Efficient production equipment for silicon nitride particles

Abstract

The utility model discloses efficient production equipment for silicon nitride particles, which relates to the technical field of production equipment and comprises a treatment box and a reaction kettle, a cutting box is movably mounted on the left side of an inner cavity of the treatment box, and a filter tank is movably mounted on the right side of the cutting box. According to the efficient production equipment for the silicon nitride particles, linkage control can be carried out through cleaning of the coarse grid, the fine grid and the membrane grid and pollution discharge side actions, so that it is ensured that equipment of all filtering levels can work in the optimal state, blockage is reduced, the filtering effect is improved, generated wastewater is subjected to primary treatment, and the production efficiency is improved. Comprising the steps of removing large-particle impurities, adjusting the pH value and the like, an acid-base water pump is arranged, so that an acid-base reagent can be conveniently conveyed to a pH adjusting tank, the pH value of sewage can be effectively adjusted, then a biodegradation method is utilized, organic waste is degraded into harmless substances, and biochemical treatment technologies such as an activated sludge method or a biological filter tank method are adopted.

Description

Technical Field

[0001] The utility model belongs to the technical field of silicon nitride particle production, and in particular relates to a high-efficiency production device for silicon nitride particles. Background Art

[0002] At present, efficient production equipment for silicon nitride particles mainly includes the following technical routes: gas phase production equipment, which uses the gas phase method to produce silicon nitride particles. The main process includes preparing silicon nitride particles by thermal decomposition or redox reaction of ammonia and silicon dioxide gas; sol-gel production equipment, which prepares silicon nitride particles under specific conditions by mixing a nitrogen source with a silicon source to form a sol, and then gelling it; chemical vapor deposition (CVD) equipment: a silicon nitride film is deposited on the surface of a substrate through a gas phase chemical reaction. As the reaction proceeds, silicon nitride particles can be formed.

[0003] At present, the sol-gel production equipment has great difficulty in treating wastewater during use, and will produce a large amount of wastewater containing chemicals and impurities, which puts high demands on wastewater treatment and is difficult to treat. Utility Model Content

[0004] The technical problem to be solved by the utility model is that the current production equipment has great difficulty in treating wastewater during use, which will lead to substandard wastewater treatment effect and cause environmental pollution.

[0005] The technical solution adopted by the utility model to solve its technical problems is: a high-efficiency silicon nitride particle production equipment, including a processing box and a reactor, a cutting box is movably installed on the left side of the inner cavity of the processing box, a filtering tank is movably installed on the right side of the cutting box, a sedimentation tank is movably installed on the right side of the filtering tank, a disinfection tank is movably installed on the right side of the sedimentation tank, a PH regulating tank is movably installed on the right side of the disinfection tank, a through hole is opened on the right side of the PH regulating tank, and a water outlet pipe is movably installed in the inner cavity of the through hole.

[0006] As a preferred embodiment of the utility model, a top plate is movably installed on the top of the cutting box, a water inlet pipe is arranged on the top of the top plate, a sol preparation stirring box is arranged on the top of the reactor, a sewage drainage pipe is fixedly installed on the bottom of the reactor, and one end of the sewage drainage pipe is fixedly connected to the water inlet pipe, and the two are interconnected.

[0007] As a preferred embodiment of the utility model, an operation panel is movably installed on the left side of the processing box, a connecting wire tube is fixedly installed on the right side of the operation panel, an electric motor is fixedly installed on the right side of the connecting wire tube, a rotating shaft is movably installed on the back of the motor and passes through the inner cavity of the cutting box, and a cutting blade is movably installed on the surface of the rotating shaft.

[0008] As a preferred embodiment of the utility model, a coarse grid is movably installed on the left side of the inner cavity of the filter tank, a fine grid is movably installed on the right side of the coarse grid, and a membrane grid is movably installed on the right side of the fine grid.

[0009] As a preferred embodiment of the utility model, a disinfection water pump is movably installed on the back side of the disinfection pool, a first conveying line pipe is movably installed on the top of the disinfection water pump, and a disinfection nozzle is movably installed on the top of the first conveying line pipe.

[0010] As a preferred embodiment of the utility model, an acid-base water pump is movably installed on the back of the pH regulating tank, a second conveying line pipe is movably installed on the top of the acid-base water pump, and an acid-base nozzle is movably installed on the top of the second conveying line pipe.

[0011] As a preferred embodiment of the utility model, a slide bar is movably mounted on the top of the disinfection tank and the top of the pH adjustment tank, and a slider is movably mounted on the top of the slide bar.

[0012] As a preferred embodiment of the present invention, a delivery pipeline is fixedly installed at the bottom of the sol preparation stirring box, and the end of the delivery pipeline is fixedly connected to one side of the reaction kettle and communicated with each other.

[0013] The beneficial effects of the utility model are:

[0014] 1. The cleaning and sewage discharge side actions of the coarse grid, fine grid and membrane grid can be controlled in linkage to ensure that the equipment at each filtration level can work in the best condition, reduce blockage and improve the filtration effect. The generated wastewater is preliminarily treated, including removing large particle impurities, adjusting the pH value, etc. The setting of the acid and alkali water pump is convenient for conveying acid and alkali reagents to the pH adjustment tank, which can effectively adjust the pH value of the sewage. Subsequently, the organic waste is degraded into harmless substances by biodegradation methods. The biochemical treatment technology such as the activated sludge method or the biological filter method is adopted to convert the organic waste into stable inorganic substances through the action of microorganisms, ensuring that the wastewater meets the environmental protection requirements after treatment, and effectively ensuring the effective treatment of the wastewater generated in the production. BRIEF DESCRIPTION OF THE DRAWINGS

[0015] Figure 1 It is a schematic diagram of the overall structure provided by an embodiment of the utility model;

[0016] Figure 2 It is a partial cross-sectional view of the processing box structure provided by the embodiment of the utility model;

[0017] Figure 3 It is a cross-sectional view of the processing box structure provided by the embodiment of the utility model;

[0018] Figure 4 It is a three-dimensional diagram of the structure of a cutting machine provided by an embodiment of the utility model.

[0019] Explanation of the markings in the figure: 1. Treatment box; 2. Cutting box; 3. Filter tank; 4. Sedimentation tank; 5. Disinfection tank; 6. PH adjustment tank; 7. Through hole; 8. Outlet pipe; 9. Top plate; 10. Sol preparation mixing box; 11. Reactor; 12. Operation panel; 13. Connecting wire pipe; 14. Motor; 15. Rotating shaft; 16. Cutting blade; 17. Coarse grid; 18. Fine grid; 19. Membrane grid; 20. Disinfection water pump; 21. First conveying line pipe; 22. Disinfection nozzle; 23. Acid and alkali water pump; 24. Second conveying line pipe; 25. Acid and alkali nozzle; 26. Slide rod; 27. Sliding block; 28. Conveying pipeline; 29. ​​Sewage drainage pipeline; 30. Water inlet pipe. DETAILED DESCRIPTION

[0020] The following will be combined with the drawings in the embodiments of the utility model to clearly and completely describe the technical solutions in the embodiments of the utility model. Obviously, the described embodiments are only part of the embodiments of the utility model, not all of the embodiments. Based on the embodiments in the utility model, all other embodiments obtained by ordinary technicians in this field without creative work are within the scope of protection of the utility model.

[0021] Embodiment 1:

[0022] See also Figure 1-4 , the technical solution provided by this embodiment is as follows:

[0023] A highly efficient production device for silicon nitride particles comprises a processing box 1 and a reaction kettle 11, wherein a cutting box 2 is movably installed on the left side of the inner cavity of the processing box 1, a filtering tank 3 is movably installed on the right side of the cutting box 2, a sedimentation tank 4 is movably installed on the right side of the filtering tank 3, a disinfection tank 5 is movably installed on the right side of the sedimentation tank 4, a pH adjustment tank 6 is movably installed on the right side of the disinfection tank 5, a through hole 7 is opened on the right side of the pH adjustment tank 6, and a water outlet pipe 8 is movably installed in the inner cavity of the through hole 7.

[0024] See also Figure 1 , Figure 3 and Figure 4A top plate 9 is movably installed on the top of the cutting box 2, and a water inlet pipe 30 is arranged on the top of the top plate 9. A sol preparation stirring box 10 is arranged on the top of the reactor 11, and a sewage drainage pipe 29 is fixedly installed on the bottom of the reactor 11. One end of the sewage drainage pipe 29 is fixedly connected to the water inlet pipe 30 and is interconnected. An operation panel 12 is movably installed on the left side of the processing box 1, a connecting wire pipe 13 is fixedly installed on the right side of the operation panel 12, and a motor 14 is fixedly installed on the right side of the connecting wire pipe 13. A rotating shaft 15 is movably installed on the back of the motor 14 and passes through the inner cavity of the cutting box 2, and a cutting blade 16 is movably installed on the surface of the rotating shaft 15. A coarse grid 17 is movably installed on the left side of the inner cavity of the filter tank 3, a fine grid 18 is movably installed on the right side of the coarse grid 17, and a membrane grid 19 is movably installed on the right side of the fine grid 18.

[0025] Specifically, by setting the motor 14 inside the cutting box 2 to drive, the rotating shaft 15 can be driven to rotate and drive the cutting blade 16 to operate, so that the solid matter in the sewage can be cut and crushed, which is convenient for filtering the sewage. By setting the water inlet pipe 30, the sewage can be transported to the cutting box 2, and the coarse grid 17 is used to remove larger solid particles. The wastewater is sent to the coarse grid 17 for preliminary filtration, which can prevent these large particles from clogging the fine grid 18 and the membrane grid 19, and can also protect the fine grid 18 and the membrane grid 19. The fine grid 18 can further remove the particles that the coarse grid 17 fails to remove. The smaller particles and suspended matter are removed, and the solid particles, sediments and turbidity in the water are further filtered to improve the working efficiency of the subsequent treatment equipment. The membrane grille 19 can further remove tiny particles, bacteria and organic matter. Its microporous structure can effectively filter tiny particles and dissolved substances in the water. In conjunction with the membrane grille 19, higher standards of water filtration and improved water quality can be achieved. The cleaning and sewage side actions of the coarse grille 17, fine grille 18 and membrane grille 19 can be controlled in linkage to ensure that equipment at each filtration level can work in the best condition, reduce blockage and improve the filtration effect.

[0026] Embodiment 2:

[0027] See also Figure 1 and Figure 2A disinfection water pump 20 is movably installed on the back of the disinfection tank 5, a first conveying line pipe 21 is movably installed on the top of the disinfection water pump 20, a disinfection nozzle 22 is movably installed on the top of the first conveying line pipe 21, an acid-base water pump 23 is movably installed on the back of the pH adjusting tank 6, a second conveying line pipe 24 is movably installed on the top of the acid-base water pump 23, an acid-base nozzle 25 is movably installed on the top of the second conveying line pipe 24, a sliding rod 26 is movably installed on the top of the disinfection tank 5 and the top of the pH adjusting tank 6, a slider 27 is movably installed on the top of the sliding rod 26, a conveying pipe 28 is fixedly installed on the bottom of the sol preparation stirring box 10, and the end of the conveying pipe 28 is fixedly connected to one side of the reactor 11 and communicated with each other.

[0028] Specifically, the provision of the disinfection water pump 20 facilitates the delivery of disinfectant to the disinfection pool 5, which can effectively disinfect the sewage. The provision of the acid-base water pump 23 facilitates the delivery of acid-base reagents to the pH adjustment pool 6, which can effectively adjust the pH value of the sewage.

[0029] Working principle: The stirring box 10 can be used to mix solvents and solutes to prepare sol through sol preparation. The equipment for converting sol into gel state is usually achieved by controlling parameters such as temperature, humidity, pH value, etc. of the sol. Then, the drying mechanism arranged in the reactor 11 is used to gradually remove moisture from the gel to form dry silicon nitride particles. Then, the wastewater will pass through the sewage drainage pipe 29 and then enter the treatment box 1 through the water inlet pipe 30. The motor 14 arranged inside the cutting box 2 is driven, and at the same time, the rotating shaft 15 can be driven to rotate and drive the cutting blade 16 to operate, so that the solid matter in the sewage can be cut and crushed, which is convenient for filtering sewage. The water inlet pipe 30 can be used to transport sewage to the cutting box 2, and the coarse grid 17 is used to remove larger solid particles and send the wastewater into the coarse grid. The grid 17 performs preliminary filtration to prevent these large particles from clogging the fine grid 18 and the membrane grid 19, and also protects the fine grid 18 and the membrane grid 19. The fine grid 18 can further remove smaller particles and suspended matter that the coarse grid 17 fails to remove, and further filter the solid particles, sediments and turbidity in the water, thereby improving the working efficiency of subsequent treatment equipment. The membrane grid 19 can further remove tiny particles, bacteria and organic matter, and its microporous structure can effectively filter tiny particles and dissolved matter in the water. In conjunction with the membrane grid 19, higher standards of filtration and water quality improvement can be achieved. The sewage can be precipitated by setting the sedimentation tank 4, the disinfectant can be transported to the disinfection tank 5 by the disinfection water pump 20, and the acid-base water pump 23 can transport acid-base reagents to the pH adjustment tank 6.

[0030] In summary: the efficient silicon nitride particle production equipment can be linked and controlled through the cleaning and sewage side actions of the coarse grid 17, the fine grid 18 and the membrane grid 19 to ensure that the equipment at each filtering level can work in the best condition, reduce blockage and improve the filtering effect, and perform preliminary treatment on the generated wastewater, including removing large particle impurities, adjusting the pH value, etc. The setting of the acid-base water pump 23 facilitates the delivery of acid-base reagents to the pH adjustment tank, which can effectively adjust the pH value of the sewage, and then utilizes the biodegradation method to degrade the organic waste into harmless substances. The biochemical treatment technology such as the activated sludge method or the biological filter method is adopted to convert the organic waste into stable inorganic substances through the action of microorganisms, ensuring that the wastewater meets the environmental protection requirements after treatment, effectively ensuring the effective treatment of the wastewater generated in the production, and solving the problem that the current sol-gel production equipment has the problem that the wastewater treatment is difficult during use, a large amount of wastewater will be generated, and the wastewater contains chemical agents and impurities, which puts forward higher requirements for wastewater treatment and is difficult to treat.

[0031] It should be noted that, in this article, relational terms such as first and second, etc. are only used to distinguish one entity or operation from another entity or operation, and do not necessarily require or imply any such actual relationship or order between these entities or operations. Moreover, the terms "include", "comprise" or any other variations thereof are intended to cover non-exclusive inclusion, so that a process, method, article or device that includes a series of elements includes not only those elements, but also other elements not explicitly listed, or also includes elements inherent to such process, method, article or device;

[0032] Although the embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that various changes, modifications, substitutions and variations may be made to the embodiments without departing from the principles and spirit of the present invention, and the scope of the present invention is defined by the appended claims and their equivalents;

[0033] The above description only describes the specific implementation methods of the utility model. Various examples do not limit the essential content of the utility model. Ordinary technicians in the relevant technical field can modify or deform the specific implementation methods described above after reading the description without departing from the essence and scope of the utility model.

Claims

1. An efficient production device for silicon nitride particles, comprising a processing box (1) and a reaction kettle (11), characterized in that: A cutting box (2) is movably mounted on the left side of the inner cavity of the processing box (1), a filtering tank (3) is movably mounted on the right side of the cutting box (2), a sedimentation tank (4) is movably mounted on the right side of the filtering tank (3), a disinfection tank (5) is movably mounted on the right side of the sedimentation tank (4), a pH adjustment tank (6) is movably mounted on the right side of the disinfection tank (5), a through hole (7) is opened on the right side of the pH adjustment tank (6), and a water outlet pipe (8) is movably mounted in the inner cavity of the through hole (7).

2. The high-efficiency production equipment for silicon nitride particles according to claim 1, characterized in that: A top plate (9) is movably mounted on the top of the cutting box (2), a water inlet pipe (30) is arranged on the top of the top plate (9), a sol preparation stirring box (10) is arranged on the top of the reaction kettle (11), a sewage drainage pipe (29) is fixedly mounted on the bottom of the reaction kettle (11), one end of the sewage drainage pipe (29) is fixedly connected to the water inlet pipe (30), and the two are interconnected.

3. The high-efficiency production equipment for silicon nitride particles according to claim 1, characterized in that: An operation panel (12) is movably mounted on the left side of the processing box (1), a connecting wire tube (13) is fixedly mounted on the right side of the operating panel (12), a motor (14) is fixedly mounted on the right side of the connecting wire tube (13), a rotating shaft (15) is movably mounted on the back side of the motor (14) and passes through the inner cavity of the cutting box (2), and a cutting blade (16) is movably mounted on the surface of the rotating shaft (15).

4. The high-efficiency production equipment for silicon nitride particles according to claim 1, characterized in that: A coarse grid (17) is movably mounted on the left side of the inner cavity of the filter tank (3), a fine grid (18) is movably mounted on the right side of the coarse grid (17), and a membrane grid (19) is movably mounted on the right side of the fine grid (18).

5. The high-efficiency production equipment for silicon nitride particles according to claim 1, characterized in that: A disinfection water pump (20) is movably mounted on the back of the disinfection pool (5), a first conveying line pipe (21) is movably mounted on the top of the disinfection water pump (20), and a disinfection nozzle (22) is movably mounted on the top of the first conveying line pipe (21).

6. The high-efficiency production equipment for silicon nitride particles according to claim 1, characterized in that: An acid-base water pump (23) is movably mounted on the back of the pH regulating tank (6), a second conveying line pipe (24) is movably mounted on the top of the acid-base water pump (23), and an acid-base spray nozzle (25) is movably mounted on the top of the second conveying line pipe (24).

7. The high-efficiency production equipment for silicon nitride particles according to claim 1, characterized in that: A slide bar (26) is movably mounted on the top of the disinfection tank (5) and the top of the pH adjustment tank (6), and a slider (27) is movably mounted on the top of the slide bar (26).

8. The high-efficiency production equipment for silicon nitride particles according to claim 2, characterized in that: A delivery pipe (28) is fixedly installed at the bottom of the sol preparation stirring box (10), and the end of the delivery pipe (28) is fixedly connected to one side of the reaction kettle (11) and communicated with each other.

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