Steel lining fluorine-bromine water comprehensive separation bottle for extracting bromine from seawater

Abstract

The utility model belongs to the technical field of separation bottle devices, and particularly relates to a steel lining fluorine-bromine water comprehensive separation bottle for extracting bromine from seawater, which comprises a bottom frame, a separation bottle body is arranged above the bottom frame, one end of the separation bottle body is fixedly connected with a separation pipe, and an annular frame is arranged in the separation bottle body. Corresponding connecting holes are formed in the annular frame and the separation pipe, a through hole is formed in the rotating ring, connecting rods are fixedly connected to one side of the rotating ring, a fixing block is fixedly connected between the connecting rods, and a rotating rod is fixedly connected to one side of the fixing block; bromine water can be separated through a liquid inlet pipe and a separation bottle body, and one end of a rotating rod is located outside the center of the separation bottle body, so that a fixed block can be rotated by the rotating rod, the height of a through hole located on an annular frame is adjusted, the through hole can correspond to the bottom position of water, and the water is extracted and discharged; the device can be used for extracting and separating water separated from bromine water under the condition of ensuring that the device is sealed.

Description

Technical Field

[0001] The utility model belongs to the technical field of separation bottle devices, and in particular relates to a steel-lined fluorine-bromine water comprehensive separation bottle for extracting bromine from seawater. Background Art

[0002] The steel-lined fluorine-bromine water separation bottle is a separation bottle device used for extracting bromine from seawater. Its main features and advantages include: Corrosion resistance: By lining the bottle with ethylene-polytetrafluoroethylene copolymer, it can well withstand the corrosion of bromine, solving the problem of bromine corrosive to most metals. Sturdy and durable: The bottle body is made of steel-lined fluorine material, which is stronger than the glass separation bottle and not easy to be damaged, solving the problem of the bottle body being fragile. Safe and reliable: The interface flange connection can ensure that the bolts are tightened and the connection is reliable, preventing running, bubbling, dripping and leaking, ensuring safe production. Intuitive observation: A sight glass is welded on one side of the bottle body, which is convenient for process observation and control, taking into account the advantages of the glass separation bottle;

[0003] However, when the existing steel-lined fluorine-bromine water separation bottle is used to separate bromine water, it is difficult to determine the content of bromine liquid in the separated water before separation. Therefore, when it is necessary to discharge the separated water at the top, it is difficult to accurately discharge the separated water in the separation bottle. At the same time, the bottle body needs to be opened, and the bottom of the pipeline of the water extraction device needs to be moved to the bottom of the water before extraction and discharge. This is not conducive to the sealing and separation effect of the device on bromine water, and the gas generated by the volatilization of bromine is easy to affect the staff. Utility Model Content

[0004] The utility model provides a steel-lined fluorine-bromine water comprehensive separation bottle for extracting bromine from seawater, which has the characteristics of solving the problem that the sealing separation effect of the device on bromine water is not conducive, and the gas generated by the volatilization of bromine is easy to affect the staff.

[0005] The utility model provides the following technical solution: it comprises a base frame, a separation bottle body is arranged above the base frame, a separation tube is fixedly connected to one end of the separation bottle body, an annular frame is arranged inside the separation bottle body, corresponding connection holes are provided on the annular frame and the separation tube, a slide groove connected to the connection hole is provided on one side of the annular frame, a rotating ring is slidably connected to the inner wall of the slide groove, a through hole is provided on the rotating ring, a connecting rod is fixedly connected to one side of the rotating ring, a fixing block is fixedly connected between the connecting rods, a rotating rod is fixedly connected to one side of the fixing block, and one end of the rotating rod passes through the center of the separation bottle body.

[0006] Wherein, a support plate is fixedly connected to the top of the bottom frame, an observation hole is opened on the separation bottle body, and a glass plate is fixedly connected to the inner wall of the observation hole.

[0007] Among them, a mounting plate is fixedly connected to the top of the separation bottle body, a liquid inlet pipe is installed on the mounting plate, the liquid inlet pipe is connected to the inner cavity of the separation bottle body, and a liquid discharge pipe is fixedly connected to the other end of the separation bottle body, and the liquid inlet pipe, the separation tube and one end of the liquid discharge pipe are all fixedly connected with a connecting ring.

[0008] A limiting block is fixedly connected at the connection between the rotating ring and the slide slot, a limiting ring groove for limiting the limiting block is opened on the inner wall of the slide slot, and a sealing gasket is fixedly connected at the connection between the rotating ring and the limiting block and the slide slot.

[0009] Wherein, a rotation hole for giving way to the rotation rod is opened at the center of the separation bottle body, and a rotation block is fixedly connected to the outer wall of the rotation rod.

[0010] The beneficial effects of the utility model are as follows: bromine water can be separated through the liquid inlet pipe and the separation bottle body, and one end of the rotating rod is located outside the center of the separation bottle body, so that the fixed block can be rotated by the rotating rod, and the rotating ring is driven to rotate on the inner wall of the slide groove under the connection of the connecting rod, so that the height of the through hole on the annular frame can be adjusted, so that the through hole can correspond to the bottom position of the water, and the water can be extracted and discharged, so that the device can extract and separate the water separated from the bromine water while ensuring the sealing of the device, avoiding the situation that the content of the separated water cannot be determined and it is not convenient to accurately discharge it.

[0011] The parts not involved in the device are the same as those in the prior art or can be implemented by using the prior art. BRIEF DESCRIPTION OF THE DRAWINGS

[0012] Figure 1 It is a three-dimensional structural schematic diagram of the utility model;

[0013] Figure 2 It is a three-dimensional cross-sectional structural schematic diagram of the utility model;

[0014] Figure 3 It is a three-dimensional structural schematic diagram of the utility model;

[0015] Figure 4 It is a schematic diagram of the three-dimensional cross-sectional structure of the rotating ring in the utility model.

[0016] In the figure: 1. base frame; 11. support plate; 2. separation bottle body; 21. observation hole; 211. glass plate; 22. mounting plate; 23. liquid inlet pipe; 24. separation pipe; 25. liquid discharge pipe; 26. connecting hole; 27. connecting ring; 3. annular frame; 31. slide groove; 32. limit ring groove; 33. rotating ring; 34. limit block; 35. sealing gasket; 36. through hole; 4. fixing block; 41. connecting rod; 42. rotating rod; 421. rotating hole; 422. rotating block. DETAILED DESCRIPTION

[0017] See also Figure 1-Figure 4 The utility model provides the following technical solutions: it includes a base frame 1, a separation bottle body 2 is arranged above the base frame 1, a separation tube 24 is fixedly connected to one end of the separation bottle body 2, an annular frame 3 is arranged inside the separation bottle body 2, corresponding connection holes 26 are provided on the annular frame 3 and the separation tube 24, a slide groove 31 connected to the connection hole 26 is provided on one side of the annular frame 3, a rotating ring 33 is slidably connected to the inner wall of the slide groove 31, a through hole 36 is provided on the rotating ring 33, a connecting rod 41 is fixedly connected to one side of the rotating ring 33, a fixing block 4 is fixedly connected between the connecting rods 41, a rotating rod 42 is fixedly connected to one side of the fixing block 4, and one end of the rotating rod 42 passes through the center of the separation bottle body 2.

[0018] In this embodiment: the bottom frame 1 is at the bottom of the device, and carries the separation bottle 2. The separation bottle 2 is used to store the bromine water mixed liquid produced by extracting bromine from seawater. When the bromine water is separated, the bromine water can be connected to the liquid inlet pipe 23 through the dredging pipeline. The liquid inlet pipe 23 is relatively long, and cotton or filter paper can be filled in its inner wall to reduce the speed of the bromine water downward discharge, so that the bromine water will gradually be stratified in the liquid inlet pipe 23, and the bromine with higher density will settle at the bottom, while the water with lower density will float on it. Wait for a period of time to allow the bromine water to be fully stratified, so that the bromine water can settle at the bottom of the separation bottle 2, while the water with lower density can be on the bromine water, so that the staff can easily stratify the bromine water. During separation, the bromine liquid is a reddish-brown liquid at room temperature, so that the staff can directly judge the separation position of the bromine liquid and the water. When the water above the bromine liquid needs to be discharged, the rotating rod 42 can be rotated. The rotating rod 42 rotates at the center of one end of the separation bottle body 2. When the rotating rod 42 rotates, the end of the rotating rod 42 in the separation bottle body 2 can be connected to the fixed block 4, so that the fixed block 4 can be driven to rotate. The connecting rod 41 fixedly connected to the outer wall of the fixed block 4 can be located at the center of the inner cavity of the separation bottle body 2 for synchronous rotation. One end of the connecting rod 41 is fixedly connected to the rotating ring 33, and the rotating ring 33 is in a circular ring shape. The rotating ring 33 is in the annular frame 3. The slide groove 31 on one side of the annular frame 3 is connected to the rotating ring 33. The rotating ring 33 is matched with the rotating ring 33 so that the rotating ring 33 can rotate synchronously with it. When the rotating ring 33 rotates, the through hole 36 opened on one side of the rotating ring 33 is connected with the inner cavity of the rotating ring 33, so that the height of the through hole 36 can be adjusted. When separating bromine water, the position of the through hole 36 is adjusted to the top position in advance to prevent the bromine liquid at the bottom from entering the through hole 36 during the upper and lower separation of the liquids. After the bromine water is separated, the through hole 36 can be adjusted to the intersection position of the two liquids according to the color difference between the water and the bromine liquid, so that the upper liquid can enter the through hole 36, and is connected to the separation tube 24 through the extraction device. The separation tube 24 is connected with the inner cavity of the chute 31 through the connecting hole 26, so that the water above can enter the chute After the inner cavity of the groove 31, it can be extracted through the connecting hole 26 under the extraction device and discharged outward, so that the water can be separated from the bromine liquid precipitated below, so that the device can separate the unused amount of bromine-water mixed liquid according to the bromine liquid content, and then discharge the water at the top, thereby ensuring that the device can discharge the separated water at the top in time, so as to quickly take out the separated bromine water for use, so that the device can extract and separate the separated water in the bromine water while ensuring the sealing of the device, avoiding the uncertainty of the separated water content, inconvenience for its accurate discharge, avoiding the need to open the device to accurately discharge the water, thereby reducing the impact of the volatilization of bromine water on the staff during work.

[0019] A support plate 11 is fixedly connected to the top of the base frame 1, an observation hole 21 is opened on the separation bottle body 2, and a glass plate 211 is fixedly connected to the inner wall of the observation hole 21; the support plate 11 fixedly connected to the top of the base frame 1 is used to support and set up the base frame 1, and the glass plate 211 fixedly connected to the inner wall of the observation hole 21 is used to facilitate the staff to directly observe the bromine water separation situation in the base frame 1, so as to facilitate the adjustment of the position of the through hole 36.

[0020] A mounting plate 22 is fixedly connected to the top of the separation bottle body 2, and a liquid inlet pipe 23 is installed on the mounting plate 22. The liquid inlet pipe 23 is connected to the inner cavity of the separation bottle body 2, and a liquid discharge pipe 25 is fixedly connected to the other end of the separation bottle body 2. The liquid inlet pipe 23, the separation pipe 24 and one end of the liquid discharge pipe 25 are all fixedly connected to a connecting ring 27; the mounting plate 22 fixedly connected to the top of the separation bottle body 2 is used to install the liquid inlet pipe 23, so that the liquid inlet pipe 23 can separate the bromine water when the bromine water is added, and the liquid discharge pipe 25 fixedly connected to the other end of the separation bottle body 2 is used to connect the liquid discharge pipe 25 to the extraction pipeline to extract the bromine liquid for use after the water is discharged through the separation pipe 24, and the connecting ring 27 is used to connect the liquid inlet pipe 23, the separation pipe 24 and the liquid discharge pipe 25 to the pipeline

[0021] A limiting block 34 is fixedly connected to the connection between the rotating ring 33 and the slide groove 31. A limiting ring groove 32 for limiting the limiting block 34 is opened on the inner wall of the slide groove 31. A sealing gasket 35 is fixedly connected to the connection between the rotating ring 33, the limiting block 34 and the slide groove 31; the limiting block 34 is used to slide in the limiting ring groove 32 so that the rotating ring 33 can be limited, so that when the rotating ring 33 slides on the inner wall of the slide groove 31, the rotating ring 33 is prevented from separating from the inner wall of the slide groove 31. The sealing gasket 35 is used to ensure the sealing of the connection between the rotating ring 33 and the inner wall of the slide groove 31 to avoid water outflow due to poor sealing when water is pumped out.

[0022] A rotating hole 421 for making way for the rotating rod 42 is opened at the center of the separation bottle body 2, and a rotating block 422 is fixedly connected to the outer wall of the rotating rod 42; the rotating hole 421 opened at the center of the separation bottle body 2 is used to install the rotating rod 42, so that the rotating rod 42 can rotate the fixed block 4 by rotating the rotating hole 421, thereby synchronously rotating the connecting rod 41, so that the rotating ring 33 can be adjusted to the position of the through hole 36.

[0023] The working principle and use process of the utility model are as follows: bromine water can be connected to the liquid inlet pipe 23 through the dredging pipeline. The liquid inlet pipe 23 is relatively long and can be filled with cotton or filter paper on its inner wall to reduce the downward discharge speed of bromine water, so that the bromine water will gradually be layered in the liquid inlet pipe 23, and the bromine with higher density will settle at the bottom, while the water with lower density will float on it. After waiting for a period of time, the bromine water will be fully layered, so that the bromine water can be settled at the bottom of the separation bottle 2. After the bromine water is separated from the upper and lower parts, the fixed block 4 can be driven to rotate by rotating the rotating rod 42. The connecting rod 41 fixedly connected to the outer wall of the fixed block 4 is fixedly connected to the rotating ring 33, so that the height of the through hole 36 can be adjusted. After the bromine water is separated, According to the color difference between water and bromine liquid, the through hole 36 can be adjusted to the intersection position of the two liquids, so that the upper liquid can enter the through hole 36, and is connected to the separation tube 24 through the extraction device. The separation tube 24 is connected to the inner cavity of the chute 31 through the connecting hole 26. After the upper water enters the inner cavity of the chute 31, it can be extracted through the connecting hole 26 under the extraction device and discharged outward, so that the water can be separated from the bromine liquid precipitated below, so that the device can extract and separate the water separated from the bromine water while ensuring the sealing of the device, avoiding the situation that the content of the separated water cannot be determined and it is inconvenient to discharge it accurately, avoiding the need to open the device to accurately discharge the water, thereby reducing the impact of the volatilization of bromine water on the staff during work.

Claims

1. A steel-lined fluorine-bromine water integrated separation bottle for extracting bromine from seawater, comprising a base frame (1), characterized in that: A separation bottle body (2) is arranged above the base frame (1), one end of the separation bottle body (2) is fixedly connected to a separation tube (24), an annular frame (3) is arranged inside the separation bottle body (2), corresponding connection holes (26) are provided on the annular frame (3) and the separation tube (24), one side of the annular frame (3) is provided with a slide groove (31) connected to the connection hole (26), the inner wall of the slide groove (31) is slidably connected to a rotating ring (33), a through hole (36) is provided on the rotating ring (33), one side of the rotating ring (33) is fixedly connected to a connecting rod (41), a fixing block (4) is fixedly connected between the connecting rods (41), one side of the fixing block (4) is fixedly connected to a rotating rod (42), one end of the rotating rod (42) passes through the center of the separation bottle body (2).

2. The steel-lined fluorine-bromine water comprehensive separation bottle for extracting bromine from seawater according to claim 1, characterized in that: A support plate (11) is fixedly connected to the top of the base frame (1), an observation hole (21) is provided on the separation bottle body (2), and a glass plate (211) is fixedly connected to the inner wall of the observation hole (21).

3. The steel-lined fluorine-bromine water comprehensive separation bottle for extracting bromine from seawater according to claim 1, characterized in that: The top of the separation bottle body (2) is fixedly connected to a mounting plate (22), a liquid inlet pipe (23) is mounted on the mounting plate (22), the liquid inlet pipe (23) is communicated with the inner cavity of the separation bottle body (2), the other end of the separation bottle body (2) is fixedly connected to a liquid discharge pipe (25), and one end of the liquid inlet pipe (23), the separation pipe (24) and the liquid discharge pipe (25) are all fixedly connected to a connecting ring (27).

4. The steel-lined fluorine-bromine water comprehensive separation bottle for extracting bromine from seawater according to claim 1, characterized in that: A limit block (34) is fixedly connected to the connection between the rotating ring (33) and the slide groove (31); a limit ring groove (32) for limiting the limit block (34) is provided on the inner wall of the slide groove (31); and a sealing gasket (35) is fixedly connected to the connection between the rotating ring (33), the limit block (34) and the slide groove (31).

5. The steel-lined fluorine-bromine water comprehensive separation bottle for extracting bromine from seawater according to claim 1, characterized in that: A rotating hole (421) for making way for the rotating rod (42) is provided at the center of the separation bottle body (2), and a rotating block (422) is fixedly connected to the outer wall of the rotating rod (42).

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