Efficient ionone purification device

Abstract

The utility model belongs to the technical field of purification devices, and discloses an efficient ionone purification device which comprises a purification tank and a heating pad, a beaker is attached to the top end of the heating pad, a cavity is formed in the beaker, a condensation pipe is arranged in the cavity of the beaker in a penetrating mode, and a liquid outlet is formed in the outer side of the condensation pipe in a penetrating mode. A supporting sliding ring is connected to the outer side of the liquid outlet in a sleeving mode, a collecting box is arranged at the bottom end of the liquid outlet, a filter screen is slidably connected into the collecting box, and a circular groove is formed in the filter screen. And after the container is used, substances are adhered to the inner wall and are difficult to clean manually.

Description

Technical Field

[0001] The utility model belongs to the technical field of purification devices, in particular to a high-efficiency ionone purification device. Background Art

[0002] β-ionone is an important synthetic flavor and an important intermediate for synthesizing vitamin A in the pharmaceutical industry. It can be cyclized under acidic conditions after the condensation of citral and acetone to generate pseudoionone.

[0003] At the same time, the patent with application number 202022126843.X discloses a device for continuously preparing pseudoionone, including a packed tower, an acetone tank, an alkali liquid tank, a citral tank, a liquid storage tank and a product tank; the outlet of the acetone tank and the outlet of the alkali liquid tank are connected to the top of the packed tower through a pipe; the outlet of the citral tank is connected to the bottom of the packed tower through a pipe; the liquid outlet at the bottom of the packed tower is connected to the liquid storage tank through a pipe.

[0004] However, in the implementation of relevant technologies, it was found that the above-mentioned device for preparing pseudoionone by a continuous method has separation difficulties and high viscosity. During the production process, it is processed through a container, and substances will adhere to the inner wall of the container after use, which is difficult to clean manually. Utility Model Content

[0005] In order to solve the problems raised in the above-mentioned background technology, the utility model provides a high-efficiency purification device for ionone, which has the advantages of separating impurities from ionone by centrifugal force, extracting objects inside the solution by high temperature, generating steam through continuous heating, and filtering, and finally obtaining ionone with higher purity.

[0006] To achieve the above-mentioned purpose, the utility model provides the following technical solutions: a highly efficient purification device for ionone, comprising a purification tank and a heating pad, a beaker is attached to the top of the heating pad, a cavity is arranged inside the beaker, a condenser is penetrated inside the cavity of the beaker, a liquid outlet is penetrated on the outside of the condenser, a support slip ring is sleeved on the outside of the liquid outlet, a collecting box is arranged at the bottom end of the liquid outlet, a filter screen is slidably connected to the inside of the collecting box, and a circular groove is opened inside the filter screen.

[0007] Preferably, the interior of the purification tank is configured as a cavity, a driving source is provided at the top of the purification tank, the output end of the driving source is arranged through the cavity of the purification tank, the output end of the driving source is fixedly connected to an extension rod, the bottom end of the extension rod is fixedly connected to a stirring rod, a protective shell is provided on the outside of the stirring rod, and the protective shell is arranged inside the cavity of the purification tank.

[0008] Preferably, a feed port is fixedly connected to the top of the purification tank, a feed rod is fixedly connected to the bottom of the feed port, and the feed rod is arranged inside the cavity of the purification tank.

[0009] Preferably, a centrifuge is sleeved on the outer side of the feed rod, the interior of the centrifuge is arranged as a cavity, a circular hole groove is opened on the outer side of the cavity of the centrifuge, the circular hole groove of the centrifuge is arranged in several groups, and the bottom end of the centrifuge is rotatably connected to a rotating base.

[0010] Preferably, a connecting pipe is provided through the left side of the purification tank, and the connecting pipe is provided through the left side of the beaker.

[0011] Preferably, a water spray pipe is provided inside the cavity of the purification tank, a slide groove is opened inside the water spray pipe, an extension pipe is slidably connected inside the slide groove of the water spray pipe, the bottom end of the extension pipe is rotatably connected to a first rotating arm, and a second rotating arm is fixedly connected to the outer side of the first rotating arm.

[0012] Preferably, a cleaning plate is fixedly connected to the outer side of the second rotating arm, a slide groove is provided inside the cleaning plate, a scraper is slidably connected inside the slide groove of the cleaning plate, and the outer side of the scraper is tightly arranged on the inner wall of the cavity of the purification tank.

[0013] Compared with the prior art, the beneficial effects of the utility model are as follows:

[0014] 1. The utility model adds a stirring device inside the purification tank to break up the ionone, then puts in the additive to dissolve and dilute it, and finally separates the mixed ionone by centrifugal force. At this time, the ionone is thrown out of the outside of the centrifuge, and the solution enters the inside of the beaker through the connecting pipe.

[0015] 2. The utility model heats the beaker by means of a heating pad. At this time, the substances inside the beaker have different boiling points, causing ionone to vaporize and enter the interior of the condenser. At this time, the ionone passing through the interior of the condenser passes through a cold medium, vaporizes and becomes liquefied, flows out from the interior of the liquid outlet, enters the interior of the collection box, and is filtered through the filter net at the top. BRIEF DESCRIPTION OF THE DRAWINGS

[0016] Figure 1 It is a schematic diagram of the overall structure of the utility model;

[0017] Figure 2 This is a schematic diagram of the structure of the water spray pipe of the utility model;

[0018] Figure 3 This is a schematic diagram of the structure of the purification tank of the utility model;

[0019] Figure 4 This is a schematic diagram of the structure of the centrifuge of the utility model;

[0020] Figure 5 This is a schematic diagram of the protective shell structure of the utility model.

[0021] In the figure: 1. purification tank; 101. connecting pipe; 2. driving source; 201. extension rod; 202. stirring rod; 203. feed port; 204. feed rod; 205. protective shell; 206. rotating base; 3. centrifuge; 4. heating pad; 401. beaker; 402. condenser; 403. support slip ring; 404. liquid outlet; 405. collection box; 406. filter; 5. water spray pipe; 501. extension pipe; 502. first rotating arm; 503. second rotating arm; 504. cleaning plate; 505. scraper. DETAILED DESCRIPTION

[0022] The following will be combined with the drawings in the embodiments of the utility model to clearly and completely describe the technical solutions in the embodiments of the utility model. Obviously, the described embodiments are only part of the embodiments of the utility model, not all of the embodiments. Based on the embodiments in the utility model, all other embodiments obtained by ordinary technicians in this field without creative work are within the scope of protection of the utility model.

[0023] like Figures 1 to 5 As shown, the utility model provides a highly efficient purification device for ionone, comprising a purification tank 1 and a heating pad 4, a beaker 401 is placed on the top of the heating pad 4, a condenser 402 is provided through the cavity of the beaker 401, a liquid outlet 404 is provided through the outside of the condenser 402, a support slip ring 403 is sleeved on the outside of the liquid outlet 404, a collecting box 405 is provided at the bottom of the liquid outlet 404, a filter screen 406 is slidably connected to the inside of the collecting box 405, a circular groove is provided inside the filter screen 406, the heating pad 4 heats the beaker 401, at this time, the substance inside the beaker 401 has different boiling points, causing the ionone to vaporize and enter the inside of the condenser 402, at this time, the ionone passing through the inside of the condenser 402 is vaporized and liquefied when passing through the cold medium, and flows out from the inside of the liquid outlet 404, at this time entering the inside of the collecting box 405, and being filtered through the filter screen 406 at the top.

[0024] Specifically, the interior of the purification tank 1 is configured as a cavity, a driving source 2 is provided at the top of the purification tank 1, the output end of the driving source 2 is arranged through the cavity of the purification tank 1, the output end of the driving source 2 is fixedly connected to an extension rod 201, the bottom end of the extension rod 201 is fixedly connected to a stirring rod 202, a protective shell 205 is provided on the outside of the stirring rod 202, and the protective shell 205 is arranged in the cavity of the purification tank 1. By adding a stirring device, ionone is broken up, and then additives are added to dissolve and dilute them. Finally, the mixed ionone is separated by centrifugal force. At this time, ionone is thrown out of the outside of the centrifuge 3, and the solution enters the inside of the beaker 401 through the connecting pipe 101.

[0025] Furthermore, ionone is placed inside the feed port 203 at the top of the purification tank 1 , and then ionone enters the inside of the feed rod 204 through the feed port 203 , and the feed rod 204 is arranged inside the cavity of the purification tank 1 .

[0026] Furthermore, the outer side of the feed rod 204 is sleeved with a centrifuge 3, the interior of the centrifuge 3 is set as a cavity, the outer side of the cavity of the centrifuge 3 is provided with a circular hole groove, the circular hole groove of the centrifuge 3 is provided with a plurality of groups, and the bottom end of the centrifuge 3 is rotatably connected to a rotating base 206, the centrifuge 3 is rotated by the rotating base 206, and the solution is separated by the action of centrifugal force.

[0027] It is worth noting that a connecting pipe 101 is provided through the left side of the purification tank 1 , and the connecting pipe 101 is provided through the left side of the beaker 401 , so that the treated solution flows into the interior of the beaker 401 through the connecting pipe 101 .

[0028] It is worth noting that a water spray pipe 5 is provided inside the cavity of the purification tank 1, and a slide groove is opened inside the water spray pipe 5. An extension pipe 501 is slidably connected to the slide groove of the water spray pipe 5 to spray water on ionone, and the outer side of the first rotating arm 502 drives the second rotating arm 503 to rotate.

[0029] It is worth mentioning that a cleaning plate 504 is welded to the outer side of the second rotating arm 503, and a slide groove is opened inside the cleaning plate 504. At this time, the scraper 505 slides out from the slide groove of the cleaning plate 504, and the outer side of the scraper 505 rotates in the cavity of the purification tank 1 and scrapes it clean for the next use.

[0030] Among them, the driving source 2 is the prior art and will not be described in detail;

[0031] Working principle:

[0032] First, the staff pours ionone into the feed port 203 at the top of the purification tank 1. At this time, ionone passes through the inside of the feed rod 204, and is driven by the extension rod 201 at the bottom of the driving source 2 to disperse in the inside of the protective shell 205, and enters the inside of the centrifuge 3. The additive is poured into the inside of the centrifuge 3 and mixed. At this time, the speed of the centrifuge 3 is increased. The high-speed rotating centrifuge 3 fully mixes and stirs the ionone inside. The ionone and the additive are mixed to produce solid impurities. At this time, the fixed impurities remain in the inside of the centrifuge 3. The mixed liquid is thrown out of the inner cavity of the purification tank 1 through the inside of the centrifuge 3. At this time, the liquid flows from the connecting pipe 101 outside the purification tank 1 to the inside of the beaker 401, and the heating pad 4 is turned on to heat the beaker 401. At this time, the substances in the beaker 401 have different boiling points, causing the ionone to vaporize and enter the inside of the condenser 402. At this time, the ionone passing through the inside of the condenser 402 is vaporized and liquefied when passing through the cold medium, and flows out from the inside of the liquid outlet 404, and then enters the inside of the collection box 405, and is filtered through the filter screen 406 at the top;

[0033] When the purification tank 1 is finished using, start the switch, and the water spray pipe 5 and the extension pipe 501 at the bottom are used to rinse the inner wall of the purification tank 1. The first rotating arm 502 drives the second rotating arm 503 to press the cleaning plate 504 against the inside of the purification tank 1, and the scraper 505 is extended to scrape the purification tank 1 clean for the next use.

[0034] It should be noted that, in this article, relational terms such as first and second, etc. are only used to distinguish one entity or operation from another entity or operation, and do not necessarily require or imply any such actual relationship or order between these entities or operations. Moreover, the terms "include", "comprise" or any other variants thereof are intended to cover non-exclusive inclusion, so that a process, method, article or device including a series of elements includes not only those elements, but also other elements not explicitly listed, or also includes elements inherent to such process, method, article or device.

[0035] Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that various changes, modifications, substitutions and variations may be made to the embodiments without departing from the principles and spirit of the present invention, and that the scope of the present invention is defined by the appended claims and their equivalents.

Claims

1. An efficient ionone purification device, comprising a purification tank (1) and a heating pad (4), characterized in that: A beaker (401) is attached to the top of the heating pad (4), a cavity is provided inside the beaker (401), a condenser (402) is provided through the cavity of the beaker (401), a liquid outlet (404) is provided through the outside of the condenser (402), a support slip ring (403) is sleeved on the outside of the liquid outlet (404), a collecting box (405) is provided at the bottom of the liquid outlet (404), a filter screen (406) is slidably connected to the inside of the collecting box (405), and a circular groove is provided inside the filter screen (406).

2. The device for efficiently purifying ionone according to claim 1, characterized in that: The interior of the purification tank (1) is arranged as a cavity. A driving source (2) is arranged at the top of the purification tank (1). The output end of the driving source (2) is arranged through the cavity of the purification tank (1). The output end of the driving source (2) is fixedly connected to an extension rod (201). The bottom end of the extension rod (201) is fixedly connected to a stirring rod (202). A protective shell (205) is arranged on the outside of the stirring rod (202). The protective shell (205) is arranged inside the cavity of the purification tank (1).

3. The device for efficiently purifying ionone according to claim 2, characterized in that: The top end of the purification tank (1) is fixedly connected to a feed port (203), the bottom end of the feed port (203) is fixedly connected to a feed rod (204), and the feed rod (204) is arranged inside the cavity of the purification tank (1).

4. The device for efficiently purifying ionone according to claim 3, characterized in that: The outer side of the feed rod (204) is sleeved with a centrifuge (3), the interior of the centrifuge (3) is arranged as a cavity, the outer side of the cavity of the centrifuge (3) is provided with a circular hole groove, the circular hole groove of the centrifuge (3) is arranged in a plurality of groups, and the bottom end of the centrifuge (3) is rotatably connected to a rotating base (206).

5. The device for efficiently purifying ionone according to claim 3, characterized in that: A connecting pipe (101) is provided through the left side of the purification tank (1), and the connecting pipe (101) is provided through the left side of the beaker (401).

6. The device for efficiently purifying ionone according to claim 5, characterized in that: A water spray pipe (5) is arranged inside the cavity of the purification tank (1), a slide groove is provided inside the water spray pipe (5), an extension pipe (501) is slidably connected inside the slide groove of the water spray pipe (5), a first rotating arm (502) is rotatably connected to the bottom end of the extension pipe (501), and a second rotating arm (503) is fixedly connected to the outer side of the first rotating arm (502).

7. The device for efficiently purifying ionone according to claim 6, characterized in that: A cleaning plate (504) is fixedly connected to the outer side of the second rotating arm (503), a sliding groove is provided inside the cleaning plate (504), a scraper (505) is slidably connected inside the sliding groove of the cleaning plate (504), and the outer side of the scraper (505) is tightly arranged on the inner wall of the cavity of the purification tank (1).

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