decreases, and the weldability also deteriorates. Therefore, the C content is set to 0.020-0.45%. The C content is preferably 0.040% or more, and more preferably 0.050% or more. In addition, the C content is preferably 0.40% or less, and more preferably 0.30% or less.

[0119] Si: 0.01~1.0%

[0120] Si is an element that increases the strength of steel by solid solution strengthening. In order to obtain such an effect, 0.01% or more of Si is contained. However, when the Si content is greater than 1.0%, oxides are easily generated in the resistance weld portion, and the characteristics of the weld portion are reduced. In addition, the yield ratio of the parent material portion other than the resistance weld portion increases, and the toughness decreases. Therefore, the Si content is set to 0.01-1.0%. The Si content is preferably greater than 0.02%, and more preferably greater than 0.05%. In addition, the Si content is preferably less than 0.50%, and more preferably less than 0.40%.

[0121] Mn: 0.30~3.0%

[0122] Mn is an element that increases the strength of steel by solid solution strengthening. In addition, Mn is an element that contributes to the refinement of the structure by lowering the starting temperature of ferrite transformation. In order to obtain such an effect, 0.30% or more of Mn is contained. However, when the Mn content is greater than 3.0%, oxides are easily generated in the resistance welded portion, and the characteristics of the welded portion are reduced. In addition, due to solid solution strengthening and refinement of the structure, the yield stress increases and the desired yield ratio cannot be obtained. Therefore, the Mn content is set to 0.30-3.0%. The Mn content is preferably greater than 0.40%, and more preferably greater than 0.50%. In addition, the Mn content is preferably less than 2.5%, and more preferably less than 2.0%.

[0123] P: 0.10% or less

[0124] P segregates at grain boundaries and causes inhomogeneity of the material. Therefore, as an inevitable impurity, it is preferably reduced as much as possible, but 0.10% or less is allowed. Therefore, the P content is set to 0.10% or less. The P content is preferably 0.050% or less, and more preferably 0.030% or less. It should be noted that there is no particular lower limit for P, and excessive reduction will lead to a rise in smelting costs. Therefore, the P content is preferably set to 0.002% or more.

[0125] S: 0.050% or less

[0126] S usually exists in the form of MnS in steel, but MnS is thinly extended in the hot rolling process and has an adverse effect on ductility. Therefore, in the present invention, it is preferred to reduce S as much as possible, but 0.050% or less is allowed. Therefore, the S content is set to 0.050% or less. The S content is preferably 0.030% or less, and more preferably 0.010% or less. It should be noted that there is no special lower limit for S, and excessive reduction will lead to a rise in smelting costs. Therefore, S is preferably set to 0.0002% or more.

[0127] Al: 0.005~0.10%

[0128] Al is an element that acts as a strong deoxidizer. In order to obtain such an effect, it is necessary to contain 0.005% or more of Al. However, when the Al content is greater than 0.10%, weldability deteriorates, and the number of alumina inclusions increases, deteriorating the surface properties. In addition, the toughness of the weld is also reduced. Therefore, the Al content is set to 0.005-0.10%. The Al content is preferably greater than 0.010%, more preferably greater than 0.015%. The Al content is preferably less than 0.080%, more preferably less than 0.070%.

[0129] N: 0.010% or less

[0130] N is an inevitable impurity and an element that has the effect of reducing toughness by firmly fixing the movement of dislocations. In the present invention, N as an impurity is preferably reduced as much as possible, but the N content can be allowed to be 0.010% or less. Therefore, the N content is set to 0.010% or less. The N content is preferably 0.0080% or less. From the perspective of refining cost, the N content is preferably 0.0008% or more.

[0131] Ti: 0.001~0.15%

[0132] Ti is an element that contributes to improving the strength of steel by forming fine carbides and nitrides in steel. In addition, it has a high affinity with N, and therefore is an element that contributes to improving the toughness of steel by rendering N in the steel harmless in the form of nitrides. In order to obtain the above-mentioned effects, it is preferred to contain 0.001% or more of Ti. However, when the Ti content is greater than 0.15%, the yield ratio increases and the toughness decreases. Therefore, the Ti content is set to 0.15% or less. The Ti content is more preferably 0.002% or more, and further preferably 0.005% or more. The Ti content is more preferably 0.10% or less, and further preferably 0.08% or less.

[0133] The balance other than the above components is Fe and inevitable impurities. However, as an inevitable impurity, 0.0050% or less of O may be contained. Here, O refers to the total oxygen including O in the form of oxides. Nb: 0 to less than 0.001%, V: 0 to less than 0.001%, Cr: 0 to less than 0.01%, Mo: 0 to less than 0.01%, Cu: 0 to less than 0.01%, Ni: 0 to less than 0.01%, Ca: 0 to less than 0.0002%, B: 0 to less than 0.0001% are treated as inevitable impurities.

[0134] In the present invention, the above components are preferably used as the basic component composition. The above preferred elements can obtain the properties targeted by the present invention, but in order to further improve the properties, one or more selected from Nb: 0.001-0.15%, V: 0.001-0.15%, Cr: 0.01-1.0%, Mo: 0.01-1.0%, Cu: 0.01-1.0%, Ni: 0.01-1.0%, Ca: 0.0002-0.010%, B: 0.0001-0.010% can be contained as needed.

[0135] Nb: 0.001~0.15%

[0136] Nb is an element that contributes to the improvement of the strength of steel by forming fine carbides and nitrides in steel, and also contributes to the refinement of the structure by inhibiting the coarsening of austenite during hot rolling, and can be contained as needed. In order to obtain the above-mentioned effect, when Nb is contained, it is preferred to contain 0.001% or more of Nb. However, when the Nb content is greater than 0.15%, the yield ratio increases and the toughness decreases. Therefore, when Nb is contained, the Nb content is preferably set to 0.15% or less. The Nb content is more preferably 0.002% or more, and more preferably 0.005% or more. The Nb content is more preferably 0.10% or less, and more preferably 0.08% or less.

[0137] V: 0.001~0.15%

[0138] V is an element that contributes to improving the strength of steel by forming fine carbides and nitrides in steel, and can be contained as needed. In order to obtain the above-mentioned effect, when V is contained, it is preferred to contain 0.001% or more of V. However, when the V content is greater than 0.15%, the yield ratio increases and the toughness decreases. Therefore, when V is contained, the V content is preferably set to 0.15% or less. The V content is more preferably 0.002% or more, and further preferably 0.005% or more. The V content is more preferably 0.10% or less, and further preferably 0.08% or less.

[0139] Cr: 0.01~1.0%

[0140] Cr is an element that improves the hardenability of steel and increases the strength of steel, and can be contained as needed. In order to obtain the above-mentioned effect, when Cr is contained, the Cr content is preferably set to 0.01% or more. On the other hand, the inclusion of more than 1.0% Cr may lead to a decrease in toughness and deterioration of weldability. Therefore, when Cr is contained, the Cr content is preferably set to 1.0% or less. The Cr content is more preferably 0.02% or more, and further preferably 0.05% or more. In addition, the Cr content is more preferably 0.90% or less, and further preferably 0.80% or less.

[0141] Mo: 0.01~1.0%

[0142] Mo is an element that improves the hardenability of steel and increases the strength of steel, and can be contained as needed. In order to obtain the above-mentioned effect, when Mo is contained, the Mo content is preferably set to 0.01% or more. On the other hand, the inclusion of more than 1.0% Mo may lead to a decrease in toughness and deterioration of weldability. Therefore, when Mo is contained, the Mo content is preferably set to 1.0% or less. The Mo content is more preferably 0.02% or more, and further preferably 0.05% or more. In addition, the Mo content is more preferably 0.90% or less, and further preferably 0.80% or less.

[0143] Cu: 0.01~1.0%

[0144] Cu is an element that increases the strength of steel by solid solution strengthening, and can be contained as needed. In order to obtain the above-mentioned effect, when Cu is contained, the Cu content is preferably set to 0.01% or more. On the other hand, the inclusion of more than 1.0% Cu may lead to a decrease in toughness and deterioration of weldability. Therefore, when Cu is contained, the Cu content is preferably set to 1.0% or less. The Cu content is more preferably 0.02% or more, and further preferably 0.05% or more. In addition, the Cu content is more preferably 0.80% or less, and further preferably 0.60% or less.

[0145] Ni: 0.01~1.0%

[0146] Ni is an element that increases the strength of steel by solid solution strengthening, and can be contained as needed. In order to obtain the above-mentioned effect, when Ni is contained, the Ni content is preferably set to 0.01% or more. On the other hand, the inclusion of more than 1.0% Ni may lead to a decrease in toughness and deterioration of weldability. Therefore, when Ni is contained, the Ni content is preferably set to 1.0% or less. The Ni content is more preferably 0.02% or more, and further preferably 0.05% or more. In addition, the Ni content is more preferably 0.80% or less, and further preferably 0.60% or less.

[0147] Ca: 0.0002~0.010%

[0148] Ca is an element that contributes to improving the toughness of steel by spheroidizing sulfides such as MnS that are thinly stretched in the hot rolling process in the manufacture of raw steel plates, and can be contained as needed. In order to obtain the above-mentioned effect, when Ca is contained, it is preferred to contain 0.0002% or more of Ca. However, when the Ca content is greater than 0.010%, Ca oxide clusters are formed in the steel, and the toughness deteriorates. Therefore, when Ca is contained, the Ca content is preferably set to 0.010% or less. The Ca content is more preferably 0.0005% or more, and further preferably 0.0010% or more. In addition, the Ca content is more preferably 0.008% or less, and further preferably 0.0060% or less.

[0149] B: 0.0001~0.010%

[0150] B is an element that contributes to the refinement of the structure by lowering the ferrite transformation start temperature, and can be contained as needed. In order to obtain the above-mentioned effect, when B is contained, it is preferred to contain 0.0001% or more of B. However, when the B content is greater than 0.010%, the yield ratio increases and the toughness deteriorates. Therefore, when B is contained, the B content is preferably set to 0.010% or less. The B content is more preferably 0.0005% or more, and further preferably 0.0008% or more. The B content is more preferably 0.0050% or less, further preferably 0.0030% or less, and further preferably 0.0020% or less.

[0151] Next, the steel structure is described. In the steel structure at the center of the wall thickness of the flat plate portion of the square steel pipe 10 of the present invention, the total volume ratio of ferrite and bainite is 70% or more and 95% or less relative to the entire steel structure at the center of the wall thickness of the flat plate portion, and the remainder is composed of one or more selected from pearlite, martensite, and austenite, and when the region surrounded by the boundary where the orientation difference of adjacent crystals is 15° or more is set as a grain, the average grain size of the grain is 15.0 μm or less, and the total volume ratio of the grains with a grain size of 40 μm or more relative to the entire steel structure at the center of the wall thickness of the flat plate portion is preferably 40% or less.

[0152] Total volume fraction of ferrite and bainite: 70% or more and 95% or less

[0153] Ferrite is a soft structure. In addition, bainite is harder than ferrite, softer than pearlite, martensite and austenite, and is a structure with excellent toughness. When hard structures (pearlite, martensite and austenite) are mixed in ferrite and bainite, the yield ratio is reduced, but on the other hand, the interface is easily the starting point of destruction due to stress concentration caused by hardness difference, and the toughness is reduced. Therefore, in order to obtain the above-mentioned yield ratio and toughness, the total volume ratio of ferrite and bainite at the center of the wall thickness of the flat plate portion is preferably 70% or more and 95% or less relative to the overall steel structure at the center of the wall thickness of the flat plate portion. When the total volume ratio of ferrite and bainite is less than 70%, the proportion of hard structures is high, the yield stress increases, and therefore, the yield ratio increases and the toughness decreases. In addition, when the total volume ratio of ferrite and bainite is greater than 95%, the tensile strength decreases, so the yield ratio increases. More preferably, it is 73% or more and 93% or less. It is further preferably 75% or more and 92% or less.

[0154] It should be noted that the remainder structure (remainder structure) other than ferrite and bainite is one or more selected from pearlite, martensite, and austenite. When the total volume ratio of the remainder structure is less than 5%, the tensile strength decreases, so the yield ratio increases. In addition, when the total volume ratio of the remainder structure is greater than 30%, the proportion of hard structures is high, the yield stress increases, and thus the yield ratio increases and the toughness decreases. Therefore, the total volume ratio of the remainder structure is preferably 5% or more and 30% or less relative to the overall steel plate structure at the center of the wall thickness of the flat plate. More preferably, it is 7% or more and 27% or less. It is further preferably 8% or more and 25% or less.

[0155] The above-mentioned various structures (ferrite, bainite, pearlite, martensite) other than austenite use the austenite grain boundary or the deformation band in the austenite grain as the nucleation site. In the hot rolling of the raw steel plate in the manufacturing process of the electric resistance welded steel pipe (blank tube) used in the manufacture of square steel pipes, by increasing the reduction at a low temperature where the recrystallization of austenite is not easy to occur, a large number of dislocations can be introduced into the austenite to make the austenite finer, and a large number of deformation bands can be introduced into the grains. As a result, the area of ​​the nucleation site increases, the nucleation frequency increases, and the steel structure can be refined.

[0156] In the present invention, even if the above-mentioned steel structure exists within the range of ±1.0 mm in the wall thickness direction with the center of the wall thickness as the center, the above-mentioned effect can be obtained in the same manner. Therefore, in the present invention, "steel structure at the center of the wall thickness" means that the above-mentioned steel structure exists within any range of ±1.0 mm in the wall thickness direction with the center of the wall thickness as the center.

[0157] As the observation of steel structure, first, the test piece for organization observation is cut in a way that the observation surface is parallel to the length direction and the wall thickness direction of the square steel pipe and becomes the center of the wall thickness of the flat plate, mirror polished, and then nitric acid ethanol solution is corroded and made. In the organization observation, an optical microscope (magnification: 1000 times) or a scanning electron microscope (SEM, magnification: 1000 times) is used to observe and photograph the organization at the center of the wall thickness. The area ratios of ferrite, bainite and remainder (pearlite, martensite, austenite) are obtained from the obtained optical microscope image and SEM image. About the area ratio of each organization, observe in more than 5 visual fields, and calculate with the average value of the values ​​obtained in each visual field. The area ratio obtained by organization observation is used as the volume ratio of each organization.

[0158] Here, ferrite is a product of diffusion phase transformation, and has a low dislocation density and a substantially restored structure, including polygonal ferrite and pseudo-polygonal ferrite.

[0159] Bainite is a duplex structure of lath-shaped ferrite and cementite with a high dislocation density.

[0160] Pearlite is a eutectic structure of iron and iron carbide (ferrite + cementite), and presents a layered structure in which linear ferrite and cementite are alternately arranged.

[0161] Martensite is a lath-shaped low-temperature phase transformation structure with a very high dislocation density. In the SEM image, it shows a brighter contrast than ferrite and bainite. It should be noted that it is difficult to distinguish martensite and austenite using optical microscope images and SEM images. Therefore, the area ratio of the structure observed in the form of martensite or austenite is measured from the obtained SEM image, and the volume ratio of austenite measured by the method described later is subtracted therefrom, and the obtained value is used as the volume ratio of martensite.

[0162] The volume fraction of austenite was measured by X-ray diffraction using a test piece prepared in the same manner as the test piece used for the measurement of dislocation density. The volume fraction of austenite was determined from the integrated intensities of the (200), (220), and (311) planes of fcc iron and the (200) and (211) planes of bcc iron.

[0163] Average grain size of crystal grains: 15.0 μm or less

[0164] In the present invention, average crystal grain size refers to the average equivalent circle diameter of the crystal grain when the region surrounded by the boundary with the orientation difference of adjacent crystals being 15° or more is set as the crystal grain (grain boundary). In addition, equivalent circle diameter (crystal grain size) refers to the diameter of a circle having the same area as the crystal grain as the object.

[0165] When the average crystal grain size of the crystal grains is greater than 15.0 μm, the total area of ​​the grain boundaries that become an obstacle to crack propagation is small, so the desired toughness cannot be obtained. Therefore, in the present invention, the average crystal grain size of the crystal grains is set to be less than 15.0 μm. The average crystal grain size of the crystal grains is preferably less than 13.0 μm, and more preferably less than 10.0 μm. It should be noted that the smaller the average crystal grain size, the higher the yield ratio, so the average crystal grain size is preferably more than 2.0 μm.

[0166] Total volume ratio of grains with a grain size of 40 μm or more: 40% or less

[0167] Even if the upper limit of the maximum crystal grain size is specified, if there is a certain amount of coarse grains, there will be a small area of ​​the total area of ​​the grain boundary that becomes an obstacle to the propagation of cracks, so the toughness is greatly reduced. Therefore, in order to obtain good toughness, it is necessary to also specify the upper limit of the proportion of coarse grains that exist. Therefore, in the present invention, the total volume rate of grains with a grain size of 40 μm or more is set to 40% or less. More preferably, it is 30% or less. Based on the above reasons, it is expected that there are fewer coarse grains, and the total volume rate of the above-mentioned grains is preferably 0%.

[0168] Here, the average crystal grain size of the grains and the total volume rate of the grains with a crystal grain size of 40 μm or more are determined as follows. First, the test piece for organization observation is cut in a manner that the observation surface is a cross section parallel to both the length direction and the wall thickness direction of the square steel pipe and becomes the center of the wall thickness of the flat plate. After mirror polishing, the histogram of the particle size distribution (a graph with the horizontal axis being the particle size and the vertical axis being the existence ratio (area ratio) of each particle size) is calculated using the SEM / EBSD method in the center of the wall thickness. The average crystal grain size is obtained from the above histogram as the arithmetic mean of the particle size. The total volume rate of the grains with a particle size of 40 μm or more is obtained from the above histogram as the total existence ratio of the grains with a particle size of 40 μm or more. As measurement conditions, the acceleration voltage is set to 15 kV, the measurement area is set to 500 μm × 500 μm, and the measurement step (measurement resolution) is set to 0.5 μm. In addition, in the crystal grain size analysis, crystal grains having a grain size of less than 2.0 μm were excluded from the analysis object as measurement noise.

[0169] <Method for manufacturing square steel pipe>

[0170] Next, a method for producing the square steel pipe 10 of the present invention will be described.

[0171] The manufacturing method of the square steel pipe 10 of the present invention is as follows: a steel plate as a raw material is cold rolled, and then both ends of the cold rolled steel plate in the width direction are resistance welded to form a resistance welded steel pipe, and then the resistance welded steel pipe is reduced in diameter by a sizing rack, and then squared by a square forming rack to manufacture a square steel pipe. At this time, the plate width W of the steel plate is relative to the circumference C of the square steel pipe on the outlet side of the square forming rack. OUT The ratio satisfies the formula (1), and the circumference C of the electric resistance welded steel pipe on the inlet side of the square forming rack IN The circumference C of the square steel pipe relative to the outlet side of the square forming rack OUT The gap between the rollers of the sizing stand immediately before square forming and the gap between the rollers of the square forming stand are controlled so that the ratio satisfies the formula (2).

[0172] 1.000+0.050×t / H<W / C OUT <1.000+0.50×t / H…Formula (1)

[0173] 0.30×t / H+0.99≤C IN / C OUT <0.50×t / H+0.99…Formula (2)

[0174] Here, in formula (1) and formula (2),

[0175] W: The width of the steel plate as the raw material (mm),

[0176] C IN : The circumference of the electric resistance welded steel pipe on the inlet side of the first section of the square forming rack (mm),

[0177] C OUT : The circumference of the square steel pipe at the outlet side of the square forming rack in the final stage (mm), t: The average wall thickness of the flat plate after square forming (mm),

[0178] H: average side length of the flat plate portion after square forming (mm).

[0179] In the case of using a square forming frame of one stage to perform square forming, the square forming frame of the first stage and the square forming frame of the final stage refer to the same square forming frame.

[0180] It should be noted that the average wall thickness t is calculated by the above-mentioned formula (3), and the average side length H is calculated by the above-mentioned formula (4).

[0181] use Figure 2 and Figure 3 , the manufacturing method of the square steel pipe 10 of the present invention is described in detail. Figure 2 2 is a diagram for explaining a pipe manufacturing process of a square steel pipe blank (electric resistance welded steel pipe) according to the present invention. Figure 3 2 is a diagram illustrating a forming process of a square steel pipe according to the present invention.

[0182] First, the electric resistance welded steel pipe 7 is manufactured using a steel plate (steel strip) as a raw material (pipe manufacturing step).

[0183] like Figure 2 As shown, the steel plate 1 (hot-rolled steel plate, hot-rolled steel strip) having the above-mentioned composition wound into a coil is unwound, straightened by a leveler 2, and intermediately formed by a row of rolls 3 consisting of two or more rolls to form a cylindrical open tube. Then, the fin-shaped roll group 4 consisting of two or more rolls is used for finishing forming. The above-mentioned open tube is formed into a cylindrical shape by cold rolling.

[0184] It should be noted that the square steel pipe of the present invention preferably has the above-mentioned steel structure. As described above, the square steel pipe of the present invention is manufactured by further square-forming the electric resistance welded steel pipe (blank tube) formed by cold rolling the raw steel plate, so the raw steel plate (steel plate 1) also preferably has the above-mentioned component composition and steel structure. The preferred manufacturing conditions of the steel plate 1 will be described later, so the description here is omitted.

[0185] The open tube after fine processing and forming is crimped by the extrusion roller 5, and at the same time, a pair of butt joints (two ends in the width direction) facing each other along the circumferential direction of the steel plate 1 are resistance welded (resistance welded) by the welding machine 6 to form a resistance welded steel tube 7. In the above-mentioned resistance welding, the butt joints are heated and melted by, for example, high-frequency induction heating or high-frequency resistance heating, and then crimped and solidified to complete the joining. As a result, the welded portion (resistance welded portion) 13 is extended in the tube axis direction. The manufacturing equipment used in the manufacture of the resistance welded steel tube 7 is not limited to having Figure 2 Manufacturing equipment for the pipe making process shown.

[0186] It should be noted that in the present invention, in the process of manufacturing the electric resistance welded steel pipe, the upset amount by the squeeze roll 5 is preferably set to a range of 20% or more and 100% or less relative to the wall thickness of the electric resistance welded steel pipe 7. When the upset amount is less than 20% of the wall thickness, the discharge of molten steel becomes insufficient, and the toughness of the welded portion deteriorates. On the other hand, when the upset amount is greater than 100% of the wall thickness, the load on the squeeze roll increases, and the work hardening amount of the welded portion (electric resistance welded portion) 13 increases, and the hardness increases excessively.

[0187] Next, the obtained electric resistance welded steel pipe 7 is used as a base pipe to produce a square steel pipe (forming step). The forming step includes a sizing step and a square forming step.

[0188] like Figure 3 As shown, the resistance welded steel pipe 7 is reduced in diameter in a cylindrical shape by a sizing roller group (sizing rack) 8 composed of two or more rollers arranged at the top, bottom, left and right relative to the resistance welded steel pipe 7 (sizing process). Then, by a square forming roller group (square forming rack) 9 composed of two or more rollers arranged at the top, bottom, left and right relative to the resistance welded steel pipe 7, it is sequentially square-formed into the shapes shown by R1, R2, and R3 to form a square steel pipe 10 (square forming process). Each roller constituting the square forming rack 9 is a hole-shaped roller (diameter roller) having a caliber curvature, and the caliber curvature increases as it becomes a rear-stage rack. In this way, the flat plate portion and corner portion of the square steel pipe are formed.

[0189] It should be noted that the number of stands constituting the sizing roll group 8 and the square forming roll group 9 is not particularly limited. There are cases where the stands are composed of two or more stages, and there are cases where the stands are composed of one stage. In addition, when the diameter curvature of each roll in the sizing roll group 8 or the square forming roll group 9 is not constant (having two or more curvatures), it becomes a cause of irregular shape when the electric resistance welded steel pipe 7 being formed is twisted in the circumferential direction, so the diameter curvature of each roll is preferably constant.

[0190] In the present invention, as described above, the plate width W of the steel plate is set to be equal to the circumference C of the square steel pipe at the outlet side of the square forming frame. OUT The ratio satisfies the formula (1), and the circumference C of the electric resistance welded steel pipe on the inlet side of the square forming rackIN The circumference C of the square steel pipe relative to the outlet side of the square forming rack OUT It is important to control the gap between the rollers of the sizing stand immediately before square forming and the gap between the rollers of the square forming stand in a manner that satisfies the formula (2). Thus, even for a roll-formed square steel pipe having a large ratio (t / H) of the average wall thickness t to the average side length H and a small radius of curvature R of the corner, the ductility and toughness of the outer surface of the corner can be improved.

[0191] First, the plate width W (mm) of the raw steel plate (steel plate) 1 and the circumference of the square steel pipe 10 just after the square forming (the circumference of the steel pipe on the outlet side of the square forming machine stand in the final stage (mm), hereinafter referred to as "C OUT ”) ratio (W / C OUT ), and the reason why the ratio (t / H) of the average wall thickness t after the rigid square forming to the average side length H after the rigid square forming is controlled to satisfy the above-mentioned formula (1) is explained.

[0192] like Figure 2 and Figure 3 As shown, after a flat steel plate 1 (raw steel plate) is cold rolled to form a cylindrical electric resistance welded steel pipe 7 (blank pipe), the cylindrical electric resistance welded steel pipe is square-formed to produce a square steel pipe 10. During the manufacturing process (pipe making process, forming process), in addition to the bending deformation in the circumferential direction of the pipe, the steel plate 1 and the electric resistance welded steel pipe 7 are also subjected to elongation deformation in the longitudinal direction of the pipe due to the reduction in diameter in the circumferential direction of the pipe. In order to reduce the reduction in diameter in the circumferential direction of the pipe during the manufacturing process, the above-mentioned two ratios "t / H" and "W / C" are appropriately controlled. OUT ” is effective.

[0193] The above ratio "W / C OUT ” is less than the value on the left side of formula (1), the circumferential bending strain of the steel plate 1 in the pipe making process and the circumferential bending strain and bending response of the electric resistance welded steel pipe 7 in the forming process are reduced. As a result, the processing of the steel plate 1 and the electric resistance welded steel pipe 7 becomes insufficient, a flat flat plate portion cannot be obtained, and the curvature radius R of the outer side of the corner portion becomes larger than 3.0 times (3.0t) the average wall thickness t.

[0194] On the other hand, the above ratio "W / C OUT When " is greater than the value on the right side of formula (1), the difference in the circumference of the tube (or open tube) before and after the tube making process and the forming process becomes larger. As a result, the diameter reduction in the circumferential direction of the tube is large, so the corner is greatly work-hardened, and the desired ductility and toughness of the outer surface of the corner cannot be obtained.

[0195] The above ratio "W / C OUT" is preferably not less than (1.000+0.080×t / H) and not more than (1.000+0.48×t / H), more preferably not less than (1.000+0.10×t / H) and not more than (1.000+0.45×t / H).

[0196] Next, the circumference of the electric resistance welded steel pipe 7 immediately before square forming (the circumference of the electric resistance welded steel pipe 7 at the inlet side of the first stage square forming machine frame (mm), hereinafter referred to as "C IN ”) and the circumference of the square steel tube 10 after the square is formed (C OUT ) IN / C OUT ), and the reason why the ratio (t / H) of the average wall thickness t after the rigid square is formed to the average side length H after the rigid square is formed is controlled to satisfy the above-mentioned formula (2) is explained.

[0197] like Figure 3 As shown in the figure, when the cylindrical electric resistance welded steel pipe 7 is square-shaped into the square steel pipe 10, as described above, the steel pipe is passed through the square forming roller group 9, thereby gradually being formed from the cylindrical shape into the square shape. In such square forming, the straight line portion (flat portion 11) of the side is bent back, the corner portion 12 is bent, and the electric resistance welded steel pipe 7 is deformed by reducing the diameter in the circumferential direction.

[0198] In particular, around the corner 12, the rollers of the square forming roller group 9 are almost non-contacted to complete the square forming. In the square forming, the corner 12 is formed by protruding by utilizing free deformation. At this time, the higher the rigidity of the corner 12 and the smaller the circumferential diameter reduction, the smaller the bending deformation of the corner 12 and the larger the curvature radius of the outer side of the corner. On the other hand, the lower the rigidity of the corner 12 and the larger the circumferential diameter reduction, the larger the bending deformation of the corner 12 and the smaller the curvature radius of the outer side of the corner.

[0199] In addition, the larger the ratio of the average wall thickness t to the average side length H (t / H), the higher the rigidity of the corner portion 12 against bending deformation. IN / C OUT ) is used to calculate, the larger it is, the greater the circumferential diameter reduction is.

[0200] Therefore, when t / H increases, it is difficult to form the corner 12 by bending deformation. Therefore, in order to obtain the desired corner curvature radius, it is necessary to increase the perimeter ratio (C IN / C OUT ) and increase the circumferential diameter reduction. For this reason, the above two ratios "t / H" and "C IN / C OUT ” is effective.

[0201] Perimeter ratio (C IN / C OUT ) is smaller than the value on the left side of formula (2), the difference in the circumferential length of the tube before and after the forming process is reduced, and the circumferential diameter reduction of the electric resistance welded steel tube 7 is reduced. As a result, the processing of the flat plate portion 11 and the corner portion 12 becomes insufficient, a flat flat plate portion cannot be obtained, and the curvature radius R of the outer side of the corner portion becomes larger than 3.0 times (3.0t) the average wall thickness t.

[0202] On the other hand, the perimeter ratio (C IN / C OUT ) is greater than the value on the right side of formula (2), the difference in the circumference of the tube before and after the forming process increases. As a result, the reduction in diameter in the circumferential direction of the tube is large, so the corner is greatly work-hardened, and the desired ductility and toughness of the corner cannot be obtained. In addition, the radius of curvature R of the outer side of the corner is less than 2.0 times (2.0t) the average wall thickness t.

[0203] Perimeter ratio (C IN / C OUT ) is preferably not less than (0.33×t / H+0.99) and not more than (0.47×t / H+0.99), and more preferably not less than (0.35×t / H+0.99) and not more than (0.45×t / H+0.99).

[0204] In addition, in the present invention, from the viewpoint of further improving the earthquake resistance, it is preferable to control under the following conditions in addition to the conditions of the above-mentioned formula (1) and formula (2).

[0205] When the average wall thickness of the flat plate portion of the square steel pipe 10 is set to t (mm) and the average side length of the flat plate portion is set to H (mm), it is preferred that the above-mentioned average wall thickness t is set to be greater than 0.030 times relative to the above-mentioned average side length H. Thus, the endurance and rigidity of the column material are increased, and as a result, the earthquake resistance is improved. The ratio (t / H) of the average wall thickness t to the average side length H is more preferably 0.035 times or more. In addition, in order to ensure the ductility and toughness of the corner, it is preferably less than 0.10 times, and more preferably less than 0.080 times.

[0206] In addition, the average wall thickness t is preferably set to 20 mm or more and 40 mm or less. It should be noted that the reason is the same as the reason for controlling the average wall thickness t of the square steel pipe described above, so it is omitted.

[0207] Furthermore, it is preferable to control the gap between the sizing roll and the square forming roll.

[0208] In addition, C IN and C OUTThe control is performed by controlling the gap between the concave parts of the diameter rollers. When the difference between the maximum gap between the concave parts of the rollers of the sizing stand immediately before square forming (hereinafter also referred to as "the gap of the sizing stand") and the maximum gap between the concave parts of the rollers of the square forming stand (hereinafter also referred to as "the gap of the square forming stand") is set to △g, it is preferred to adjust the gap of the sizing stand immediately before square forming in such a way that the value G (=△g / (t / H)) obtained by dividing △g by (t / H) is 70 or more and 180 or less.

[0209] When G is less than 70, in the above formula (2), (C IN / C OUT ) is smaller than the value on the left, as described above, the curvature radius of the outer side of the flat plate portion and the corner portion, which is the target of the present invention, cannot be obtained. On the other hand, when G is greater than 180, in the above formula (2), (C IN / C OUT ) is greater than the value on the right, as described above, the ductility and toughness of the corner portion targeted by the present invention cannot be obtained. Preferably, G is greater than 80 and less than 170.

[0210] It should be noted that, when there are more than two stages of sizing racks, the gap of the sizing rack just before square forming can be the same as the gap of other sizing racks. In addition, when there are more than two stages of square forming racks, the gap of the square forming rack is preferably set to the gap of the square forming rack of the first stage. The gaps of the first stage and other square forming racks can all be the same.

[0211] Here, the above C IN It refers to the circumference (length of the outer circumference in the circumferential direction of the tube) of the electric resistance welded steel pipe 7 at the inlet side of the first stage square forming frame (mm). Figure 3 As shown, C IN It is obtained by the following method: when the pipe making direction is set as the positive direction of the X-axis, the X-coordinate of the rotation axis of any one of the sizing roll groups 8 immediately before square forming is set as Xa(m), and the X-coordinate of the rotation axis of any one of the first-stage square forming roll groups 9 is set as Xb(m), the outer circumference of the circumferential section of the pipe in the plane X=(Xa+Xb) / 2(m) perpendicular to the X-axis is measured using a tape measure.

[0212] The above C OUT It refers to the circumference of the square steel pipe 10 at the outlet side of the square forming rack in the final stage (the length of the outer circumference in the circumferential direction of the pipe) (mm). Figure 3 As shown, C OUT The method is as follows: let the X coordinate of the rotation axis of any one of the square forming stands in the final stage of the roll group be Xc(m), and measure the outer circumference of the circumferential section of the pipe in the plane X=Xc+1(m) perpendicular to the X axis with a tape measure.

[0213] In the method for manufacturing a square steel pipe of the present invention, in order to reduce the fluctuation of the flatness of each flat plate portion and the radius of curvature of each corner portion during the forming process from the electric resistance welded steel pipe (blank pipe), the following conditions can be used in addition to the above conditions.

[0214] In the sizing process after resistance welding, in order to meet the preferred roundness, the steel pipe can be reduced in diameter in such a way that the circumference of the steel pipe is reduced by a total of 0.30% or more. As a result, in the subsequent square forming process, each flat plate portion and each corner portion are formed uniformly (symmetrically), and the fluctuation of flatness and curvature radius is reduced. The above-mentioned "preferred roundness" means that the vertical outer diameter D1 and the horizontal outer diameter D2 of the pipe are |D1-D2| / ((D1+D2) / 2)≤0.020.

[0215] However, when the diameter reduction is performed so that the circumference of the steel pipe is reduced by a total ratio of more than 2.0%, the bending amount in the pipe axial direction when the roll passes increases, and the yield ratio increases. Therefore, it is preferable to perform the diameter reduction so that the circumference of the steel pipe is reduced by a ratio of 0.30% or more and 2.0% or less.

[0216] In the sizing step, in order to minimize the amount of bending in the pipe axial direction when the roll passes through and to suppress the generation of residual stress in the pipe axial direction, it is preferred to perform diameter reduction in two or more stages using two or more stands. In this case, the diameter reduction in each stand is preferably performed so that the circumference of the steel pipe is reduced by a ratio of 1.0% or less compared to the diameter reduction in the stand immediately preceding the stand.

[0217] As described above, in the square steel pipe of the present invention, the electric resistance welded steel pipe is used for the blank pipe. Whether the square steel pipe 10 is obtained from the electric resistance welded steel pipe 7 can be judged by the following method: the square steel pipe 10 is cut vertically along the pipe axis direction, the cut surface including the welded portion (electric resistance welded portion) 13 is polished, corroded, and observed with an optical microscope. When the width of the molten solidified portion of the welded portion (electric resistance welded portion) 13 in the pipe circumferential direction is 1.0 μm or more and 1000 μm or less in the total thickness of the pipe, it is the electric resistance welded steel pipe 7. It should be noted that the etching liquid can be selected appropriately according to the steel composition and the type of steel pipe.

[0218] Here, use Figure 4 The welded portion (resistance welded portion) will be described. Figure 4 2 is a schematic diagram of the melted and solidified portion 16 of the welded portion 13 . Figure 4 The cut surface including the welded portion is polished and etched. The molten solidified portion 16 can be identified as Figure 4The region having a different structure and contrast from the base material portion 14 and the heat-affected zone 15. For example, the molten solidified portion 16 of the electric resistance welded steel pipe of carbon steel and low alloy steel can be specified as a region observed relatively white under an optical microscope in the above cross section after etching with nital.

[0219] Next, a preferred method for producing a raw material steel plate of an electric resistance welded steel pipe used for producing a square steel pipe of the present invention will be described.

[0220] For example, it is preferred that the steel material having the above-mentioned composition is heated to a heating temperature of 1100°C to 1300°C, and then subjected to hot rolling treatment (hot rolling process) with a rough rolling end temperature of 850°C to 1150°C, a finish rolling end temperature of 750°C to 900°C, and a total reduction ratio of 50% or more at 950°C or below, and then cooled under the conditions of an average cooling rate of 5°C / s to 30°C / s and a cooling stop temperature of 400°C to 650°C (cooling process), and then coiled at 400°C to 650°C (coiling process) to produce a hot-rolled steel plate (steel plate 1).

[0221] It should be noted that, in the following description of the manufacturing method, unless otherwise specified, the "℃" expression related to temperature is set to the surface temperature of the steel raw material and the steel plate (hot-rolled steel plate). These surface temperatures can be measured using a radiation thermometer or the like. In addition, the temperature at the center of the steel plate wall thickness can be obtained by calculating the temperature distribution in the cross section of the steel plate using heat transfer analysis and correcting the result with the surface temperature of the steel plate. In addition, "hot-rolled steel plate" also includes hot-rolled plates and hot-rolled steel strips.

[0222] In the present invention, the smelting method of the steel raw material (steel billet) is not particularly limited, and known smelting methods such as converters, electric furnaces, and vacuum melting furnaces are suitable. The casting method is also not particularly limited, and the desired size is produced by known casting methods such as continuous casting. It should be noted that there is no problem in applying the ingot casting-opening billet rolling method instead of the continuous casting method. The molten steel can be further subjected to secondary refining such as ladle refining.

[0223] Hot rolling process

[0224] Heating temperature: 1100°C or higher and 1300°C or lower

[0225] When the heating temperature is lower than 1100°C, the deformation resistance of the rolled material increases, and rolling becomes difficult. On the other hand, when the heating temperature exceeds 1300°C, the austenite grains coarsen, and fine austenite grains cannot be obtained in the subsequent rolling (rough rolling, finish rolling), and it is difficult to ensure the average grain size of the steel structure of the electric resistance welded steel pipe as the target of the present invention. Therefore, the heating temperature in the hot rolling process is set to 1100°C or higher and 1300°C or lower. The heating temperature is more preferably 1120°C or higher. In addition, the heating temperature is more preferably 1280°C or lower.

[0226] It should be noted that in the present invention, in addition to the existing method of temporarily cooling the steel billet (slab) to room temperature after manufacturing and then heating it again, it is also possible to apply energy-saving direct rolling processes such as loading it into a heating furnace in a warm sheet state without cooling it to room temperature, or rolling it immediately after slightly keeping it warm.

[0227] Rough rolling end temperature: 850℃ or higher and 1150℃ or lower

[0228] When the rough rolling end temperature is lower than 850°C, the surface temperature of the steel plate becomes below the ferrite transformation start temperature in the subsequent finish rolling, a large amount of processed ferrite is generated, and the yield ratio increases. On the other hand, when the rough rolling end temperature exceeds 1150°C, the reduction amount within the austenite non-recrystallization temperature range is insufficient, and fine austenite grains cannot be obtained. As a result, it is difficult to ensure the average grain size of the steel structure of the square steel pipe, and the toughness is reduced. The rough rolling end temperature is more preferably above 860°C. In addition, the rough rolling end temperature is more preferably below 1000°C.

[0229] The start temperature of the finishing rolling is preferably above 800°C and below 980°C. When the start temperature of the finishing rolling is lower than 800°C, the surface temperature of the steel plate becomes below the start temperature of the ferrite transformation during the finishing rolling, a large amount of processed ferrite is generated, and the yield ratio increases. On the other hand, when the start temperature of the finishing rolling exceeds 980°C, the austenite coarsens and sufficient deformation bands are not introduced into the austenite. Therefore, it is difficult to ensure the average grain size of the steel structure of the above-mentioned square steel pipe, and the toughness is reduced. The start temperature of the finishing rolling is more preferably above 820°C. In addition, the start temperature of the finishing rolling is more preferably below 950°C.

[0230] Finish rolling end temperature: 750℃ or higher and 900℃ or lower

[0231] When the finishing temperature of the finishing rolling is lower than 750°C, the surface temperature of the steel plate becomes below the ferrite transformation start temperature during the finishing rolling, a large amount of processed ferrite is generated, and the yield ratio increases. On the other hand, when the finishing temperature of the finishing rolling exceeds 900°C, the reduction amount within the austenite non-recrystallization temperature range is insufficient, and fine austenite grains cannot be obtained. As a result, it is difficult to ensure the average grain size of the steel structure of the above-mentioned square steel pipe, and the toughness is reduced. The finishing temperature of the finishing rolling is more preferably above 770°C. In addition, the finishing temperature of the finishing rolling is more preferably below 880°C.

[0232] Total reduction ratio at 950℃ or below: 50% or more

[0233] In the present invention, by refining the subgrains in austenite in the hot rolling process, the ferrite, bainite and residual structure generated in the subsequent cooling process and coiling process are refined, and the steel structure of the square steel pipe having the above-mentioned strength and toughness can be obtained. In order to refine the subgrains in austenite in the hot rolling process, it is necessary to increase the reduction rate in the austenite non-recrystallization temperature range and introduce sufficient processing strain. In order to achieve this purpose, in the present invention, the total reduction rate at 950°C or below is set to 50% or more.

[0234] When the total reduction rate at 950°C or less is less than 50%, sufficient processing strain cannot be introduced in the hot rolling process, so the structure with the average grain size of the above-mentioned square steel pipe cannot be obtained. The total reduction rate at 950°C or less is more preferably 55% or more, and more preferably 57% or more. There is no particular upper limit. When it is greater than 80%, the effect of improving toughness relative to the increase in the reduction rate is reduced, and only the equipment load increases. Therefore, the total reduction rate at 950°C or less is preferably 80% or less. More preferably, it is 70% or less.

[0235] The above-mentioned total reduction ratio at 950°C or lower refers to the total reduction ratio of each rolling pass in the temperature range of 950°C or lower.

[0236] Cooling process

[0237] After the hot rolling step, the hot rolled sheet is cooled in a cooling step. In the cooling step, the hot rolled sheet is cooled at an average cooling rate of 5°C / s to 30°C / s and a cooling stop temperature of 400°C to 650°C.

[0238] Average cooling rate from the start of cooling to the stop of cooling (end of cooling): 5°C / s or more and 30°C / s or less

[0239] When the average cooling rate in the temperature range from the start of cooling to the stop of cooling described later is less than 5°C / s, the nucleation frequency of ferrite or bainite is reduced, and they are coarsened, so the organization with the average grain size of the above-mentioned square steel pipe cannot be obtained. On the other hand, when the average cooling rate is greater than 30°C / s, a large amount of martensite is generated, and the toughness is reduced. The average cooling rate is preferably more than 10°C / s. In addition, the average cooling rate is preferably less than 25°C / s.

[0240] In addition, in the present invention, from the viewpoint of suppressing the formation of ferrite on the surface of the steel sheet before cooling, it is preferred to start cooling immediately after the finish rolling is completed.

[0241] Cooling stop temperature: 400°C or higher and 650°C or lower

[0242] When the cooling stop temperature is lower than 400°C based on the wall thickness center temperature of the hot rolled plate, a large amount of martensite is generated, and the toughness is reduced. On the other hand, when the cooling stop temperature exceeds 650°C, the nucleation frequency of ferrite or bainite is reduced, and they are coarsened, so the organization with the average grain size of the above-mentioned square steel pipe cannot be obtained. The cooling stop temperature is preferably above 430°C. In addition, the cooling stop temperature is preferably below 620°C.

[0243] It should be noted that, in the present invention, unless otherwise specified, the average cooling rate is set to a value (cooling rate) obtained by ((wall thickness center temperature of the hot-rolled plate before cooling - wall thickness center temperature of the hot-rolled plate after cooling) / cooling time). The cooling method may include water cooling such as spraying water from a nozzle, cooling by spraying a cooling gas, etc. In the present invention, in order to cool both sides of the hot-rolled plate under the same conditions, it is preferred to perform cooling operation (treatment) on both sides of the hot-rolled plate.

[0244] Coiling process

[0245] After the cooling process, in the coiling process, the hot-rolled steel sheet is coiled into a coil shape and then cooled. In the coiling process, in order to obtain the above-mentioned steel sheet structure, it is preferably coiled at a coiling temperature of 400°C or more and 650°C or less. When the coiling temperature is lower than 400°C, a large amount of martensite is generated and the toughness is reduced. When the coiling temperature exceeds 650°C, the nucleation frequency of ferrite or bainite decreases, and they coarsen, so a structure having the average grain size of the above-mentioned square steel pipe cannot be obtained. The coiling temperature is preferably above 430°C. In addition, the coiling temperature is preferably below 620°C.

[0246] <Architectural structures>

[0247] Next, use Figure 5 , an embodiment of a building structure using the square steel pipe 10 of the present invention is described. Figure 51 shows an example of a building structure 100 in which the square steel pipe 10 of the present invention is used as a member (eg, a column) of the building structure.

[0248] like Figure 5 As shown, in the building structure 100 of the present invention, two or more square steel pipes 10 (column materials) are set up via a partition 17 and welded to each other. A beam 18 is set between adjacent square steel pipes 10, and a small beam 19 is set between adjacent beams 18. In addition, for the installation of walls, etc., a spacer 20 is also appropriately provided. In addition, known components can be used for the building structure 100.

[0249] As described above, the corner 12 of the square steel pipe 10 of the present invention has a small radius of curvature and a flat plate 11, and has excellent shape characteristics. In addition, the outer surface of the corner 12 of the square steel pipe 10 of the present invention has excellent ductility and toughness. Therefore, the building structure 100 of the present invention using the square steel pipe 10 as a column material can ensure the plastic deformation capacity of the entire structure, and therefore, it can exert better earthquake resistance than the building structure using the conventional square steel pipe.

[0250] Example

[0251] Hereinafter, the present invention will be described in more detail based on examples. It should be noted that the present invention is not limited to the following examples.

[0252] The square steel pipe of the present invention is manufactured under the following conditions.

[0253] Molten steel having the component composition shown in Table 1 was melted to produce slabs (steel raw materials). The obtained slabs were subjected to a hot rolling process, a cooling process, and a coiling process under the conditions shown in Table 2-1 to produce hot-rolled steel sheets.

[0254] The obtained hot-rolled steel plate (raw steel plate) is cold-formed into an open tube with an elliptical cross-section by using a row roll group and a fin-pass roll group. Then, the opposite end faces (both ends in the width direction) of the open tube are heated to a temperature above the melting point by high-frequency induction heating or high-frequency resistance heating, and are crimped by an extrusion roll to form an electric resistance welded steel tube.

[0255] The obtained electric resistance welded steel pipe (blank pipe) was reduced in diameter by a 2-stand (2-stage) sizing roll group, and then square-formed by a 4-stand (4-stage) square forming roll group to obtain square steel pipes of the sizes shown in Table 2-2. In the square forming process, the gap between the sizing rolls and the gap between the square forming rolls immediately before square forming were controlled under the conditions shown in Table 2-2. The obtained square steel pipe was approximately rectangular when viewed from a cross section perpendicular to the pipe axis.

[0256] It should be noted that the average wall thickness t (mm) of the square steel pipe shown in Table 2-2 is calculated using the above formula (3), and the average side length H (mm) of the square steel pipe is calculated using the above formula (4). Figure 1 The side length of the flat plate portion of the position shown was measured. The width W (mm) of the original steel plate was measured just after passing through the leveler. The circumference C of the electric resistance welded steel pipe at the inlet side of the first stage square forming stand IN (mm), the circumference C of the square steel pipe at the outlet side of the final stage of the square forming rack OUT (mm), and the difference (Δg) between the maximum gap between the diameter roller of the sizing stand immediately before square forming and the diameter roller of the first stage square forming stand are measured by the above method. Then, G (=Δg / (t / H)) is calculated using the above difference (Δg), the average wall thickness t and the average side length H.

[0257] In addition, for the obtained square steel pipes, each square steel pipe was cut perpendicularly to the pipe axis direction, and the cut surface including the resistance welded portion was polished, then etched with nital solution, and observed with an optical microscope. It was also confirmed that the width of the molten solidified portion of the resistance welded portion in the pipe circumferential direction was 1.0 μm or more and 1000 μm or less in the total thickness of the pipe. The molten solidified portion can be specified as a region observed relatively white with an optical microscope in the above cross section after etching with nital solution.

[0258] The steel structure of the obtained square steel pipe was quantified, tested, and evaluated by the method shown below.

[0259] (1) Steel structure of square steel pipe

[0260] The steel structure of the square steel pipe was quantitatively measured by the above method. The obtained results are shown in Table 3.

[0261] (2) The radius of curvature of the outer surface of the corner of the square steel pipe

[0262] Regarding the radius of curvature of the corners of the obtained square steel pipe, the radius of curvature (mm) of the outer surface of the four corners (outside of the corners) was measured at any 10 positions in the pipe axis direction. The maximum value Rmax and the minimum value Rmin were respectively calculated from the measured values ​​at a total of 40 positions. The values ​​are shown in Table 4. Here, when the maximum value Rmax and the minimum value Rmin of the radius of curvature are within the range of 2.0t or more and 3.0t or less, it is evaluated that the radius of curvature of the outer surface of the corner is small.

[0263] It should be noted that the radius of curvature of the outer side of the corner is measured using a radial measuring instrument. Figure 1The above-described method is used to perform the measurement.

[0264] (3) Flatness of the flat plate of the square steel pipe

[0265] use Fig.10 The flatness measurement method is described below. In the flatness measurement, the four flat plate portions are measured at 10 random positions in the pipe axis direction of the square steel pipe, and the measurement is performed at 40 positions in total. Fig.10 As shown in Table 4, the maximum bulge and the maximum depression with respect to the straight line passing through two points at both ends of the outer surface of each flat plate portion are measured. The bulge is set as a positive value, and the depression is set as a negative value, and the measured values ​​are shown in Table 4. Then, the absolute value of the maximum bulge and the maximum depression of each measurement position is obtained, and the maximum value is taken as the flatness of the flat plate portion, which is shown in Table 4. However, when there is no bulge or depression, the value of the bulge or depression is set to 0.

[0266] Here, when the flatness (mm) of the flat plate portion was 2.5 mm or less, it was evaluated that the flat plate portion was flat.

[0267] (4) Tensile test of flat plate and corner of square steel tube

[0268] Using the obtained square steel pipe, a tensile test was carried out by the following method. Figure 6 The cutting positions of the tensile test pieces for the flat plate and the corner are shown in FIG. Figure 7 The detailed cutting position of the tensile test piece at the corner is shown in FIG.

[0269] like Figure 6 As shown in the figure, JIS No. 5 tensile test pieces and JIS No. 12B tensile test pieces indicated by dotted lines are cut from the flat plate and corner of the square steel pipe in such a way that the tensile direction is parallel to the pipe axis direction. The tensile test pieces are cut by grinding them in such a way that their thickness is 5 mm and the center of the thickness is at a position 1 / 4t of the wall thickness t from the outer surface of the pipe. It should be noted that Figure 7 As shown, the tensile test piece of the corner portion is cut from a line passing through the intersection points respectively extended from the outer surfaces of the flat plate portions on both sides adjacent to the corner portion and forming a 45° angle with the outer surface of the flat plate portion.

[0270] Using these tensile test pieces, a tensile test was carried out in accordance with the provisions of JIS Z 2241 to measure the yield strength YS, tensile strength TS, and uniform elongation (flat portion: E1, corner portion: E2) of the flat portion and the corner portion. The uniform elongation was set to the value of the total elongation at the maximum load. For the corner portion, the yield strength and tensile strength obtained were used to calculate the yield ratio defined by (yield strength) / (tensile strength)×100(%). In addition, the value of the uniform elongation E2 of the corner portion relative to the uniform elongation E1 of the flat portion was calculated.

[0271] The number of tensile test pieces was set to 2 each, and the average values ​​were calculated to obtain the yield strength YS (MPa), tensile strength TS (MPa), yield ratio (%), and uniform elongation (%). These values ​​are shown in Table 4.

[0272] Here, when the uniform elongation E2 of the corner portion relative to the uniform elongation E1 of the flat portion is 0.60 or more, the ductility of the outer surface of the corner portion is evaluated to be excellent. When the yield ratio of the corner portion is 90% or less, it is evaluated to be good, when the yield strength YS of the flat portion is 295 MPa or more, it is evaluated to be good, and when the tensile strength TS of the flat portion is 400 MPa or more, it is evaluated to be good.

[0273] It should be noted that if Figure 6 As shown, the tensile test piece of the flat plate portion is cut from the center of the width of the flat plate portion 11b adjacent to the flat plate portion 11a including the resistance welded portion 13 of the square steel pipe. The tensile test piece of the corner portion is cut from the corner portion 12a adjacent to the flat plate portion 11a including the resistance welded portion 13.

[0274] (5) Charpy impact test on the corners of square steel pipes

[0275] Using the obtained square steel pipe, a Charpy impact test was performed by the following method. Figure 8 The cutting position of the Charpy test piece at the corner is shown in FIG. Fig. 9 The detailed cutting position of the Charpy test piece at the corner is shown in FIG.

[0276] like Figure 8 and Fig. 9 As shown in FIG. 1 , in the Charpy impact test, a V-notch standard test piece according to the provisions of JIS Z 2242 is used, which is cut at a position 1 / 4t of the wall thickness t from the outer surface of the square steel pipe so that the length direction of the test piece is parallel to the pipe axis direction. The Charpy test piece of the corner is cut from the corner 12a adjacent to the flat plate portion 11a including the resistance welded portion 13. More specifically, as shown in FIG. Fig. 9As shown, the test piece is cut from the line passing through the intersection extending from the outer surface of the flat plate portion on both sides adjacent to the corner portion 12a and forming an angle of 45° with the outer surface of the flat plate portion. According to the provisions of JIS Z 2242, the Charpy impact test is carried out at a test temperature of -10°C to obtain the Charpy absorbed energy (J). It should be noted that the number of test pieces is set to 3 each, and their average value is calculated to obtain the Charpy absorbed energy (J). The value is shown in Table 4.

[0277] Here, when the Charpy absorbed energy at -10°C of the corner portion is 100 J or more, it is evaluated that the toughness of the outer surface of the corner portion is excellent.

[0278]

[0279]

[0280]

[0281]

[0282]

[0283] In Table 2-1 to Table 4, No. 1 to 3 and 8 to 13 are examples of the present invention, and No. 4 to 7 are comparative examples.

[0284] The square steel pipes of the examples of the present invention all have a radius of curvature R of the outer side of the corner that is greater than or equal to 2.0t and less than or equal to 3.0t, a flatness of the outer surface of the flat plate portion in the tube axis direction of less than or equal to 2.5mm, a uniform elongation E2 at a position 1 / 4t from the outer surface of the corner that is greater than or equal to 0.60 times the uniform elongation E1 at a position 1 / 4t from the outer surface of the flat plate portion, and a Charpy absorbed energy of the corner at -10°C of greater than or equal to 100J.

[0285] On the other hand, in the case of Comparative Example No. 4, "W / C OUT The value of " is lower than the range of formula (1), and therefore the radius of curvature of the outer side of the corner portion exceeds the range of the present invention, and a flat plate portion is not obtained.

[0286] Regarding Comparative Example No. 5, "W / C OUT " exceeds the range of formula (1), and therefore, the ratio of uniform elongation between the flat portion and the corner portion (E2 / E1) and the Charpy absorption energy at -10°C of the corner portion do not reach the expected values. In addition, the yield ratio of the corner portion also shows a value of more than 90%.

[0287] Regarding Comparative Example No. 6, “C IN / C OUTThe value of " is lower than the range of formula (2), and therefore, the radius of curvature of the outer side of the corner portion exceeds the range of the present invention, and a flat plate portion is not obtained.

[0288] Regarding Comparative Example No. 7, “C IN / C OUT " exceeds the range of formula (2), and therefore, the radius of curvature of the outer side of the corner is lower than the range of the present invention, and the ratio of the uniform elongation of the flat portion to the corner (E2 / E1) and the Charpy absorption energy of the corner at -10°C do not reach the expected values. In addition, the yield ratio of the corner also shows a value of more than 90%.

[0289] Explanation of symbols

[0290] 1Steel plate (steel strip)

[0291] 2 Leveling Machine

[0292] 3-row roller set

[0293] 4-fin hole roller set

[0294] 5 squeeze rollers

[0295] 6Welding Machine

[0296] 7. Electric resistance welded steel pipe

[0297] 8 Sizing roller group

[0298] 9 square forming roller set

[0299] 10 Square steel pipe

[0300] 11 Flat plate

[0301] 12 corners

[0302] 13 Welding section (resistance welding section)

[0303] 14 Parent material department

[0304] 15 Heat affected zone

[0305] 16 Melting and solidification section

[0306] 17 Bulkhead

[0307] 18 Beam

[0308] 19 Xiaoliang

[0309] 20 columns

[0310] 100 Building structures

Claims

1. A square steel pipe having a flat portion and a corner portion, wherein: When the average thickness of the flat plate portion is t (mm), the radius of curvature R of the outer side of the corner portion is greater than or equal to 2.0t and less than or equal to 3.0t, The flatness of the outer surface of the flat plate portion is less than 2.5 mm, The uniform elongation E2 at a position 1 / 4t from the outer surface of the corner portion in the wall thickness direction is 0.60 times or more relative to the uniform elongation E1 at a position 1 / 4t from the outer surface of the flat plate portion in the wall thickness direction, The Charpy absorbed energy at -10°C at a position 1 / 4t from the outer surface of the corner in the wall thickness direction is 100 J or more, The square steel pipe has a composition, in mass%, of C: 0.020-0.45%, Si: 0.01-1.0%, Mn: 0.30-3.0%, P: 0.10% or less, S: 0.050% or less, Al: 0.005-0.10%, N: 0.010% or less, Ti: 0.001-0.15%, and the balance is Fe and unavoidable impurities. In the steel structure at the center of the wall thickness of the flat plate portion, the total volume fraction of ferrite and bainite is 70% or more and 95% or less relative to the entire steel structure at the center of the wall thickness of the flat plate portion, and the remainder is composed of one or more selected from pearlite, martensite, and austenite, When the region surrounded by the boundary where the orientation difference between adjacent crystals is 15° or more is defined as a crystal grain, The average grain size of the crystal grains is 15.0 μm or less, The total volume ratio of the crystal grains having a grain size of 40 μm or more is 40% or less with respect to the entire steel structure at the center of the wall thickness of the flat plate portion.

2. The square steel tube according to claim 1, wherein: The average wall thickness t is greater than 0.030 times the average side length H (mm) of the flat plate portion.

3. The square steel tube according to claim 1, wherein: The average wall thickness t is greater than or equal to 20 mm and less than or equal to 40 mm.

4. The square steel tube according to claim 2, wherein: The average wall thickness t is greater than or equal to 20 mm and less than or equal to 40 mm.

5. The square steel tube according to claim 1, wherein: The yield strength of the flat plate portion is 295 MPa or more. The tensile strength of the flat plate portion is 400 MPa or more. The yield ratio of the corner portion is 90% or less.

6. The square steel tube according to claim 2, wherein: The yield strength of the flat plate portion is 295 MPa or more. The tensile strength of the flat plate portion is 400 MPa or more. The yield ratio of the corner portion is 90% or less.

7. The square steel tube according to claim 3, wherein: The yield strength of the flat plate portion is 295 MPa or more. The tensile strength of the flat plate portion is 400 MPa or more. The yield ratio of the corner portion is 90% or less.

8. The square steel tube according to claim 4, wherein: The yield strength of the flat plate portion is 295 MPa or more. The tensile strength of the flat plate portion is 400 MPa or more. The yield ratio of the corner portion is 90% or less.

9. The square steel pipe according to any one of claims 1 to 8, wherein In addition to the above-mentioned component composition, it also contains, in terms of mass%, one or more selected from the group consisting of Nb: 0.001-0.15%, V: 0.001-0.15%, Cr: 0.01-1.0%, Mo: 0.01-1.0%, Cu: 0.01-1.0%, Ni: 0.01-1.0%, Ca: 0.0002-0.010%, and B: 0.0001-0.010%.

10. A method for manufacturing a square steel pipe, which is the method for manufacturing a square steel pipe according to any one of claims 1 to 9, wherein: The steel plate is cold rolled and both ends of the steel plate in the width direction are resistance welded to form a resistance welded steel pipe. Then, the resistance welded steel pipe is reduced in diameter using a sizing rack and then squared using a square forming rack to produce a square steel pipe. At this time, The width W of the steel plate is relative to the circumference C of the square steel pipe at the outlet side of the square forming frame. OUT The ratio satisfies the formula (1), and the circumference C of the electric resistance welded steel pipe at the inlet side of the square forming rack is IN The circumference C of the square steel pipe relative to the outlet side of the square forming rack OUT The gap between the rollers of the sizing stand immediately before square forming and the gap between the rollers of the square forming stand are controlled in such a way that the ratio of satisfies the formula (2). 1.000+0.050×t / H<W / C OUT <1.000+0.50×t / H…Formula (1) 0.30×t / H+0.99≤C IN / C OUT <0.50×t / H+0.99…Formula (2) Here, in formula (1) and formula (2), W: The width of the steel plate as the raw material (mm), C IN : The circumference of the electric resistance welded steel pipe on the inlet side of the first section of the square forming rack (mm), C OUT : The circumference of the square steel pipe on the outlet side of the square forming rack in the final section (mm), t: average wall thickness of the flat plate after square forming (mm), H: average side length of the flat plate after square forming (mm), Wherein, in the case of using a square forming frame of one section to perform square forming, the square forming frame of the first section and the square forming frame of the final section refer to the same square forming frame.

11. The method for manufacturing a square steel pipe according to claim 10, wherein: The steel plate was obtained as follows: After heating the steel material to a heating temperature of 1100° C. to 1300° C., hot rolling is performed with a rough rolling end temperature of 850° C. to 1150° C., a finish rolling end temperature of 750° C. to 900° C., and a total reduction ratio of 50% or more at 950° C. or less. Next, cooling is performed under the conditions that the average cooling rate is 5°C / s to 30°C / s at the wall thickness center temperature and the cooling stop temperature is 400°C to 650°C. Next, coiling is performed at 400°C to 650°C.

12. The method for manufacturing a square steel pipe according to claim 10, wherein: The average wall thickness t is greater than 0.030 times the average side length H of the flat plate portion.

13. The method for manufacturing a square steel pipe according to claim 11, wherein: The average wall thickness t is greater than 0.030 times the average side length H of the flat plate portion.

14. The method for manufacturing a square steel pipe according to any one of claims 10 to 13, wherein: The average wall thickness t is greater than or equal to 20 mm and less than or equal to 40 mm.

15. A building structure, wherein: The square steel pipe according to any one of claims 1 to 9 is used as the column material.

Citation Information

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