Baffle plate extraction tower containing solid extraction operation
By setting a bevel design on the outer ring plate and inner conical plate of the pulse baffle extraction tower and adopting a multi-rod support structure, the problem of solid phase deposition during processing of high solid content materials is solved, and the continuous discharge of the solid phase and the improvement of equipment flux is achieved.
Patent Information
- Application Number
- CN202421565202.6
- Authority / Receiving Office
- CN · China
- Patent Type
- Utility models(China)
- Current Assignee / Owner
- Filing Date
- 2024-07-04
- Publication Date
- 2025-06-06
- Estimated Expiration
- 2034-07-04
AI Technical Summary
When the existing pulse baffle extraction towers treat materials with high solid content, solid particles are prone to deposit and adhere to the outer ring plate and tower wall, resulting in clogging of the equipment and affecting normal operation.
By setting a specific bevel design on the outer ring plate and the inner conical plate, and combining the multi-rod support structure, the flow field structure is improved, the deposition of the solid phase in the tower is reduced, and the continuous discharge of the solid phase is achieved.
It effectively avoids local enrichment of solid phase during the defluxation process, improves the flux and processing capacity of the equipment, and extends the normal operation cycle of the equipment.
Smart Images

Figure CN222942974U_ABST
Abstract
Description
Technical Field
[0001] The utility model belongs to the technical field of extraction in chemical separation, and in particular relates to a baffle extraction tower containing solid extraction operation. Background Art
[0002] Solvent extraction is an important separation technology in chemical and metallurgical processes. It has the advantages of high selectivity, strong adaptability, good separation effect and easy large-scale continuous production. It is currently widely used in hydrometallurgy, nuclear chemical industry, petrochemical industry, environmental engineering, new energy and new materials and other fields. The realization of the liquid-liquid extraction process depends on the development of extraction equipment. With the continuous expansion of production scale and the increasing complexity of separation objects, the requirements for extraction equipment are also getting higher and higher. In practical production, liquid-liquid-solid extraction systems containing solid phases are often encountered. The solid particles in this type of extraction gas are easily deposited in the extraction equipment and reduce the equipment flux, thereby causing equipment blockage and affecting its normal operation and long-term operation. Therefore, it is very important to develop an extraction device that is resistant to blockage, high-throughput and can achieve continuous liquid-solid discharge for separation of solid-containing extraction operations while ensuring high mass transfer efficiency.
[0003] The pulse baffle extraction tower has the advantages of simple structure, large flux, no internal moving parts, good sewage discharge performance and easy maintenance. Compared with other mechanical stirring extraction towers, this type of extraction tower has a wider operating area, increased operational stability, and can also handle materials containing solid particles. However, the existing pulse baffle extraction tower is only suitable for low solid content operation. When the solid content of the system is too high, the particles will be excessively deposited and adhered at the connection between the outer ring plate and the tower wall, and produce a "snowball" effect, rapidly accumulating and expanding, affecting the normal operation of the equipment, and in severe cases, causing the extraction tower to be blocked.
[0004] The utility model patent publication with publication number CN102698467A discloses a method for extracting and purifying natural uranium using a vibrating annular baffle extraction tower. By setting annular baffles under vibration conditions, it is possible to process solid-containing raw materials, but the baffles are all flat plate structures, and the vibration has limited effect on excessive deposition and adhesion as well as enrichment. In addition, it is set as a central column, and the flux is limited. Utility Model Content
[0005] In view of the above technical problems, the utility model proposes an improved pulse baffle extraction tower suitable for solid-containing extraction operations. The internal components are improved and designed based on the analysis of the flow field structure in the baffle extraction tower, so as to reduce the deposition of solid phase on the outer ring plate and the inner plate, eliminate tower body blockage, increase flow flux, and realize continuous discharge of solid phase, so as to improve the extraction tower's processing capacity for solid-containing extraction systems.
[0006] In order to achieve the above purpose, the utility model adopts the following technical solutions:
[0007] A baffle extraction tower with solid extraction operation comprises an upper tower body component, a main tower body component and a lower tower body component.
[0008] The upper tower body component includes an upper tower body, a light phase outlet and a heavy phase distributor; the lower tower body component includes a lower tower body, a heavy phase outlet, a solid phase outlet and a light phase distributor.
[0009] The main tower body component includes a main tower body, an inner cone plate, an outer ring plate and a support rod component; the outer ring plate and the inner cone plate are both provided with a plurality, and the outer ring plates are spaced apart from the inner cone plate; the outer ring plate is a circular ring plate-shaped structure, and the top surface of the outer ring plate is provided with an inclined surface, and the height of the top surface of the outer edge of the outer ring plate is higher than the height of the top surface of the inner ring of the outer ring plate (that is, the upper side surface of the outer ring plate is processed into an inner inclined surface suitable for a multiphase flow field, or the upper side surface and the lower side surface of the outer ring plate are simultaneously processed into outer inclined surfaces suitable for a multiphase flow field), the outer edge of the outer ring plate is in contact with the inner wall of the main tower body, and a plurality of outer ring support holes that pass through from top to bottom are provided on each outer ring plate; the inner cone plate is a conical plate with a thick middle and a thin edge (that is, the upper side surface of the inner cone plate is processed into an outer inclined surface suitable for a multiphase flow field) or a middle An umbrella-shaped plate with a high center and a low edge (i.e., the upper and lower sides of the inner cone plate are simultaneously processed into outer inclined surfaces suitable for the multiphase flow field), the inner cone top in the center of the top of the inner cone plate is the highest point of the inner cone plate in the vertical position, the diameter of the inner ring portion of the outer ring plate is smaller than the diameter of the outer edge portion of the inner cone plate, and a plurality of inner cone support holes that pass through from top to bottom are provided on each inner cone plate near the outer edge portion of the inner cone plate; a plurality of support rod components are provided, and each includes an inner rod and a support sleeve, the apertures of the inner cone support hole and the outer ring support hole are larger than the outer diameter of the inner rod and smaller than the outer diameter of the support sleeve; the inner rod passes through all the inner cone plates and the outer ring plates at intervals through the inner cone support hole and the outer ring support hole, and the support sleeve is sleeved on the outside of the inner rod between adjacent inner cone plates and outer ring plates.
[0010] The upper tower body, the main tower body and the lower tower body are connected in sequence from top to bottom.
[0011] The included angle between the top surface of the inner cone plate and the horizontal plane is α, and the included angle between the top surface of the outer ring plate and the horizontal plane is β, satisfying 0<α≤30°, 0<β≤30°.
[0012] Technically speaking, the slope of the inner cone plate and the outer ring plate needs to be such that the component force generated by the gravity of the solid particles along the slope direction can destroy the force balance and promote the falling of the solid particles. It is generally necessary to set it between 0 and 30 degrees. At the same time, the slope of the inner cone plate and the outer ring plate is consistent with the vortex formed by the multiphase fluid of the tower material, which can prevent the formation of flow dead zones and reduce the deposition of particles.
[0013] Furthermore, the heavy phase outlet and the solid phase outlet are both opened on the side wall of the lower tower body, and in terms of height, the heavy phase outlet is located above the solid phase outlet, and the light phase distributor is arranged inside the lower tower body, and in terms of height, the light phase distributor is located below the solid phase outlet.
[0014] Furthermore, the lower tower body component also includes a pulse inlet and a drain outlet. The pulse inlet is opened on the side wall of the lower tower body and is located at a height between the heavy phase outlet and the solid phase outlet. The drain outlet is located below the light phase distributor.
[0015] Furthermore, the light phase outlet is opened on the side wall of the upper tower body, and the heavy phase distributor is arranged inside the upper tower body, and in terms of height, the heavy phase distributor is located below the light phase outlet.
[0016] Furthermore, the bottom surface of the outer ring plate is horizontally arranged, the top surface of the outer ring plate is inclined, and the height of the position close to the outer edge of the outer ring plate is higher than the height of the inner ring of the outer ring plate (that is, only the upper side surface of the outer ring plate is processed into an inner slope suitable for the multiphase flow field).
[0017] Furthermore, the vertical spacing between adjacent inner cone plates and outer ring plates is h, and the tower diameter of the main tower body is d, satisfying (Tower diameter is the diameter of the main tower body).
[0018] Furthermore, the area of the gap between the inner cone plate and the inner wall of the main tower is S1, the area of the area enclosed by the inner ring of the outer ring plate is S2, the horizontal projection area of the inner cone plate is S3, and the horizontal projection area of the outer ring plate is S4, satisfying (This means that the average opening ratio is controlled to be 16 to 32%).
[0019] Furthermore, three inner rods are provided, and the connecting line of the three inner rods at any horizontal plane forms an equilateral triangle.
[0020] Furthermore, both ends of each inner rod are provided with external threads, and the support rod component also includes a nut, and the nut is tightened at the external threads of each inner rod.
[0021] Furthermore, the inner diameter of the upper tower body is larger than the inner diameter of the main tower body, and the inner diameter of the lower tower body is larger than the inner diameter of the main tower body.
[0022] The positional limitations such as "vertical", "horizontal plane", "up", "down", "bottom", "top", "side" and so on described in the utility model are all relative positions when the device is working normally. When the whole device turns, each relative position changes according to the turning form. The positional limitations do not have a limiting effect on the absolute position. The "outer diameter" and "inner diameter" recorded in the utility model are both diameters.
[0023] The technical effects of the utility model are:
[0024] The utility model greatly improves the flow of the solid phase during the solid extraction operation and avoids the local enrichment of the solid phase during the baffle process by setting an outer ring plate and an inner cone plate with a specific tilting mode and a specific matching mode, and replaces the existing center rod support with a multi-rod support. First, the outer ring plate and the inner ring plate of the traditional pulse baffle extraction tower are improved, and a specific inclined surface design structure is adopted to make the surface of the internal component produce a gravity component along the inclined surface direction, which promotes the movement of particles; the multiphase flow field structure in the baffle extraction tower has a better fit with the inclined surface plate, eliminating the flow dead zone in the tower and preventing solid phase deposition; and the three-rod edge support method is combined to eliminate the area occupied by the single-rod center support method on the center of the extraction tower, thereby improving the flux of the extraction tower. Combined with the specific processing method of the pulse, it is conducive to the movement of the solid phase to the next level of the tower plate, and the processing capacity of the baffle extraction tower is improved. At the same time, the utility model adopts a sleeve-type internal component connection method, which is convenient for disassembly of the internal components and adjustment of the plate spacing. The sleeve-internal component-sleeve arrangement combination is adopted on the support rod, which can realize the fixation of the inner cone plate and the outer ring plate, and the combination of the sleeve and the support rod is convenient for the disassembly of the internal components and adjustment of the plate spacing; the solid phase discharge port installed at the expansion section can realize the continuous discharge of the solid phase, so that the baffle extraction tower can maintain long-term stable operation. BRIEF DESCRIPTION OF THE DRAWINGS
[0025] Figure 1 It is a structural schematic diagram of a partial combination of an inner cone plate, an outer ring plate and a support rod component in one embodiment of the utility model.
[0026] Figure 2 It is a structural schematic diagram of a partial combination of a support rod component and an outer ring plate in one embodiment of the utility model.
[0027] Figure 3 The present invention is a schematic diagram of the cross-sectional structure of a baffle extraction tower according to one embodiment of the present invention.
[0028] Figure 4 It is a schematic diagram of the three-dimensional structure of an inner cone plate according to one embodiment of the utility model.
[0029] Figure 5 The schematic diagram of the top view of the inner cone plate in one embodiment of the utility model is shown.
[0030] Figure 6 It is a schematic diagram of the side structure of an inner cone plate according to one embodiment of the utility model.
[0031] Figure 7 It is a schematic diagram of the three-dimensional structure of the outer ring plate according to one embodiment of the utility model.
[0032] Figure 8 The figure is a schematic diagram of the top structure of the outer ring plate according to one embodiment of the utility model.
[0033] Fig. 9 It is a schematic diagram of the side structure of the outer ring plate of one embodiment of the utility model.
[0034] Fig.10 (a) is a schematic structural diagram of a support sleeve according to an embodiment of the utility model.
[0035] Fig.10 (b) is a schematic diagram of a partial cross-sectional structure of a support sleeve and an inner rod combination according to an embodiment of the utility model.
[0036] Fig.11 (a) is a velocity flow field distribution diagram of the baffle of the comparative implementation scheme.
[0037] Fig.11 (b) is a velocity flow field distribution diagram of a conical baffle in one embodiment of the utility model.
[0038] Fig.12 (a) is a flow dead zone distribution diagram of the baffle of a comparative implementation scheme.
[0039] Fig.12 (b) is a flow dead zone distribution diagram of a conical baffle according to an embodiment of the utility model.
[0040] Fig.13 (a) is a diagram showing the solid content distribution of the baffles of a comparative embodiment.
[0041] Fig.13 (b) is a solid content distribution diagram of a conical baffle according to an embodiment of the present invention.
[0042] in:
[0043] 001-upper tower body, 002-main tower body, 003-lower tower body;
[0044] 101-light phase outlet, 102-heavy phase distributor; 201-outer ring plate, 202-support rod component, 203-inner cone plate; 301-heavy phase outlet, 302-solid phase outlet, 303-pulse inlet, 304-light phase distributor, 305-drainage outlet;
[0045] 111 - outer ring support hole, 112 - outer edge of outer ring plate, 113 - inner ring of outer ring plate, 211 - inner rod, 212 - nut, 213 - support sleeve, 311 - inner cone support hole, 312 - inner cone top, 313 - outer edge of inner cone plate. DETAILED DESCRIPTION
[0046] The process technology scheme of the utility model is further explained below by combining embodiments and drawings. The orientations involved in this specification are based on the orientations of the utility model during normal operation, and do not limit the orientations during storage and transportation. They only represent relative positional relationships, not absolute positional relationships. Specific implementation methods Unless otherwise described, each feature is only an example of a series of equivalent or similar features. Just to help understand the utility model, those skilled in the art should understand that the embodiments are only to help understand the utility model and should not be regarded as specific limitations of the utility model.
[0047] The device configuration of this embodiment is exemplarily as follows Figure 3 A baffled extraction tower for solid extraction operation is shown, and the baffled extraction tower for solid extraction operation comprises an upper tower body component, a main tower body component and a lower tower body component.
[0048] like Figure 3 As shown, the upper tower body components include an upper tower body 001, a light phase outlet 101 and a heavy phase distributor 102; the lower tower body components include a lower tower body 003, a heavy phase outlet 301, a solid phase outlet 302, a light phase distributor 304, a pulse inlet 303 and a sewage outlet 305.
[0049] like Figure 1 , Figure 2 and Figure 3 As shown, the main tower body component includes a main tower body 002, an inner cone plate 203, an outer ring plate 201 and a support rod component 202; Figure 3 As shown, the outer ring plate 201 and the inner cone plate 203 are both provided in plurality, and the outer ring plate 201 is spaced apart from the inner cone plate 203; Figure 7 , Figure 8 and Fig. 9 As shown, the outer ring plate 201 is a circular ring plate structure, and the top surface of the outer ring plate 201 is an inclined surface, and the height of the top surface of the outer edge portion 112 of the outer ring plate is higher than the height of the top surface of the inner ring portion 113 of the outer ring plate (that is, either the top surface and the bottom surface of the same plate are inclined, or the top surface of the outer thick and inner thin is inclined). Figure 3 As shown, the outer edge portion 112 of the outer ring plate contacts the inner wall of the main tower body 002. Figure 7 As shown, each outer ring plate 201 is provided with a plurality of outer ring support holes 111 extending vertically therethrough; Figure 4 , Figure 5 and Figure 6 As shown, the inner cone plate 20) is a conical plate with a thick middle and thin edges or an umbrella-shaped plate with a high middle and low edges. The inner cone top 312 at the center of the top of the inner cone plate is the highest point of the inner cone plate 203 in the vertical position, as shown in FIG. Figure 3 As shown, the diameter of the inner ring portion 113 of the outer ring plate is smaller than the diameter of the outer edge portion 313 of the inner cone plate. Figure 4 As shown, a plurality of inner cone support holes 311 extending vertically are provided on each inner cone plate 203 near the outer edge 313 of the inner cone plate; Figure 3 The support rod components 202 shown in the figure are provided with three, and each includes three inner rods 211 and a support sleeve 213 of a multiple of three. The apertures of the inner cone support hole 311 and the outer ring support hole 111 are larger than the outer diameter of the inner rod 211 and smaller than the outer diameter of the support sleeve 213. The inner rod 211 passes through all the inner cone plates 203 and outer ring plates 201 at intervals through the inner cone support hole 311 and the outer ring support hole 111, and the support sleeve 213 is sleeved on the outer side of the inner rod 211 between the adjacent inner cone plates 203 and outer ring plates 201. Fig.10 (a) and Fig.10 As shown in (b), the outer part of the inner rod 211 is provided with the support sleeve 213, and as shown in Fig.10 (a) and Fig.10 As shown in (b), the bottom surface of the support sleeve 213 is uneven, which is to match the inclination of the top surface of the outer ring plate 201 or the top surface of the inner cone plate 203.
[0050] like Figure 3 As shown, the upper tower body 001, the main tower body 002 and the lower tower body 003 are connected in sequence from top to bottom. The inner diameter of the upper tower body 001 is larger than the inner diameter of the main tower body 002, and the inner diameter of the lower tower body 003 is larger than the inner diameter of the main tower body 002.
[0051] The angle between the top surface of the inner cone plate 203 and the horizontal plane is α, and the angle between the top surface of the outer ring plate (201) and the horizontal plane is β, satisfying 0<α≤30° (15° in this embodiment), 0<β≤30° (15° in this embodiment).
[0052] like Figure 3 As shown, the heavy phase outlet 301 and the solid phase outlet 302 are both opened on the side wall of the lower tower body 003, and the heavy phase outlet 301 is located above the solid phase outlet 302 in terms of height. The light phase distributor 304 is arranged inside the lower tower body 003, and the light phase distributor 304 is located below the solid phase outlet 302 in terms of height. Figure 3As shown, the pulse inlet 303 is opened on the side wall of the lower tower body 003 and is located at a height between the heavy phase outlet 301 and the solid phase outlet 302 , and the sewage outlet 305 is located below the light phase distributor 304 .
[0053] like Figure 3 As shown, the light phase outlet 101 is opened on the side wall of the upper tower body 001 , and the heavy phase distributor 102 is arranged inside the upper tower body 001 , and in terms of height, the heavy phase distributor 102 is located below the light phase outlet 101 .
[0054] like Fig. 9 As shown, the bottom surface of the outer ring plate 201 of this embodiment is horizontally arranged, the top surface of the outer ring plate 201 is inclined, and the height of the position close to the outer edge portion 112 of the outer ring plate is higher than the height of the inner ring portion 113 of the outer ring plate.
[0055] In this embodiment, the vertical distance between adjacent inner cone plates 203 and outer ring plates 201 is h, and the tower diameter of the main tower body 002 is d. satisfy
[0056] In this embodiment, the area of the gap between the inner cone plate 203 and the inner wall of the main tower body 002 is S1, the area of the inner ring portion 113 of the outer ring plate is S2, the horizontal projection area of the inner cone plate 203 is S3, and the horizontal projection area of the outer ring plate 201 is S4. satisfy requirements.
[0057] like Figure 1 , Figure 2 and Figure 3 As shown, the connection line of the three inner rods 211 at any horizontal plane forms an equilateral triangle, that is, the three inner rods 211 are evenly distributed inside the main tower body.
[0058] like Figure 2 As shown, both ends of each inner rod 211 are provided with external threads, and the support rod component 202 further includes a nut 212 , and the nut 212 is screwed on the external threads of each inner rod 211 .
[0059] So far, the device structure of the utility model has been exemplarily shown. The specific use effects of the device of the utility model are illustrated and compared with usage examples below.
[0060] Example 1
[0061] 20% P204-kerosene was used as the light phase, and an aqueous solution containing Ni, Co, Mn, Mg, Cu, Zn, Ca, Fe (Ca 2+>0.2g / L) as the heavy phase for fluid mechanics experiments. The experimental conditions are that the total flow rate of the two phases is 350L / h, the flow ratio of the organic phase to the aqueous phase is 0.8-1.5, and the organic phase is continuous. The above-mentioned baffle extraction tower containing solid extraction operation of the utility model is used. The operation steps are to fill the baffle extraction tower containing solid extraction operation of the utility model with 20% P204-kerosene from the light phase inlet, and the aqueous phase is input through the heavy phase distributor, and the two-phase flow rate is adjusted to 200L / h for the organic phase and 150L / h for the aqueous phase. The pulse stroke is set to a fixed value of 0.5mm, and the pulse frequency control device is turned on to make the liquid surface fluctuate periodically. The product of the amplitude and frequency of the vibration of the droplets in the extraction tower is the pulse intensity. The flow rate of the heavy phase outlet in the heavy phase clarification section (i.e., the lower tower body) is adjusted to maintain the height of the interface between the light phase and the heavy phase at the clarification section stable and unchanged.
[0062] Comparative Example 1
[0063] This comparative example adopts the existing traditional pulse baffle extraction tower, the outer ring plate and the inner ring plate of the traditional pulse baffle extraction tower are both flat plates, and the support rod component is a single-rod center-supported baffle extraction tower with a central support, and the plate spacing and opening rate of the outer ring plate and the inner ring plate of the traditional pulse baffle extraction tower are kept the same as the specific implementation method of the utility model used in Example 1, and the same extraction raw materials, parameters and methods as in Example 1 are used. The comparative experimental data of Example 1 and Comparative Example 1 are shown in Table 1. Table 1 is a comparison table of fluid mechanics experimental results of Example 1 and Comparative Example 1.
[0064] Table 1
[0065] Pulse intensity Continuous phase flow rate Dispersed phase flow rate Example 1 Comparative Example 1 0 0.002 0.0015 O X 0 0.004 0.003 XO X 0.005m / s 0.002 0.0015 O XO 0.005m / s 0.004 0.003 O X 0.01m / s 0.004 0.003 O X 0.015m / s 0.004 0.003 O XO 0.02m / s 0.004 0.003 O O
[0066] Note: X indicates flooding, O indicates good operation, and XO indicates poor operation.
[0067] Through the comparative data in Table 1, it can be obtained that under different pulse intensities and different flow rates, the overall operational flexibility of the three-rod edge-supported baffle extraction tower of the utility model is higher than that of the single-rod center-supported baffle extraction tower of Comparative Example 1. In particular, as shown in Table 1, the traditional baffle extraction tower of Comparative Example 1 cannot operate normally under the condition of no pulse intensity, while the baffle extraction tower of the present invention can also achieve good operation at low flow rates. For the traditional baffle extraction tower of Comparative Example 1, stable operation at a low flow rate can only be achieved under high pulse conditions (pulse intensity>0.02m / s), while the extraction tower of the present invention can achieve stable operation of the extraction equipment when the pulse is 0.005m / s. Therefore, the extraction tower of the present invention is not only suitable for extraction systems containing solid materials, but also consumes significantly less energy than the traditional extraction tower of Comparative Example 1.
[0068] By performing a tower droplet behavior and fluid mechanics simulation on Example 1 and Comparative Example 1, the specific Figures 11 to 13 As shown, the simulation process sets the tower diameter to DN250, the opening rate to 25.6%, the spacing between the inner ring plate and the outer ring plate to 113 mm, and the angles between the top surfaces of the inner cone plate and the outer ring plate and the horizontal plane (i.e., α and β) to 15°. Fig.11 (a) is the velocity flow field distribution diagram of comparative example 1, Fig.11 (b) is the velocity flow field distribution diagram of Example 1, Fig.12 (a) is the flow dead zone distribution diagram of comparative example 1, Fig.12 (b) is the flow dead zone distribution diagram of Example 1, Fig.13 (a) is the solid content distribution diagram of Comparative Example 1, Fig.13 (b) is the solid content distribution diagram of Example 1.
[0069] Through the above analysis of the droplet behavior and fluid mechanics simulation in the tower, it can be seen that there is a big difference between the fluid vortex structure in the traditional extraction tower and the geometric structure of the tower. Fig.11 The vortex formed above the inner and outer ring plates shown in (a) is not fully developed and should be smaller than Fig.11 (b) shows the eddy current intensity, which leads to Fig.11 The eddy current area (grey) defined by velocity as shown in (a) is smaller than Fig.11 (b) shows the distribution of eddy current areas. Fig.12 The dead zone distribution (black) shown in (a) is larger than Fig.12 (b) The dead zone distribution shown; the elimination of flow dead zone is beneficial to reduce the deposition of solid phase, thus Fig.13 The solid volume fraction on the plate shown in (b) is less than Fig.13 The solid volume content shown in (a) proves that the design of the internal components of the utility model is not simply to set the upper surface of the baffle plate as an inclined structure, but through the setting of parameters such as the distance and area ratio between the various components, and the coordinated use of the dispersed setting of multiple rods (three rods in this embodiment), the turbulent characteristics of the eddy current between the plates can be fully utilized to prevent solid phase deposition, thereby improving the processing capacity of the entire tower for solid-containing extraction systems.
[0070] The technical principle of the present invention is described above in combination with specific embodiments. These descriptions are only for explaining the principle of the present invention and cannot be interpreted as limiting the protection scope of the present invention in any way. Based on the explanations here, technicians in this field can think of other specific implementation methods of the present invention without creative work, and these methods will fall within the protection scope of the present invention.
Claims
1. A baffled extraction tower for solid extraction operation, characterized in that: The baffle extraction tower containing solid extraction operation comprises an upper tower body component, a main tower body component and a lower tower body component; The upper tower body component comprises an upper tower body (001), a light phase outlet (101) and a heavy phase distributor (102); the lower tower body component comprises a lower tower body (003), a heavy phase outlet (301), a solid phase outlet (302) and a light phase distributor (304); The main tower body component comprises a main tower body (002), an inner cone plate (203), an outer ring plate (201) and a support rod component (202); a plurality of the outer ring plates (201) and the inner cone plate (203) are provided, and the outer ring plates (201) are spaced apart from the inner cone plate (203); the outer ring plate (201) is a circular ring plate structure, and the top surface of the outer ring plate (201) is an inclined surface, and the outer edge portion (112) of the outer ring plate is The height of the surface is higher than the height of the top surface of the inner ring portion (113) of the outer ring plate, the outer edge portion (112) of the outer ring plate contacts the inner side wall of the main tower body (002), and a plurality of outer ring support holes (111) are opened on each outer ring plate (201) and penetrate up and down; the inner cone plate (203) is a conical plate with a thick middle and a thin edge or an umbrella-shaped plate with a high middle and a low edge, and the inner cone top (312) at the center of the top of the inner cone plate is the vertical position of the inner cone plate (203). The diameter of the inner ring portion (113) of the outer ring plate is smaller than the diameter of the outer edge portion (313) of the inner cone plate, and a plurality of inner cone support holes (311) extending vertically through each inner cone plate (203) near the outer edge portion (313) of the inner cone plate are provided; the support rod component (202) is provided with a plurality of inner cone support holes (311), each of which comprises an inner rod (211) and a support sleeve (213), and the inner cone support hole (311) and the outer ring support hole ( The diameter of the holes (111) is larger than the outer diameter of the inner rod (211) and smaller than the outer diameter of the support sleeve (213); the inner rod (211) passes through all the inner cone plates (203) and the outer ring plates (201) at intervals through the inner cone support holes (311) and the outer ring support holes (111), and the support sleeve (213) is sleeved on the outside of the inner rod (211) between adjacent inner cone plates (203) and outer ring plates (201); The upper tower body (001), the main tower body (002) and the lower tower body (003) are connected in sequence from top to bottom; The included angle between the top surface of the inner cone plate (203) and the horizontal plane is α, and the included angle between the top surface of the outer ring plate (201) and the horizontal plane is β, satisfying 0<α≤30°, 0<β≤30°.
2. The baffled extraction tower containing solid extraction operation according to claim 1, characterized in that: The heavy phase outlet (301) and the solid phase outlet (302) are both opened on the side wall of the lower tower body (003), and in terms of height, the heavy phase outlet (301) is located above the solid phase outlet (302), and the light phase distributor (304) is arranged inside the lower tower body (003), and in terms of height, the light phase distributor (304) is located below the solid phase outlet (302).
3. The baffled extraction tower containing solid extraction operation according to claim 1 or 2, characterized in that: The lower tower body component also includes a pulse inlet (303) and a drain outlet (305). The pulse inlet (303) is opened on the side wall of the lower tower body (003) and is located at a height between the heavy phase outlet (301) and the solid phase outlet (302). The drain outlet (305) is located below the light phase distributor (304).
4. The baffled extraction tower containing solid extraction operation according to claim 1, characterized in that: The light phase outlet (101) is opened on the side wall of the upper tower body (001), and the heavy phase distributor (102) is arranged inside the upper tower body (001), and in terms of height, the heavy phase distributor (102) is located below the light phase outlet (101).
5. The baffled extraction tower with solid extraction operation according to claim 1, characterized in that: The bottom surface of the outer ring plate (201) is arranged horizontally, the top surface of the outer ring plate (201) is arranged inclined, and the height of the position close to the outer edge portion (112) of the outer ring plate is higher than the height of the inner ring portion (113) of the outer ring plate.
6. The baffled extraction tower containing solid extraction operation according to claim 1, characterized in that: The vertical distance between adjacent inner cone plates (203) and outer ring plates (201) is h, and the tower diameter of the main tower body (002) is d, satisfying 7. The baffled extraction tower with solid extraction operation according to claim 1, characterized in that: The area of the gap between the inner cone plate (203) and the inner wall of the main tower body (002) is S1, the area of the area enclosed by the inner ring portion (113) of the outer ring plate is S2, the horizontal projection area of the inner cone plate (203) is S3, and the horizontal projection area of the outer ring plate (201) is S4, satisfying 8. The baffled extraction tower with solid extraction operation according to claim 1, characterized in that: Three inner rods (211) are provided, and the connecting line of the three inner rods (211) at any horizontal plane forms an equilateral triangle.
9. The baffled extraction tower with solid extraction operation according to claim 1, characterized in that: Both ends of each inner rod (211) are provided with external threads, and the support rod component (202) further comprises a nut (212), and the nut (212) is screwed onto the external threads of each inner rod (211).
10. The baffled extraction tower with solid extraction operation according to claim 1, characterized in that: The inner diameter of the upper tower body (001) is greater than the inner diameter of the main tower body (002), and the inner diameter of the lower tower body (003) is greater than the inner diameter of the main tower body (002).
Citation Information
Patent Citations
Method for extracting and purifying natural uranium by using vibrating ring-shaped traverse baffle extracting tower
CN102698467A