Chinese angelica plant moisturizing and soothing stock solution

Abstract

The invention discloses an angelica sinensis plant moisturizing and soothing stock solution which comprises the following raw materials in percentage by weight: 92% of water, 4% of an angelica sinensis root extract, 3.6% of an acanthopanax gracilistylus root bark extract and 0.4% of a citrus peel extract, and the water is plasma water. According to the Chinese angelica plant moisturizing and soothing stock solution, water extract, alcohol extract, polysaccharide and ferulic acid which are rich in Chinese angelica in the Chinese angelica root extract have a very strong function of inhibiting tyrosinase activity, so that the formation of melanin can be inhibited, namely, the purpose of fading spots is achieved, and meanwhile, the polysaccharide also has a moisturizing function, so that the effect of soothing the skin is achieved. The main component gallnut tannic acid in the acanthopanax gracilistylus root and bark extract has an obvious bacteriostatic effect and can inhibit growth and reproduction of various common pathogenic bacteria on skin, and the citrus peel extract is rich in flavonoid and carboside compounds, has strong antioxidant activity, can neutralize free radicals, and has a good anti-aging effect. Inflammation and injury caused by oxidative stress are relieved, so that the effects of relieving and protecting the skin are further achieved.

Description

Technical Field

[0001] The invention relates to the technical field of cosmetics, in particular to angelica plant moisturizing and soothing stock solution. Background Art

[0002] The term "stock liquid" originated from industrial manufacturing and is used to describe the concentrated liquid matrix of a certain industrial raw material. After being introduced into the cosmetics industry, stock solution specifically refers to a type of skin care product. Stock solution in the cosmetics industry refers to a beauty product that adds a relatively single high-concentration skin care ingredient, which can provide more direct, safer and more effective care for the skin for various skin needs, allowing the skin to restore to its best condition in a short time. Stock solutions are divided into different types according to their functions. After searching, it is found that the soothing stock solution in the prior art is typically such as the publication number CN104983651A, a sunflower SPA softening soothing stock solution and a preparation method thereof, which is prepared with 2,3-butylene glycol, polyethylene glycol-8, propylene glycol, and betaine as moisturizers, sunflower extract, β-glucan, allantoin, and sodium hyaluronate as skin conditioning agents, PVM / MA decadiene cross-linked polymer as a lubricant, polyacrylic acid as a thickener, triethanolamine as a PH regulator, methylparaben and phenoxyethanol as preservatives, disodium EDTA as a chelating agent, essence as a fragrance, menthol lactate as a cooling agent, and water as a solvent. Its main feature is to cut the leaves and stems of the sunflower, and when its own immune system produces restorative secretions in response to stress, the secretions are extracted for cell culture to obtain secondary metabolites, which can deliver a variety of vitamins and unsaturated fatty acids to the skin, gently nourish it, relieve external damage to the skin, enhance skin tolerance, and soothe sensitive skin.

[0003] For example, the publication number CN109303724A is a new type of soothing and repairing stock solution composition containing mugwort, which contains, by weight percentage: anti-allergic soothing agent 0.1-5.0%, skin repair agent 0.1-5.0%, preservative 0.1%-1.0%, moisturizer 1-15.0%, thickener 4%-10%. Water: balance. The skin repair composition of the present invention can be made into cream and water solution, which can be directly applied to the affected area and is non-toxic and harmless to human skin. The skin soothing and repairing composite component has strong anti-allergic and repairing, anti-inflammatory and astringent effects; other auxiliary added components are selected from moisturizers, preservatives, etc. that can make the skin soft, smooth, moisturized and mild and non-irritating to the skin. It is easy to use, anti-inflammatory and itchy, and repairs damaged skin. It is suitable for sensitive skin and skin allergies, itching, desquamation, redness, swelling, and other phenomena caused by improper use of cosmetics.

[0004] In summary, the existing soothing liquid ingredients contain more or less chemical substances and additives, which may cause certain harm to the skin. At the same time, certain chemical elements may also cause allergies, thereby further increasing the burden on the skin. In view of the above problems, the existing equipment needs to be improved. Summary of the invention

[0005] The purpose of the present invention is to provide an angelica plant moisturizing and soothing stock solution to solve the problem that the existing soothing stock solution ingredients mentioned in the above background technology contain more or less chemical substances and additives, which cause certain harm to the skin, and certain chemical elements may also cause allergies, thereby further increasing the burden on the skin.

[0006] To achieve the above-mentioned purpose, the present invention provides the following technical scheme: Angelica plant moisturizing and soothing stock solution, comprising the following raw materials in weight percentage: 92% water, 4% Angelica root extract, 3.6% Acanthopanax scapularis root bark extract, and 0.4% citrus peel extract, wherein the water is ionized water.

[0007] Preferably, the extraction process of the angelica root extract includes: weighing, freeze-drying, crushing and water extraction, and the weighing is carried out by using a balance for quantitative weighing, and the crushing needs to be followed by screening.

[0008] Preferably, the freeze-drying operation of the angelica root extract uses fresh angelica roots, and the freeze-drying operation includes two stages: pre-freezing and vacuum drying. The pre-freezing temperature range is controlled between -20°C and -5°C, and the pre-freezing duration is 3-6 hours.

[0009] Preferably, the freeze-drying operation of the angelica root extract is carried out under a vacuum degree of 5-100 Pa, and the vacuum drying operation is to gradually increase the temperature from -75--30°C to 40-60°C for 20-35 hours.

[0010] Preferably, in the water extraction operation of the angelica root extract, the extraction solvent is 10-30 vol% ethanol solution, the extraction temperature is 45-55°C; the extraction time is 1 hour, and the number of water extractions is 2-3 times. After the water extraction, the extract is concentrated and spray-dried to obtain the extract.

[0011] Preferably, the extraction process of the Acanthopanax gracilis root bark extract includes: washing and decocting, combining and filtering, heating and concentrating, standing and settling, extracting the supernatant and washing and drying, and the washing and decocting operation uses 6-16 times of water for decocting, and the number of extractions is 2-4 times.

[0012] Preferably, the combined filtration operation of the Acanthopanax Root Bark Extract is to combine the filtrates and concentrate the filtrates, the washing volume is 1 to 4 times the column volume; the washing solution is an ethanol solution with a concentration of 60%, and the amount of the ethanol solution is 2 to 3 times the column volume.

[0013] Preferably, the water washing of the Acanthopanax Root Bark Extract is a gradient elution, and the mobile phase B changes from 2% to 6% from 1 minute to 15 minutes; the mobile phase B changes from 6% to 9% from 15 minutes to 25 minutes; the mobile phase B changes from 9% to 13% from 25 minutes to 35 minutes, the mobile phase B changes from 17% to 25% from 45 minutes to 60 minutes, and the mobile phase B is 25% from 60 minutes to 75 minutes.

[0014] Preferably, the extraction process of the citrus peel extract includes: weighing and washing, pulp removal, ripening and crushing, ultrasonic extraction and concentration filtration, and the weighing and washing is to quantitatively weigh a corresponding amount of tangerines, pomeloes, oranges, bitter oranges, grapefruits and lemons and wash their surfaces, the ultrasonic extraction operation is repeated 2-3 times, and after the extraction, a filter is used to filter and remove impurities.

[0015] Preferably, the removal of pulp in the citrus peel extract refers to cutting the various raw materials after washing into pieces and removing the pulp inside them, and the ripening and crushing refers to completely drying the separated peels at 35-40°C, and then evenly cutting them into uniform sizes of about 0.2-0.3 cm, and putting them into a container, moistening them with water, and steaming them. The steaming time is 12-13 hours and the cooking temperature is 110°C. After steaming, they are further heated at 40°C until completely dried, and then powdered using a crusher.

[0016] Compared with the prior art, the invention has the following beneficial effects: the Angelica sinensis plant moisturizing and soothing stock solution,

[0017] The present invention can effectively solve the problem that the existing soothing stock solution ingredients contain more or less chemical substances and additives, which cause certain harm to the skin, and some chemical elements may also cause allergies, thereby further increasing the burden on the skin. The present invention can effectively solve the problem that the existing soothing stock solution ingredients contain more or less chemical substances and additives, which cause certain harm to the skin, and some chemical elements may also cause allergies, thereby further increasing the burden on the skin. The pure plant formula stock solution is obtained by mixing and extracting a variety of raw materials and water, angelica root extract, Acanthopanax scapularis root bark extract and citrus peel extract, thereby avoiding skin allergies and other adverse symptoms caused by chemical additives. In addition, the angelica root extract is rich in water extract, alcohol extract, polysaccharide and ferulic acid, which have a strong function of inhibiting tyrosinase activity, thereby inhibiting melanin. In addition, the active ingredients it contains have antioxidant and sedative effects, which can reduce the damage of the skin to environmental pollution, ultraviolet radiation and other factors, relieve skin sensitivity and redness, and polysaccharides also have moisturizing function. The main ingredient of Acanthopanax gracilis root bark extract, gallic acid, has obvious antibacterial effect, which can inhibit the growth and reproduction of many common pathogens on the skin. Citrus peel extract is rich in flavonoids and glycoside compounds, which have strong antioxidant activity, can neutralize free radicals, reduce inflammation and damage caused by oxidative stress, and further play a role in soothing and protecting the skin. BRIEF DESCRIPTION OF THE DRAWINGS

[0018] Figure 1 It is a schematic diagram of the composition of the present invention;

[0019] Figure 2 The figure is a schematic diagram of the preparation process of the angelica extract of the present invention;

[0020] Figure 3 The figure is a schematic diagram of the preparation process of the citrus peel extract of the present invention. DETAILED DESCRIPTION

[0021] The following will be combined with the drawings in the embodiments of the present invention to clearly and completely describe the technical solutions in the embodiments of the present invention. Obviously, the described embodiments are only part of the embodiments of the present invention, not all of the embodiments. Based on the embodiments of the present invention, all other embodiments obtained by ordinary technicians in this field without creative work are within the scope of protection of the present invention.

[0022] See also Figure 1-3 The present invention provides a technical solution: Angelica plant moisturizing and soothing stock solution, comprising the following raw materials in weight percentage: 92% water, 4% Angelica root extract, 3.6% Acanthopanax scapularis root bark extract, 0.4% citrus peel extract, and the water is ion water.

[0023] The extraction process of the angelica root extract includes: weighing, freeze-drying, crushing and water extraction, and the weighing is carried out by using a balance for quantitative weighing, and the angelica root extract needs to be sieved after crushing.

[0024] The freeze-drying operation of the angelica root extract uses fresh angelica roots, and the freeze-drying operation includes two stages: pre-freezing and vacuum drying. The pre-freezing temperature range is controlled between -20°C and -5°C, and the pre-freezing duration is 3-6 hours.

[0025] The freeze-drying operation of the angelica root extract is carried out under a vacuum degree of 5-100 Pa. The vacuum drying operation is to gradually increase the temperature from -75--30°C to 40-60°C for 20-35 hours.

[0026] In the water extraction operation of angelica root extract, the extraction solvent is 10-30 vol% ethanol solution, and the extraction temperature is 45-55°C; the extraction time is 1 hour, and the number of water extractions is 2-3 times. After water extraction, the extract is concentrated and spray-dried to obtain the extract. The water extract, alcohol extract, polysaccharide and ferulic acid in angelica can inhibit melanin synthesis for whitening or treatment of chloasma. In addition, its rich active ingredients also have antioxidant and sedative effects. Angelica contains relatively rich amino acids and trace elements, which can moisturize and lubricate the skin. At the same time, ferulic acid has a good absorption effect on a certain range of ultraviolet rays, which can effectively protect the skin from damage by ultraviolet rays and avoid skin sensitivity and redness.

[0027] The extraction process of the Acanthopanax gracilis root bark extract includes: washing and decocting, combining and filtering, heating and concentrating, standing and settling, extracting the supernatant and washing and drying. The washing and decocting operation uses 6-16 times of water for decoction, and the number of extractions is 2-4 times.

[0028] The combined filtration operation of the Acanthopanax Root Bark Extract is to combine the filtrates and concentrate the filtrates. The water washing volume is 1 to 4 times the column volume. The water washing solution is an ethanol solution with a concentration of 60%, and the amount of the ethanol solution is 2 to 3 times the column volume.

[0029] The water washing of the Acanthopanax Root Bark Extract is a gradient elution, and the mobile phase B changes from 2% to 6% from 1 minute to 15 minutes; from 15 minutes to 25 minutes, the mobile phase B changes from 6% to 9%; from 25 minutes to 35 minutes, the mobile phase B changes from 9% to 13%, from 45 minutes to 60 minutes, the mobile phase B changes from 17% to 25%, and from 60 minutes to 75 minutes, the mobile phase B is 25%. The Acanthopanax Root Bark Extract is rich in gallic tannic acid, which has obvious antibacterial effects and can inhibit the growth and reproduction of many common pathogens on the skin, avoiding skin inflammation.

[0030] The extraction process of citrus peel extract includes: weighing and washing, pulp removal, ripening and crushing, ultrasonic extraction and concentrated filtration, and the weighing and washing is to quantitatively weigh the corresponding amount of tangerines, pomeloes, oranges, bitter oranges, grapefruits and lemons for surface washing, and the ultrasonic extraction operation is repeated 2-3 times, and after the extraction, the filter is used to filter and remove impurities.

[0031] The pulp removal in citrus peel extract refers to cutting the various raw materials into pieces after washing and removing the pulp inside them. The ripening and crushing refers to completely drying the separated peels at 35-40°C, and then evenly cutting them into uniform sizes of about 0.2-0.3 cm, and putting them into a container, moistening them with water and steaming them. The steaming time is 12-13 hours, and the cooking temperature is 110°C. After steaming, it is further heated at 40°C until completely dry, and then powdered by a crusher. Citrus peel extract is rich in vitamin C, flavonoids and other ingredients. Flavonoids have antioxidant properties and can help scavenge free radicals and protect cells from oxidative damage; flavonoids can regulate inflammatory responses and reduce inflammatory manifestations such as tissue redness and swelling; flavonoids provide protection by absorbing and scattering ultraviolet rays, reducing skin damage caused by sun exposure; flavonoids can stimulate fibroblasts to produce collagen, which helps maintain skin elasticity and firmness; flavonoids can interfere with the biosynthesis process of melanin, thereby reducing pigmentation.

[0032] Embodiment 1

[0033] First, the Radix Angelicae Sinensis extract, the Radix Acanthopanacis Columnaris root bark extract and the citrus peel extract are prepared respectively, and the fresh Radix Angelicae Sinensis is weighed, freeze-dried, crushed and water-extracted in sequence to obtain the Radix Angelicae Sinensis extract, and the Radix Acanthopanacis Columnaris root bark is washed, decocted, combined and filtered, heated and concentrated, allowed to stand for precipitation, the supernatant is extracted and washed and dried to obtain the Radix Acanthopanacis Columnaris root bark extract, and a variety of fresh citrus fruits are prepared, including but not limited to pomelo, pomelo, orange, bitter orange, grapefruit and lemon, and the citrus peel extract is obtained by weighing, washing, pulp removal, ripening and crushing, ultrasonic extraction and concentration and filtration in sequence, and finally the required amount of plasma is measured with a measuring cup for use, and then the Radix Angelicae Sinensis extract, the Radix Acanthopanacis Columnaris root bark extract and the citrus peel extract are mixed and stirred with plasma water according to the formula, and filtered and extracted to obtain a moisturizing and soothing stock solution.

[0034] The specific preparation process of the extract of Acanthopanax acanthopanax root bark is as follows: add 15 times the amount of water and boil for 3 times for 30 minutes, combine the water decoctions, heat and evaporate to a small volume and concentrate to 5000ml, filter out the precipitate, and pass the supernatant through a D101 macroporous resin column with a macroporous resin dosage of 4kg, an inner diameter of 15cm, and a column length of 70cm. First, use 2 times the column volume (BV) of distilled water to wash away impurities, then elute with 2BV of 60% ethanol solution, collect the eluted fractions, recover the ethanol, and spray dry the concentrate at 60°C to obtain a yellow-brown powder.

[0035] Test subjects: 200 healthy women aged 25-50, randomly divided into 20 groups, 10 people in each group;

[0036] Test area: face (blank sample was used on the left face, and moisturizing and soothing stock solution of the control example was used on the right face);

[0037] Usage: Apply once in the morning and evening every day for 4 weeks;

[0038] Testing instruments: CK skin tester (Germany), VISIA full face analyzer (Germany);

[0039] Effect: The lower the transepidermal water loss rate, the better the moisturizing effect, spots and acne marks fade; redness and swelling subside and are soothed.

[0040] Although the present invention has been described in detail with reference to the aforementioned embodiments, it is still possible for those skilled in the art to modify the technical solutions described in the aforementioned embodiments, or to make equivalent substitutions for some of the technical features therein. Any modifications, equivalent substitutions, improvements, etc. made within the spirit and principles of the present invention should be included in the protection scope of the present invention.

Claims

1. Angelica plant moisturizing and soothing stock solution, characterized in that: The invention comprises the following raw materials in percentage by weight: 92% of water, 4% of angelica root extract, 3.6% of Acanthopanax scoparia root bark extract and 0.4% of citrus peel extract, wherein the water is ion water.

2. The Angelica plant moisturizing and soothing stock solution according to claim 1, characterized in that: The extraction process of the angelica root extract includes: weighing, freeze-drying, crushing and water extraction, and the weighing is carried out by using a balance for quantitative weighing, and the angelica root extract needs to be sieved after crushing.

3. The Angelica plant moisturizing and soothing stock solution according to claim 1, characterized in that: The freeze-drying process of the angelica root extract uses fresh angelica roots, and the freeze-drying process includes two stages: pre-freezing and vacuum drying. The pre-freezing temperature range is controlled between -20°C and -5°C, and the pre-freezing duration is 3-6 hours.

4. The Angelica plant moisturizing and soothing stock solution according to claim 1, characterized in that: The freeze-drying operation of the angelica root extract is carried out under the condition of a vacuum degree of 5-100 Pa. The vacuum drying operation is to gradually increase the temperature from -75--30°C to 40-60°C for 20-35 hours.

5. The Angelica plant moisturizing and soothing stock solution according to claim 1, characterized in that: In the water extraction operation of the angelica root extract, the extraction solvent is 10-30 vol% ethanol solution, the extraction temperature is 45-55° C., the extraction time is 1 hour, and the water extraction times are 2-3 times. After the water extraction, the extract is concentrated and spray-dried to obtain the extract.

6. The Angelica Root Moisturizing and Soothing Stock Solution according to claim 1, characterized in that: The extraction process of the Acanthopanax gracilis root bark extract comprises: washing and decocting, combining and filtering, heating and concentrating, standing and settling, extracting the supernatant, washing and drying, and the washing and decocting operation uses 6-16 times of water for decocting, and the number of extractions is 2-4 times.

7. The Angelica sinensis plant moisturizing and soothing stock solution according to claim 1, characterized in that: The combined filtration operation of the Acanthopanax Root Bark Extract is to combine the filtrates and concentrate the filtrates. The washing volume is 1 to 4 times the column volume. The washing solution is an ethanol solution with a concentration of 60%, and the amount of the ethanol solution is 2 to 3 times the column volume.

8. The Angelica sinensis plant moisturizing and soothing stock solution according to claim 1, characterized in that: The water washing of the fine column Acanthopanax Root Bark Extract is a gradient elution, wherein the mobile phase B changes from 2% to 6% from 1 minute to 15 minutes; the mobile phase B changes from 6% to 9% from 15 minutes to 25 minutes; the mobile phase B changes from 9% to 13% from 25 minutes to 35 minutes, the mobile phase B changes from 17% to 25% from 45 minutes to 60 minutes, and the mobile phase B is 25% from 60 minutes to 75 minutes.

9. The Angelica plant moisturizing and soothing stock solution according to claim 1, characterized in that: The extraction process of the citrus peel extract includes: weighing and washing, pulp removal, ripening and crushing, ultrasonic extraction and concentration filtration, and the weighing and washing is to quantitatively weigh a corresponding amount of tangerines, pomeloes, oranges, bitter oranges, grapefruits and lemons to wash their surfaces, the ultrasonic extraction operation is repeated 2-3 times, and after the extraction, a filter is used to filter and remove impurities.

10. The Angelica plant moisturizing and soothing stock solution according to claim 1, characterized in that: The pulp removal in the citrus peel extract refers to cutting the various raw materials into pieces after washing and removing the pulp inside them, and the ripening and crushing refers to completely drying the separated peels at 35-40°C, and then evenly cutting them into uniform sizes of about 0.2-0.3 cm, and putting them into a container, moistening them with water, and steaming them. The steaming time is 12-13 hours, and the cooking temperature is 110°C. After steaming, they are further heated at 40°C until they are completely dry, and then they are powdered using a crusher.

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