Intelligent integrated distillation instrument

Abstract

The utility model discloses an intelligent integrated distillation instrument, which relates to the technical field of distillation instruments and comprises a distillation instrument body, a support is arranged at the top of one side of the distillation instrument body, a condenser pipe is arranged in the support, a collecting bottle is correspondingly arranged below the condenser pipe, two arc-shaped plates are attached to the bottom of the condenser pipe, and the two arc-shaped plates are arranged on the support. A sliding rod is fixedly arranged on one side of the arc-shaped plate, one end of the sliding rod penetrates through the support and is fixedly provided with a circular plate, the sliding rod is sleeved with a first spring, and moving assemblies for moving the sliding rod are arranged on the two sides of the support; the utility model has the beneficial effects that the fixing and dismounting process of the condenser pipe is simplified, the operation and subsequent maintenance efficiency is improved, and the workload of experimenters is reduced; the device is simple in structure and convenient to use, the collecting bottle can be conveniently and stably clamped, the collecting bottle cannot topple over in the using process, normal proceeding of an experiment is guaranteed, the collecting bottle cannot be damaged, and experiment safety accidents are avoided.

Description

Technical Field

[0001] This utility model relates to a distillation apparatus, and more particularly to an intelligent integrated distillation apparatus, belonging to the field of distillation apparatus technology. Background Technology

[0002] Distillation is a commonly used purification technique in laboratories. It utilizes the different boiling points of components in a liquid mixture or liquid-solid system, causing the lower-boiling-point component to evaporate and then condense to separate the relevant components. Compared with other separation methods, such as extraction, filtration, and crystallization, distillation has the advantage of not requiring the use of additional solvents during the process. This means that no new impurities are introduced during distillation, effectively ensuring the purity of the product. Currently, intelligent distillation apparatuses are generally used for distillation operations.

[0003] Currently, most intelligent distillation apparatuses on the market use two arc-shaped clamps and bolts to secure the condenser tubes. This method has significant drawbacks: when the condenser tubes are damaged or need replacement due to long-term use, the bolts must be removed, resulting in low maintenance efficiency and increased workload for experimenters. Furthermore, the collection bottles used to collect distilled water are often placed directly on the tray. Experimenters may accidentally touch the edge of the tray or bump it while operating other instruments, which could easily cause the collection bottles to tip over, leading to experimental failure or even damage to the collection bottles, resulting in experimental safety accidents. Utility Model Content

[0004] The purpose of this invention is to provide an intelligent integrated distillation apparatus to solve the problem mentioned in the background art that current intelligent distillation apparatuses mostly use arc-shaped clamps and bolts to fix the condenser tubes, which requires disassembling the bolts during maintenance, resulting in low efficiency and increased burden on experimental personnel.

[0005] To achieve the above objectives, this utility model provides the following technical solution: an intelligent integrated distillation apparatus, comprising a distillation apparatus body, a plurality of supports on the top of one side of the distillation apparatus body, a condenser tube inside the supports, a collection bottle correspondingly below the condenser tube, two fitting arc-shaped plates at the bottom of the condenser tube, a slide rod fixedly mounted on one side of the arc-shaped plates, one end of the slide rod passing through the supports and fixedly mounted on a circular plate, a spring sleeved on the outside of the slide rod, moving components for moving the slide rod on both sides of the supports, clamping plates on both sides of the collection bottle, a support plate fixedly mounted at the bottom of the distillation apparatus body, and a tensioning component inside the support plate.

[0006] As a preferred embodiment of this utility model, a base is fixedly provided at the bottom of the distillation apparatus body, and an anti-slip pad is fixedly provided at the bottom of the base. The anti-slip pad is made of rubber. A first anti-slip pad is fixedly provided on the inner wall of the arc-shaped plate, and a second anti-slip pad is fixedly provided on the inner wall of the clamping plate.

[0007] As a preferred embodiment of this utility model, a plurality of heating frames are fixedly provided on one side of the top of the distillation apparatus body, a flask is placed inside the heating frame, and a ceramic heating plate for heating the flask is provided at the bottom of the heating frame. A box is fixedly provided in the middle of the top of the distillation apparatus body, and a plurality of evenly spaced pull ropes are fixedly provided on one side of the box. One end of the pull rope is provided with a sealing plug for sealing the flask. An extension tube is fixedly provided on the top of one side of the flask, and a rubber stopper is fixedly provided between the extension tube and the condenser tube.

[0008] As a preferred embodiment of this utility model, a water inlet pipe is fixedly provided at the bottom of the two condenser tubes located in the middle. One end of the water inlet pipe is fixedly connected to the water outlet pipe built into the distillation apparatus body. A connecting pipe is fixedly provided between the other two adjacent condenser tubes. One end of the connecting pipe located on the side is fixedly connected to the reflux pipe built into the distillation apparatus body.

[0009] As a preferred embodiment of this utility model, a rubber tube is fitted at the bottom end of the condenser tube, an mounting plate is fixedly provided on one side of the top of the bracket, and a bolt is slidably provided inside the mounting plate. A threaded hole for threaded connection with the bolt is provided on the top of one side of the distillation apparatus body.

[0010] As a preferred embodiment of this utility model, the movable component includes two support blocks, which are symmetrically arranged on one side of the bracket. A pressing plate is rotatably provided between the two support blocks. The top of one side of the pressing plate is in contact with one side of the circular plate. An arc-shaped groove is provided on the top of the pressing plate to cooperate with the sliding rod. Several evenly spaced anti-slip grooves are provided on the bottom of one side of the pressing plate. One end of the spring is fixedly connected to one side of the arc-shaped plate, and the other end is fixedly connected to the inner wall of the bracket.

[0011] As a preferred technical solution of this utility model, the tensioning assembly includes a plurality of tensioning rods, which are slidably arranged at even intervals inside the support plate. One end of each tensioning rod is fixedly connected to one side of the clamping plate on the left side, and the bottom end of the clamping plate on the right side is fixedly connected to the bottom of the distillation apparatus body. A second spring is sleeved in the middle of each tensioning rod, one end of which is fixedly connected to one side of the clamping plate, and the other end is fixedly connected to one side of the support plate.

[0012] As a preferred embodiment of the present invention, a tension cap is fixedly provided at the other end of the tension rod, and two guide rods are symmetrically fixed on one side of the clamping plate on the left side, with one end of the guide rod penetrating the support plate and extending to the outside of the support plate.

[0013] Compared with related technologies, the intelligent integrated distillation apparatus provided by this utility model has the following beneficial effects:

[0014] 1. With the addition of a movable component, the experimenter only needs to press two pressing plates simultaneously to move the slide bar and the arc plate by means of their contact and linkage with the circular plate. This simplifies the process of fixing and disassembling the condenser tube, improves the efficiency of operation and subsequent maintenance, and reduces the workload of the experimenter.

[0015] 2. The tensioning component allows the left clamp to be stretched and moved to cooperate with the right clamp, thus facilitating stable clamping of the collection bottle and preventing it from tipping over during use. This ensures the normal conduct of the experiment, prevents damage to the collection bottle, and avoids experimental safety accidents. Attached Figure Description

[0016] Figure 1 This is a schematic diagram of the structure of this utility model;

[0017] Figure 2 This is an exploded structural diagram of the distillation apparatus body of this utility model;

[0018] Figure 3 This is an exploded structural diagram of the bracket of this utility model;

[0019] Figure 4 This is a schematic diagram of the structure of the condenser tube of this utility model;

[0020] Figure 5 This is a schematic diagram of the structure of the bracket of this utility model;

[0021] Figure 6 This is a cross-sectional structural diagram of the bracket of this utility model;

[0022] Figure 7 This is a schematic diagram of the structure of the clamping plate of this utility model;

[0023] Figure 8 This is an exploded structural diagram of the clamping plate of this utility model.

[0024] In the diagram: 1. Distillation apparatus body; 2. Support; 3. Condenser; 4. Collection bottle; 5. Arc plate; 6. Slide rod; 7. Spring 1; 8. Circular plate; 9. Clamping plate; 10. Support plate; 11. Moving assembly; 1101. Support block; 1102. Pressing plate; 1103. Arc groove; 1104. Anti-slip groove; 12. Tensioning assembly; 1201. Tensioning rod; 1202. Spring 2; 1203. Guide rod; 1204. Tensioning cap; 13. Water inlet pipe; 14. Connecting pipe; 15. Box body; 16. Heating frame; 17. Flask; 18. Extension tube; 19. Rubber stopper; 20. Pull rope; 21. Sealing plug; 22. Base; 23. Rubber tube; 24. Mounting plate; 25. Bolt. Detailed Implementation

[0025] The technical solutions of the present utility model will be clearly and completely described below with reference to the accompanying drawings of the embodiments. Obviously, the described embodiments are only some embodiments of the present utility model, and not all embodiments. Based on the embodiments of the present utility model, all other embodiments obtained by those of ordinary skill in the art without creative effort are within the protection scope of the present utility model.

[0026] Please see Figure 1-8 This utility model provides an intelligent integrated distillation apparatus, including a distillation apparatus body 1. Several evenly spaced supports 2 are provided on the top of one side of the distillation apparatus body 1. A condenser tube 3 is installed inside each support 2, and the interior of the condenser tube 3 is spirally arranged. The spiral tube is used to drain distilled water, increasing the contact area with cold water and improving the distillation effect. A collection bottle 4 is correspondingly located below the condenser tube 3. Two arc-shaped plates 5 are attached to the bottom of the condenser tube 3. A slide rod 6 is fixed to one side of each arc-shaped plate 5. One end of the slide rod 6 passes through the support 2 and is fixed to a circular plate 8. A spring 7 is sleeved on the outside of the slide rod 6. Moving components 11 for moving the slide rod 6 are provided on both sides of the support 2. Through the moving components 11, the distillation process is completed. The experimenter only needs to move the two circular plates 8 simultaneously to easily move the sliding rod 6 and the arc plate 5, simplifying the fixing and disassembly process of the condenser tube 3, improving the efficiency of operation and subsequent maintenance, and reducing the workload of the experimenter. The collecting bottle 4 is equipped with clamping plates 9 on both sides, and the bottom of the distillation apparatus body 1 is fixedly equipped with a support plate 10. The support plate 10 is equipped with a tensioning component 12 inside. Through the tensioning component 12, the clamping plate 9 on the left side can be moved. Combined with the clamping plate 9 on the left side, it is easy to stably clamp the collecting bottle 4, so that the collecting bottle 4 will not tip over during use, ensuring the normal conduct of the experiment, preventing the collecting bottle 4 from being damaged, and avoiding experimental safety accidents.

[0027] The movable component 11 includes two support blocks 1101, which are symmetrically arranged on one side of the support 2. A pressing plate 1102 is rotatably positioned between the two support blocks 1101. The top of one side of the pressing plate 1102 is in contact with one side of the circular plate 8. An arc-shaped groove 1103 is formed on the top of the pressing plate 1102 to cooperate with the sliding rod 6. Several evenly spaced anti-slip grooves 1104 are formed on the bottom of one side of the pressing plate 1102. One end of the spring 7 is fixedly connected to one side of the arc-shaped plate 5, and the other end is fixedly connected to the inner wall of the support 2. With the movable component 11, the experimenter only needs to press the two pressing plates simultaneously. 1102, through its contact and linkage with the circular plate 8, can easily move the sliding rod 6 and the arc plate 5, simplifying the process of fixing and disassembling the condenser tube 3, improving the efficiency of operation and subsequent maintenance, and reducing the workload of experimental personnel; the arc groove 1103 on the pressing plate 1102 cooperates with the sliding rod 6 to make the pressing plate 1102 swing without any restriction; its bottom anti-slip groove 1104 increases the friction when pressing, prevents hand slippage, and ensures operational safety; at the same time, the spring 7 can play a reset and rebound effect on the arc plate 5, which can provide a continuous and stable clamping force when fixing the condenser tube 3, ensuring that the object is firmly fixed.

[0028] The tensioning assembly 12 includes a plurality of tension rods 1201, which are evenly spaced and slidably disposed inside the support plate 10. One end of each tension rod 1201 is fixedly connected to one side of the clamping plate 9 on the left side, and the bottom end of the clamping plate 9 on the right side is fixedly connected to the bottom of the distillation apparatus body 1. A second spring 1202 is fitted in the middle of each tension rod 1201. One end of the second spring 1202 is fixedly connected to one side of the clamping plate 9, and the other end is fixedly connected to one side of the support plate 10. A tension cap 1204 is fixedly fitted to the other end of each tension rod 1201. The cap 1204 is located on one side of the clamping plate 9 on the left side. Two guide rods 1203 are fixedly provided, and one end of the guide rod 1203 passes through the support plate 10 and extends to the outside of the support plate 10. Through the tensioning assembly 12, the tensioning cap 1204 can drive the tensioning rod 1201 and the left clamping plate 9 to stretch and move, so as to cooperate with the right clamping plate 9. Under the reset and rebound of the spring 1202, the collection bottle 4 can be stably clamped, so as not to cause the collection bottle 4 to tip over during use, ensuring the normal conduct of the experiment, preventing the collection bottle 4 from being damaged, and avoiding experimental safety accidents.

[0029] Several heating frames 16 are fixedly installed on one side of the top of the distillation apparatus body 1. Flasks 17 are placed inside the heating frames 16, and ceramic heating plates for heating the flasks 17 are provided at the bottom of the heating frames 16. A housing 15 is fixedly installed in the middle of the top of the distillation apparatus body 1. Several evenly spaced pull ropes 20 are fixedly installed on one side of the housing 15. One end of each pull rope 20 is equipped with a sealing plug 21 to seal the flasks 17. An extension tube 18 is fixedly installed on the top of one side of the flasks 17, and a rubber stopper 19 is fixed between the extension tube 18 and the condenser tube 3. The multiple heating frames 16 installed at the top of the distillation apparatus body 1 can simultaneously heat multiple flasks 17, significantly improving experimental efficiency. Efficiency is ensured to meet diverse experimental needs. The bottom of the heating frame 16 uses a ceramic heating plate, which features rapid heating and uniform heating. The pull rope 20 on one side of the box 15 works in conjunction with the sealing plug 21 to facilitate quick sealing and opening of the flask 17 by the experimenter. This not only prevents steam leakage during distillation and ensures experimental safety, but also facilitates the addition of reactants at any time. The flask 17 is connected to the condenser 3 through the extension tube 18 and the rubber stopper 19, ensuring that the steam of the distillation product can be smoothly introduced into the condenser 3 for cooling and liquefaction. Moreover, the elastic sealing effect of the rubber stopper 19 can effectively prevent steam from escaping, while also facilitating disassembly and installation, and making it convenient for the maintenance and cleaning of the experimental equipment.

[0030] Two condenser tubes 3 located in the middle are fixedly equipped with water inlet pipes 13 at their bottoms. One end of the water inlet pipe 13 is fixedly connected to the water outlet pipe inside the distiller body 1. Connecting pipes 14 are fixedly connected between the other two adjacent condenser tubes 3. One end of the connecting pipe 14 located on the side is fixedly connected to the reflux pipe inside the distiller body 1. This pipe connection design allows the cold water inside the distiller body 1 to circulate. The central condenser tube 3 is connected to the water outlet pipe of the distiller body 1 through the water inlet pipe 13, which can precisely control the directional flow of cooling water, ensuring that the condenser tube 3 can continuously and stably cool, quickly converting vapor into liquid, and improving condensation efficiency. The connecting pipes 14 between adjacent condenser tubes 3 form a circulation path, allowing cooling water to flow through multiple condenser tubes 3, making full use of water resources and ensuring the heat exchange efficiency of the entire distillation system. The connection between the side connecting pipe 14 and the reflux pipe can promptly send the cold water back to the interior of the distiller body 1, realizing recycling.

[0031] A rubber tube 23 is fitted at the bottom of the condenser tube 3, and a mounting plate 24 is fixedly installed on one side of the top of the bracket 2. A bolt 25 is slidably installed inside the mounting plate 24, and a screw hole for threaded connection with the bolt 25 is opened on the top of one side of the distillation apparatus body 1. The rubber tube 23 facilitates the use of some taller collection bottles 4, making it easier to place them inside the taller collection bottles 4, and making it more convenient to use. The design of the mounting plate 24 on one side of the top of the bracket 2, together with the sliding bolt 25 and the screw hole of the distillation apparatus body 1, realizes the convenience of installing and disassembling the condenser tube 3, and makes it easy to disassemble the bracket 2 as needed.

[0032] A base 22 is fixedly installed at the bottom of the distillation apparatus body 1. An anti-slip pad made of rubber is fixedly installed at the bottom of the base 22. A first anti-slip pad is fixedly installed on the inner wall of the arc-shaped plate 5, and a second anti-slip pad is fixedly installed on the inner wall of the clamping plate 9. The rubber anti-slip pad on the base 22 at the bottom of the distillation apparatus body 1 increases the friction between the distillation apparatus body 1 and the placement surface, effectively preventing displacement of the instrument due to vibration or external force during operation, and ensuring the stability and safety of experimental operation. The first anti-slip pad on the inner wall of the arc-shaped plate 5 and the second anti-slip pad on the inner wall of the clamping plate 9 can closely fit the surface of the fixed object, providing a stable clamping force while avoiding scratch damage to the surface of the object. By increasing the contact area and friction, the clamped object is further prevented from loosening or slipping, ensuring that the distillation process is carried out safely and orderly.

[0033] In use, open the sealing plug 21, add an appropriate amount of the solution to be heated into the flask 17, then place the flask 17 on the inner wall of the heating frame 16, connect the tubing, and then use the tension cap 1204 to move the tension rod 1201 and the left clamp 9 to stretch and move the collection bottle 4 between the two clamps 9. Release the tension cap 1204, and the spring 1202 will return to its original position, allowing it to be stably clamped by the right clamp 9, preventing the collection bottle 4 from tipping over during use, ensuring the experiment proceeds normally, preventing damage to the collection bottle 4, and avoiding experimental safety accidents. Then control the heating... The ceramic heating plate at the bottom of frame 16 enables rapid and uniform heating of the solution inside flask 17 during operation. Simultaneously, the cooling water inside the distillation apparatus 1 is controlled to ensure stable and continuous cooling of the condenser tubes 3, rapidly converting vapor into liquid and improving condensation efficiency. Furthermore, the connecting pipes 14 between adjacent condenser tubes 3 form a circulation path, allowing cooling water to flow through multiple condenser tubes 3, ensuring the heat exchange efficiency of the entire distillation system. The connection between the side connecting pipes 14 and the reflux pipe allows cold water to be promptly returned to the interior of the distillation apparatus 1 for recycling. The water produced during distillation is collected in the collection bottle 4 via rubber tubing 23.

[0034] After collection is complete, turn off all electrical appliances. Stretch the set tension cap 1204 again and repeat the above steps. Remove the collection bottle 4 in sequence, and clean the flask 17 in sequence. Finally, when it is necessary to disassemble and maintain the condenser tube 3, remove the tube bodies on both sides of the condenser tube 3. By pressing the two pressing plates 1102 at the same time, the sliding rod 6 and the arc plate 5 can be easily moved by their contact with the circular plate 8. This simplifies the process of fixing and disassembling the condenser tube 3, improves the efficiency of operation and subsequent maintenance, and reduces the workload of experimental personnel.

[0035] Although embodiments of the present invention have been shown and described, it will be understood by those skilled in the art that various changes, modifications, substitutions and alterations can be made to these embodiments without departing from the principles and spirit of the present invention, the scope of which is defined by the appended claims and their equivalents.

Claims

1. An intelligent integrated distillation apparatus, comprising an apparatus body (1), characterized in that, The top of one side of the distillation apparatus body (1) is provided with several supports (2), the inside of the supports (2) is provided with condenser tubes (3), the bottom of the condenser tubes (3) is provided with a collection bottle (4), the bottom of the condenser tubes (3) is provided with two closely fitting arc-shaped plates (5), a slide rod (6) is fixedly provided on one side of the arc-shaped plate (5), one end of the slide rod (6) passes through the supports (2) and is fixedly provided with a circular plate (8), a spring (7) is sleeved on the outside of the slide rod (6), a moving component (11) is provided on both sides of the supports (2), a clamping plate (9) is provided on both sides of the collection bottle (4), a support plate (10) is fixedly provided at the bottom of the distillation apparatus body (1), and a tensioning component (12) is provided inside the support plate (10). The moving component (11) includes two support blocks (1101), which are symmetrically arranged on one side of the bracket (2). A pressing plate (1102) is rotatably provided between the two support blocks (1101). The top of one side of the pressing plate (1102) is in contact with one side of the circular plate (8). The top of the pressing plate (1102) is provided with an arc groove (1103) that moves in coordination with the slide rod (6). The bottom of one side of the pressing plate (1102) is provided with several evenly spaced anti-slip grooves (1104). One end of the spring (7) is fixedly connected to one side of the arc plate (5), and the other end is fixedly connected to the inner wall of the bracket (2).

2. The intelligent integrated distillation apparatus according to claim 1, characterized in that: The bottom of the distillation apparatus body (1) is fixedly provided with a base (22), and the bottom of the base (22) is fixedly provided with an anti-slip pad, which is made of rubber. The inner wall of the arc plate (5) is fixedly provided with a first anti-slip pad, and the inner wall of the clamp (9) is fixedly provided with a second anti-slip pad.

3. The intelligent integrated distillation apparatus according to claim 1, characterized in that: Several heating frames (16) are fixedly provided on one side of the top of the distillation apparatus body (1). A flask (17) is placed inside the heating frame (16), and a ceramic heating plate for heating the flask (17) is provided at the bottom of the heating frame (16). A box (15) is fixedly provided in the middle of the top of the distillation apparatus body (1). Several evenly spaced pull ropes (20) are fixedly provided on one side of the box (15). A sealing plug (21) for sealing the flask (17) is provided at one end of the pull rope (20). An extension tube (18) is fixedly provided on the top of one side of the flask (17). A rubber stopper (19) is fixed between the extension tube (18) and the condenser tube (3).

4. The intelligent integrated distillation apparatus according to claim 1, characterized in that: The bottom of the two condenser tubes (3) located in the middle is fixedly provided with water inlet pipes (13). One end of the water inlet pipes (13) is fixedly connected to the water outlet pipe built into the body of the distillation apparatus (1). A connecting pipe (14) is fixedly provided between the other two adjacent condenser tubes (3). One end of the connecting pipe (14) located on the side is fixedly connected to the reflux pipe built into the body of the distillation apparatus (1).

5. The intelligent integrated distillation apparatus according to claim 1, characterized in that: The bottom end of the condenser tube (3) is fitted with a rubber tube (23), and a mounting plate (24) is fixedly provided on one side of the top of the bracket (2). A bolt (25) is slidably provided inside the mounting plate (24), and a screw hole is provided on the top of one side of the distillation apparatus body (1) for threaded connection with the bolt (25).

6. The intelligent integrated distillation apparatus according to claim 1, characterized in that: The tensioning assembly (12) includes several tension rods (1201), which are evenly spaced and slidably disposed inside the support plate (10). One end of each tension rod (1201) is fixedly connected to one side of the clamping plate (9) on the left side, and the bottom end of the clamping plate (9) on the right side is fixedly connected to the bottom of the distillation apparatus body (1). A second spring (1202) is sleeved in the middle of each tension rod (1201). One end of the second spring (1202) is fixedly connected to one side of the clamping plate (9), and the other end is fixedly connected to one side of the support plate (10).

7. The intelligent integrated distillation apparatus according to claim 6, characterized in that: The other end of the tension rod (1201) is fixedly provided with a tension cap (1204), and two guide rods (1203) are symmetrically fixed on one side of the clamp (9) on the left side, and one end of the guide rod (1203) passes through the support plate (10) and extends to the outside of the support plate (10).

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