Chloride ion adding device

By introducing a constant pressure gas input and flow control valve control system into the chloride ion addition device, combined with the adaptability design of the telescopic rod, the problem of insufficient adaptability of the chloride ion addition device on different production lines is solved, and the uniformity of the chloride ion solution is achieved. Continuous output improves reaction stability.

CN222196873UActive Publication Date: 2024-12-20JIANGXI HANGDIAN COPPER FOIL CO LTD
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Patent Information

Application Number
CN202420857344.3
Authority / Receiving Office
CN · China
Patent Type
Utility models(China)
Current Assignee / Owner
Filing Date
2024-04-24
Publication Date
2024-12-20
Estimated Expiration
2034-04-24

AI Technical Summary

Technical Problem

The existing chloride ion addition devices have poor adaptability in different production lines, which makes it difficult to control the uniformity and sustainability of the chloride ion solution, affecting the stability of the reaction.

Method used

A chloride ion addition device including a constant pressure gas input pipe, a flow control valve and a DCS module was designed to maintain the pressure in the tank through a constant pressure gas, and use a flow control valve and a DCS module to accurately control the amount and speed of solution addition, and to expand and contract. The rods are adapted to different production line equipment to ensure the consistency of solution flow rate.

Benefits of technology

It realizes the stable and uniform output of chloride ion solution, improves the reaction stability and adaptability of addition, and is suitable for equipment in different production lines.

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Abstract

The utility model provides a chloride ion adding device which comprises a tank body, the top of the tank body is communicated with a constant-pressure gas input pipe so as to input constant-pressure gas into the tank body, the bottom of the tank body is communicated with a solution output pipe, a first flow control valve is arranged on the solution output pipe, and one end, far away from the tank body, of the solution output pipe is connected with a first butt joint port; the first docking port is used for connecting a matching pipe, one end, away from the first docking port, of the matching pipe is connected with a second docking port, one end, back to the matching pipe, of the second docking port is communicated with a second flow control valve, one end, away from the second docking port, of the second flow control valve is connected with a discharge pipe, and the first flow control valve and the second flow control valve are electrically connected with the DCS module. According to the chloride ion adding device, the constant-pressure gas input pipe, the first flow control valve and the second flow control valve are arranged, the DCS module is adopted to control parameters of the two flow control valves, and the first butt joint port and the second butt joint port are arranged, so that the chloride ion adding process has good uniformity and continuity, and the chloride ion adding device can adapt to different production lines.
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Description

Technical Field

[0001] The utility model relates to the technical field of copper foil production, in particular to a chloride ion adding device. Background Art

[0002] Chloride ion (Cl-) is a -1 valence ion that plays an important role in copper foil production. In the preparation of copper sulfate electrolyte during copper foil production, chloride ion materials need to be added to adjust the properties of copper sulfate electrolyte, which can improve the electrode reaction rate and inhibit the generation of impurities.

[0003] There are two ways to add chloride ions. One is the traditional one-time addition method, which adds the chloride ion material all at once, and the other is to add an appropriate amount continuously. Among them, the one-time addition method has a long stable period search process at the beginning of production, and the addition amount and adsorption amount are not constant, which is difficult to control. The method of continuous addition of an appropriate amount is easy to find the addition amount ratio, which is conducive to finding and maintaining the stable period. The control of the addition amount is the key to affecting production.

[0004] Existing chloride ion continuous addition devices usually use flow valves and other technologies to control the flow of chloride ion solution. The flow valve is usually set in the area of ​​the tank body close to the reserve solution, and the chloride ion solution relies on self-weight overflow to enter the copper sulfate electrolyte tank. However, due to different production line equipment, there is often a certain height difference between the existing chloride ion addition device tank body and the copper sulfate electrolyte tank. The chloride ion solution is affected by gravity in the pipeline. Faced with different height differences in different production lines, the speed at which the chloride ion solution enters the copper sulfate electrolyte tank will be different. The lack of precise control over the addition of chloride ion solution may lead to an unstable reaction, which has a negative impact on the uniformity and continuity of the addition. In addition, the chloride ion addition device has poor adaptability to different production lines. Utility Model Content

[0005] In view of the deficiencies in the prior art, the purpose of the present invention is to provide a chloride ion adding device, aiming to solve the problems of insufficient addition uniformity and poor adaptability to different production lines in the prior art chloride ion adding device.

[0006] In order to achieve the above purpose, the utility model is implemented through the following technical solutions:

[0007] A chloride ion adding device comprises a tank body, wherein the top of the tank body is connected to a constant pressure gas input pipe so as to input constant pressure gas into the tank body, the bottom of the tank body is connected to a solution output pipe, a first flow control valve is arranged on the solution output pipe, an end of the solution output pipe away from the tank body is connected to a first pairing port, the first pairing port is used to connect a matching pipe, an end of the matching pipe away from the first pairing port is connected to a second pairing port, an end of the second pairing port facing away from the matching pipe is connected to a second flow control valve, an end of the second flow control valve away from the second pairing port is connected to a discharge pipe, and the first flow control valve and the second flow control valve are both electrically connected to a DCS module.

[0008] Compared with the prior art, the beneficial effects of the utility model are as follows: by setting the constant pressure gas input pipe, constant pressure gas is input into the tank body, which helps to maintain a constant pressure in the tank body and is beneficial to improving the stability of the chloride ion solution output from the tank body; by setting the first flow control valve and the second flow control valve, and using the DCS module to control the parameters of the two flow control valves, the addition amount and addition speed of the chloride ion solution can be conveniently and accurately controlled. When the path for the tank body to transport the solution to the copper sulfate electrolyte tank is long and has a certain height difference, the second flow control valve can perform secondary control on the solution flow rate to prevent the problem of inaccurate speed control entering the copper sulfate electrolyte tank due to the change of the flow rate of the solution caused by gravity acceleration, thereby destroying the stability of the reaction, so that the chloride ion addition process has good uniformity and continuity; by setting the first docking interface and the second docking interface, the matching tubes of different lengths can be connected between the two docking interfaces, so that the chloride ion addition device can adapt to different production lines.

[0009] Furthermore, the top of the tank body is connected to a solution input pipe, and a one-way valve is arranged on the solution input pipe.

[0010] Furthermore, a first sealing sleeve is provided at one end of the solution input pipe connected to the tank body, a second sealing sleeve is provided at one end of the constant pressure gas input pipe connected to the tank body, and a third sealing sleeve is provided at one end of the solution output pipe connected to the tank body.

[0011] Furthermore, a stabilizing portion is provided at the bottom of the tank body, the stabilizing portion is connected to the covering portion, and the covering portion is connected to the third sealing sleeve and the solution output tube.

[0012] Furthermore, a support column is provided at the bottom of the tank body, a first support rod is connected to the support column, and an end of the first support rod away from the support column is connected to the covering portion.

[0013] Furthermore, a plurality of second support rods are connected to the support column, and one end of the second support rod away from the support column is connected to the tank body.

[0014] Furthermore, one end of the support column away from the tank body is connected to the cylinder.

[0015] Furthermore, one end of the cylinder away from the support column is connected to a base.

[0016] Furthermore, a plurality of telescopic rods are connected between the first pair of interfaces and the second pair of interfaces, and the lengths of the telescopic rods are adapted to the matching tubes. BRIEF DESCRIPTION OF THE DRAWINGS

[0017] Figure 1 This is a schematic diagram of the structure of the chloride ion adding device in the embodiment of the utility model;

[0018] Figure 2 This is a schematic structural diagram of a stabilizing portion and a coating portion in a chloride ion adding device in an embodiment of the utility model;

[0019] Description of main component symbols:

[0020] Tank 100 Support column 110 First support rod 111 cylinder 120 Base 130 Coating 140 Solution inlet tube 200 First sealing ferrule 210 Check valve 220 Constant pressure gas inlet pipe 300 Second sealing ferrule 310 Solution output tube 400 The third sealing ferrule 410 First flow control valve 420 The first pair of interfaces 430 The second pair of interfaces 440 Telescopic rod 450 Second flow control valve 460 Discharge pipe 470 DCS Module 500 Matching tube 600

[0021] The following specific implementation manner will further illustrate the present utility model in conjunction with the above-mentioned drawings. DETAILED DESCRIPTION

[0022] In order to facilitate the understanding of the present invention, the present invention will be described more fully below with reference to the relevant drawings. Several embodiments of the present invention are given in the drawings. However, the present invention can be implemented in many different forms and is not limited to the embodiments described herein. On the contrary, the purpose of providing these embodiments is to make the disclosure of the present invention more thorough and comprehensive.

[0023] It should be noted that when an element is referred to as being "fixed to" another element, it may be directly on the other element or there may be a central element. When an element is considered to be "connected to" another element, it may be directly connected to the other element or there may be a central element at the same time. The terms "vertical", "horizontal", "left", "right" and similar expressions used herein are for illustrative purposes only.

[0024] Unless otherwise defined, all technical and scientific terms used herein have the same meaning as those commonly understood by those skilled in the art in the technical field of the present invention. The terms used herein in the specification of the present invention are only for the purpose of describing specific embodiments and are not intended to limit the present invention. The term "and / or" used herein includes any and all combinations of one or more related listed items.

[0025] See also Figure 1 and Figure 2The chloride ion adding device in the embodiment of the utility model comprises a tank body 100, the top of the tank body 100 is connected to a solution input pipe 200, a one-way valve 220 is arranged on the solution input pipe 200, the top of the tank body 100 is connected to a constant pressure gas input pipe 300, so as to input constant pressure gas into the tank body 100, the bottom of the tank body 100 is connected to a solution output pipe 400, a first sealing sleeve 210 is arranged at one end of the solution input pipe 200 connected to the tank body 100, a second sealing sleeve 310 is arranged at one end of the constant pressure gas input pipe 300 connected to the tank body 100, a third sealing sleeve 410 is arranged at one end of the solution output pipe 400 connected to the tank body 100, and a first flow control valve is arranged on the solution output pipe 400. 420, the end of the solution output pipe 400 away from the tank body 100 is connected to the first docking port 430, the first docking port 430 is used to connect the matching pipe 600, the end of the matching pipe 600 away from the first docking port 430 is connected to the second docking port 440, a plurality of telescopic rods 450 are connected between the first docking port 430 and the second docking port 440, the length of the telescopic rod 450 is adapted to the matching pipe 600, the end of the second docking port 440 facing away from the matching pipe 600 is connected to the second flow control valve 460, the end of the second flow control valve 460 away from the second docking port 440 is connected to the discharge pipe 470, the first flow control valve 420 and the second flow control valve 460 are electrically connected to the DCS module 500. Preferably, the discharge pipe 470 is connected to the copper sulfate electrolyte tank, the chloride ion solution used is an AR-grade reagent without impurities, the telescopic rod 450 can be fixed with bolts after adjusting the length according to the matching pipe 600, maintain the current length, which is conducive to stabilizing the pipeline. It can be understood that the matching tube 600 is selected according to the different equipment sizes of the production line, so that the chloride ion adding device can adapt to different types of production lines. When the length of the matching tube 600 is long, that is, the path for transporting the chloride ion solution to the copper sulfate electrolyte tank is long and the height difference is large, even if the flow rate of the chloride ion solution after the flow is controlled by the first flow control valve 420 is increased due to gravity, it can be restored to the required speed under the control of the second flow control valve 460, which is conducive to controlling the uniform speed of the chloride ion solution. Under the system control of the DCS module, the control of the first flow control valve 420 and the second flow control valve 460 is convenient and accurate, which greatly improves the addition uniformity of the chloride ion adding device, and can adapt to different production equipment with excellent flexibility.

[0026] Furthermore, the constant pressure gas input pipe 300 can deliver constant pressure gas into the tank body 100 to maintain a constant gas pressure in the tank body 100, which is beneficial for the solution output pipe 400 to maintain a stable state when outputting the solution, and pressurization can increase the flow rate range of the chloride ion solution to meet the demand for higher flow rates.

[0027] A stabilizing portion is provided at the bottom of the tank body 100, and the stabilizing portion is connected to the covering portion 140, and the covering portion 140 is connected to the third sealing sleeve 410 and the solution output pipe 400. A support column 110 is provided at the bottom of the tank body 100, and a first support rod 111 is connected to the support column 110, and one end of the first support rod 111 away from the support column 110 is connected to the covering portion 140, and a plurality of second support rods are connected to the support column 110, and one end of the second support rod away from the support column 110 is connected to the tank body 100, and one end of the support column 110 away from the tank body 100 is connected to the cylinder 120, and one end of the cylinder 120 away from the support column 110 is connected to the base 130. It can be understood that the stabilizing portion and the covering portion 140 are beneficial to maintaining the pipeline of the solution output pipe 400. Even when the pressure at the solution output pipe 400 is high and the flow rate is fast, the stability of the pipeline can be maintained, which is beneficial to improving the stability and uniformity of the chloride ion addition process. Furthermore, the first support rod 111 further improves the stability between the solution output pipe 400 and the tank body 100 and the support column 110. The second support rod and the base 130 can improve the overall structural stability of the chloride ion adding device. The cylinder 120 can adjust the height of the tank body 100, so that the chloride ion adding device can more conveniently make height adjustments to cope with different production line equipment.

[0028] In the description of this specification, the description with reference to the terms "one embodiment", "some embodiments", "example", "specific example", or "some examples" means that the specific features, structures, materials or characteristics described in conjunction with the embodiment or example are included in at least one embodiment or example of the utility model. In this specification, the schematic representation of the above terms does not necessarily refer to the same embodiment or example. Moreover, the specific features, structures, materials or characteristics described can be combined in any one or more embodiments or examples in a suitable manner.

[0029] The above-mentioned embodiments only express several implementation methods of the utility model, and the descriptions thereof are relatively specific and detailed, but they cannot be understood as limiting the scope of the patent of the utility model. It should be pointed out that, for ordinary technicians in this field, several variations and improvements can be made without departing from the concept of the utility model, and these all belong to the protection scope of the utility model. Therefore, the protection scope of the utility model patent shall be based on the attached claims.

Claims

1. A chloride ion adding device, characterized in that: It includes a tank body, the top of the tank body is connected to a constant pressure gas input pipe to input constant pressure gas into the tank body, the bottom of the tank body is connected to a solution output pipe, a first flow control valve is arranged on the solution output pipe, an end of the solution output pipe away from the tank body is connected to a first pairing port, the first pairing port is used to connect a matching pipe, an end of the matching pipe away from the first pairing port is connected to a second pairing port, an end of the second pairing port facing away from the matching pipe is connected to a second flow control valve, an end of the second flow control valve away from the second pairing port is connected to a discharge pipe, and the first flow control valve and the second flow control valve are both electrically connected to a DCS module.

2. The chloride ion adding device according to claim 1, characterized in that: The top of the tank is connected to a solution input pipe, and a one-way valve is arranged on the solution input pipe.

3. The chloride ion adding device according to claim 2, characterized in that: A first sealing sleeve is arranged at one end of the solution input pipe connected to the tank body, a second sealing sleeve is arranged at one end of the constant pressure gas input pipe connected to the tank body, and a third sealing sleeve is arranged at one end of the solution output pipe connected to the tank body.

4. The chloride ion adding device according to claim 3, characterized in that: A stabilizing portion is provided at the bottom of the tank body, the stabilizing portion is connected to the covering portion, and the covering portion is connected to the third sealing sleeve and the solution output pipe.

5. The chloride ion adding device according to claim 4, characterized in that: A support column is arranged at the bottom of the tank body, a first support rod is connected to the support column, and an end of the first support rod away from the support column is connected to the covering portion.

6. The chloride ion adding device according to claim 5, characterized in that: A plurality of second support rods are connected to the support column, and one end of the second support rod away from the support column is connected to the tank body.

7. The chloride ion adding device according to claim 5, characterized in that: One end of the support column away from the tank body is connected to the cylinder.

8. The chloride ion adding device according to claim 7, characterized in that: One end of the cylinder away from the supporting column is connected to the base.

9. The chloride ion adding device according to claim 1, characterized in that: A plurality of telescopic rods are connected between the first pair of interfaces and the second pair of interfaces, and the lengths of the telescopic rods are adapted to the matching tubes.