Dewatering and drying device and method for producing bromochlorohydantoin

The design of alternating lifting of the multifunctional inner disc and the guide tube and the replacement of the position of the sponge liner, combined with hot air drying, solves the problems of particle breakage and sponge contamination in the production of bromochlorohydantoin, and achieves efficient and stable dehydration and automatic discharge.

CN120740283AActive Publication Date: 2025-10-03LONGKOU KEDA CHEM
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Patent Information

Application Number
CN202511220902.0
Authority / Receiving Office
CN · China
Patent Type
Applications(China)
Current Assignee / Owner
Filing Date
2025-08-29
Publication Date
2025-10-03
Estimated Expiration
2045-08-29

AI Technical Summary

Technical Problem

In the existing bromochlorohydantoin production process, centrifugal dehydration and drying leads to particle breakage and material loss, and sponge filtration is easily contaminated, affecting product quality and output.

Method used

The design of alternating lifting of the multifunctional inner disc and the guide tube is adopted, combined with the position replacement of the sponge liner and hot air drying, to achieve the alternating use of the sponge liner and efficient dehydration and drying, and the cooperation of the transmission block and the top spring is used to realize automatic discharge.

Benefits of technology

It improves the dehydration and drying efficiency, prevents particle breakage, reduces secondary pollution, ensures high-quality particle discharge, and simplifies the cleaning and discharge process.

✦ Generated by Eureka AI based on patent content.

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Abstract

The invention discloses a dewatering and drying device and method for bromochlorohydantoin production, and relates to the technical field of centrifugal dewatering. The device comprises a dehydration tank, a centrifugal cylinder is rotatably installed in the dehydration tank, two sets of pressing rings are arranged in the centrifugal cylinder, a multifunctional inner disc is clamped between the two sets of pressing rings, the multifunctional inner disc is composed of two sets of conical discs and a middle pipe, and the two sets of conical discs are symmetrically distributed relative to the middle pipe; and a sponge liner is arranged between the multifunctional inner disc and the centrifugal cylinder. The multifunctional inner disc and the guide pipes are arranged, the upper guide pipe and the lower guide pipe alternately ascend and descend, sponge inner container switching can be achieved, when the upper guide pipe descends, the sponge inner containers are twisted together in a pocket tying mode, the sponge inner containers are preliminarily extruded and dried through the cooperation of the pressing ring, hot air is injected through the lower guide pipe, and the drying efficiency is improved. And secondary drying is conducted on the sponge inner container, so that alternate use and alternate drying of the sponge inner container can be achieved, and the dewatering and drying efficiency is improved.
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Description

Technical Field

[0001] The invention relates to the technical field of centrifugal dehydration, and in particular to a dehydration drying device and method for producing bromochlorohydantoin. Background Art

[0002] Bromochlorohydantoin is an important organic chemical raw material, widely used in pesticides, medicine, and the chemical industry, especially in the pharmaceutical industry. The production of bromochlorohydantoin often involves multiple steps, including solvent extraction, reaction synthesis, and subsequent dehydration and drying.

[0003] Currently, common methods for dehydrating bromochlorohydantoin include heating, vacuum drying, and centrifugal drying. During the centrifugal drying process, the high-speed centrifugal force can subject bromochlorohydantoin particles to mechanical stress, leading to particle breakage or material loss. This not only affects final product quality but can also result in yield losses, especially when maintaining particle integrity is crucial. A utility model patent (publication number: CN211552242U) discloses a centrifugal dehydration device comprising a barrel, wherein a servo motor is mounted on the lower end surface of the barrel, and a storage rack is mounted on the output shaft of the servo motor. The rack comprises an I-shaped plate fixedly connected to the servo motor output shaft in the middle portion of the lower surface. A first telescopic rod is mounted on the upper surface of the I-shaped plate, and a fastening knob is mounted on the upper end of the side of the fixed end of the first telescopic rod. A circular plate is mounted on the top of the first telescopic rod, and the circular plate has evenly distributed through-holes on its upper surface. The I-shaped plate has slots corresponding to the through-holes on its upper surface. An annular sponge pad is positioned within the barrel, its outer surface contacting the inner side surface of the barrel. Although this patent proposes the concept of using an annular sponge pad as a centrifugal filtration buffer, when applied to the filtration of bromochlorohydantoin particles of the present invention, due to the small size of the bromochlorohydantoin particles, the particles will be pressed and embedded in the sponge during the centrifugal filtration process. The water absorbed by the sponge can easily cause secondary contamination of the bromochlorohydantoin particles. The water in the sponge needs to be completely drained, which affects the filtration efficiency. Moreover, after the filtration is completed, the bromochlorohydantoin particles are easily adhered to the sponge, making discharge difficult. Therefore, it is urgently needed to provide a centrifugal dehydration and drying device specifically for small particles to meet the production requirements of bromochlorohydantoin. Summary of the Invention

[0004] The purpose of the present invention is to solve the above problems and provide a dehydration and drying device and method for the production of bromochlorohydantoin.

[0005] In order to achieve the above-mentioned purpose, the present invention specifically adopts the following technical solutions: A dehydration and drying device for producing bromochlorohydantoin, comprising a dehydration tank, wherein a centrifugal drum is rotatably mounted inside the dehydration tank, wherein two sets of pressure rings are provided inside the centrifugal drum, a multifunctional inner disk is sandwiched between the two sets of pressure rings, and the multifunctional inner disk is composed of two sets of conical disks and an intermediate tube, wherein the two sets of conical disks are symmetrically distributed about the intermediate tube, the radius of the upper conical disk is smaller than the radius of the lower conical disk, a sponge liner is provided between the multifunctional inner disk and the centrifugal drum, an outer shaping piece is provided on the outer surface of the sponge liner, and the sponge liner between the lower conical disk and the centrifugal drum is tightly squeezed, multiple sets of triangular transmission openings are provided in an annular shape on the outer side of the lower conical disk, multiple sets of transmission boxes are provided in an annular shape on the outer side of the centrifugal drum, a transmission block is slidably connected to the interior of the transmission box, a top spring is provided between the transmission block and the transmission box, the transmission block is plugged into the triangular transmission opening, the plugging end of the transmission block is arranged in a right-angled triangle, and a ball bearing is rotatably mounted on the outer side of the straight side; Both ends of the intermediate tube are provided with guide tubes that can be raised and lowered. A feeding tee is provided in the middle of the intermediate tube, and the feeding tee can be inserted into the guide tube. The two ends of the external shaping part respectively pass through the corresponding multifunctional inner disk and the pressure ring, and are respectively fixedly installed on the two groups of guide tubes.

[0006] Furthermore, a spiral guide groove is provided inside the intermediate tube, and an external spiral protrusion is provided on the outside of the conduit. The external spiral protrusion is threadedly connected in the spiral guide groove, and the thickness of the external spiral protrusion is smaller than the depth of the spiral guide groove.

[0007] Furthermore, two groups of lifting cylinders are fixedly installed on the outside of the dehydration tank, and the telescopic ends of the lifting cylinders are fixedly installed with lifting rods, and lifting tubes are rotatably installed inside the lifting rods. The lifting tubes are fixedly connected to the corresponding conduits, and the ends of the lifting tubes away from the conduits are fixedly installed with hot air pipes. A feeding branch pipe is provided on the outside of the upper hot air pipe, and a clamping cylinder is fixedly installed on the top of the upper lifting rod, and the telescopic end of the clamping cylinder can clamp the lifting tube and fix it in the lifting rod.

[0008] Furthermore, the inner wall of the dehydration tank is provided with two groups of inner partitions, and the centrifugal cylinder is rotatably installed between the two groups of inner partitions. The top and bottom of the centrifugal cylinder are provided with smoke exhaust pipes, and the outside of the dehydration tank is provided with a drain pipe, which is located directly above the lower inner partition. A discharge valve is provided at the bottom of the dehydration tank.

[0009] Furthermore, a driving motor is fixedly installed below the dehydration tank, a driving wheel is fixedly installed at the output end of the driving motor, the driving wheel is located in the dehydration tank, a driven wheel is fixedly installed at the bottom of the centrifugal cylinder, the driving wheel is meshed with the driven wheel, and a lock is provided at the output end of the driving motor.

[0010] Furthermore, the top of the inner partition below is tilted outward.

[0011] Furthermore, the bottom of the centrifugal cylinder is configured in a conical shape.

[0012] Furthermore, the outer shaping member is composed of a plurality of groups of drawstrings arranged in an annular shape on the outside of the sponge liner.

[0013] Furthermore, the outer shaping member adopts an outer wrapping net.

[0014] A dehydration and drying method for producing bromochlorohydantoin comprises the following steps: S1. Loading: Bromochlorohydantoin chemical synthesis particles are injected into the equipment through the feeding branch pipe and compressed air, and then enter the centrifuge cylinder through the conduit and the feeding tee pipe; S2. Dehydration and drying: Start the equipment, and the centrifugal drum dehydrates and dries the bromochlorohydantoin chemical synthesis particles. The sponge liner plays a protective and water-absorbing role, improving the efficiency of centrifugal dehydration and drying. During the centrifugal dehydration process, the upper and lower guide tubes are alternately raised and lowered to achieve the position replacement of the sponge liner and the removal of water from the sponge, completing high-speed and high-quality dehydration and drying. S3. Discharging: Turn off the equipment and stop the centrifuge cylinder. Then control the multifunctional inner disc to rotate relative to the centrifuge cylinder. When the transmission block is separated from the triangular transmission port, the dehydrated and dried bromochlorohydantoin chemical synthesis particles are discharged through the triangular transmission port. Then open the discharge valve to discharge the material.

[0015] The beneficial effects of the present invention are as follows: 1. The present invention adopts the setting of multifunctional inner disk and conduit, and utilizes the upper and lower conduits to alternately rise and fall, and can realize the switching of sponge liner while filtering. When the upper conduit descends, the sponge liner is twisted together by tying the bag, and then cooperates with the use of the pressure ring to realize the initial squeezing and drying of the sponge liner, and then hot air is injected through the lower conduit to perform secondary drying of the sponge liner, thereby realizing the alternating use and alternating drying of the sponge liner, thereby improving the dehydration and drying efficiency.

[0016] 2. The present invention controls the lifting and lowering of the upper guide tube, which not only can repeatedly scrape and press the sponge liner, but also the upper guide tube drives the multifunctional inner disk to rotate relative to the centrifugal cylinder, and pushes the transmission block away from the triangular transmission port through the inclined surface of the transmission block. The triangular transmission port opens and the particles are automatically discharged. At the same time, under the action of the top spring, the transmission block repeatedly strikes the multifunctional inner disk, causing the sponge liner to vibrate, which can shake off the particles stuck on the sponge liner. There is no need for manual cleaning and discharge, and the discharge efficiency is high. BRIEF DESCRIPTION OF THE DRAWINGS

[0017] Figure 1 It is a schematic diagram of the three-dimensional structure of the present invention; Figure 2 It is a schematic diagram of the internal structure of the dehydration tank of the present invention; Figure 3 This is a schematic diagram of the cross-sectional structure of the dehydration tank of the present invention; Figure 4 This is a schematic diagram of the cross-sectional structure of the centrifugal cylinder of the present invention; Figure 5 This is a schematic diagram of the sponge liner structure of the present invention; Figure 6 It is an exploded view of the internal structure of the sponge liner of the present invention.

[0018] Figure markings: 1. Dehydration tank; 11. Inner partition; 12. Drain pipe; 13. Smoke exhaust pipe; 14. Discharge valve; 2. Centrifugal cylinder; 21. Driven wheel; 22. Pressure ring; 23. Transmission box; 24. Transmission block; 25. Top spring; 26. Ball; 3. Lifting cylinder; 31. Lifting rod; 32. Clamping cylinder; 4. Multi-function inner plate; 41. Triangular transmission port; 42. Spiral guide groove; 43. Feeding tee; 5. Sponge liner; 51. External shaping part; 6. Conduit; 61. External spiral protrusion; 7. Lifting pipe; 8. Hot air pipe; 9. Driving motor; 10. Driving wheel. DETAILED DESCRIPTION

[0019] To make the objectives, technical solutions and advantages of the embodiments of the present invention more clear, the technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the accompanying drawings in the embodiments of the present invention.

[0020] Example 1, as Figures 1-6 As shown, a dehydration and drying device for the production of bromochlorohydantoin includes a dehydration tank 1, a centrifugal drum 2 is rotatably installed inside the dehydration tank 1, two groups of pressure rings 22 are provided inside the centrifugal drum 2, a multifunctional inner disk 4 is sandwiched between the two groups of pressure rings 22, and the multifunctional inner disk 4 is composed of two groups of conical disks and an intermediate tube. The two groups of conical disks are symmetrically distributed about the intermediate tube. The radius of the upper conical disk is smaller than the radius of the lower conical disk. A sponge liner 5 is provided between the multifunctional inner disk 4 and the centrifugal drum 2. The outer surface of the sponge liner 5 is provided with an external shaping member 51. The sponge liner 5 between the lower conical disk and the centrifugal drum 2 is tightly squeezed. The outer side of the lower conical disk is annularly provided with multiple groups of triangular transmission openings 41. The outer side of the centrifugal drum 2 is annularly provided with multiple groups of transmission boxes 23. The transmission block 24 is slidably connected to the transmission box 23. A top spring 25 is provided between the transmission block 24 and the transmission box 23. The transmission block 24 is plugged into the triangular transmission opening 41. The plug-in end of the transmission block 24 is arranged in a right triangle. A ball 26 is rotatably installed on the outer side of the straight side. Both ends of the intermediate tube are provided with a guide tube 6 that can be raised and lowered. A feeding tee tube 43 is provided in the middle of the intermediate tube. The feeding tee tube 43 can be inserted into the guide tube 6. The two ends of the outer shaping part 51 respectively pass through the corresponding multifunctional inner disk 4 and the pressure ring 22, and are respectively fixedly installed on the two groups of guide tubes 6.

[0021] The inner wall of the dehydration tank 1 is provided with two groups of inner partitions 11, and the centrifugal cylinder 2 is rotatably installed between the two groups of inner partitions 11. The top and bottom of the centrifugal cylinder 2 are provided with smoke exhaust pipes 13. The outside of the dehydration tank 1 is provided with a drain pipe 12, and the drain pipe 12 is located directly above the lower inner partition 11. A discharge valve 14 is provided at the bottom of the dehydration tank 1.

[0022] A drive motor 9 is fixedly installed at the bottom of the dehydration tank 1, and a drive wheel 10 is fixedly installed at the output end of the drive motor 9. The drive wheel 10 is located in the dehydration tank 1. A driven wheel 21 is fixedly installed at the bottom of the centrifugal cylinder 2. The drive wheel 10 is engaged with the driven wheel 21, and a lock is provided at the output end of the drive motor 9.

[0023] Loading: The upper conduit 6 descends to the bottom, and the conduit 6 gathers the excess part of the sponge liner 5 above the multifunctional inner plate 4, and the loading tee 43 is plugged into the bottom of the upper conduit 6. Then, bromochlorohydantoin particles are injected into the space between the sponge liner 5 and the multifunctional inner plate 4 through the conduit 6 and the loading tee 43 to complete the loading.

[0024] Centrifugal dehydration and drying: Start the equipment, drive motor 9 drives driving wheel 10 to rotate, driving wheel 10 drives centrifugal drum 2 to rotate through driven wheel 21. At this time, the vertical surface of transmission block 24 is in close contact with the vertical surface of triangular transmission port 41. Centrifugal drum 2 drives multifunctional inner disk 4 to rotate synchronously through transmission block 24. Centrifugal drum 2, multifunctional inner disk 4 and sponge liner 5 rotate synchronously. Bromochlorohydrazine particles are pressed on sponge liner 5 under the action of centrifugal force. Sponge liner 5 provides buffering force to bromochlorohydrazine particles and can absorb moisture to prevent bromochlorohydrazine particles from breaking.

[0025] After the slurry is dried, the upper and lower guide tubes 6 are rotated, and the lower guide tubes 6 are rotated, so that the lower end of the sponge liner 5 is rotated. Scraping, preliminarily removes the absorbed moisture, and can prevent bromochlorohydantoin particles from being taken out, and then hot air is introduced through the upper conduit 6, the hot air enters the multifunctional inner disk 4, blows downward to the gathered sponge liner 5, and performs secondary drying and water removal. After running for a period of time, the above method is used to control the upper and lower sets of conduits 6 to descend synchronously again, and the sponge liner 5 is better again. It should be noted that the radius of the upper cone disk is smaller than the radius of the lower cone disk. Therefore, the distance between the upper cone disk and the centrifugal cylinder 2 is larger, and the sponge liner 5 will not be scraped when passing through the distance. It will be scraped when entering between the upper pressure ring 22 and the upper cone disk. The scraped water will not flow back downward, and will be discharged to the bottom of the dehydration tank 1 under the guiding action of the multifunctional inner disk 4, and finally discharged through the discharge valve 14. The overall dehydration and drying efficiency is high, and secondary pollution is prevented. The dried sponge liner 5 has a certain stability, can indirectly perform thermal drying on the particles, and the drying is more stable. During the dehydration and drying process, the hot air after participating in the drying is discharged through the exhaust pipe 13 for centralized treatment.

[0026] Automatic and fast discharge: Since the discharge valve 14 performs a drainage operation during the dehydration and drying process, the residual water in the sponge liner 5 is a trace amount during the centrifugal dehydration process. Therefore, a small amount of water may hang on the wall at the bottom of the centrifugal cylinder 2 and the bottom of the dehydration tank 1. Therefore, it is necessary to first introduce hot air into the dehydration tank 1 through the upper conduit 6 for a period of time to evaporate the water. The trace water evaporates quickly, and generally 1 minute is enough. At this time, the output end of the drive motor 9 is locked with a lock, and the centrifugal cylinder 2 cannot rotate. At this time, the multifunctional inner disk 4 is controlled to rotate relative to the centrifugal cylinder 2, and the rotation direction is the same as the working direction of the centrifugal cylinder 2. Therefore, the multifunctional inner disk 4 is pushed through the triangular transmission port 41 and the inclined surface of the transmission block 24. The dynamic transmission block 24 slides to the inside of the transmission box 23. When the transmission block 24 is misaligned with the triangular transmission port 41, the triangular transmission port 41 is fully opened. At this time, the particles are discharged from the triangular transmission port 41. Since a cone disk is provided under the multifunctional inner disk 4, the particles will slide obliquely to the position of the triangular transmission port 41, and the particles can be completely discharged. When the transmission block 24 is aligned with the triangular transmission port 41 again, under the action of the top spring 25, the transmission block 24 knocks in the triangular transmission port 41, causing the centrifugal cylinder 2, the multifunctional inner disk 4 and the sponge liner 5 to vibrate, which can shake off the particles remaining in the sponge liner 5, ensuring complete discharge. The particles fall into the bottom of the dehydration tank 1 through the centrifugal cylinder 2 and are then discharged through the discharge valve 14.

[0027] Embodiment 2, based on the above embodiment, further includes: a spiral guide groove 42 is opened inside the intermediate tube, an outer spiral protrusion 61 is provided on the outer side of the conduit 6, the outer spiral protrusion 61 is threadedly connected in the spiral guide groove 42, and the thickness of the outer spiral protrusion 61 is less than the depth of the spiral guide groove 42.

[0028] Through the present embodiment, when the catheter 6 is inserted into the middle tube at the bottom, the catheter 6 rotates under the guidance of the outer spiral protrusion 61 and the spiral guide groove 42. It should be noted that the pitch of the spiral guide groove 42 is set to 5-10 cm. The pitch is large and can generate rotational drive. The catheter 6 will drive the sponge liner 5 to twist, which can just discharge the water absorbed inside it, and the sponge liner 5 can be switched alternately in a smaller space.

[0029] Since the thickness of the outer spiral protrusion 61 is smaller than the depth of the spiral guide groove 42, when the outer spiral protrusion 61 is threadedly connected to the spiral guide groove 42, there is an air cavity between the outer spiral protrusion 61 and the spiral guide groove 42, and the hot air is spirally discharged through the cavity so that the sponge liner 5 can be dried with hot air more evenly.

[0030] Through the arrangement of this embodiment, there is no need to give additional rotational drive to the multifunctional inner disk 4. During the discharge process, the conduit 6 is locked to restrict the rotation of the conduit 6. Then, when the conduit 6 is controlled to descend, the conduit 6 drives the multifunctional inner disk 4 to rotate, and the rotation direction is the same as the working direction of the centrifuge barrel 2. When rising, the conduit 6 is unlocked, and the conduit 6 rotates relative to the multifunctional inner disk 4. Therefore, as the conduit 6 moves up and down, the multifunctional inner disk 4 rotates unidirectionally to discharge.

[0031] Embodiment three, on the basis of the above embodiment, further includes: two groups of lifting cylinders 3 are fixedly installed on the outside of the dehydration tank 1, and the telescopic ends of the lifting cylinders 3 are fixedly installed with lifting rods 31, and the lifting tubes 7 are rotatably installed inside the lifting rods 31. The lifting tubes 7 are fixedly connected to the corresponding conduits 6, and the ends of the lifting tubes 7 away from the conduits 6 are fixedly installed with hot air pipes 8. A feeding branch pipe is provided on the outside of the upper hot air pipe 8, and a clamping cylinder 32 is fixedly installed on the top of the upper lifting rod 31. The telescopic end of the clamping cylinder 32 can clamp and fix the lifting tube 7 in the lifting rod 31.

[0032] The lifting rod 31 is controlled by the lifting cylinder 3, and the lifting rod 31 drives the guide tube 6 to move up and down through the lifting tube 7, which is simple to control; During the discharging process, when the control conduit 6 is lowered, the clamping cylinder 32 fixes the lifting tube 7 on the lifting rod 31, and the lifting tube 7 limits the rotation of the conduit 6. The conduit 6 drives the multifunctional inner disk 4 to rotate, and the rotation direction is the same as the working direction of the centrifuge cylinder 2. When rising, the clamping cylinder 32 releases the lifting tube 7, the conduit 6 is unlocked, and the conduit 6 rotates relative to the multifunctional inner disk 4. Therefore, as the conduit 6 moves up and down, the multifunctional inner disk 4 rotates unidirectionally to perform discharging.

[0033] Embodiment 4, based on the above embodiment, further includes that the top of the lower inner partition 11 is tilted outward. This design facilitates the discharge of centrifugally shed water during centrifugal dehydration and drying.

[0034] Furthermore, the bottom of the centrifugal cylinder 2 is conical. This design can guide the particles during discharge, resulting in a good discharge effect.

[0035] Embodiment 5, based on the above embodiment, further includes that the outer shaping member 51 is composed of multiple groups of pull ropes arranged in a ring shape on the outside of the sponge liner 5. Through the setting of the pull ropes, the transmission stability is ensured while the overall buffering effect on the sponge liner 5 is small, and the sponge liner 5 can be prevented from being pulled apart.

[0036] Embodiment 6, based on the above embodiment, further includes that the outer shaping member 51 adopts an outer wrapping net. The arrangement of this embodiment has a certain impact on the dehydration efficiency, but the impact is relatively small, but the anti-breaking effect is better.

[0037] Example 7, a dehydration and drying method for producing bromochlorohydantoin, comprising the following steps: S1, loading: through the feeding branch pipe, bromochlorohydantoin chemical synthesis particles are injected into the equipment by compressed air, and enter the centrifuge cylinder 2 through the conduit 6 and the feeding tee pipe 43; S2, dehydration and drying: Start the equipment, centrifuge drum 2 centrifuges and dehydrates the bromochlorohydantoin chemical synthesis particles, and the sponge liner 5 plays a protective and water-absorbing function, thereby improving the efficiency of centrifugal dehydration and drying. During the centrifugal dehydration process, the upper and lower guide tubes 6 are alternately raised and lowered to achieve the position replacement of the sponge liner 5 and the removal of water from the sponge, thereby completing high-speed and high-quality dehydration and drying; S3, unloading: turn off the equipment, stop the centrifuge cylinder 2, and then control the multifunctional inner disk 4 to rotate relative to the centrifuge cylinder 2. When the transmission block 24 disengages from the triangular transmission port 41, the dehydrated and dried bromochlorohydantoin chemical synthesis particles are discharged through the triangular transmission port 41, and then open the discharge valve 14 to discharge the material.

[0038] The above description of the disclosed embodiments is intended to enable one skilled in the art to implement or use the present invention. Various modifications to these embodiments will be readily apparent to one skilled in the art, and the general principles defined herein may be implemented in other embodiments without departing from the spirit or scope of the present invention. Therefore, the present invention is not limited to the embodiments shown herein but is intended to conform to the widest scope consistent with the principles and novel features disclosed herein.

Claims

1. A dehydration and drying device for producing bromochlorohydantoin, comprising a dehydration tank (1), characterized in that: A centrifugal cylinder (2) is rotatably mounted inside the dehydration tank (1), and two groups of pressure rings (22) are provided inside the centrifugal cylinder (2). A multifunctional inner disk (4) is sandwiched between the two groups of pressure rings (22). The multifunctional inner disk (4) is composed of two groups of cone disks and an intermediate tube. The two groups of cone disks are symmetrically distributed about the intermediate tube. The radius of the upper cone disk is smaller than the radius of the lower cone disk. A sponge liner (5) is provided between the multifunctional inner disk (4) and the centrifugal cylinder (2). The outer surface of the sponge liner (5) is provided with an outer shaping member (51). The lower cone disk is symmetrically distributed with respect to the intermediate tube. The sponge liner (5) between the centrifugal cylinders (2) is tightly squeezed, and a plurality of triangular transmission ports (41) are provided in an outer ring of the lower cone disk. A plurality of transmission boxes (23) are provided in an outer ring of the centrifugal cylinder (2). A transmission block (24) is slidably connected to the inside of the transmission box (23). A top spring (25) is provided between the transmission block (24) and the transmission box (23). The transmission block (24) is plugged into the triangular transmission port (41). The plug-in end of the transmission block (24) is provided in a right-angled triangle shape, and a ball (26) is rotatably installed on the outer side of the straight side. Both ends of the intermediate tube are provided with guide tubes (6) that can be raised and lowered. A feeding tee (43) is provided in the middle of the intermediate tube. The feeding tee (43) can be plugged into the guide tube (6). Both ends of the external shaping member (51) pass through the corresponding multifunctional inner disk (4) and the pressure ring (22) and are fixedly mounted on the two sets of guide tubes (6).

2. A dehydration and drying device for producing bromochlorohydantoin according to claim 1, characterized in that: A spiral guide groove (42) is provided inside the intermediate tube, and an outer spiral protrusion (61) is provided on the outer side of the conduit (6). The outer spiral protrusion (61) is threadedly connected to the spiral guide groove (42), and the thickness of the outer spiral protrusion (61) is less than the depth of the spiral guide groove (42).

3. A dehydration and drying device for producing bromochlorohydantoin according to claim 2, characterized in that, Two sets of lifting cylinders (3) are fixedly installed on the outside of the dehydration tank (1), and lifting rods (31) are fixedly installed on the telescopic ends of the lifting cylinders (3). A lifting pipe (7) is rotatably installed inside the lifting rod (31), and the lifting pipe (7) is fixedly connected to the corresponding conduit (6). A hot air pipe (8) is fixedly installed on the end of the lifting pipe (7) away from the conduit (6). A feeding branch pipe is provided on the outside of the upper hot air pipe (8). A clamping cylinder (32) is fixedly installed on the top of the upper lifting rod (31), and the telescopic end of the clamping cylinder (32) can clamp and fix the lifting pipe (7) in the lifting rod (31).

4. A dehydration and drying device for producing bromochlorohydantoin according to claim 3, characterized in that, The inner wall of the dehydration tank (1) is provided with two groups of inner baffles (11), and the centrifugal cylinder (2) is rotatably installed between the two groups of inner baffles (11). The top and bottom of the centrifugal cylinder (2) are both provided with smoke exhaust pipes (13). The outer side of the dehydration tank (1) is provided with a drainage pipe (12), and the drainage pipe (12) is located directly above the lower inner baffle (11). The bottom of the dehydration tank (1) is provided with a discharge valve (14).

5. A dehydration and drying device for producing bromochlorohydantoin according to claim 4, characterized in that, A driving motor (9) is fixedly mounted below the dehydration tank (1), a driving wheel (10) is fixedly mounted on the output end of the driving motor (9), and the driving wheel (10) is located in the dehydration tank (1). A driven wheel (21) is fixedly mounted on the bottom of the centrifugal cylinder (2), and the driving wheel (10) is meshed with the driven wheel (21). A lock is provided at the output end of the driving motor (9).

6. A dehydration and drying device for producing bromochlorohydantoin according to claim 5, characterized in that: The top of the inner partition (11) below is tilted outward.

7. A dehydration and drying device for producing bromochlorohydantoin according to claim 6, characterized in that: The bottom of the centrifugal cylinder (2) is arranged in a conical shape.

8. A dehydration and drying device for producing bromochlorohydantoin according to claim 1, characterized in that: The outer shaping member (51) is composed of multiple groups of drawstrings arranged in an annular shape on the outside of the sponge liner (5).

9. A dehydration and drying device for producing bromochlorohydantoin according to claim 1, characterized in that: The outer shaping member (51) is an outer wrapping net.

10. A dehydration and drying method for producing bromochlorohydantoin, using the dehydration and drying device for producing bromochlorohydantoin according to any one of claims 7 to 9, characterized in that: The following steps are involved: S1, feeding: injecting bromochlorohydantoin chemical synthesis particles into the equipment through the feeding branch pipe and using compressed air, and entering the centrifuge cylinder (2) through the conduit (6) and the feeding tee pipe (43); S2, dehydration and drying: start the equipment, centrifuge drum (2) centrifuges and dehydrates the bromochlorohydantoin chemical synthesis particles, the sponge liner (5) plays a protective and water-absorbing function, and improves the efficiency of centrifugal dehydration and drying. During the centrifugal dehydration process, the upper and lower guide tubes (6) are alternately raised and lowered to achieve the position replacement of the sponge liner (5) and the removal of water from the sponge, thereby completing high-speed and high-quality dehydration and drying; S3, unloading: the equipment is turned off, the centrifugal cylinder (2) stops rotating, and then the multifunctional inner disc (4) is controlled to rotate relative to the centrifugal cylinder (2). When the transmission block (24) is separated from the triangular transmission port (41), the dehydrated and dried bromochlorohydantoin chemical synthesis particles are discharged through the triangular transmission port (41), and then the discharge valve (14) is opened to discharge the material.

Citation Information

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