Preparation method of high-purity low-alloy ultrahigh-strength steel bar

By employing a synergistic process of LF refining, RH cyclic degassing, and vacuum consumable smelting, combined with optimization of parameters across the entire process chain, the problems of high equipment investment and difficulty in achieving both high purity in the preparation of 300M steel have been solved. This has enabled the efficient preparation of high-strength steel bars, meeting the stringent requirements of high-end fields such as aerospace.

CN122256599APending Publication Date: 2026-06-23DAYE SPECIAL STEEL CO LTD
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Patent Information

Application Number
CN202610470420.9
Authority / Receiving Office
CN · China
Patent Type
Applications(China)
Current Assignee / Owner
Filing Date
2026-04-10
Publication Date
2026-06-23

AI Technical Summary

Technical Problem

Existing processes for preparing low-alloy ultra-high-strength steel (300M steel) suffer from problems such as large equipment investment, long production cycles, high costs, and difficulty in adapting to large-scale industrial production. In single-vacuum processes, inclusions are prone to secondary adsorption of gas, making simultaneous removal impossible. The RH vacuum degassing process does not take into account the alloy characteristics of 300M steel, resulting in insufficient floating force for inclusions. Each process step is operated independently with mismatched parameters, making it difficult to achieve both steel purity and mechanical properties.

Method used

The dual synergistic smelting process of LF refining + RH circulating degassing + vacuum consumable remelting is adopted. Combined with precise optimization of the parameters of the entire process chain and multi-pass forging-heat treatment, the synergistic control of gas removal and inclusion flotation is achieved by designing the steel circulation parameters of RH degassing and the convection parameters of the molten pool of vacuum consumable remelting, thereby refining the grains and optimizing the microstructure.

Benefits of technology

A high-purity 300M steel bar with excellent strength and toughness was prepared, with a tensile strength of 1930-2070MPa and a fracture toughness of ≥55MPa·m0.5. This breakthrough overcomes the technical bottleneck of traditional processes that make it difficult to balance purity and mechanical properties, reduces production costs, adapts to large-scale production, and improves service safety.

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Abstract

The invention provides a preparation method of a high-purity low-alloy ultrahigh-strength steel bar, which adopts a double collaborative smelting process of LF refining, RH circulating degassing and vacuum consumable smelting, and is matched with a full-process-chain parameter precise optimization and multi-pass forging-heat treatment collaborative process. By designing molten steel circulation parameters of RH degassing and molten pool convection parameters of vacuum consumable remelting, cooperative control over molten steel gas removal and inclusion floating is achieved, meanwhile, grains are refined, the structure is optimized, the 300M steel bar high in purity and excellent in toughness matching performance is prepared, it is guaranteed that the tensile strength is kept at 1930-2070 MPa, the fracture toughness is kept at 930-970 MPa, and the tensile strength of the 300M steel bar is greatly improved. The technical bottleneck that the purity and the mechanical property are difficult to consider in the traditional process is broken through.
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