Water-free cooperative treatment device

Abstract

The utility model belongs to the technical field of molecular sieve processing, particularly relates to an anhydrous cooperative processing device, and provides the following scheme aiming at the problems of non-uniform dispersion and too fast blanking in the background technology: the anhydrous cooperative processing device comprises a baking section furnace stainless steel pipe, and a blanking hopper for guiding a molecular sieve to be blanked is arranged on the outer wall of the top of the baking section furnace stainless steel pipe; a spiral discharging assembly and a molecular sieve dispersing assembly are arranged in the baking section furnace stainless steel pipe, and the spiral discharging assembly is located above the molecular sieve dispersing assembly. Through the synergistic effect of the spiral discharging assembly and the molecular sieve dispersing assembly, the discharging time is prolonged, molecular sieves can be fully dried, and then the molecular sieves are uniformly dispersed through the guide plate of the conical dispersing disc and are prevented from being stacked. The blanking speed of the molecular sieve is slowed down through the cooperation of the striker plate and the feed port, the retention time of the molecular sieve in the stainless steel pipe of the baking section furnace is further prolonged, and the overall thermal insulation performance is improved and the energy consumption is reduced by combining the directional airflow control of the breather pipe.

Description

Technical Field

[0001] This utility model relates to the field of molecular sieve processing technology, and in particular to an anhydrous co-processing device. Background Technology

[0002] The anhydrous co-processing unit is a device specifically designed for molecular sieve processing, primarily used for the anhydrous preparation of organic solvents and the efficient regeneration of molecular sieves. Molecular sieves, as porous materials, are widely used in adsorption, separation, and catalysis, playing a crucial role, especially in solvent dehydration. Traditional molecular sieve processing methods often employ static adsorption or simple dynamic circulation, resulting in low adsorption efficiency, incomplete regeneration, and high energy consumption. The anhydrous co-processing unit integrates spiral feeding, dynamic dispersion, and multi-stage calcination technologies, achieving uniform heating and dehydration of molecular sieves in a continuous flow state, significantly improving processing efficiency and product regeneration quality. This unit is particularly suitable for the production of high-purity organic solvents, such as pharmaceutical intermediates and electronic chemicals, and has broad market prospects.

[0003] Current molecular sieve dehydration technology has some problems in practical applications:

[0004] Uneven dispersion and excessively fast feeding: Traditional devices rely on gravity feeding, which makes molecular sieves prone to accumulating into clumps, resulting in uneven heating. In some areas, moisture is not completely removed, leading to poor regeneration. Due to incomplete dehydration, residual moisture may cause side reactions between the molecular sieve and the solvent, reducing product purity. Utility Model Content

[0005] In view of the shortcomings of the prior art, this utility model provides a waterless co-processing device, which overcomes the shortcomings of the prior art and effectively solves the problems of uneven dispersion and excessively fast feeding.

[0006] To achieve the above objectives, the present invention adopts the following technical solution:

[0007] A waterless co-processing device includes a calcining furnace stainless steel tube. The top outer wall of the calcining furnace stainless steel tube is provided with a feeding hopper for guiding molecular sieve feeding. The interior of the calcining furnace stainless steel tube is respectively provided with a spiral feeding assembly and a molecular sieve dispersion assembly, with the spiral feeding assembly located above the molecular sieve dispersion assembly.

[0008] The spiral feeding assembly includes a vertical pipe installed inside the stainless steel tube of the baking section furnace, spiral auger blades welded to the outer wall of the vertical pipe, a baffle plate welded to the bottom outer wall of the spiral auger blades, a feed inlet opened at the bottom of the outer wall of the vertical pipe, and a discharge cylinder welded to the bottom outer wall of the vertical pipe. The feed inlet is located on one side of the baffle plate, and the discharge cylinder has a discharge port located directly above the molecular sieve dispersion assembly on the bottom outer wall.

[0009] Preferably, the molecular sieve dispersion assembly includes a conical dispersion disk welded to the inner wall of the stainless steel tube of the baking furnace, guide plates evenly distributed on the outer wall of the conical dispersion disk, and positioning holes opened on the outer wall of the conical dispersion disk.

[0010] Preferably, a fixing ring is welded to the top of the outer wall of the stainless steel tube of the baking section furnace, and a support rod is welded between the fixing ring and the feeding hopper.

[0011] Preferably, a flange is welded to the outer wall of the bottom of the stainless steel tube of the baking section furnace.

[0012] Preferably, support frames are welded to the outer walls of both ends of the vertical pipe, and the support frames are welded to the inner wall of the stainless steel pipe of the baking furnace.

[0013] Preferably, the conical dispersion disc includes a ramp and a central plate, wherein the guide plate is disposed on the outer wall of the ramp, and the central plate is located at the top center of the ramp.

[0014] Preferably, a vent pipe is welded to one side of the outer wall of the stainless steel tube of the baking section furnace, and the vent pipe is located at the top of one side of the conical dispersion plate.

[0015] The beneficial effects of this utility model are as follows:

[0016] 1. The anhydrous co-processing device designed in this invention utilizes the synergistic effect of the screw feeder and the molecular sieve dispersion assembly. During the feeding process, the molecular sieve is conveyed layer by layer by the screw conveyor blades, extending the feeding time and allowing it to dry thoroughly. Afterward, the molecular sieve is evenly dispersed by the guide plate of the conical dispersion disc, preventing accumulation. The dispersed molecular sieve is fully exposed to the thermal environment of the stainless steel tubes in the baking furnace, achieving comprehensive and uniform heating, further improving dehydration efficiency.

[0017] 2. The waterless co-processing device in this design slows down the feeding speed of the molecular sieve by coordinating the baffle plate and the feed port, further extending its residence time in the stainless steel tube of the baking section furnace. Combined with the directional airflow control of the vent pipe, it improves the overall heat preservation performance and reduces energy consumption. Attached Figure Description

[0018] Figure 1 This is a schematic diagram of the overall structure of a waterless co-processing device proposed in this utility model.

[0019] Figure 2 This is a schematic diagram of the internal structure of the stainless steel tube of the baking section furnace in the waterless co-processing device proposed in this utility model.

[0020] Figure 3 A schematic diagram of the spiral feeding assembly structure of the waterless co-processing device proposed in this utility model. Figure 1 ;

[0021] Figure 4A schematic diagram of the spiral feeding assembly structure of the waterless co-processing device proposed in this utility model. Figure 2 ;

[0022] Figure 5 This is a schematic diagram of the molecular sieve dispersion component of an anhydrous synergistic treatment device proposed in this utility model.

[0023] In the diagram: 1. Stainless steel pipe of the baking section furnace; 2. Feed hopper; 3. Spiral feeding assembly; 31. Vertical pipe; 32. Spiral auger blades; 33. Baffle plate; 34. Feed inlet; 35. Discharge cylinder; 4. Molecular sieve dispersion assembly; 41. Conical dispersion disc; 42. Guide plate; 43. Positioning hole; 5. Fixing ring; 6. Support rod; 7. Flange; 8. Support frame; 9. Discharge port; 10. Slope; 11. Center plate; 12. Vent pipe. Detailed Implementation

[0024] The technical solutions of the present utility model will be clearly and completely described below with reference to the accompanying drawings of the embodiments of the present utility model. Obviously, the described embodiments are only some embodiments of the present utility model, and not all embodiments.

[0025] Reference Figures 1-5 Example 1: A waterless co-processing device includes a calcining furnace stainless steel tube 1. The top outer wall of the calcining furnace stainless steel tube 1 is provided with a feeding hopper 2 for guiding molecular sieve feeding. The interior of the calcining furnace stainless steel tube 1 is respectively provided with a spiral feeding assembly 3 and a molecular sieve dispersion assembly 4. The spiral feeding assembly 3 is located above the molecular sieve dispersion assembly 4.

[0026] The spiral feeding assembly 3 includes a vertical pipe 31 disposed inside the stainless steel pipe 1 of the baking section furnace, spiral auger blades 32 welded to the outer wall of the vertical pipe 31, a baffle plate 33 welded to the bottom outer wall of the spiral auger blades 32, a feed inlet 34 opened on the bottom of the outer wall of the vertical pipe 31, and a discharge cylinder 35 welded to the bottom outer wall of the vertical pipe 31. The feed inlet 34 is located on one side of the baffle plate 33, and the bottom outer wall of the discharge cylinder 35 is provided with a discharge port 9 located directly above the molecular sieve dispersion assembly 4.

[0027] In this embodiment, the vertical tube 31 is located at the inner center of the stainless steel tube 1 of the baking section furnace. The outer wall of the vertical tube 31 is welded with spiral auger blades 32. The baffle plate 33 is a stainless steel plate and is welded to the bottom of the spiral auger blades 32. The outer wall of the vertical tube 31 has an inlet 34 located on one side of the baffle plate 33.

[0028] Example 2: A waterless co-processing device, wherein the molecular sieve dispersion component 4 includes a conical dispersion disk 41 welded to the inner wall of the stainless steel tube 1 of the calcining furnace, guide plates 42 evenly distributed on the outer wall of the conical dispersion disk 41, and positioning holes 43 formed on the outer wall of the conical dispersion disk 41. The conical dispersion disk 41 includes a ramp 10 and a central plate 11, wherein the guide plates 42 are disposed on the outer wall of the ramp 10, and the central plate 11 is located at the top center of the ramp 10. A vent pipe 12 is welded to one side of the outer wall of the stainless steel tube 1 of the calcining furnace, and the vent pipe 12 is located at the top of one side of the conical dispersion disk 41.

[0029] In this embodiment, a conical dispersion disk 41 is welded to the inner wall of the stainless steel tube 1 of the baking furnace, and equidistant guide plates 42 are provided on the upper surface of the conical dispersion disk 41. The guide plates 42 are radially distributed to uniformly guide the falling molecular sieve into the positioning holes 43. Positioning holes 43 for dispersing the molecular sieve are opened on the outer walls of the center plate 11 and the ramp 10.

[0030] A fixing ring 5 is welded to the top of the outer wall of the stainless steel tube 1 of the baking furnace, and a support rod 6 is welded between the fixing ring 5 and the feeding hopper 2. A flange 7 is welded to the bottom outer wall of the stainless steel tube 1 of the baking furnace. Support frames 8 are welded to the outer walls of both ends of the vertical tube 31, and the support frames 8 are welded to the inner wall of the stainless steel tube 1 of the baking furnace.

[0031] The vent pipe 12 is welded to the side wall of the stainless steel pipe 1 of the baking furnace. The inlet can be connected to a nitrogen source, and the outlet points to the top of the stainless steel pipe 1 of the baking furnace, forming an inert gas protective layer. The flange 7 has a ring structure and can be connected to an external heating furnace by bolts to ensure a tight connection.

[0032] Working principle:

[0033] Molecular sieves enter the stainless steel tube 1 of the baking furnace through the feed hopper 2. The molecular sieves spiral downwards along the outer wall of the spiral auger blades 32 and are conveyed downwards along the vertical pipe 31, slowing down the feeding speed of the molecular sieves. At the same time, nitrogen can be introduced through the vent pipe 12 to replace the residual oxygen in the furnace. The gas can carry away the moisture in the molecular sieves to complete the drying operation. Afterwards, the baffle plate 33 is used to block the molecular sieves, causing them to fall onto the conical dispersion plate 41 through the feed port 34. Under the guidance of the guide plate 42, the molecular sieves diffuse in all directions and continue to fall into the positioning hole 43.

[0034] The above description is only a preferred embodiment of the present utility model, but the protection scope of the present utility model is not limited thereto. Any equivalent substitutions or changes made by those skilled in the art within the technical scope disclosed in the present utility model, based on the technical solution and the inventive concept of the present utility model, should be included within the protection scope of the present utility model.

Claims

1. A waterless co-processing device comprising a calcination section of a furnace stainless steel tube (1), characterized in that, The top outer wall of the calcination section furnace stainless steel pipe (1) is provided with a discharging hopper (2) for guiding the discharging of molecular sieve, and the inner part of the calcination section furnace stainless steel pipe (1) is respectively provided with a spiral discharging assembly (3) and a molecular sieve dispersing assembly (4), wherein the spiral discharging assembly (3) is located above the molecular sieve dispersing assembly (4); The spiral discharging assembly (3) comprises a vertical pipe (31) arranged inside the calcination section furnace stainless steel pipe (1), spiral auger blades (32) welded on the outer wall of the vertical pipe (31), a baffle plate (33) welded on the bottom outer wall of the spiral auger blades (32), a feeding port (34) opened on the bottom outer wall of the vertical pipe (31), and a discharging cylinder (35) welded on the bottom outer wall of the vertical pipe (31), wherein the feeding port (34) is located on one side of the baffle plate (33), and the bottom outer wall of the discharging cylinder (35) is located directly above the molecular sieve dispersing assembly (4) and is provided with a discharging port (9).

2. A waterless co-processing device according to claim 1, wherein, The molecular sieve dispersing assembly (4) comprises a conical dispersing disc (41) welded on the inner wall of the calcination section furnace stainless steel pipe (1), equidistantly distributed guide plates (42) arranged on the outer wall of the conical dispersing disc (41), and positioning holes (43) opened on the outer wall of the conical dispersing disc (41).

3. A waterless co-processing device according to claim 1, wherein, The top outer wall of the calcination section furnace stainless steel pipe (1) is welded with a fixing ring (5), and a support rod (6) is welded between the fixing ring (5) and the discharging hopper (2).

4. A waterless co-processing device according to claim 1, wherein, The bottom outer wall of the calcination section furnace stainless steel pipe (1) is welded with a flange plate (7).

5. A waterless co-processing device according to claim 1, wherein, The outer walls of both ends of the vertical pipe (31) are welded with support frames (8), and the support frames (8) are welded on the inner wall of the calcination section furnace stainless steel pipe (1).

6. A waterless co-processing device according to claim 2, wherein, The conical dispersing disc (41) comprises a slope (10) and a center plate (11), wherein the guide plates (42) are arranged on the outer wall of the slope (10), and the center plate (11) is located at the top center of the slope (10).

7. A waterless co-processing device according to claim 1, wherein, The outer wall of one side of the calcination section furnace stainless steel pipe (1) is welded with an air pipe (12), and the air pipe (12) is located at the top of one side of the conical dispersing disc (41).

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