Rectification and purification barrel for anthraquinone production

Abstract

The utility model relates to the technical field of purification barrels, and discloses a rectification purification barrel for anthraquinone production, which comprises a stirring mechanism, a purification mechanism and a discharging mechanism. During use, a material enters the stirring barrel through the feeding pipe, a solvent is added according to the proportion and enters the stirring barrel through the solvent pipe, at the moment, a heating rod heats the material in the stirring barrel through heating, meanwhile, a fixing block is fixed to the inner wall of the stirring barrel, a fixing column is fixed to the outer wall of the fixing block, and a motor is fixed to the interior of the fixing column. The fixing column protects the motor from being damaged by high temperature and liquid, the fixing rod is fixed to the output end of the motor, the stirring blades are fixed to the outer wall of the fixing rod, the contact area between a solvent and raw materials is increased through slow stirring, the solvent and the raw materials make full contact, and therefore the solubility is improved, and the dissolution process of the solvent and solute is accelerated through full mixing; and meanwhile, the consistency of the product quality can be ensured, and the efficiency of the production process can be improved.

Description

TECHNICAL FIELD

[0001] The utility model relates to purification bucket technical field especially relates to a rectification purification bucket for anthraquinone production. BACKGROUND

[0002] The purification bucket is usually a device used in chemical, industrial or laboratory processes, mainly used to remove impurities from liquids or gases, improve purity. In different industries and applications, the specific structure and function of the purification bucket may be different, but its basic function is to remove impurities in the liquid by physical, chemical or mechanical means, so that it meets the required purity standard.

[0003] The prior art anthraquinone purification bucket may not have stirring, so that the solvent and the raw material may not be fully mixed, the mixing of the solvent is uneven, which may cause incomplete dissolution of the raw material, and the quality of the final product is reduced. UTILITY MODEL CONTENT

[0004] To solve the above technical problems, the utility model provides a rectification purification bucket for anthraquinone production.

[0005] The utility model adopts the following technical scheme: a rectification purification bucket for anthraquinone production, characterized by: including stirring mechanism, purification mechanism and discharge mechanism, the stirring mechanism is located at the top of the discharge mechanism, the purification mechanism is located at the right side of the stirring mechanism;

[0006] The stirring mechanism includes an outer shell, a heating rod is fixedly connected to the inner wall of the outer shell, a feed pipe is fixedly connected inside the outer shell, a stirring barrel is communicatively provided in the feed pipe, the stirring barrel is fixedly connected to the outer wall of the heating rod, a solvent pipe is communicatively provided inside the stirring barrel, the solvent pipe is fixedly connected to the inside of the outer shell, a fixed block is fixedly connected to the inner wall of the stirring barrel, a fixed column is fixedly connected to the outer wall of the fixed block, a motor is fixedly connected to the inside of the fixed column, a fixed rod is fixedly connected to the output end of the motor, and a stirring blade is fixedly connected to the outer wall of the fixed rod.

[0007] Through the above technical scheme, when the material enters the inside of the stirring barrel through the feed pipe, the solvent is added according to the proportion, the solvent enters the inside of the stirring barrel through the solvent pipe, the heating rod heats the material in the stirring barrel at this time, the fixed block is fixed on the inner wall of the stirring barrel, the fixed column is fixed on the outer wall of the fixed block, the motor is fixed in the fixed column, the fixed column protects the motor from high temperature and liquid damage, so that the motor can run normally, the fixed rod is fixed on the output end of the motor, and the stirring blade is fixed on the outer wall of the fixed rod. By slow stirring, the contact area between the solvent and the raw material is increased, so that they are fully contacted, the solubility is improved, the mixing is sufficient, which helps to accelerate the dissolution process of the solvent and the solute, so as to promote the reaction, at the same time, the consistency of product quality can be ensured and the efficiency of production process is improved.

[0008] As a further improvement of the above-mentioned scheme, the purification mechanism comprises a steam pipe, which is communicated and arranged inside the stirring barrel, and a condenser pipe, which is communicated and arranged at one end of the steam pipe away from the stirring barrel, and a cooling pipe, which is fixedly connected to the outer wall of the condenser pipe.

[0009] As a further improvement of the above-mentioned scheme, the cooling pipe is communicated and arranged with a liquid inlet pipe inside, and a water pump, which is communicated and arranged at one end of the liquid inlet pipe away from the cooling pipe, and a fixed block one, which is fixedly connected to the outer wall of the water pump, and a coiled pipe, which is communicated and arranged at one end of the water pump away from the liquid inlet pipe.

[0010] As a further improvement of the above-mentioned scheme, the coiled pipe is fixedly connected to a support block, which is fixedly connected to the bottom of the fixed block one and the outer wall of the shell, and the coiled pipe is communicated and arranged at one end away from the water pump.

[0011] As a further improvement of the above-mentioned scheme, the coiled pipe is communicated and arranged inside the cooling pipe at one end away from the coiled pipe, and a support seat is fixedly connected to the inner wall of the support block at the bottom, and a motor one is fixedly connected to the top of the support seat, and a rotating rod is fixedly connected to the output end of the motor one.

[0012] As a further improvement of the above-mentioned scheme, the rotating rod is fixedly connected to a fan blade, and the condenser pipe is communicated and arranged with an exhaust pipe at one end close to the liquid outlet pipe, and the condenser pipe is communicated and arranged with a collection barrel at one end away from the steam pipe.

[0013] Through the above technical scheme, since the temperature of the raw material is increased to generate steam, the steam enters the inside of the condenser pipe through the steam pipe, and the cooling pipe is fixedly connected to the outer wall of the condenser pipe, the water pump delivers the cooling liquid into the inside of the cooling pipe through the liquid inlet pipe, the cooling liquid contacts the outer wall of the condenser pipe, thereby reducing the temperature of the condenser pipe and making the water vapor into liquid to enter the inside of the collection barrel, and the cooling liquid enters the inside of the coiled pipe through the liquid outlet pipe, the coiled pipe is communicated with the water pump, thereby completing the circulation, and the motor one drives the fan blade to rotate through the rotating rod, thereby accelerating the cooling of the cooling liquid in the coiled pipe and accelerating the condensation effect of the water vapor, thereby improving the condensation rate of the equipment and enhancing the operation efficiency of the whole system, facilitating fast collection.

[0014] As a further improvement of the above-mentioned scheme, the discharging mechanism comprises a discharge pipe, which is communicated and arranged inside the stirring barrel, a fixed rod one, which is rotatably connected inside the discharge pipe, a ball valve, which is fixedly connected to the back of the fixed rod one and contacted and arranged to the inner wall of the discharge pipe, and a handle, which is fixedly connected to one end of the fixed rod one away from the ball valve.

[0015] Through the above technical scheme, the bottom of the stirring barrel is communicated with the discharging pipe, the handle drives the fixed rod one to rotate, the fixed rod one rotates in the discharging pipe, and the fixed rod one is fixed with the ball valve, so that the waste liquid can be conveniently discharged, and the next work can be quickly prepared.

[0016] Compared with the prior art, the utility model has the advantages that:

[0017] The utility model discloses a stirring barrel for material mixing, which comprises a stirring barrel body, a feeding pipe, a solvent pipe, a motor, a stirring blade, a heating rod, a fixed rod, a fixed column, a fixed block and a ball valve.

[0018] The utility model discloses a stirring barrel for material mixing, which comprises a stirring barrel body, a feeding pipe, a solvent pipe, a motor, a stirring blade, a heating rod, a fixed rod, a fixed column, a fixed block and a ball valve. BRIEF DESCRIPTION OF DRAWINGS

[0019] Figure 1 It is whole structure schematic diagram of the utility model;

[0020] Figure 2 It is structure schematic diagram of stirring mechanism of the utility model;

[0021] Figure 3 It is structure schematic diagram of purification mechanism of the utility model;

[0022] Figure 4 It is cross section structure schematic diagram of support block of the utility model;

[0023] Figure 5 It is structure schematic diagram of discharging mechanism of the utility model.

[0024] Main symbol explanation:

[0025] 1, stirring mechanism; 101, the shell; 102, heating rod; 103, feed pipe; 104, stirring barrel; 105, solvent pipe; 106, fixed block; 107, fixed column; 108, motor; 109, fixed rod; 110, stirring blade; 2, purification mechanism; 201, steam pipe; 202, condenser pipe; 203, cooling pipe; 204, liquid inlet pipe; 205, water pump; 206, fixed block one; 207, coiled pipe; 208, support block; 209, liquid outlet pipe; 210, support seat; 211, motor one; 212, rotating rod; 213, fan blade; 214, exhaust pipe; 215, collection barrel; 3, discharge mechanism; 301, discharge pipe; 302, fixed rod one; 303, ball valve; 304, handle. DETAILED DESCRIPTION

[0026] The utility model will be described further, combined with the drawings and specific implementation, it is to be explained that under the premise of not conflicting, the following described each embodiment or each technical feature between can be arbitrarily combined to form new embodiment.

[0027] Embodiment:

[0028] Please combine Figures 1-5 The embodiment of the application is a rectification and purification barrel for anthraquinone production, which comprises a stirring mechanism 1, a purification mechanism 2, and a discharge mechanism 3. The stirring mechanism 1 is located at the top of the discharge mechanism 3, and the purification mechanism 2 is located at the right side of the stirring mechanism 1.

[0029] The stirring mechanism 1 comprises a shell 101. A heating rod 102 is fixedly connected to the inner wall of the shell 101. A feed pipe 103 is fixedly connected to the inside of the shell 101. The feed pipe 103 is communicatively connected to a stirring barrel 104. The stirring barrel 104 is fixedly connected to the outer wall of the heating rod 102. A solvent pipe 105 is communicatively connected to the inside of the stirring barrel 104. The solvent pipe 105 is fixedly connected to the inside of the shell 101. A fixed block 106 is fixedly connected to the inner wall of the stirring barrel 104. A fixed column 107 is fixedly connected to the outer wall of the fixed block 106. A motor 108 is fixedly connected to the inside of the fixed column 107. A fixed rod 109 is fixedly connected to the output end of the motor 108. A stirring blade 110 is fixedly connected to the outer wall of the fixed rod 109.

[0030] The purification mechanism 2 comprises a steam pipe 201. The steam pipe 201 is communicatively connected to the inside of the stirring barrel 104. A condenser pipe 202 is communicatively connected to the end of the steam pipe 201 away from the stirring barrel 104. A cooling pipe 203 is fixedly connected to the outer wall of the condenser pipe 202.

[0031] A liquid inlet pipe 204 is communicatively connected to the inside of the cooling pipe 203. A water pump 205 is communicatively connected to the end of the liquid inlet pipe 204 away from the cooling pipe 203. A fixed block one 206 is fixedly connected to the outer wall of the water pump 205. A coiled pipe 207 is communicatively connected to the end of the water pump 205 away from the liquid inlet pipe 204.

[0032] The outer wall of the coiled tube 207 is fixedly connected with a support block 208, the support block 208 is fixedly connected at the bottom of the fixed block one 206, the support block 208 is fixedly connected at the outer wall of the shell 101, and the end, away from the water pump 205, of the coiled tube 207 is communicatively provided with a liquid outlet pipe 209.

[0033] The end, away from the coiled tube 207, of the liquid outlet pipe 209 is communicatively provided inside the cooling pipe 203, the inner wall of the support block 208 is fixedly connected with a support seat 210, the top of the support seat 210 is fixedly connected with a motor one 211, and the output end of the motor one 211 is fixedly connected with a rotating rod 212.

[0034] The outer wall of the rotating rod 212 is fixedly connected with a fan blade 213, the end, close to the liquid outlet pipe 209, of the condensing pipe 202 is communicatively provided with an exhaust pipe 214, and the end, away from the steam pipe 201, of the condensing pipe 202 is communicatively provided with a collection bucket 215.

[0035] The discharging mechanism 3 comprises a discharging pipe 301, the discharging pipe 301 is communicatively provided inside the stirring barrel 104, a fixed rod one 302 is rotatably connected inside the discharging pipe 301, a ball valve 303 is fixedly connected at the back of the fixed rod one 302, the ball valve 303 is contactively provided at the inner wall of the discharging pipe 301, and a handle 304 is fixedly connected at the end, away from the ball valve 303, of the fixed rod one 302.

[0036] The implementation principle of the rectification and purification barrel for anthraquinone production in the embodiment of the application is as follows: when in use, the material enters the stirring barrel 104 through the feeding pipe 103, and the solvent is added according to the proportion, and the solvent enters the stirring barrel 104 through the solvent pipe 105, at this time, the heating rod 102 heats the material in the stirring barrel 104, the fixed block 106 is fixed on the inner wall of the stirring barrel 104, the fixed column 107 is fixed on the outer wall of the fixed block 106, the motor 108 is fixed in the fixed column 107, the fixed column 107 protects the motor 108 from high temperature and liquid damage, so that the motor 108 can operate normally, the fixed rod 109 is fixed on the output end of the motor 108, and the stirring blade 110 is fixed on the outer wall of the fixed rod 109, through slow stirring, the contact area between the solvent and the raw material is increased, so that the two are fully contacted, the solubility is improved, and the mixing is sufficient, which helps to accelerate the dissolution process of the solvent and the solute, so that the reaction is promoted, the consistency of the product quality can be ensured, and the efficiency of the production process is improved, because the temperature of the raw material is increased, so that steam is generated, the steam enters the condensing pipe 202 through the steam pipe 201, the cooling pipe 203 is fixed on the outer wall of the condensing pipe 202, the water pump 205 sends the cooling liquid to the inside of the cooling pipe 203 through the liquid inlet pipe 204, the cooling liquid contacts the outer wall of the condensing pipe 202, so that the temperature of the condensing pipe 202 is reduced, the water vapor is changed into liquid, and then enters the collecting barrel 215, at the same time, the cooling liquid enters the serpentine pipe 207 through the liquid outlet pipe 209, the serpentine pipe 207 is communicated with the water pump 205, so that the circulation is completed, at the same time, the motor one 211 drives the fan blade 213 to rotate through the rotating rod 212, so that the cooling of the cooling liquid in the serpentine pipe 207 is accelerated, the condensation effect of the water vapor is accelerated, the condensation rate of the equipment is improved, the operation efficiency of the whole system is enhanced, the waste liquid can be conveniently discharged, and the next work can be prepared quickly.

[0037] The above embodiment is only a preferred embodiment of the utility model, and cannot be used to limit the range of protection of the utility model, and any non-substantial change and replacement made by the person skilled in the art on the basis of the utility model belongs to the range of protection of the utility model.

Claims

1. A distillation and purification tank for anthraquinone production, characterized in that: It includes a stirring mechanism (1), a purification mechanism (2) and a discharge mechanism (3), wherein the stirring mechanism (1) is located on top of the discharge mechanism (3) and the purification mechanism (2) is located on the right side of the stirring mechanism (1); The stirring mechanism (1) includes a housing (101), a heating rod (102) is fixedly connected to the inner wall of the housing (101), a feed pipe (103) is fixedly connected inside the housing (101), a stirring tank (104) is connected to the feed pipe (103), the stirring tank (104) is fixedly connected to the outer wall of the heating rod (102), a solvent pipe (105) is connected inside the stirring tank (104), the solvent pipe (105) is fixedly connected inside the housing (101), a fixing block (106) is fixedly connected to the inner wall of the stirring tank (104), a fixing column (107) is fixedly connected to the outer wall of the fixing block (106), a motor (108) is fixedly connected inside the fixing column (107), a fixing rod (109) is fixedly connected to the output end of the motor (108), and a stirring blade (110) is fixedly connected to the outer wall of the fixing rod (109).

2. The distillation and purification tank for anthraquinone production as described in claim 1, characterized in that, The purification mechanism (2) includes a steam pipe (201), which is connected to the inside of the stirring tank (104). A condenser pipe (202) is connected to one end of the steam pipe (201) away from the stirring tank (104), and a cooling pipe (203) is fixedly connected to the outer wall of the condenser pipe (202).

3. The distillation and purification tank for anthraquinone production as described in claim 2, characterized in that, The cooling pipe (203) is internally connected to an inlet pipe (204), and a water pump (205) is connected to one end of the inlet pipe (204) away from the cooling pipe (203). A fixing block (206) is fixedly connected to the outer wall of the water pump (205), and a serpentine pipe (207) is connected to one end of the water pump (205) away from the inlet pipe (204).

4. The distillation and purification tank for anthraquinone production as described in claim 3, characterized in that, The outer wall of the serpentine tube (207) is fixedly connected to a support block (208), the support block (208) is fixedly connected to the bottom of the fixed block (206), the support block (208) is fixedly connected to the outer wall of the outer shell (101), and the end of the serpentine tube (207) away from the water pump (205) is connected to an outlet pipe (209).

5. The distillation and purification tank for anthraquinone production as described in claim 4, characterized in that, The end of the outlet pipe (209) away from the serpentine pipe (207) is connected to the inside of the cooling pipe (203). The bottom of the inner wall of the support block (208) is fixedly connected to the support base (210). The top of the support base (210) is fixedly connected to the motor (211). The output end of the motor (211) is fixedly connected to the rotating rod (212).

6. The distillation and purification tank for anthraquinone production as described in claim 5, characterized in that, The outer wall of the rotating rod (212) is fixedly connected with a fan blade (213), and the end of the condenser tube (202) near the liquid outlet tube (209) is connected to an exhaust pipe (214), and the end of the condenser tube (202) away from the steam pipe (201) is connected to a collection bucket (215).

7. The distillation and purification tank for anthraquinone production as described in claim 1, characterized in that, The discharge mechanism (3) includes a discharge pipe (301), which is connected to the inside of the mixing tank (104). A fixed rod (302) is rotatably connected inside the discharge pipe (301). A ball valve (303) is fixedly connected to the back of the fixed rod (302). The ball valve (303) is in contact with the inner wall of the discharge pipe (301). A handle (304) is fixedly connected to the end of the fixed rod (302) away from the ball valve (303).

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