Device for recovering graphene in micro-etching liquid
By designing a graphene recovery device in micro-etching liquid, using a stirring rod rotation and heater to improve the contact and molecular activity of the drug and micro-etching liquid, the problem of low graphene recovery efficiency in micro-etching liquid is solved, and more efficient graphene recovery is achieved.
Patent Information
- Application Number
- CN202421637497.3
- Authority / Receiving Office
- CN · China
- Patent Type
- Utility models(China)
- Current Assignee / Owner
- Filing Date
- 2024-07-11
- Publication Date
- 2025-07-29
- Estimated Expiration
- 2034-07-11
AI Technical Summary
In the prior art, the recovery efficiency of graphene in the microetching liquid is low, mainly due to the small contact range between the drug and the microetching liquid and the slow reaction.
A graphene recovery device in micro-etching liquid is designed, including a main mechanism and an auxiliary mechanism. By driving the motor to drive the stirring rod to rotate, the contact between the drug and the micro-etching liquid is enhanced, and the molecular activity is improved through the heater and the reaction is accelerated. At the same time, the pumping pump and filter plate are used to achieve convenient recycling of graphene.
The reaction efficiency between drugs and microetching liquid and graphene recovery efficiency are improved, making the reaction faster, the molecular activity is higher, and the recycling process is more convenient.
Smart Images

Figure CN223159248U_ABST
Abstract
Description
Technical Field
[0001] The utility model relates to the technical field of graphene recovery, and particularly relates to a graphene recovery device in a micro-etching solution. Background Technique
[0002] The micro-etching solution, also known as a micro-etching reagent or a chemical etchant, is a chemical reagent used for the surface treatment and analysis of metal specimens, while graphene is a two-dimensional material made of carbon atoms by chemical vapor deposition or mechanical exfoliation.
[0003] When the existing technology recovers graphene in the micro-etching solution, it usually needs to use drugs to react with the micro-etching solution to separate the graphene in the micro-etching solution. However, during the reaction, the contact range between the drug and the micro-etching solution is small, and the reaction is slow, resulting in a low recovery efficiency of graphene. Summary of the Utility Model
[0004] (I) Technical Problems to be Solved
[0005] The purpose of the utility model is to provide a graphene recovery device in a micro-etching solution to solve the problem that during the reaction, the contact range between the drug and the micro-etching solution is small, the reaction is slow, and the recovery efficiency of graphene is low as mentioned in the above background technique.
[0006] (II) Technical Solutions
[0007] To achieve the above purpose, the utility model provides the following technical solutions: A graphene recovery device in a micro-etching solution includes a main body mechanism and an auxiliary mechanism. The auxiliary mechanism is located outside the main body mechanism. The main body mechanism includes a device main body, a control panel, control buttons, a driving motor, and a reaction chamber. The control panel is fixedly installed at the left end of the device main body. The control buttons are movably installed at the left end of the control panel. The driving motor is fixedly installed at the upper end of the device main body. The driving motor is electrically connected to the control panel. The reaction chamber is fixedly arranged at the upper inner side of the device main body.
[0008] Preferably, the main body mechanism further includes a transmission rod, a stirring rod, a filter plate, a positioning piece, a heater, a moving base, and locking universal wheels. The transmission rod is movably installed at the transmission end of the driving motor.
[0009] Preferably, the stirring rods are fixedly installed at the left and right ends of the transmission rod. The filter plate is fixedly installed at the lower end of the reaction chamber. The positioning piece is fixedly installed at the upper end of the filter plate. The upper surface of the positioning piece is slidably connected to the lower surface of the transmission rod including.
[0010] Preferably, the heater is fixedly installed at the left and right ends inside the reaction chamber. The heater is electrically connected to the control panel. The moving base is fixedly installed at the lower end of the device body, and the locking universal wheels are movably installed at the lower end of the moving base.
[0011] Preferably, the auxiliary mechanism includes a discharge cabinet door, a cabinet door handle, a liquid inlet pipe, a liquid inlet, a feeding trough, a liquid storage tank, a water pump, a water outlet pipe, and a water suction pipe. The discharge cabinet door is movably installed at the right end of the device body.
[0012] Preferably, the cabinet door handle is fixedly installed at the right end of the discharge cabinet door. The liquid inlet pipe is fixedly installed at the right end of the driving motor. The liquid inlet is fixedly arranged at the upper end of the liquid inlet pipe. The feeding trough is fixedly installed at the left end of the driving motor.
[0013] Preferably, the liquid storage tank is fixedly arranged at the lower end of the filter plate. The water pump is fixedly installed at the left end of the device body. The water pump is electrically connected to the control panel. The water outlet pipe is fixedly installed at the water outlet end of the water pump, and the water suction pipe is fixedly installed at the water inlet end of the water pump.
[0014] Compared with the prior art, the beneficial effects of the present utility model are as follows:
[0015] 1. For this graphene recovery device in the micro-etching solution, by installing the main body mechanism, when the device is in use, the driving motor can be started through the control panel, so that the transmission rod drives the stirring rod to rotate, thereby stirring the drugs and the micro-etching solution in the device, enabling them to come into contact more fully, with a faster reaction efficiency. Moreover, through the provided heater, the interior can be heated, making the molecular activity higher and the reaction speed faster, thus improving the graphene recovery efficiency.
[0016] 2. For this graphene recovery device in the micro-etching solution, by installing the auxiliary mechanism, when the device is in use, the micro-etching solution and drugs can be added respectively through the liquid inlet pipe and the feeding trough, which is more convenient during use. After the reaction is completed, the water pump can be started to pump out the micro-etching solution in the liquid storage tank. The recovered graphene is filtered and blocked by the filter plate. At this time, hold the cabinet door handle and open the discharge cabinet door to recover the graphene on the filter plate, which is more convenient during use. Description of the Drawings
[0017] Figure 1 is a three-dimensional structural schematic diagram of the present utility model;
[0018] Figure 2 is a sectional structural schematic diagram of the present utility model;
[0019] Figure 3 is a sectional structural schematic diagram of the main body mechanism of the present utility model;
[0020] Figure 4 This is a schematic diagram of the enlarged partial details of the main body mechanism of the present utility model.
[0021] In the figure: 1. Main body mechanism; 101. Device main body; 102. Control panel; 103. Control button; 104. Driving motor; 105. Reaction chamber; 106. Transmission rod; 107. Stirring rod; 108. Filter plate; 109. Positioning piece; 110. Heater; 111. Moving base; 112. Locking universal wheel; 2. Auxiliary mechanism; 201. Discharge cabinet door; 202. Cabinet door handle; 203. Liquid inlet pipe; 204. Liquid inlet; 205. Feeding trough; 206. Liquid storage tank; 207. Water pump; 208. Outlet pipe; 209. Water suction pipe. Specific embodiments
[0022] Next, the technical solutions in the embodiments of the present utility model will be clearly and completely described in conjunction with the accompanying drawings in the embodiments of the present utility model. Obviously, the described embodiments are only a part of the embodiments of the present utility model, rather than all the embodiments. Based on the embodiments of the present utility model, all other embodiments obtained by those of ordinary skill in the art without creative efforts shall fall within the protection scope of the present utility model.
[0023] Please refer to Figure 1 - Figure 4 The present utility model provides a technical solution: a graphene recovery device in a micro-etching solution, including a main body mechanism 1 and an auxiliary mechanism 2. The auxiliary mechanism 2 is located outside the main body mechanism 1. The main body mechanism 1 includes a device main body 101, a control panel 102, a control button 103, a driving motor 104 and a reaction chamber 105. The control panel 102 is fixedly installed at the left end of the device main body 101. The control button 103 is movably installed at the left end of the control panel 102. The driving motor 104 is fixedly installed at the upper end of the device main body 101. The driving motor 104 is electrically connected to the control panel 102. The reaction chamber 105 is fixedly arranged at the upper inner side of the device main body 101.
[0024] The main body mechanism 1 further includes a transmission rod 106, a stirring rod 107, a filter plate 108, a positioning piece 109, a heater 110, a moving base 111 and a locking universal wheel 112. The transmission rod 106 is movably installed at the transmission end of the driving motor 104. The stirring rods 107 are fixedly installed at the left and right ends of the transmission rod 106. The filter plate 108 is fixedly installed at the lower end of the reaction chamber 105. The positioning piece 109 is fixedly installed at the upper end of the filter plate 108. The upper surface of the positioning piece 109 is slidably connected to the lower surface of the transmission rod 106 including. The heaters 110 are fixedly installed at the left and right ends inside the reaction chamber 105. The heaters 110 are electrically connected to the control panel 102. The moving base 111 is fixedly installed at the lower end of the device main body 101. The locking universal wheels 112 are movably installed at the lower end of the moving base 111. When the device is in use, the driving motor 104 can be started through the control panel 102, so that the transmission rod 106 drives the stirring rod 107 to rotate, thereby stirring the medicine and the micro-etching solution in the device, making them contact more fully, with a faster reaction efficiency. And through the arranged heaters 110, the inside can be heated, making the molecular activity higher and the reaction speed faster, so that the recovery efficiency of graphene is higher.
[0025] The auxiliary mechanism 2 includes a discharge cabinet door 201, a cabinet door handle 202, a liquid inlet pipe 203, a liquid inlet 204, a feeding trough 205, a liquid storage tank 206, a water pump 207, a water outlet pipe 208 and a water suction pipe 209. The discharge cabinet door 201 is movably installed at the right end of the device main body 101. The cabinet door handle 202 is fixedly installed at the right end of the discharge cabinet door 201. The liquid inlet pipe 203 is fixedly installed at the right end of the driving motor 104. The liquid inlet 204 is fixedly arranged at the upper end of the liquid inlet pipe 203. The feeding trough 205 is fixedly installed at the left end of the driving motor 104. The liquid storage tank 206 is fixedly arranged at the lower end of the filter plate 108. The water pump 207 is fixedly installed at the left end of the device main body 101. The water pump 207 is electrically connected to the control panel 102. The water outlet pipe 208 is fixedly installed at the water outlet end of the water pump 207. The water suction pipe 209 is fixedly installed at the water inlet end of the water pump 207. When the device is in use, the micro-etching solution and the medicine can be added respectively through the liquid inlet pipe 203 and the feeding trough 205, which is more convenient in use. And after the reaction is completed, the water pump 207 can be started to pump out the micro-etching solution in the liquid storage tank 206. The recovered graphene is filtered and blocked by the filter plate 108. At this time, hold the cabinet door handle 202 and open the discharge cabinet door 201 to recover the graphene on the filter plate 108, which is more convenient in use.
[0026] Working principle: When the device is in use, the drive motor 104 can be started through the control panel 102, so that the transmission rod 106 drives the stirring rod 107 to rotate, thereby stirring the drugs and micro-etching solution in the device, making them contact more fully, with a faster reaction efficiency. And through the installed heater 110, the interior can be heated, making the molecular activity higher and the reaction speed faster, resulting in a higher recovery efficiency of graphene. When the device is in use, the micro-etching solution and drugs can be added separately through the liquid inlet pipe 203 and the feed tank 205, which is more convenient during use. And after the reaction is completed, the micro-etching solution in the liquid storage tank 206 can be pumped out by starting the water pump 207. The recovered graphene is filtered and blocked by the filter plate 108. At this time, hold the cabinet door handle 202 and open the discharge cabinet door 201 to recover the graphene on the filter plate 108, which is more convenient during use.
[0027] Finally, it should be noted that the above content is only used to illustrate the technical solution of the present invention, rather than a limitation on the protection scope of the present invention. Any simple modification or equivalent replacement of the technical solution of the present invention by those of ordinary skill in the art does not depart from the essence and scope of the technical solution of the present invention.
Claims
1. A graphene recovery device in a micro-etching solution, comprising a main body mechanism (1) and an auxiliary mechanism (2), characterized in that: The auxiliary mechanism (2) is located outside the main body mechanism (1). The main body mechanism (1) includes a device main body (101), a control panel (102), control buttons (103), a drive motor (104), and a reaction chamber (105). The control panel (102) is fixedly installed at the left end of the device main body (101). The control buttons (103) are movably installed at the left end of the control panel (102). The drive motor (104) is fixedly installed at the upper end of the device main body (101). The drive motor (104) is electrically connected to the control panel (102). The reaction chamber (105) is fixedly arranged at the upper inner side of the device main body (101).
2. The graphene recovery device in a micro-etching solution according to claim 1, wherein: The main body mechanism (1) further includes a transmission rod (106), a stirring rod (107), a filter plate (108), a positioning piece (109), a heater (110), a moving base (111), and locking universal wheels (112). The transmission rod (106) is movably installed at the transmission end of the drive motor (104).
3. The graphene recovery device in a micro-etching solution according to claim 2, characterized in that: The stirring rods (107) are fixedly installed at the left and right ends of the transmission rod (106). The filter plate (108) is fixedly installed at the lower end of the reaction chamber (105). The positioning piece (109) is fixedly installed at the upper end of the filter plate (108). The upper surface of the positioning piece (109) is slidably connected to the lower surface of the transmission rod (106).
4. The graphene recovery device in a micro-etching solution according to claim 3, wherein: The heaters (110) are fixedly installed at the left and right ends inside the reaction chamber (105). The heaters (110) are electrically connected to the control panel (102). The moving base (111) is fixedly installed at the lower end of the device main body (101). The locking universal wheels (112) are movably installed at the lower end of the moving base (111).
5. The graphene recovery device in a micro-etching solution according to claim 4, characterized in that: The auxiliary mechanism (2) includes a discharge cabinet door (201), a cabinet door handle (202), a liquid inlet pipe (203), a liquid inlet (204), a feed trough (205), a liquid storage tank (206), a water pump (207), a water outlet pipe (208), and a water suction pipe (209). The discharge cabinet door (201) is movably installed at the right end of the device main body (101).
6. The graphene recovery device in a micro-etching solution according to claim 5, wherein: The cabinet door handle (202) is fixedly installed at the right end of the discharge cabinet door (201). The liquid inlet pipe (203) is fixedly installed at the right end of the drive motor (104). The liquid inlet (204) is fixedly arranged at the upper end of the liquid inlet pipe (203). The feed trough (205) is fixedly installed at the left end of the drive motor (104).
7. The graphene recovery device in a micro-etching solution according to claim 6, characterized in that: The liquid storage tank (206) is fixedly arranged at the lower end of the filter plate (108). The water pump (207) is fixedly installed at the left end of the device main body (101). The water pump (207) is electrically connected to the control panel (102). The water outlet pipe (208) is fixedly installed at the water outlet end of the water pump (207). The water suction pipe (209) is fixedly installed at the water inlet end of the water pump (207).