Inorganic silicate liquid production material preparation kettle

The chemical reactor, designed with a cylindrical tube and a spraying mechanism, utilizes high-temperature hot steam to accelerate the chemicaling and rotate the liquid material. Combined with an electrically controlled valve body and a detachable chemicaling plate, it achieves rapid and efficient preparation and convenient cleaning of inorganic silicate liquid materials, solving the problems of long chemicaling cycles and inconvenient cleaning and maintenance.

CN116351349BActive Publication Date: 2026-05-05LUOYANG QIHANG CHEM IND CO LTD
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Patent Information

Authority / Receiving Office
CN · China
Patent Type
Patents(China)
Current Assignee / Owner
LUOYANG QIHANG CHEM IND CO LTD
Filing Date
2023-04-26
Publication Date
2026-05-05

AI Technical Summary

Technical Problem

The existing chemical reaction kettles used for the production of inorganic silicate liquid materials have long chemical reaction cycles, are inconvenient to clean and maintain, and require opening the chemical reaction kettle to discharge the slag.

Method used

The design employs a cylindrical tube and spraying mechanism, utilizing high-temperature steam to accelerate the material processing. The rotation of the liquid material is achieved through the cooperation of a sealing plate and a diversion pipe, further accelerating the material processing. After the material processing is completed, the slag can be discharged without opening the material processing vessel. Cleaning and venting are achieved using an electrically controlled valve body and a stepper motor. A detachable material processing plate and an arc-shaped sealing plate are provided for quick material loading and cleaning.

Benefits of technology

The material processing cycle is shortened, cleaning and maintenance are convenient, and the discharge of slag is time-saving and labor-saving, which improves production efficiency and ease of operation.

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Abstract

This application discloses a high-efficiency chemical reaction vessel for the production of inorganic silicate liquid materials, including a cylindrical body. An upper end cover is provided on the upper end face of the cylindrical body. The upper end cover is equipped with a pressure relief pipe, a safety valve, a discharge pipe, and a water injection pipe. A cylindrical tube is slidably connected to the middle of the upper surface of the upper end cover. The upper end face of the cylindrical tube is connected to the cylindrical body via a lifting mechanism. A steam supply pipe and a cleaning pipe are connected to the upper end of the outer side face of the cylindrical tube. This high-efficiency chemical reaction vessel for the production of inorganic silicate liquid materials has a short chemical reaction cycle, enabling rapid and efficient preparation of liquid silicate. Simultaneously, the vessel is easy to clean and maintain; when discharging slag, there is no need to open the vessel, saving time and effort. Opening the valve on the discharge pipe allows the high pressure inside the cylindrical body to quickly discharge the liquid material. The steam supply pipe is used to introduce hot steam into the cylindrical body to accelerate the chemical reaction process, and the cleaning pipe is used to introduce cleaning liquid and hot air into the cylindrical body.
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Description

Technical Field

[0001] This application relates to the technical field of inorganic silicate production equipment, specifically a chemical reaction vessel for the production of inorganic silicate liquid materials. Background Technology

[0002] A chemical reaction vessel for producing inorganic silicate liquid is a piece of equipment used to produce silicate chemicals. This equipment typically consists of a vessel body, a stirrer, a heating device, and a cooling device, and can be used to manufacture chemical products such as sodium silicate. In the specific operation, quartz sand, alkali metal hydroxides, and water are conventionally used as raw materials, and a chemical reaction is carried out under high temperature and high pressure conditions to produce liquid silicate.

[0003] To improve the production efficiency of liquid silicates, existing technologies typically employ the method of introducing hot steam into the reaction vessel to heat and pressurize the materials, thereby increasing the solid material's reaction efficiency. Using this method, a single reaction cycle takes approximately 3-4 hours, which is quite time-consuming. Furthermore, existing reaction vessels used for producing inorganic silicate liquids require opening for cleaning and slag removal after each reaction, which is inconvenient due to the large internal dimensions of the vessels. Summary of the Invention

[0004] This application provides a chemical reaction vessel for the production of inorganic silicate liquid. This chemical reaction vessel has a short chemical reaction cycle and can quickly and efficiently prepare liquid silicate. At the same time, this chemical reaction vessel is easy to clean and maintain. When discharging slag, there is no need to open the chemical reaction vessel, which saves time and effort and can effectively solve the problems in the background technology.

[0005] To achieve the above objectives, this application provides the following technical solution: a chemical reactor for the production of inorganic silicate liquid materials, comprising a cylinder, an upper end cover on the upper end face of the cylinder, a pressure relief pipe, a safety valve, a discharge pipe and a water injection pipe on the upper end cover, a cylindrical tube slidably connected to the middle of the upper surface of the upper end cover, the upper end face of the cylindrical tube being connected to the cylinder through a lifting mechanism, and a steam supply pipe and a cleaning pipe connected to the upper end of the outer side face of the cylindrical tube.

[0006] The lower end face of the cylindrical tube is connected to a spraying mechanism, which includes a sealing cover. The upper part of the outer side of the sealing cover is provided with a feed inlet, which is connected to the discharge port of the cylindrical tube. The outer side of the sealing cover is provided with a diverter pipe. Both the outer end and the lower end of the outer side of the diverter pipe are provided with nozzles. The nozzles are inclined downwards, and the nozzles of the nozzles located at the lower end of the outer side of the diverter pipe face the same direction. The sealing cover is provided with a sealing plate inside. The lower surface of the sealing plate is provided with a return spring.

[0007] Inside the cylinder, above the spraying mechanism, there is a material-dissolving plate. The material-dissolving plate includes a hopper. The bottom of the inner side of the hopper has a through hole. The inside of the hopper has a strip groove. The outer side of the hopper has a slider. The outer side of the slider has an arc-shaped sealing plate. The outer side of the cylinder has an arc-shaped groove for the material-dissolving plate to pass through. The arc-shaped groove and the arc-shaped sealing plate are sealed and correspondingly arranged. The arc-shaped sealing plate includes a semi-circular sealing plate. The inner side of the semi-circular sealing plate has a sealing strip.

[0008] The outer side of the cylinder is provided with an open shell near the arc groove. The open shell is slidably connected to the slider. The end of the slider is connected to a push plate through a guide rod. The push plate is connected to a hydraulic telescopic rod provided on the outer side of the cylinder. A cover plate is slidably connected to the upper surface of the open shell. The cover plate is provided with a lifting lug.

[0009] The lower end face of the cylinder is provided with an electrically controlled valve body, which includes a cylindrical sealing shell. The upper part of the outer side of the cylindrical sealing shell is provided with a material guide hood, which is connected to the lower end face of the cylinder. The cylindrical sealing shell has a sealing shaft inside, and the end of the sealing shaft is connected to the output end of a stepper motor. The stepper motor is mounted on the cylindrical sealing shell. The lower end of the outer side of the cylindrical sealing shell is provided with a material guide hood, and the end of the outer side of the cylindrical sealing shell is provided with an air collecting pipe. The sealing shaft includes a cylindrical roller body, and the outer side of the cylindrical roller body is provided with a rubber sealing layer. The cylindrical roller body is provided with a through groove and an exhaust channel. The exhaust channel is connected to the air collecting pipe, and the through groove is connected to the material guide hood.

[0010] Preferably, the cylinder is a pressure vessel, and the outer surface of the cylinder is covered with an insulated shell.

[0011] Preferably, the outer surface of the cylindrical tube is sealed to the upper end cap.

[0012] Preferably, the outer side of the cylinder is provided with an annular support, the upper end face of the cylindrical tube is provided with a support plate, and the lower surface of the support plate is connected to the annular support through an electrically controlled telescopic rod.

[0013] Preferably, the outer side of the annular support is provided with a support rod, the upper end of the support rod is provided with a sleeve rod, and the two ends of the outer side of the sleeve rod are respectively fitted with an air supply pipe lifting ring and a cleaning pipe lifting ring. The air supply pipe lifting ring is connected to the outer side of the steam supply pipe, and the cleaning pipe lifting ring is connected to the outer side of the cleaning pipe. Both the steam supply pipe and the cleaning pipe are provided with solenoid valves.

[0014] Preferably, the cylindrical tube consists of a fixed tube and a moving tube, and a clutch is provided at the connection between the fixed tube and the moving tube, so that the fixed tube and the moving tube are in sealed rotating contact.

[0015] Preferably, the clutch includes a top support, an upper gear plate, a lower gear plate, and a pneumatic telescopic rod. The top support is installed on the fixed pipe, the upper gear plate is slidably connected to a groove provided on the moving pipe, and the top support is connected to the upper gear plate through the pneumatic telescopic rod. The upper gear plate and the lower gear plate are correspondingly engaged.

[0016] Preferably, the bottom of the outer side of the cylinder is provided with a sealing plate, and a rotating shaft is sealed and connected to the sealing plate. A cylindrical mesh cage is provided at the end of the rotating shaft. The cylindrical mesh cage is set inside the cylinder. The lower end face of the discharge pipe is set close to the outer side of the cylindrical mesh cage, and the discharge pipe is set close to the inner side of the cylinder.

[0017] Preferably, a waste collection box is connected to the lower part of the guide cover, the waste collection box has a pull-out box inside, and an observation window is provided on the outer side of the waste collection box; an air nozzle is provided on the upper surface of the cover plate, and a collection pipe is provided on the lower surface of the open shell. The collection pipe is connected to the waste collection box, and a control valve is provided on the collection pipe.

[0018] Preferably, the gas collecting pipe is connected to a cyclone separator via a flexible air guide tube, and a dust filter bag is provided at the outlet of the cyclone separator.

[0019] Compared with the prior art, the beneficial effects of this application are:

[0020] 1. This inorganic silicate liquid material production reactor has a short chemical reaction cycle, which can quickly and efficiently prepare liquid silicates. At the same time, this chemical reaction reactor is easy to clean and maintain. When discharging slag, there is no need to open the chemical reaction reactor, which saves time and effort.

[0021] 2. Open the valve on the discharge pipe. The high pressure inside the cylinder can quickly discharge the liquid material. The steam supply pipe is used to introduce hot steam into the cylinder to accelerate the material processing. The cleaning pipe is used to send cleaning fluid and hot air into the cylinder.

[0022] 3. The cylindrical tube introduces high-temperature steam into the interior of the sealing cover. The steam pushes the sealing plate downward, and the synchronous reset spring is compressed. At the same time as the sealing plate moves downward, the air inlet of the diversion pipe opens, and the steam enters the interior of the diversion pipe. Finally, it is spirally sprayed out through the nozzle. The liquid material rotates under the push of the steam, which accelerates the chemical process. Attached Figure Description

[0023] Figure 1 This is a schematic diagram of the structure of this application;

[0024] Figure 2 This is the main view of this application;

[0025] Figure 3 This is a schematic diagram of the clutch structure;

[0026] Figure 4 This is a schematic diagram of the structure of an electrically controlled valve body;

[0027] Figure 5 This is a schematic diagram of the sealed shaft structure;

[0028] Figure 6 This is a top view of this application;

[0029] Figure 7 This is a sectional view of the cylinder;

[0030] Figure 8 for Figure 7 Enlarged view of a portion of point A in the middle;

[0031] Figure 9 This is a schematic diagram of the spraying mechanism.

[0032] Figure 10 This is a front sectional view of the spraying mechanism;

[0033] Figure 11 This is a schematic diagram of the chemical material plate structure;

[0034] Figure 12 This is a schematic diagram of the arc-shaped sealing plate structure.

[0035] In the diagram: 1. Air supply pipe lifting ring; 2. Support plate; 3. Sleeve rod; 4. Cleaning pipe lifting ring; 5. Cleaning pipe; 6. Cylindrical pipe; 61. Fixed pipe; 62. Moving pipe; 7. Electrically controlled telescopic rod; 8. Pressure relief pipe; 9. Safety valve; 10. Cover plate; 11. Push plate; 12. Cyclone separator; 13. Hydraulic telescopic rod; 14. Waste collection box; 15. Observation window; 16. Electrically controlled valve body; 161. Material guide cover; 162. Stepper motor; 163. Sealing shaft; 1631. Through groove; 1632. Cylindrical roller; 1633. Exhaust channel; 164. Discharge guide cover; 165. Cylindrical sealing shell; 17. Pull-out box; 18. Annular support; 19. Cylinder; 20. Upper end cover; 21. Discharge pipe; 22. Water injection pipe; 23. Support. 24. Steam supply pipe, 25. Clutch, 251. Top support, 252. Upper toothed plate, 253. Lower toothed plate, 254. Pneumatic telescopic rod, 26. Air collection pipe, 27. Collection pipe, 28. Air guide hose, 29. Air nozzle, 30. Lifting lug, 31. Open shell, 32. Guide rod, 33. Spraying mechanism, 331. Diverter pipe, 332. Feed inlet, 333. Sealing cover, 334. Nozzle, 335. Sealing plate, 336. Return spring, 34. Material processing plate, 341. Strip groove, 342. Through hole, 343. Hopper, 344. Arc-shaped sealing plate, 3441. Semi-circular sealing plate, 3442. Sealing strip, 345. Slider, 35. Sealing plate, 36. Rotating shaft, 37. Columnar mesh cage. Detailed Implementation

[0036] The technical solutions of the embodiments of this application will be clearly and completely described below with reference to the accompanying drawings. Obviously, the described embodiments are only some embodiments of this application, and not all embodiments. Based on the embodiments of this application, all other embodiments obtained by those skilled in the art without creative effort are within the scope of protection of this application.

[0037] In the description of this application, if directional descriptions are involved, such as "up," "down," "front," "back," "left," "right," etc., indicating directional or positional relationships, they are based on the appendix. Figure 2 The orientations or positional relationships shown are for the convenience of describing this application and simplifying the description only, and are not intended to indicate or imply that the device or element referred to must have a specific orientation, or be constructed and operated in a specific orientation, and therefore should not be construed as a limitation of this application. When a feature is referred to as "set", "fixed", or "connected" to another feature, it can be directly set, fixed, or connected to the other feature, or it can be indirectly set, fixed, or connected to the other feature. Example 1:

[0038] Please see Figure 1 This application provides the following technical solution: a chemical reactor for the production of inorganic silicate liquid materials, including a cylinder 19, an upper end cover 20 on the upper end face of the cylinder 19, a pressure relief pipe 8, a safety valve 9, a discharge pipe 21 and a water injection pipe 22 on the upper end cover 20, a cylindrical pipe 6 slidably connected to the middle of the upper surface of the upper end cover 20, the upper end face of the cylindrical pipe 6 being connected to the cylinder 19 through a lifting mechanism, and a steam supply pipe 24 and a cleaning pipe 5 connected to the upper end of the outer side face of the cylindrical pipe 6.

[0039] Specifically, the pressure relief pipe 8, safety valve 9, discharge pipe 21 and water injection pipe 22 are all equipped with independent valves. After the material is chemically processed, the valve on the discharge pipe 21 is opened, and the high pressure in the cylinder 19 can quickly discharge the liquid material. The steam supply pipe 24 is used to introduce hot steam into the cylinder 19 to accelerate the chemical process. The cleaning pipe 5 is used to send cleaning fluid and hot air into the cylinder 19.

[0040] Please see Figure 7 , 9In section 10, the lower end face of the cylindrical tube 6 is connected to a spraying mechanism 33. The spraying mechanism 33 includes a sealing cover 333. The upper part of the outer side of the sealing cover 333 is provided with a feed inlet 332, which is connected to the discharge port of the cylindrical tube 6. The outer side of the sealing cover 333 is provided with four diversion pipes 331. The outer end and the lower end of the outer side of the diversion pipe 331 are provided with nozzles 334. The nozzles 334 are inclined downwards. The nozzles 334 located at the lower end of the outer side of the diversion pipe 331 have the same nozzle orientation. The interior of the sealing cover 333 is provided with a sealing plate 335. The lower surface of the sealing plate 335 is provided with a return spring 336.

[0041] Specifically, the cylindrical tube 6 introduces high-temperature hot steam into the interior of the sealing cover 333. The hot steam pushes the sealing plate 335 downward, and the synchronous return spring 336 is compressed. At the same time as the sealing plate 335 moves downward, the air inlet of the diversion pipe 331 is opened, and the hot steam enters the interior of the diversion pipe 331. Finally, it is spirally sprayed out through the nozzle 334. The liquid material rotates under the push of the hot steam, which accelerates the chemical process.

[0042] Please see Figure 11-12 Inside the cylinder 19, above the spraying mechanism 33, there is a material-dissolving plate 34. The material-dissolving plate 34 includes a hopper 343. The bottom of the inner side of the hopper 343 has a through hole 342. The inside of the hopper 343 has a strip groove 341. The outer side of the hopper 343 has a slider 345. The outer side of the slider 345 has an arc-shaped sealing plate 344. The outer side of the cylinder 19 has an arc-shaped groove for the material-dissolving plate 344 to pass through. The arc-shaped groove and the arc-shaped sealing plate 344 are sealed and correspondingly arranged. The arc-shaped sealing plate 344 includes a semi-circular sealing plate 3441. The inner side of the semi-circular sealing plate 3441 has a sealing strip 3442.

[0043] Specifically, the solid material that needs to be processed is loaded into the hopper 343. Inserting the hopper 343 into the cylinder 19 allows for rapid loading. After processing is complete, the slag inside the hopper 343 can be quickly cleaned by pulling it out.

[0044] Please see Figure 6 An open shell 31 is provided on the outer side of the cylinder 19 near the arc groove. The open shell 31 is slidably connected to the slider 345. The end of the slider 345 is connected to the push plate 11 through the guide rod 32. The push plate 11 is connected to the hydraulic telescopic rod 13 provided on the outer side of the cylinder 19. A cover plate 10 is slidably connected to the upper surface of the open shell 31. The cover plate 10 is provided with a lifting lug 30.

[0045] Specifically, the hopper 343 can be pulled out by extending and retracting the hydraulic telescopic rod 13, which facilitates quick loading. The cover plate 10 can be opened by the lifting lug 30, which is more conducive to the filling of materials.

[0046] More specifically, the slider 345 and the hopper 343 are detachably connected, which facilitates the cleaning of material residue inside the hopper 343.

[0047] Please see Figure 4-5 The lower end face of the cylinder 19 is provided with an electrically controlled valve body 16. The electrically controlled valve body 16 includes a cylindrical sealing housing 165. The upper end of the outer side of the cylindrical sealing housing 165 is provided with a discharge guide hood 164, which is connected to the lower end face of the cylinder 19. A sealing shaft 163 is sealed and connected inside the cylindrical sealing housing 165. The end of the sealing shaft 163 is connected to the output end of a stepper motor 162. The stepper motor 162 is mounted on the cylindrical sealing housing. On the body 165, a guide cover 161 is provided at the lower end of the outer side of the cylindrical sealing housing 165, and an air collecting pipe 26 is provided at the end of the outer side of the cylindrical sealing housing 165. The sealing shaft 163 includes a cylindrical roller body 1632, and a rubber sealing layer is provided on the outer side of the cylindrical roller body 1632. A through groove 1631 and an exhaust channel 1633 are provided on the cylindrical roller body 1632. The exhaust channel 1633 communicates with the air collecting pipe 26, and the through groove 1631 communicates with the guide cover 161.

[0048] Specifically, when it is necessary to discharge solid material residue and clean the inner wall of the cylinder 19, the stepper motor 162 drives the sealing shaft 163 to rotate, rotating the through groove 1631 to a vertical position. At this time, the material residue and cleaning liquid in the cylinder 19 can be discharged through the through groove 1631.

[0049] More specifically, when it is necessary to blow the inner wall of the cylinder 19, the stepper motor 162 drives the sealing shaft 163 to rotate, rotating the exhaust channel 1633 to the lower end of the cylinder 19. At this time, the gas in the cylinder 19 carrying dust is discharged through the exhaust channel 1633.

[0050] Furthermore, the cylinder 19 is a pressure vessel, and the outer surface of the cylinder 19 is covered with an insulated shell.

[0051] Specifically, setting up an insulated shell can effectively reduce the rate at which heat is lost from the cylinder 19.

[0052] Furthermore, the outer surface of the cylindrical tube 6 is sealed to the upper end cap 20.

[0053] Specifically, the cylindrical tube 6 is sealed and rotatedly connected to the upper end cover 20.

[0054] For further details, please refer to Figure 1 The outer side of the cylinder 19 is provided with an annular support 18, and the upper end face of the cylindrical tube 6 is provided with a support plate 2. The lower surface of the support plate 2 is connected to the annular support 18 through an electrically controlled telescopic rod 7.

[0055] Specifically, the electrically controlled telescopic rod 7 can drive the cylindrical tube 6 to move up and down.

[0056] For further details, please refer to Figure 1 The outer side of the annular support 18 is provided with a support rod 23, and the upper end of the support rod 23 is provided with a sleeve rod 3. The two ends of the outer side of the sleeve rod 3 are respectively sleeved with an air supply pipe lifting ring 1 and a cleaning pipe lifting ring 4. The air supply pipe lifting ring 1 is connected to the outer side of the steam supply pipe 24, and the cleaning pipe lifting ring 4 is connected to the outer side of the cleaning pipe 5. Solenoid valves are provided on both the steam supply pipe 24 and the cleaning pipe 5.

[0057] Specifically, by setting up the air supply pipe lifting ring 1 and the cleaning pipe lifting ring 4, the steam supply pipe 24 and the cleaning pipe 5 can be effectively prevented from getting tangled.

[0058] For further details, please refer to Figure 3 The cylindrical tube 6 is composed of a fixed tube 61 and a moving tube 62. A clutch 25 is provided at the connection between the fixed tube 61 and the moving tube 62, and the fixed tube 61 and the moving tube 62 are sealed and rotated together.

[0059] Specifically, when the clutch 25 is engaged, the stationary pipe 61 and the moving pipe 62 can rotate relative to each other, thereby allowing the spraying mechanism 33 to rotate, which is beneficial for cleaning the inner wall of the reactor.

[0060] For further details, please refer to Figure 3 The clutch 25 includes a top support 251, an upper gear plate 252, a lower gear plate 253, and a pneumatic telescopic rod 254. The top support 251 is mounted on the fixed tube 61. The upper gear plate 252 is slidably connected to a groove provided on the moving tube 62. The top support 251 is connected to the upper gear plate 252 through the pneumatic telescopic rod 254. The upper gear plate 252 and the lower gear plate 253 are correspondingly engaged.

[0061] Specifically, the pneumatic telescopic rod 254 extends to engage the upper toothed plate 252 and the lower toothed plate 253 together, which can fix the relative position of the fixed tube 61 and the moving tube 62.

[0062] For further details, please refer to Figure 8 The bottom of the outer side of the cylinder 19 is provided with a sealing plate 35, and a rotating shaft 36 is sealed and connected on the sealing plate 35. A cylindrical mesh cage 37 is provided at the end of the rotating shaft 36. The cylindrical mesh cage 37 is set inside the cylinder 19. The lower end face of the discharge pipe 21 is set close to the outer side of the cylindrical mesh cage 37, and the discharge pipe 21 is set close to the inner side of the cylinder 19.

[0063] Specifically, by setting up the cylindrical mesh cage 37, the discharge pipe 21 can be effectively prevented from being blocked during the discharge process. If the discharge is not smooth, the cylindrical mesh cage 37 can be rotated and the lower end face of the discharge pipe 21 can scrape off the solid particles blocking the mesh of the cylindrical mesh cage 37.

[0064] For further details, please refer to Figure 1 and 4The waste collection box 14 is connected to the lower part of the material guide cover 161. The waste collection box 14 has a pull-out box 17 inside and an observation window 15 on the outer side of the waste collection box 14. The upper surface of the cover plate 10 is provided with an air nozzle 29, and the lower surface of the open shell 31 is provided with a collection pipe 27. The collection pipe 27 is connected to the waste collection box 14 and a control valve is provided on the collection pipe 27.

[0065] Specifically, the waste liquid and slag generated during the cleaning process can enter the interior of the pull-out box 17 through the guide cover 161. The slag can be collected through the pull-out box 17. When the air nozzle 29 is connected to the cleaning water and the chemical plate 34 is pulled out, the high-pressure water sprayed through the air nozzle 29 can complete the cleaning of the chemical plate 34. The wastewater generated during the cleaning process enters the pull-out box 17 through the collection pipe 27.

[0066] The sealed rotating connection disclosed in this invention adopts the form of bearing and sealing ring, with the sealing ring located at both ends of the bearing. Example 2:

[0067] The main difference between this embodiment and embodiment 1 is that embodiment 1 uses water washing to clean the inside of the reactor, while this embodiment uses purging to purge the inside of the reactor.

[0068] Please see Figure 1 This application provides the following technical solution: a chemical reactor for the production of inorganic silicate liquid materials, including a cylinder 19, an upper end cover 20 on the upper end face of the cylinder 19, a pressure relief pipe 8, a safety valve 9, a discharge pipe 21 and a water injection pipe 22 on the upper end cover 20, a cylindrical pipe 6 slidably connected to the middle of the upper surface of the upper end cover 20, the upper end face of the cylindrical pipe 6 being connected to the cylinder 19 through a lifting mechanism, and a steam supply pipe 24 and a cleaning pipe 5 connected to the upper end of the outer side face of the cylindrical pipe 6.

[0069] Specifically, the pressure relief pipe 8, safety valve 9, discharge pipe 21 and water injection pipe 22 are all equipped with independent valves. After the material is chemically processed, the valve on the discharge pipe 21 is opened, and the high pressure in the cylinder 19 can quickly discharge the liquid material. The steam supply pipe 24 is used to introduce hot steam into the cylinder 19 to accelerate the chemical process. The cleaning pipe 5 is used to send cleaning fluid and hot air into the cylinder 19.

[0070] Please see Figure 7 , 9In section 10, the lower end face of the cylindrical tube 6 is connected to a spraying mechanism 33. The spraying mechanism 33 includes a sealing cover 333. The upper end of the outer side of the sealing cover 333 is provided with a feed inlet 332, which is connected to the discharge port of the cylindrical tube 6. Four diversion pipes 331 are evenly distributed in a ring on the outer side of the sealing cover 333. The outer end and the lower end of the outer side of the diversion pipe 331 are provided with nozzles 334. The nozzles 334 are inclined downwards. The nozzles 334 located at the lower end of the outer side of the diversion pipe 331 have the same nozzle orientation. A sealing plate 335 is provided inside the sealing cover 333. A return spring 336 is provided on the lower surface of the sealing plate 335.

[0071] Specifically, the cylindrical tube 6 introduces high-temperature hot steam into the interior of the sealing cover 333. The hot steam pushes the sealing plate 335 downward, and the synchronous return spring 336 is compressed. At the same time as the sealing plate 335 moves downward, the air inlet of the diversion pipe 331 is opened, and the hot steam enters the interior of the diversion pipe 331. Finally, it is spirally sprayed out through the nozzle 334. The liquid material rotates under the push of the hot steam, which accelerates the chemical process.

[0072] Please see Figure 11-12 Inside the cylinder 19, above the spraying mechanism 33, there is a material-dissolving plate 34. The material-dissolving plate 34 includes a hopper 343. The bottom of the inner side of the hopper 343 has a through hole 342. The inside of the hopper 343 has a strip groove 341. The outer side of the hopper 343 has a slider 345. The outer side of the slider 345 has an arc-shaped sealing plate 344. The outer side of the cylinder 19 has an arc-shaped groove for the material-dissolving plate 344 to pass through. The arc-shaped groove and the arc-shaped sealing plate 344 are sealed and correspondingly arranged. The arc-shaped sealing plate 344 includes a semi-circular sealing plate 3441. The inner side of the semi-circular sealing plate 3441 has a sealing strip 3442.

[0073] Specifically, the solid material that needs to be processed is loaded into the hopper 343. Inserting the hopper 343 into the cylinder 19 allows for rapid loading. After processing is complete, the slag inside the hopper 343 can be quickly cleaned by pulling it out.

[0074] Please see Figure 6 An open shell 31 is provided on the outer side of the cylinder 19 near the arc groove. The open shell 31 is slidably connected to the slider 345. The end of the slider 345 is connected to the push plate 11 through the guide rod 32. The push plate 11 is connected to the hydraulic telescopic rod 13 provided on the outer side of the cylinder 19. A cover plate 10 is slidably connected to the upper surface of the open shell 31. The cover plate 10 is provided with a lifting lug 30.

[0075] Specifically, the hopper 343 can be pulled out by extending and retracting the hydraulic telescopic rod 13, which facilitates quick loading. The cover plate 10 can be opened by the lifting lug 30, which is more conducive to the filling of materials.

[0076] More specifically, the slider 345 and the hopper 343 are detachably connected, which facilitates the cleaning of material residue inside the hopper 343.

[0077] Please see Figure 4-5 The lower end face of the cylinder 19 is provided with an electrically controlled valve body 16. The electrically controlled valve body 16 includes a cylindrical sealing housing 165. The upper end of the outer side of the cylindrical sealing housing 165 is provided with a discharge guide hood 164, which is connected to the lower end face of the cylinder 19. A sealing shaft 163 is sealed and connected inside the cylindrical sealing housing 165. The end of the sealing shaft 163 is connected to the output end of a stepper motor 162. The stepper motor 162 is mounted on the cylindrical sealing housing. On the body 165, a guide cover 161 is provided at the lower end of the outer side of the cylindrical sealing housing 165, and an air collecting pipe 26 is provided at the end of the outer side of the cylindrical sealing housing 165. The sealing shaft 163 includes a cylindrical roller body 1632, and a rubber sealing layer is provided on the outer side of the cylindrical roller body 1632. A through groove 1631 and an exhaust channel 1633 are provided on the cylindrical roller body 1632. The exhaust channel 1633 communicates with the air collecting pipe 26, and the through groove 1631 communicates with the guide cover 161.

[0078] Specifically, when it is necessary to discharge solid material residue and clean the inner wall of the cylinder 19, the stepper motor 162 drives the sealing shaft 163 to rotate, rotating the through groove 1631 to a vertical position. At this time, the material residue and cleaning liquid in the cylinder 19 can be discharged through the through groove 1631.

[0079] More specifically, when it is necessary to blow the inner wall of the cylinder 19, the stepper motor 162 drives the sealing shaft 163 to rotate, rotating the exhaust channel 1633 to the lower end of the cylinder 19. At this time, the gas in the cylinder 19 carrying dust is discharged through the exhaust channel 1633.

[0080] Furthermore, the cylinder 19 is a pressure vessel, and the outer surface of the cylinder 19 is covered with an insulated shell.

[0081] Specifically, setting up an insulated shell can effectively reduce the rate at which heat is lost from the cylinder 19.

[0082] Furthermore, the outer surface of the cylindrical tube 6 is sealed to the upper end cap 20.

[0083] Specifically, the cylindrical tube 6 is sealed and rotatedly connected to the upper end cover 20.

[0084] For further details, please refer to Figure 1 The outer side of the cylinder 19 is provided with an annular support 18, and the upper end face of the cylindrical tube 6 is provided with a support plate 2. The lower surface of the support plate 2 is connected to the annular support 18 through an electrically controlled telescopic rod 7.

[0085] Specifically, the electrically controlled telescopic rod 7 can drive the cylindrical tube 6 to move up and down.

[0086] For further details, please refer to Figure 1 The outer side of the annular support 18 is provided with a support rod 23, and the upper end of the support rod 23 is provided with a sleeve rod 3. The two ends of the outer side of the sleeve rod 3 are respectively sleeved with an air supply pipe lifting ring 1 and a cleaning pipe lifting ring 4. The air supply pipe lifting ring 1 is connected to the outer side of the steam supply pipe 24, and the cleaning pipe lifting ring 4 is connected to the outer side of the cleaning pipe 5. Solenoid valves are provided on both the steam supply pipe 24 and the cleaning pipe 5.

[0087] Specifically, by setting up the air supply pipe lifting ring 1 and the cleaning pipe lifting ring 4, the steam supply pipe 24 and the cleaning pipe 5 can be effectively prevented from getting tangled.

[0088] For further details, please refer to Figure 3 The cylindrical tube 6 is composed of a fixed tube 61 and a moving tube 62. A clutch 25 is provided at the connection between the fixed tube 61 and the moving tube 62, and the fixed tube 61 and the moving tube 62 are sealed and rotated together.

[0089] Specifically, when the clutch 25 is engaged, the stationary pipe 61 and the moving pipe 62 can rotate relative to each other, thereby allowing the spraying mechanism 33 to rotate, which is beneficial for cleaning the inner wall of the reactor.

[0090] For further details, please refer to Figure 3 The clutch 25 includes a top support 251, an upper gear plate 252, a lower gear plate 253, and a pneumatic telescopic rod 254. The top support 251 is mounted on the fixed tube 61. The upper gear plate 252 is slidably connected to a groove provided on the moving tube 62. The top support 251 is connected to the upper gear plate 252 through the pneumatic telescopic rod 254. The upper gear plate 252 and the lower gear plate 253 are correspondingly engaged.

[0091] Specifically, the pneumatic telescopic rod 254 extends to engage the upper toothed plate 252 and the lower toothed plate 253 together, which can fix the relative position of the fixed tube 61 and the moving tube 62.

[0092] For further details, please refer to Figure 8 The bottom of the outer side of the cylinder 19 is provided with a sealing plate 35, and a rotating shaft 36 is sealed and connected on the sealing plate 35. A cylindrical mesh cage 37 is provided at the end of the rotating shaft 36. The cylindrical mesh cage 37 is set inside the cylinder 19. The lower end face of the discharge pipe 21 is set close to the outer side of the cylindrical mesh cage 37, and the discharge pipe 21 is set close to the inner side of the cylinder 19.

[0093] Specifically, by setting up the cylindrical mesh cage 37, the discharge pipe 21 can be effectively prevented from being blocked during the discharge process. If the discharge is not smooth, the cylindrical mesh cage 37 can be rotated and the lower end face of the discharge pipe 21 can scrape off the solid particles blocking the mesh of the cylindrical mesh cage 37.

[0094] For further details, please refer to Figure 1 and 2The gas collecting pipe 26 is connected to a cyclone separator 12 via a gas guiding hose 28, and a dust filter bag is provided at the outlet of the cyclone separator 12.

[0095] Specifically, after disengaging the clutch 25 and removing the chemical plate 34, the arc-shaped sealing plate 344 returns to its original position to seal the arc-shaped groove. At this time, hot air is sent into the interior of the spraying mechanism 33 through the cylindrical tube 6. While the spraying mechanism 33 rotates, the cylindrical tube 6 pulls the spraying mechanism 33 up and down. The airflow sprayed by the spraying mechanism 33 blows the inner wall of the cylinder 19. The dust generated during the blowing process is carried into the cyclone separator 12, and the cyclone separator 12 collects the dust.

[0096] In use: The weighed solid material is added into the hopper 343. The hydraulic telescopic rod 13 extends to push the hopper 343 into the cylinder 19. At this time, the arc-shaped sealing plate 344 is tightly attached to the outer side of the cylinder 19. Water is added into the cylinder 19 through the water injection pipe 22. After the water is added, the valve on the water injection pipe 22 is closed. High-temperature hot steam is introduced into the sealing cover 333 through the cylindrical pipe 6. The hot steam pushes the sealing plate 335 down, and the synchronous return spring 336 is compressed. At the same time as the sealing plate 335 moves down, the air inlet of the diversion pipe 331 is opened, and the hot steam enters the interior of the diversion pipe 331. Finally, it is spirally sprayed out through the nozzle 334. The liquid material rotates under the push of the hot steam, which accelerates the chemical process.

[0097] After the material is processed, open the valve on the discharge pipe 21. At this time, the liquid material in the cylinder 19 is discharged through the discharge pipe 21 under high pressure.

[0098] After the material is processed, the hopper 343 is pulled out to quickly clean the material residue inside. When it is necessary to rinse the inner wall of the cylinder 19, the valve on the cleaning pipe 5 is opened and the other valves are closed at the same time. The stepper motor 162 drives the sealing shaft 163 to rotate, and the through groove 1631 is rotated to a vertical position. At this time, the material residue and cleaning liquid in the cylinder 19 can be discharged through the through groove 1631.

[0099] Waste liquid and slag generated during the cleaning process can enter the interior of the pull-out box 17 through the guide cover 161. The slag can be collected through the pull-out box 17. When the air nozzle 29 is connected to the cleaning water and the chemical plate 34 is pulled out, the high-pressure water sprayed through the air nozzle 29 can complete the cleaning of the chemical plate 34. The wastewater generated during the cleaning process enters the pull-out box 17 through the collection pipe 27.

[0100] When it is necessary to blow the inner wall of the cylinder 19, the stepper motor 162 drives the sealing shaft 163 to rotate, rotating the exhaust channel 1633 to the lower end of the cylinder 19. At this time, the gas in the cylinder 19 carrying dust is discharged through the exhaust channel 1633.

[0101] Then, after disengaging the clutch 25 and removing the chemical plate 34, the arc-shaped sealing plate 344 returns to its original position to seal the arc-shaped groove. At this time, hot air is sent into the interior of the spraying mechanism 33 through the cylindrical tube 6. While the spraying mechanism 33 rotates, the cylindrical tube 6 pulls the spraying mechanism 33 up and down. The airflow sprayed by the spraying mechanism 33 blows the inner wall of the cylinder 19. The dust generated during the blowing process is carried into the cyclone separator 12, and the cyclone separator 12 collects the dust.

[0102] It is worth noting that the input ends of the electrically controlled telescopic rod 7, the hydraulic telescopic rod 13, and the electrically controlled valve body 16 disclosed in the above embodiments are all electrically connected to the output end of an external controller via an external power supply.

[0103] Although embodiments of this application have been shown and described, it will be understood by those skilled in the art that various changes, modifications, substitutions and variations can be made to these embodiments without departing from the principles and spirit of this application, the scope of which is defined by the appended claims and their equivalents.

Claims

1. A chemical reaction vessel for producing inorganic silicate liquid, comprising a cylindrical body (19), an upper end cover (20) provided on the upper end face of the cylindrical body (19), and a pressure relief pipe (8), a safety valve (9), a discharge pipe (21) and a water injection pipe (22) provided on the upper end cover (20), characterized in that: A cylindrical tube (6) is slidably connected to the middle of the upper surface of the upper end cover (20). The upper end face of the cylindrical tube (6) is connected to the cylinder (19) through a lifting mechanism. A steam supply pipe (24) and a cleaning pipe (5) are connected to the upper end of the outer side face of the cylindrical tube (6). The lower end face of the cylindrical tube (6) is connected to a spraying mechanism (33). The spraying mechanism (33) includes a sealing cover (333). The upper side of the outer side of the sealing cover (333) is provided with a feed inlet (332). The feed inlet (332) is connected to the discharge port of the cylindrical tube (6). The outer side of the sealing cover (333) is provided with a diversion pipe (331). The outer end and the lower end of the outer side of the diversion pipe (331) are both provided with nozzles (334). The nozzles (334) are inclined downwards. The nozzles (334) at the lower end of the outer side of the diversion pipe (331) have the same nozzle orientation. The interior of the sealing cover (333) is provided with a sealing plate (335). The lower surface of the sealing plate (335) is provided with a return spring (336). The cylindrical tube (6) introduces high-temperature hot steam into the interior of the sealing cover (333). The hot steam pushes the sealing plate (335) down, and the synchronous reset spring (336) is compressed. At the same time as the sealing plate (335) moves down, the air inlet of the diversion pipe (331) is connected, and the hot steam enters the interior of the diversion pipe (331). Finally, it is spirally sprayed out through the nozzle (334). The liquid material rotates under the push of the hot steam, which accelerates the process of material processing. Inside the cylinder (19), above the spraying mechanism (33), there is a material-dissolving plate (34). The material-dissolving plate (34) includes a hopper (343). The bottom of the inner side of the hopper (343) is provided with a through hole (342). The inside of the hopper (343) is provided with a strip groove (341). The outer side of the hopper (343) is provided with a slider (345). The outer side of the slider (345) is provided with an arc-shaped sealing plate (344). The outer side of the cylinder (19) is provided with an arc-shaped groove through which the material-dissolving plate (344) passes. The arc-shaped groove and the arc-shaped sealing plate (344) are sealed and correspondingly arranged. The arc-shaped sealing plate (344) includes a semi-circular sealing plate (3441). The inner side of the semi-circular sealing plate (3441) is provided with a sealing strip (3442). The outer side of the cylinder (19) near the arc groove is provided with an open shell (31). The open shell (31) is slidably connected to the slider (345). The end of the slider (345) is connected to a push plate (11) through a guide rod (32). The push plate (11) is connected to a hydraulic telescopic rod (13) provided on the outer side of the cylinder (19). The upper surface of the open shell (31) is slidably connected to a cover plate (10). The cover plate (10) is provided with a lifting lug (30). The lower end face of the cylinder (19) is provided with an electrically controlled valve body (16). The electrically controlled valve body (16) includes a cylindrical sealing housing (165). The upper end of the outer side of the cylindrical sealing housing (165) is provided with a discharge guide hood (164). The discharge guide hood (164) is connected to the lower end face of the cylinder (19). The cylindrical sealing housing (165) is internally sealed with a sealing shaft (163). The end of the sealing shaft (163) is connected to the output end of a stepper motor (162). The stepper motor (162) is mounted on the cylindrical sealing housing (19). On 65), a guide cover (161) is provided at the lower end of the outer side of the cylindrical sealing housing (165), and an air collecting pipe (26) is provided at the end of the outer side of the cylindrical sealing housing (165). The sealing shaft (163) includes a cylindrical roller body (1632), and a rubber sealing layer is provided on the outer side of the cylindrical roller body (1632). A through groove (1631) and an exhaust channel (1633) are provided on the cylindrical roller body (1632). The exhaust channel (1633) is connected to the air collecting pipe (26), and the through groove (1631) is connected to the guide cover (161).

2. The reaction vessel for producing inorganic silicate liquid materials according to claim 1, characterized in that: The cylinder (19) is a pressure vessel, and the outer surface of the cylinder (19) is covered with an insulated shell.

3. The reaction vessel for producing inorganic silicate liquid materials according to claim 1, characterized in that: The outer side of the cylindrical tube (6) is sealed to the upper end cap (20).

4. The reaction vessel for producing inorganic silicate liquid materials according to claim 1, characterized in that: The outer side of the cylinder (19) is provided with an annular support (18), and the upper end of the cylindrical tube (6) is provided with a support plate (2). The lower surface of the support plate (2) is connected to the annular support (18) through an electrically controlled telescopic rod (7).

5. The chemical reaction vessel for producing inorganic silicate liquid materials according to claim 4, characterized in that: The outer side of the ring support (18) is provided with a support rod (23), and the upper end of the support rod (23) is provided with a sleeve rod (3). The two ends of the outer side of the sleeve rod (3) are respectively fitted with an air supply pipe ring (1) and a cleaning pipe ring (4). The air supply pipe ring (1) is connected to the outer side of the steam supply pipe (24), and the cleaning pipe ring (4) is connected to the outer side of the cleaning pipe (5). Both the steam supply pipe (24) and the cleaning pipe (5) are provided with solenoid valves.

6. The reaction vessel for producing inorganic silicate liquid materials according to claim 1, characterized in that: The cylindrical tube (6) consists of a fixed tube (61) and a moving tube (62). A clutch (25) is provided at the connection between the fixed tube (61) and the moving tube (62), and the fixed tube (61) and the moving tube (62) are sealed and rotated together.

7. The reaction vessel for producing inorganic silicate liquid materials according to claim 6, characterized in that: The clutch (25) includes a top support (251), an upper gear plate (252), a lower gear plate (253), and a pneumatic telescopic rod (254). The top support (251) is installed on the fixed pipe (61). The upper gear plate (252) is slidably connected to the slide groove provided on the moving pipe (62). The top support (251) is connected to the upper gear plate (252) through the pneumatic telescopic rod (254). The upper gear plate (252) and the lower gear plate (253) are meshed and correspondingly arranged.

8. The chemical reaction vessel for producing inorganic silicate liquid materials according to claim 1, characterized in that: The bottom of the outer side of the cylinder (19) is provided with a sealing plate (35), and a rotating shaft (36) is sealed and connected on the sealing plate (35). A cylindrical mesh cage (37) is provided at the end of the rotating shaft (36). The cylindrical mesh cage (37) is set inside the cylinder (19). The lower end face of the discharge pipe (21) is set close to the outer side of the cylindrical mesh cage (37), and the discharge pipe (21) is set close to the inner side of the cylinder (19).

9. A chemical reaction vessel for producing inorganic silicate liquid materials according to any one of claims 1-8, characterized in that: The waste collection box (14) is connected to the bottom of the material guide cover (161). The waste collection box (14) is equipped with a pull-out box (17) inside and an observation window (15) on the outer side of the waste collection box (14). The upper surface of the cover plate (10) is equipped with an air nozzle (29), and the lower surface of the open shell (31) is equipped with a collection pipe (27). The collection pipe (27) is connected to the waste collection box (14), and a control valve is provided on the collection pipe (27).

10. A chemical reaction vessel for producing inorganic silicate liquid materials according to any one of claims 1-8, characterized in that: The gas collecting pipe (26) is connected to a cyclone separator (12) via a gas guiding hose (28), and a dust filter bag is provided at the outlet of the cyclone separator (12).

Citation Information

Patent Citations

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