Reaction kettle for removing sodium ions
By designing a reactor for sodium ion removal, the synergistic effect of the removal chamber and the filter chamber is used to solve the problem of difficult control of sodium ion content in the traditional sodium process, and efficient sodium ion removal and high-purity production of iron phosphate are achieved.
Patent Information
- Application Number
- CN202421588424.X
- Authority / Receiving Office
- CN · China
- Patent Type
- Utility models(China)
- Current Assignee / Owner
- Filing Date
- 2024-07-07
- Publication Date
- 2025-05-09
- Estimated Expiration
- 2034-07-07
AI Technical Summary
The traditional sodium process is difficult to effectively control the content of sodium ions during the synthesis of iron phosphate dihydrate, resulting in the exceeding the standard of sodium ions in the final product and unable to meet the high purity requirements of downstream customers for iron phosphate materials.
A reactor for sodium ion removal is designed, including a removal chamber and a filter chamber, equipped with an electric heating block, a stirring rod and a removable filter basket, so as to achieve efficient removal of sodium ions through synergistic action.
By precisely controlling the reaction temperature and stirring, the complete removal of sodium ions is achieved, and the purity and market competitiveness of iron phosphate are improved.
Smart Images

Figure CN222842102U_ABST
Abstract
Description
Technical Field
[0001] The utility model belongs to the technical field of chemical equipment, and particularly relates to a reaction kettle for removing sodium ions. Background Art
[0002] Iron phosphate is a key positive electrode material for lithium batteries, and its production process has an important impact on battery performance. In the production process of iron phosphate, the sodium ion content is a key indicator, because high sodium content will directly affect the discharge performance and overall quality of lithium iron phosphate batteries.
[0003] At present, the production methods of ferric phosphate are mainly divided into sodium method and ammonia method. The sodium method is widely used because of its easy availability of raw materials and relatively low cost. However, the traditional sodium method is often difficult to effectively control the sodium ion content during the synthesis of ferric phosphate dihydrate, resulting in excessive sodium ions in the final product, making it difficult to meet the high purity requirements of downstream customers for ferric phosphate materials. Utility Model Content
[0004] The utility model provides a reaction kettle for removing sodium ions, aiming to solve the problem that it is difficult to effectively control the sodium ion content in the synthesis process of ferric phosphate dihydrate in the traditional sodium process.
[0005] The utility model is implemented as follows: a sodium ion removal reactor, comprising: a sodium ion removal reactor body, the reactor body being provided with a removal chamber and a filter chamber connected and distributed up and down; an electric heating block, the electric heating block being arranged on the inner wall of the removal chamber for heating; a stirring rod, the stirring rod being rotatably mounted on the reactor body, the bottom end of the stirring rod extending into the removal chamber for stirring a sodium ion solution to be removed; a first motor, the first motor being fixedly mounted on the top of the reactor body, the output shaft of the first motor being fixedly connected to the top end of the stirring rod through a coupling; a detachable filter basket, the filter basket being arranged in the filter chamber for filtering liquid after sodium ions are removed; a first drain pipe for discharging liquid into the filter basket, the first drain pipe being fixedly connected to the bottom of the removal chamber, the first drain pipe being provided with a first solenoid valve; a cleaning mechanism for cleaning impurities in the filter basket, the cleaning mechanism being arranged on the filter basket.
[0006] Preferably, the cleaning mechanism includes: a transmission rod vertically rotatably installed on the top of the filter basket, the bottom end of the transmission rod extending into the filter basket; a cleaning brush fixed to the bottom end of the transmission rod for cleaning the filter basket; a second motor fixed to the top of the filter basket for driving the transmission rod to rotate, the output shaft of the second motor being fixedly connected to the top end of the transmission rod via a coupling.
[0007] Preferably, groove blocks are symmetrically fixedly installed on the inner wall of the filter cavity, and a pull-out and detachable connecting block is provided on the groove block, and one end of the connecting block is fixedly connected to the filter basket.
[0008] Preferably, the groove block is provided with a pin rod that can be pulled and removed, and the bottom end of the pin rod passes through the connecting block.
[0009] Preferably, a pH detector is fixedly installed on the top of the reactor body, and the monitoring end of the pH detector extends into the removal chamber. A feeding pipe is fixedly connected to the top of the reactor body, and the feeding end of the feeding pipe extends into the removal chamber. A hopper is fixedly installed on the top of the feeding pipe, a cover plate is hinged on the top of the hopper, and a handle is fixedly installed on the top of the cover plate.
[0010] Preferably, the bottom of the filter cavity is fixedly connected to a second liquid discharge pipe, a second solenoid valve is arranged on the second liquid discharge pipe, and a temperature controller is arranged on one side of the reactor body, and the temperature controller is adapted to the electric heating block.
[0011] Preferably, an exhaust pipe is fixedly installed on the top of the reactor body, the air inlet end of the exhaust pipe extends into the removal chamber, and an automatic air release valve is arranged on the outlet end of the exhaust pipe.
[0012] Compared with the related art, the reactor for removing sodium ions provided by the utility model has the following beneficial effects:
[0013] The removal chamber and the filtration chamber are responsible for the removal of sodium ions and the filtration of liquid respectively. Through the synergistic effect of these two chambers, an efficient and thorough sodium ion removal process is achieved; the electric heating block improves the reaction rate and efficiency by accurately controlling the reaction temperature, and at the same time helps the dissolution and subsequent removal of sodium ions; the stirring rod and the first motor ensure the uniform mixing of the reactants through stirring, promote the uniform progress of the reaction, and improve the reaction efficiency; the detachable filter basket facilitates the collection and cleaning of solids after filtration, and is also easy to replace and maintain, ensuring the filtration effect; the first discharge pipe and the first solenoid valve: realize automatic discharge control of liquid and improve the level of production automation. BRIEF DESCRIPTION OF THE DRAWINGS
[0014] Figure 1 This is a schematic diagram of the main structure of a sodium ion removal reactor provided by the utility model;
[0015] Figure 2 This is a schematic diagram of the main cross-sectional structure of the utility model;
[0016] Figure 3 for Figure 2 An enlarged structural diagram of part A shown in FIG.
[0017] Figure 4 It is a structural schematic diagram of the filter basket in the utility model.
[0018] Figure numerals: 1. Reactor body; 2. Removal chamber; 3. Filter chamber; 4. Electric heating block; 5. Stirring rod; 6. First motor; 7. Filter basket; 8. First drain pipe; 9. First solenoid valve; 10. Transmission rod; 11. Cleaning brush; 12. Second motor; 13. Second drain pipe; 14. Second solenoid valve; 15. Groove block; 16. Connecting block; 17. Pin rod; 18. PH detector; 19. Feeding pipe; 20. Exhaust pipe. DETAILED DESCRIPTION
[0019] Unless otherwise defined, all technical and scientific terms used herein have the same meaning as those commonly understood by technicians in the technical field of this application; the terms used in the specification of the application herein are only for the purpose of describing specific embodiments and are not intended to limit this application; the terms "including" and "having" and any variations thereof in the specification and claims of this application and the above-mentioned drawings are intended to cover non-exclusive inclusions. The terms "first", "second", etc. in the specification and claims of this application or the above-mentioned drawings are used to distinguish different objects, not to describe a specific order.
[0020] Reference to "embodiments" herein means that a particular feature, structure, or characteristic described in conjunction with the embodiments may be included in at least one embodiment of the present application. The appearance of the phrase in various locations in the specification does not necessarily refer to the same embodiment, nor is it an independent or alternative embodiment that is mutually exclusive with other embodiments. It is explicitly and implicitly understood by those skilled in the art that the embodiments described herein may be combined with other embodiments.
[0021] The utility model embodiment provides a sodium ion removal reactor, such as Figure 1-4As shown, the reactor for sodium ion removal comprises: a reactor body 1 for sodium ion removal, the reactor body 1 is provided with a removal chamber 2 and a filter chamber 3 which are connected and distributed up and down; an electric heating block 4, the electric heating block 4 is arranged on the inner wall of the removal chamber 2 for heating; a stirring rod 5, the stirring rod 5 is rotatably mounted on the reactor body 1, and the bottom end of the stirring rod 5 extends into the removal chamber 2 for stirring the sodium ion solution to be removed; a first motor 6, the first motor 6 is fixedly mounted on the top of the reactor body 1, and the output shaft of the first motor 6 is fixedly connected to the top of the stirring rod 5 through a coupling; a detachable filter basket 7, the filter basket 7 is arranged in the filter chamber 3 for filtering the liquid after the sodium ions are removed; a first drain pipe 8 for discharging liquid into the filter basket 7, the first drain pipe 8 is fixedly connected to the bottom of the removal chamber 2, and a first solenoid valve 9 is arranged on the first drain pipe 8; a cleaning mechanism for cleaning impurities in the filter basket 7, the cleaning mechanism is arranged on the filter basket 7.
[0022] It should be noted that there are various methods for producing ferric phosphate, among which the sodium method and the ammonia method (or ammonium method) are the two mainstream processes. The sodium method, also known as the phosphoric acid method, mainly uses raw materials such as phosphoric acid, liquid alkali (such as sodium hydroxide) and ferrous sulfate to react and adjust the pH value to produce ferric phosphate. This process is widely used because its raw materials are easily available and the cost is relatively low. However, the traditional sodium method does face some challenges in the synthesis of ferric phosphate dihydrate, especially in controlling the sodium ion content; in the sodium method, raw materials such as phosphoric acid and liquid alkali themselves contain a certain amount of sodium ions. These sodium ions may not fully participate in the reaction during the reaction, or enter the final product through certain side reactions, resulting in excessive sodium ion content in ferric phosphate; in the reaction process, pH adjustment is one of the key steps. However, even with the use of precise pH control equipment, pH fluctuations may occur due to improper operation or equipment accuracy limitations, which in turn affects the removal effect of sodium ions; although the sodium ion content in the product can be reduced through subsequent separation and purification steps, these steps often increase production costs and process complexity. At the same time, existing separation and purification technologies may not be able to completely remove all sodium ions, resulting in a certain amount of sodium ions in the final product; excessive sodium ions will directly affect the purity of iron phosphate, reducing its performance as a battery material or in other application areas. For example, in the battery industry, the purity of iron phosphate has an important impact on key indicators such as battery energy density, cycle life and safety; due to the high purity requirements of downstream customers for iron phosphate materials, excessive sodium ions may cause the product to fail to meet customer needs, thereby affecting the market competitiveness and customer satisfaction of the product. Based on the above, a sodium ion removal reactor is needed to solve the above problems;
[0023] In this embodiment, the reactor body 1 is the core frame of the whole equipment, carrying all functional components; the removal chamber 2 is the main place where the sodium ion removal reaction occurs. By carrying out chemical reactions in this area, the preliminary removal of sodium ions is achieved; the filter chamber 3 is used to filter the liquid after the sodium ions are removed, further remove impurities and residual sodium ions, and improve the purity of the product; the electric heating block 4 is arranged in the removal chamber 2, and promotes the chemical reaction by heating, improves the reaction rate and efficiency, and at the same time, proper heating also helps to improve the solubility of sodium ions, which is convenient for subsequent removal operations; the stirring rod 5 rotates in the removal chamber 2, and the reactants are fully mixed by stirring to ensure that the reaction is carried out evenly; the first motor 6 is the power source of the stirring rod 5, and is fixedly connected to the top of the stirring rod 5 through a coupling to realize the rotation drive of the stirring rod. This design not only simplifies the transmission structure, but also improves the stirring efficiency; the detachable filter basket 7 is arranged in the filter chamber 3, which is used to filter the liquid after the sodium ions are removed. Its detachable design is convenient for cleaning and replacement, and ensures the filtering effect; the first drain pipe 8 introduces the liquid in the removal chamber 2 into the filter chamber 3 for filtering. By setting the first solenoid valve 9, the drainage time and flow rate can be accurately controlled to ensure the smooth progress of the filtration process; the cleaning mechanism is used to regularly clean the impurities in the filter basket 7 to prevent blockage and affect the filtration effect; when removing sodium ions, the dihydrate iron phosphate with a relatively high sodium ion content (150-300ppm) after conventional washing is re-pulped, and the re-pulping concentration is adjusted to 20%-30% to ensure the uniformity and efficiency of the subsequent reaction; the re-pulped dihydrate iron phosphate slurry is sent into the removal chamber 2 of the reactor body 1 to prepare for the deep removal of sodium ions; the slurry is heated to 80±5°C by the electric heating block 4, and the acidification reaction is promoted by the increase in temperature; at the same time, a certain amount of sulfuric acid is added to the slurry. By precisely controlling the amount of addition, the pH value of the slurry is adjusted to 0.5±0.5. This step is the key to removing sodium ions. The sodium ions are converted into soluble sodium salts through the acidification reaction. The first motor 6 drives the stirring rod 5 to rotate, and the bottom end of the stirring rod 5 fully stirs the slurry in the removal chamber 2 to ensure that the sulfuric acid and the slurry are evenly mixed, thereby improving the efficiency and uniformity of the acidification reaction. After the acidification reaction is completed, the liquid containing the soluble sodium salt is discharged into the filter basket 7 in the filter chamber 3 through the first drainage pipe 8. The first solenoid valve 9 controls the drainage process to ensure that the drainage is smooth and easy to control. The filter basket 7 filters the liquid to intercept the solid impurities and incompletely dissolved substances therein, and the solution containing the removed sodium ions is discharged through the filter basket 7.
[0024] In a further preferred embodiment of the utility model, the cleaning mechanism includes: a transmission rod 10 vertically rotatably installed on the top of the filter basket 7, the bottom end of the transmission rod 10 extends into the filter basket 7; a cleaning brush 11 fixed on the bottom end of the transmission rod 10 for cleaning the filter basket 7; a second motor 12 fixed on the top of the filter basket 7 for driving the transmission rod 10 to rotate, and the output shaft of the second motor 12 is fixedly connected to the top of the transmission rod 10 through a coupling.
[0025] In this embodiment, an efficient cleaning mechanism is designed to solve the cleaning problem of impurities in the filter basket 7; the transmission rod 10 is rotatably mounted on the filter basket 7, and its bottom end extends into the filter basket 7. The transmission rod 10 serves as a support and transmission component for the cleaning brush 11, and drives the cleaning brush 11 to clean the inside of the filter basket 7 through rotational motion; the cleaning brush 11 is fixed at the bottom end of the transmission rod 10, and is used to directly contact and clean the impurities on the inner wall of the filter basket 7 and the filter screen. The material and shape of the cleaning brush 11 need to be selected according to the specific structure of the filter basket 7 and the impurity characteristics to ensure the cleaning effect; the second motor 12 is fixed at the top of the filter basket 7, and is used to drive the transmission rod 10 to rotate. The output shaft of the second motor 12 is fixedly connected to the top of the transmission rod 10 through a coupling to realize power transmission. The cleaning mechanism realizes automatic cleaning of impurities inside the filter basket 7 in a mechanized manner, avoids large-scale clogging of the filter surface of the filter basket 7, and the cleaned impurities gather together, which is also convenient for subsequent centralized cleaning.
[0026] In a further preferred embodiment of the utility model, a groove block 15 is symmetrically fixedly installed on the inner wall of the filter chamber 3, and a removable connecting block 16 is provided on the groove block 15, and one end of the connecting block 16 is fixedly connected to the filter basket 7.
[0027] In this embodiment, groove blocks 15 are symmetrically fixedly installed on the inner wall of the filter chamber 3. These groove blocks 15 provide a stable installation position for the connection block 16 and ensure the accurate positioning of the filter basket 7 in the filter chamber 3; one end of the connection block 16 is fixedly connected to the filter basket 7, and the other end can be inserted into the groove block 15. The connection block 16 is designed as a removable structure, so that the user can remove or install the filter basket 7 from the filter chamber 3 through simple operations; due to the removable design between the connection block 16 and the groove block 15, the user can complete the replacement of the filter basket 7 without complicated tools or cumbersome steps. This greatly improves the maintenance efficiency of the equipment and reduces the difficulty of operation.
[0028] In a further preferred embodiment of the present invention, a detachable pin rod 17 is disposed on the groove block 15 , and the bottom end of the pin rod 17 passes through the connecting block 16 .
[0029] In this embodiment, in order to solve the problem of fixing and removing the filter basket 7 in the filter chamber 3, a pin rod 17 that can be lifted and removed is provided on the groove block 15, so that the filter basket 7 can be quickly installed and removed; this design further simplifies the operation process and improves the maintenance efficiency and flexibility of the equipment; the groove block 15 serves as the installation base of the filter basket 7 in the filter chamber 3, and a pin hole for installing the pin rod 17 is newly added on the groove block 15. This ensures that the pin rod 17 can be firmly installed on the groove block 15; the pin rod 17 can be lifted and removed. The bottom end of the pin rod 17 passes through the connecting block 16, and the connecting block 16 (and then the filter basket 7) is fixed to the groove block 15 through physical connection; when the filter basket 7 needs to be removed, it is only necessary to lift the pin rod 17 to separate it from the connecting block 16.
[0030] In a further preferred embodiment of the utility model, a pH detector 18 is fixedly installed on the top of the reactor body 1, and the monitoring end of the pH detector 18 extends into the removal chamber 2. A feeding pipe 19 is fixedly connected to the top of the reactor body 1, and the feeding end of the feeding pipe 19 extends into the removal chamber 2. A hopper is fixedly installed on the top of the feeding pipe 19, and a cover plate is hinged on the top of the hopper, and a handle is fixedly installed on the top of the cover plate.
[0031] In this embodiment, a pH detector 18 and a feeding pipe 19 and their supporting structures are particularly added. These designs enable the reactor to monitor the pH value in the removal chamber 2 in real time and conveniently add reaction materials as needed; pH detector 18: The pH detector 18 is fixedly installed on the top of the reactor body 1, and its monitoring end extends into the removal chamber 2. The pH detector 18 can monitor the pH value of the liquid in the removal chamber 2 in real time, and feed back the data to the control system or the operator, so as to adjust the reaction conditions or add neutralizers and other substances in time to ensure the stability of the reaction process and the quality of the product; the top of the reactor body 1 is also fixedly connected to the feeding pipe 19, and its feeding end also extends into the removal chamber 2. The feeding pipe 19 is used to add the materials required for the reaction into the removal chamber 2. A hopper is fixedly installed on the top of the feeding pipe 19, and a cover plate is hinged on the top of the hopper, and a handle is also fixedly installed on the top of the cover plate. This design allows the user to easily open the cover plate and pour the material into the hopper, and the material then enters the removal chamber 2 through the feeding pipe 19 to participate in the reaction.
[0032] In a further preferred embodiment of the utility model, the bottom of the filter chamber 3 is fixedly connected to a second liquid discharge pipe 13, a second solenoid valve 14 is provided on the second liquid discharge pipe 13, and a temperature controller is provided on one side of the reactor body, and the temperature controller is adapted to the electric heating block 4.
[0033] In this embodiment, a second drain pipe 13 is fixedly connected to the bottom of the filter chamber 3 for discharging the filtered liquid; a second solenoid valve 14 is arranged on the second drain pipe 13 for controlling the opening and closing of the drainage process. By accurately controlling the opening and closing time and opening degree of the solenoid valve, precise control of the drainage process can be achieved to ensure that the drainage can be carried out only when needed and the drainage amount is controllable; a thermostat is arranged on one side of the reactor body for monitoring and controlling the temperature inside the reactor. The thermostat is adapted to the electric heating block 4 and can automatically adjust the heating power of the electric heating block 4 according to the set temperature value to maintain the constant temperature inside the reactor.
[0034] In a further preferred embodiment of the utility model, an exhaust pipe 20 is fixedly installed on the top of the reactor body 1, the air inlet end of the exhaust pipe 20 extends into the removal chamber 2, and an automatic air release valve is provided on the outlet end of the exhaust pipe 20.
[0035] In this embodiment, in view of the gas pressure problem that may be generated during the operation of the reactor body 1, an exhaust pipe 20 and its matching automatic air release valve are specially designed. This design is intended to ensure the stability of the internal pressure of the reactor, prevent safety hazards caused by excessive pressure, and improve the overall safety and reliability of the equipment; the exhaust pipe 20 is fixedly installed on the top of the reactor body 1, and its air inlet end extends into the removal chamber 2, directly connected to the area where gas may be generated inside the reactor, so that when gas is generated in the removal chamber 2 due to chemical reaction or heating process, these gases can be smoothly discharged through the exhaust pipe 20; an automatic air release valve is set at the outlet end of the exhaust pipe 20, and the automatic air release valve is a valve that can automatically open or close according to the pressure change in the pipeline. When the internal pressure of the reactor exceeds the set value, the automatic air release valve will automatically open to release excess gas, thereby maintaining the stability of the internal pressure of the reactor. Conversely, when the pressure drops to a safe range, the automatic air release valve will automatically close to prevent external air or impurities from entering the reactor.
[0036] In summary, the sodium ion removal reactor provided by the technical solution effectively solves the problem of excessive sodium ion content in the production process of iron phosphate in the sodium process through structural optimization design, precise control, efficient removal and filtration, re-slurry treatment and uniform reaction, and improves the purity and market competitiveness of the product.
[0037] Compared with the related art, the removal chamber 2 and the filtration chamber 3 are respectively responsible for the removal of sodium ions and the filtration of liquid. Through the synergistic effect of the two chambers, an efficient and thorough sodium ion removal process is achieved; the electric heating block 4 improves the reaction rate and efficiency by accurately controlling the reaction temperature, and at the same time helps the dissolution and subsequent removal of sodium ions; the stirring rod 5 and the first motor 6 ensure uniform mixing of the reactants through stirring, promote the uniform progress of the reaction, and improve the reaction efficiency; the detachable filter basket 7 facilitates the collection and cleaning of solids after filtration, and is also easy to replace and maintain, ensuring the filtration effect; the first drain pipe 8 and the first solenoid valve 9: realize automatic discharge control of the liquid and improve the level of automation in production.
[0038] It is worth noting that the circuits, electronic components and modules involved in the present utility model are all prior art and can be fully implemented by those skilled in the art. Needless to say, the content protected by the present utility model does not involve improvements to software and methods.
[0039] In the several embodiments provided in the present application, it should be understood that the disclosed device can be implemented in other ways. For example, the device embodiments described above are only schematic, such as the division of the above-mentioned units, which is only a logical function division. There may be other division methods in actual implementation, such as multiple units or components can be combined or integrated into another system, or some features can be ignored or not executed. Another point is that the mutual coupling or communication connection shown or discussed can be through some interfaces, and the indirect coupling or communication connection between devices or units can be in the form of telecommunication or other forms.
[0040] The above embodiments are only used to illustrate the technical solutions of the utility model, rather than to limit the protection scope of the utility model. Obviously, the described embodiments are only some embodiments of the utility model, rather than all embodiments. Based on these embodiments, all other embodiments obtained by ordinary technicians in this field without making creative work are within the scope of protection of the utility model. Although the utility model has been described in detail with reference to the above embodiments, ordinary technicians in this field can still combine, add, delete or make other adjustments to the features in the various embodiments of the utility model according to the circumstances without conflict, without making creative work, so as to obtain different other technical solutions that do not deviate from the concept of the utility model in essence, and these technical solutions also belong to the scope of protection of the utility model.
Claims
1. A reaction kettle for removing sodium ions, characterized in that: include: A reactor body for removing sodium ions, wherein the reactor body is provided with a removal chamber and a filtration chamber which are connected and distributed up and down; An electric heating block, the electric heating block is arranged on the inner wall of the removal chamber for heating; a stirring rod, the stirring rod is rotatably mounted on the reactor body, the bottom end of the stirring rod extends into the removal chamber for stirring the sodium ion solution to be removed; a first motor, the first motor is fixedly mounted on the top of the reactor body, and the output shaft of the first motor is fixedly connected to the top end of the stirring rod through a coupling; a detachable filter basket, the filter basket is arranged in the filter chamber for filtering the liquid after the sodium ions are removed; A first drain pipe for draining liquid into the filter basket, the first drain pipe is fixedly connected to the bottom of the removal chamber, and a first solenoid valve is arranged on the first drain pipe; a cleaning mechanism for cleaning impurities in the filter basket, the cleaning mechanism is arranged on the filter basket.
2. The sodium ion removal reactor according to claim 1, characterized in that: The cleaning mechanism includes: a transmission rod vertically rotatably installed on the top of the filter basket, the bottom end of the transmission rod extending into the filter basket; a cleaning brush fixed to the bottom end of the transmission rod for cleaning the filter basket; a second motor fixed to the top of the filter basket for driving the transmission rod to rotate, the output shaft of the second motor being fixedly connected to the top end of the transmission rod via a coupling.
3. The sodium ion removal reactor according to claim 1, characterized in that: A groove block is symmetrically fixedly installed on the inner wall of the filter cavity, and a pullable and detachable connecting block is arranged on the groove block, and one end of the connecting block is fixedly connected to the filter basket.
4. The sodium ion removal reactor according to claim 3, characterized in that: The groove block is provided with a pin rod that can be pulled and removed, and the bottom end of the pin rod passes through the connecting block.
5. The sodium ion removal reactor according to claim 1, characterized in that: A pH detector is fixedly installed on the top of the reactor body, and the monitoring end of the pH detector extends into the removal chamber. A feeding pipe is fixedly connected to the top of the reactor body, and the feeding end of the feeding pipe extends into the removal chamber. A hopper is fixedly installed on the top of the feeding pipe, and a cover plate is hinged on the top of the hopper, and a handle is fixedly installed on the top of the cover plate.
6. The sodium ion removal reactor according to claim 1, characterized in that: The bottom of the filter cavity is fixedly connected with a second liquid discharge pipe, on which a second solenoid valve is arranged. A temperature controller is arranged on one side of the reactor body, and the temperature controller is adapted to the electric heating block.
7. The sodium ion removal reactor according to claim 1, characterized in that: An exhaust pipe is fixedly installed on the top of the reactor body, the air inlet end of the exhaust pipe extends into the removal chamber, and an automatic air release valve is arranged on the outlet end of the exhaust pipe.