Multifunctional inorganic sample processing workstations
By designing a multifunctional inorganic sample processing workstation, and utilizing a modular motor to drive the extraction device and filtration system, the problem of acid gas contamination was solved, enabling real-time collection and filtration of acid gas, thus ensuring the accuracy of analytical results and environmental safety.
Patent Information
- Application Number
- CN201910964875.6
- Authority / Receiving Office
- CN · China
- Patent Type
- Patents(China)
- Current Assignee / Owner
- Filing Date
- 2019-10-11
- Publication Date
- 2025-11-21
- Estimated Expiration
- 2039-10-11
AI Technical Summary
In existing digestion and acid removal processes, the volatilization of acid gases leads to air pollution and corrosion of the laboratory environment, affecting analytical results, and there is a lack of effective environmentally friendly acid removal methods.
A multifunctional inorganic sample processing workstation was designed, including a digestion system, a base system, a module system, an extraction system, a filtration system, and an electrical control system. The extraction device is driven by a module motor to extract acid gas, and the acid gas is filtered by the filtration system. Corrosion-resistant materials and negative pressure extraction are used to achieve real-time collection and filtration of acid gas.
It effectively avoids acid gas pollution, reduces labor intensity, improves the efficiency of the digestion instrument, and ensures the accuracy of analytical results and environmental safety.
Smart Images

Figure CN112649257B_ABST
Abstract
Description
TECHNICAL FIELD
[0001] The present application relates to a multifunctional inorganic sample processing workstation, and belongs to the technical field of environmental sample detection instruments. BACKGROUND
[0002] When determining inorganic elements of environmental samples such as water samples, soil samples, solid waste and particulate matter trapped during atmospheric sampling, the environmental samples need to be digested. The role of digestion is to destroy organic matter, dissolve particulate matter, and oxidize various valence state elements to be measured into single high valence state or convert them into inorganic compounds that are easy to decompose. After digestion, the acidity of the sample needs to be reduced through acid chasing to avoid the uncertainty of the subsequent sample analysis process caused by the acidity, so digestion and acid chasing are essential basic steps in sample analysis and are also the pretreatment process of sample analysis, which has an important influence on the results of sample analysis.
[0003] In the current digestion and acid chasing process, the sample placed on the digestion tank is added with acid liquid by a digestion instrument, and then digestion is performed. Acid gas is generated during the digestion process. On the one hand, the acid gas directly volatilizes into the air, has strong corrosion, pollutes the air and the laboratory environment, and threatens the health of the experimenters for a long time. On the other hand, due to the temperature difference, the acid gas is easily condensed into acid liquid on the inner wall of the digestion tank and flows back to the sample, which affects the analysis results of the sample. At present, there is no very effective acid chasing method. SUMMARY
[0004] In view of the above problems, the technical problem to be solved by the present application is to provide a multifunctional inorganic sample processing workstation with novel structure, high accuracy and reliability, high acid chasing efficiency, strong stability and reliability, low labor intensity, real-time extraction of acid gas, gathering of acid gas, filtration of acid gas, and avoidance of environmental pollution.
[0005] The multifunctional inorganic sample processing workstation of the application comprises a digestion system, a base system, a module system, an extraction system, a filtering system and an electric control system, the base system is arranged at the bottom of the whole multifunctional inorganic sample processing workstation and is in contact with the ground, serving as the base of the whole multifunctional inorganic sample processing workstation for mounting other systems, the digestion system is arranged above the base system and can digest the sample to be analyzed, the module system is arranged on the base system and can drive the module slider on the module system to move up and down through the driving of a motor, the extraction system is fixedly installed on the module system by bolts and can move up and down along the module system to extract the acid gas digested in the digestion tank of the digestion system, the filtering system is arranged on the side of the base system and is connected with the extraction system pipe to filter the acid gas extracted in the extraction system, and the electric control system is arranged on the back side of the module system and is fixedly installed with the base system, mainly for motion control of the multifunctional inorganic sample processing workstation, and the above constitutes the whole multifunctional inorganic sample processing workstation.
[0006] As preferred, the digestion system comprises a digestion instrument and a digestion tank, the digestion instrument is arranged above the base system and is not limited in shape, which can be a cylinder or a cuboid, etc., and the cylinder is taken as an example in the embodiment, the digestion instrument can heat the sample to be analyzed to complete the digestion pretreatment, and a series of digestion holes are arranged at the upper portion, the specific number and arrangement order of the digestion holes are not limited and are within the protection scope of the patent, the digestion tank is in the shape of a cylinder and can contain the sample to be analyzed and the acidic liquid and is inserted into the digestion hole, and the sample in the digestion tank can be digested by the heating of the heating disc of the digestion instrument.
[0007] As preferred, the base system comprises foot cups, aluminum profile chassis, base work platform, locking device, the foot cup is arranged at the lower part of the base system, fixed on the aluminum profile chassis by bolts, the number of foot cups is not limited, the locking height of each foot cup can be adjusted to adjust the levelness of the base system, the aluminum profile chassis is installed together horizontally and vertically through aluminum profiles of different sizes, the specific installation structure is not limited, which supports and fixes the whole base system, the base work platform is in the form of a flat plate, fixed and installed on the aluminum profile chassis by bolts, forming a whole, the base work platform comprises water blocking groove, U-shaped groove and module installation position, the water blocking groove is arranged around the base work platform and is in the form of a protrusion, if there is liquid flowing out of the base work platform, the water blocking groove can block the liquid, the U-shaped groove is arranged at the front ends of the base work platform and is in the form of a U, used for assembling the locking device and allowing the locking device to slide upwards, the module installation position is used for installing the module system, the locking device is clamped on the U-shaped groove, the locking device comprises locking support, locking pressing plate, locking push rod, locking pressing pad, first locking pressing rod, locking light shaft and second locking pressing rod, the locking support is in the form of L, the locking pressing plate is in the form of a flat plate and arranged below the locking support, the locking push rod is fixedly installed with the locking support, the front end of the locking push rod is fixed with the locking pressing pad, the locking pressing pad has a certain elasticity, the first locking pressing rod is arranged at the rear end of the locking push rod, after pressing down the first locking pressing rod, the locking device can work and the locking pressing pad contacts the digestion instrument, the locking light shaft is in the form of a cylinder, one end is sleeved on the locking support, the other end penetrates through the base work platform and is screwed into the locking pressing plate, one end of the second locking pressing rod is sleeved on the locking support, the other end penetrates through the base work platform and is screwed into the locking pressing plate, by rotating the handle of the second locking pressing rod, the locking pressing plate can be pressed on the base work platform, then by pressing down the first locking pressing rod, the locking pressing pads on both sides of the digestion instrument are pressed on the digestion instrument, so that the digestion instrument is relatively fixed on the base system.
[0008] As preferred, the module system comprises a module cover, a module cover plate, a module column, a module, a module slider, a module motor, a reducer, a shaft coupling, a cooling fan, a decorative cover, the module cover is arranged outside the module system and is fixedly installed on the base workbench by bolts, which prevents dust and acid gas from corroding the module and other components in the module system, the module cover plate is arranged on the module cover by bolt cover, which prevents dust and acid gas from corroding the module and other components in the module system, the specific material of the module column is not limited, including iron plate, aluminum plate or other materials, which are welded or assembled together by different sizes of plates to form a whole and are installed on the module installation position, so that the module column and the base workbench form a vertical relationship, the module is fixedly installed on the module column by bolts, and the module has a lead screw, a bearing, a lead screw sleeve and other components, the rotation of the lead screw can drive the up and down movement of the lead screw sleeve, the module slider is fixedly installed with the lead screw sleeve in the module by bolts and moves up and down with the lead screw sleeve, the module motor can be a servo motor, a stepper motor, etc., and the specific motor style is not limited, which is installed above the module column, the reducer is fixedly installed below the module motor, the output shaft sleeve of the module motor is arranged in the reducer, when the module motor rotates at a certain speed, the speed is transmitted to the reducer, which can reduce the speed by a speed reduction ratio to reduce the speed of the motor and increase the torque, one end of the shaft coupling is sleeved on the output shaft of the reducer, and the other end is sleeved on the lead screw of the module, so that the reducer and the module are connected to form a whole, so that the speed of the module motor can be transmitted to the lead screw of the module, so that the module slider moves according to the set distance, in another embodiment, the reducer can be removed, so that the output shaft of the module motor is directly sleeved with the shaft coupling, so that the speed of the module motor is directly transmitted to the lead screw of the module, both embodiments are within the protection scope of the patent, the cooling fan is installed on the upper end of the module cover, through the movement of the cooling fan, the heat generated by the module, the module motor and the reducer can be quickly discharged to the outside, effectively playing a heat dissipation role, and the decorative cover is fixedly installed on the module cover 31 by bolts, which can shield the extraction system and play a role in beauty and decoration.
[0009] As preferred, the extraction system comprises an extraction frame, an extraction device, a first gas gathering device, a switch valve, a second gas gathering device, the extraction frame is fixedly installed on the module system by bolts, and is the base body of the whole extraction system for mounting and fixing other parts, the extraction frame comprises a first connecting plate, a second connecting plate, a first working platform, a second working platform, a stand, a third working platform and a side cover plate, the first connecting plate is flat, is arranged at the rear end of the extraction frame, has a plurality of first screw holes, and can be fixedly connected with the module slider through bolts, the second connecting plate is flat, is arranged in two, is arranged on the two sides of the first connecting plate, and is fixedly connected with the first connecting plate through bolts, the first working platform is flat, and the first working platform comprises a first connecting plate mounting position, a second connecting plate mounting position, a stand mounting position, a sunken platform, a locking screw hole and a second gas gathering device mounting position, the first connecting plate mounting position is used for bolt mounting of the first connecting plate, the second connecting plate mounting position is used for bolt mounting of the second connecting plate, the stand mounting position is used for bolt mounting of the stand, the sunken platform is arranged at the middle part of the first working platform, is a hollow recess, and the second working platform can be clamped and mounted in the sunken platform, the locking screw hole is not limited in number, is uniformly distributed on the sunken platform in a circumferential direction, and the second working platform can be pressed on the first working platform through bolt locking, the second gas gathering device mounting position is a circular hole, and is used for mounting the second gas gathering device, the second working platform is annular, is erected and mounted on the sunken platform of the first working platform, and the second working platform comprises an extraction device mounting position and an arc-shaped groove, the extraction device mounting position is a circular opening, has a sunken platform at the lower part, and is used for mounting the extraction device, the arc-shaped groove is an arc-shaped slot, bolts pass through the arc-shaped groove and are threadedly locked with the locking screw hole, because the arc-shaped groove has a certain arc length, the second working platform can rotate at a certain angle on the first working platform, the flexibility adjustment of the second working platform is enhanced, and it is ensured that the extraction device can be accurately inserted into the digestion tank, the stand is cylindrical, has screw holes at the upper end and the lower end, the lower part is locked with the first working platform through bolts, and the upper part is locked with the third working platform through bolts, so that the first working platform and the third working platform form an integral whole, and the length of the stand can be adjusted according to actual conditions, the third working platform is flat, is arranged at the upper part of the stand, and the third working platform is provided with a first gas gathering device mounting position for placing the second gas gathering device, the number, diameter and position of the first gas gathering device mounting position are not limited, and can be adjusted according to actual conditions, and the side cover plate is clamped in the first working platform and the third working platform, and the side cover plate is provided with a plurality of switch valve mounting positions for mounting the switch valve.
[0010] As preferred, the number of the extraction devices is determined according to the number of the digestion tanks, and the specific number and arrangement are not limited, which are within the protection scope of the patent, and are fixed on the second working platform. The extraction device comprises an extraction rod, an extraction locking nut, an extraction joint and an extraction air pipe. The extraction rod is in a circular ring shape, and the diameter is slightly smaller than the inner hole diameter of the digestion tank. The extraction rod comprises a rod body, an extraction cone part, an extraction platform, an extraction external thread part, an extraction internal inclined surface and an extraction internal thread part. The rod body is in a circular ring shape, is processed from a material resistant to high temperature, acid and corrosion, has slight elasticity, and the specific material is not limited. A through hole penetrating upward and downward is arranged in the middle part. The extraction cone part is arranged at the lower part of the rod body, is in a conical shape, is beneficial to the extraction of acidic gas, and the extraction platform is a boss at the upper part of the rod body. The upper surface of the boss is in contact with the extraction device installation position, so as to ensure the perpendicularity of the extraction rod. The extraction external thread part is arranged at the upper external end of the extraction rod. The extraction internal inclined surface is arranged at the upper internal side of the extraction rod, and is in a conical inclined surface, which is wide at the upper part and narrow at the lower part. The extraction internal thread part is arranged at the upper internal side of the extraction rod and the upper part of the extraction internal inclined surface. After a plurality of extraction rods pass through the second working platform, the extraction locking nut is used for thread locking of the extraction rod, so as to press the extraction rod on the second working platform. The extraction joint is used for tightly locking the extraction air pipe in the extraction rod, is processed from a material resistant to high temperature, acid and corrosion, has slight elasticity, and the specific material is not limited. The extraction joint comprises an extraction external inclined surface, a joint thread, a joint hand part and a joint inclined surface. The extraction external inclined surface is arranged at the lower part of the extraction joint, is in a conical inclined surface, and can be in close contact with the extraction internal inclined surface after the extraction external inclined surface is threadedly screwed with the extraction rod. The joint thread is arranged at the lower external side of the extraction joint, and can be threadedly matched with the extraction internal thread part. The joint hand part is arranged at the upper part of the extraction joint, and the extraction joint can be screwed into the extraction rod through the joint hand part. The joint inclined surface is arranged at the upper part of the extraction joint, is in a small inclined surface, and can smoothly insert the extraction air pipe into the extraction joint. The extraction air pipe is in a tubular shape, the specific length can be adjusted according to the actual situation, is processed from a material resistant to high temperature, acid and corrosion, and the specific material is not limited. The extraction air pipe is inserted into the extraction joint, extends into the inside of the rod body, and is then threadedly screwed with the extraction internal thread part through the joint thread of the extraction joint. Finally, the extraction external inclined surface and the extraction internal inclined surface are in contact with each other. Since the materials of the extraction rod and the extraction joint have certain elasticity, the extraction external inclined surface and the extraction internal inclined surface form an effective sealing relationship, and the extraction joint and the extraction air pipe also form an effective sealing relationship. Therefore, the gas extracted from the extraction cone part can only be extracted from the extraction air pipe.
[0011] As preferred, the number of the first gas gathering device is determined according to the number of the extraction device, and the specific number and arrangement are not limited, which are all within the protection scope of the patent. The extraction gas pipes on the extraction device can be gathered together and fixed on the third working platform. The first gas gathering device comprises a first gas gathering tank, a first gas gathering sealing ring, a first gas gathering upper cover, a first gas gathering adapter, a first gas gathering connector and a first gas gathering pipe. The first gas gathering tank is a cylindrical inner space. The first gas gathering tank comprises a tank shell, a tank boss, a tank thread, a tank inclined surface, a tank first connector mounting position and a tank second connector mounting position. The tank shell is the base body of the whole first gas gathering device for mounting other components. The tank boss is arranged in the middle of the first gas gathering tank to enable the first gas gathering device to be placed on the first gas gathering device mounting position. The tank thread is arranged at the upper end of the first gas gathering tank. The tank inclined surface is arranged at the lower part of the first gas gathering tank in the form of an inclined surface to enable the acidic liquid gathered in the first gas gathering tank to flow to the middle along the tank inclined surface. The tank first connector mounting position is internally provided with a thread and an inclined surface to enable the extraction gas pipe and the extraction connector to be in contact and threadedly connected to each other to form an effective sealing relationship. The tank second connector mounting position is internally provided with a thread and an inclined surface to enable the first gas gathering connector to be threadedly connected to each other to form an effective sealing relationship. The first gas gathering sealing ring is made of corrosion-resistant silica gel material and has a certain elasticity in the form of a circular ring and arranged in the upper part of the first gas gathering tank. The first gas gathering upper cover is provided with a thread at the lower part to be threadedly connected to the first gas gathering tank to press the first gas gathering sealing ring tightly on the first gas gathering tank to form an effective sealing at the upper part of the first gas gathering tank. The first gas gathering adapter is in the form of L and internally in the form of L to be assembled with the first gas gathering tank. The upper part of the first gas gathering adapter is provided with a first adapter thread and a first adapter inclined surface to form an effective sealing relationship after being threadedly connected with the tank second connector mounting position. The lower part of the first gas gathering adapter is provided with a second adapter thread and a second adapter inclined surface to form an effective sealing relationship after being assembled with the first gas gathering connector and the first gas gathering pipe. The structure of the first gas gathering connector is similar to that of the extraction connector, except that the size is adjusted according to the actual situation, which will not be described in the patent. The first gas gathering pipe can be threadedly and tightly sealed in the first gas gathering adapter. The first gas gathering pipe is in the form of a tube and has the same specific structure as the extraction gas pipe, except that the size is adjusted according to the actual situation, which will not be described in the patent.
[0012] As preferred, the switch valve is made of high-temperature-resistant, acid-resistant and corrosion-resistant material, and the specific material is not limited. The number of the switch valve is consistent with that of the first gas gathering device, which can be adjusted according to the actual situation. One end of the switch valve is connected with the first gas gathering pipe, and the other end is connected with the air inlet pipe of the second gas gathering device. The upper part of the switch valve is provided with a valve that can be opened and closed to open or close the cavity inside the switch valve, so that the switch valve can be in a connected or closed state.
[0013] As preferred, the second gas gathering device can gather the first gas gathering pipes of the first gas gathering device together, and is arranged on the installation position of the second gas gathering device, and the second gas gathering device comprises a second gas gathering tank body, a second gas gathering sealing ring, a second gas gathering upper cover, a second gas gathering connector and a second gas gathering pipe, the second gas gathering tank body is similar in structure to the first gas gathering tank body, the second gas gathering sealing ring is similar in structure to the first gas gathering sealing ring and is arranged in the clamping groove of the second gas gathering tank body, the second gas gathering upper cover is similar in structure to the first gas gathering upper cover, the second gas gathering sealing ring is pressed on the second gas gathering tank body through threads, the upper end is provided with a plurality of threaded holes, and the corresponding first gas gathering connector can fix, seal and press the first gas gathering pipe on the second gas gathering upper cover, and the second gas gathering connector is arranged at the lower part of the second gas gathering tank body and can press the second gas gathering pipe on the second gas gathering tank body through threads, so that an effective fixing and sealing relationship is formed.
[0014] As preferred, the filtering system is arranged on the side of the base system and is connected with the pipe of the extraction system, can filter the acid gas extracted in the extraction system, and comprises a filtering column, a filtering flat plate, filtering bottles, a filtering cover, a filtering connector, a connecting pipe and an outlet pipe, the filtering column is a cylinder, the upper and lower ends are provided with threads, the lower end is bolted with the working platform of the base, and the upper end is bolted with the filtering flat plate, the filtering flat plate is a flat plate, a plurality of circular holes with a certain diameter are formed in the filtering flat plate, the filtering bottles are cylinders and are arranged in the circular holes of the filtering flat plate, the number of the filtering bottles is not limited, the filtering cover is screwed on the filtering bottles, the upper part is provided with a plurality of threaded holes, the filtering connector can screw and seal the second gas gathering pipe, the connecting pipe and the outlet pipe on the filtering cover through threads, the connecting pipe connects the filtering bottles in a communicating state, and the outlet pipe is the outlet pipe of the filtering system and is connected with the pipe of the external air extraction equipment.
[0015] The beneficial effects of the present application are as follows:
[0016] 1. The multifunctional inorganic sample processing workstation has novel structure, is accurate and reliable, has high efficiency in acid extraction, high stability and reliability, reduces labor intensity, can extract acid gas in real time, gather acid gas, filter acid gas and avoid environmental pollution.
[0017] 2. The module motor on the module system can drive the extraction device to move slowly downward along with the reduction of the liquid level in the digestion tank, so that the acid gas generated in the digestion tank can be extracted in time and effectively, and the flexibility of acid gas extraction is realized.
[0018] 3. The acid gas in the extraction pipe of the extraction device can be gathered into the first gas gathering device, the acid gas and acid liquid gathered by the first gas gathering device are gathered into the second gas gathering device, the acid gas and acid liquid in the whole process are not discharged into the air, and air pollution is avoided.
[0019] 4. The switch valve setting can open or close a certain first gas gathering device, thus reducing the number of digestion tanks during the digestion process and improving the efficiency of the digester.
[0020] 5. The connector and the gas-concentrating tank body are made of corrosion-resistant and elastic materials, so that after the gas tube is inserted into the gas-concentrating tank, the connector can effectively fix and seal the gas tube in the gas-concentrating tank body to form an effective sealing relationship.
[0021] 6. The locking lever of the locking device can quickly fix the digester on the working platform;
[0022] 7. By replacing the working platform of the extraction device, it can be adapted to digesters of different sizes and numbers of wells, thus improving the flexibility of the multifunctional inorganic sample processing workstation;
[0023] 8. The filtration system is equipped with multiple filters to ensure that acid gas and acid liquid are completely neutralized and filtered, and will not cause pollution to the environment.
[0024] 9. The external extraction device of the multifunctional inorganic sample processing workstation adopts a negative pressure extraction method, which enables the acid gas generated inside the extraction device to be extracted quickly. Attached image description:
[0025] For ease of explanation, the present invention will be described in detail below with reference to specific embodiments and accompanying drawings.
[0026] Figure 1 This is a schematic diagram of the structure of the present invention;
[0027] Figure 2 This is a schematic diagram of the internal structure of the present invention;
[0028] Figure 3 This is a schematic diagram of the digestion system in this invention;
[0029] Figure 4 This is a schematic diagram of the base system in this invention;
[0030] Figure 5 This is a schematic diagram of the locking device in this invention;
[0031] Figure 6 This is a schematic diagram of the module system in this invention;
[0032] Figure 7 This is a schematic diagram of the internal structure of the module system in this invention;
[0033] Figure 8 This is a schematic diagram of the extraction system in this invention;
[0034] Figure 9Structure diagram of the extraction frame in the application;
[0035] Figure 10 Structure diagram of the first working platform in the application;
[0036] Figure 11 Structure diagram of the extraction device in the application;
[0037] Figure 12 Front view of the extraction device in the application;
[0038] Figure 13 A-A sectional view of Figure 12
[0039] Figure 14 Structure diagram of the extraction rod in the application;
[0040] Figure 15 B-B sectional view of Figure 14
[0041] Figure 16 Structure diagram of the extraction joint in the application;
[0042] Figure 17 Structure diagram of the first gas gathering device in the application;
[0043] Figure 18 Front view of the first gas gathering device in the application;
[0044] Figure 19 C-C sectional view of Figure 18
[0045] Figure 20 Structure diagram of the first gas gathering tank in the application;
[0046] Figure 21 D-D sectional view of Figure 20
[0047] Figure 22 Structure diagram of the first gas gathering adapter in the application;
[0048] Figure 23 E-E sectional view of Figure 22
[0049] Figure 24 Three-dimensional structure diagram of the first gas gathering adapter in the application;
[0050] Figure 25 Structure diagram of the second gas gathering device in the application;
[0051] Figure 26 Structure diagram of the filtering system in the application;
[0052] Figure 27 Structure diagram for the second embodiment.
[0053] 1-digestion system; 11-digestion instrument; 111-digestion hole; 12-digestion tank; 2-base system; 21-foot cup; 22-aluminum profile chassis; 23-base workbench; 231-water baffle; 232-U-shaped groove; 2 module stand 33 mounting position; 24-locking device; 241-locking bracket; 242-locking pressing plate; 243-locking push rod; 244-locking pressing pad; 245-first locking pressing rod; 246-locking optical axis; 247-second locking pressing rod; 3-module system; 31-module cover; 32-module cover plate; module stand 33 stand; 34-module; 35-module slider; 36-module motor; 37-reducer; 38-coupling; 39-radiation fan; 310-decorative cover; 4-extraction system; 41-extraction frame; 411-first connecting plate; 4111-first screw hole; 412-second connecting plate; 413-first workbench; 4131-first connecting plate mounting position; 4132-second connecting plate mounting position; 4133-stand mounting position; 4134-sink; 4135-locking screw hole; 4136-second gas collecting device mounting position; 414-second workbench; 4141-extraction device mounting position; 4142-arc-shaped groove; 415-stand; 416-third workbench; 417-side cover plate; 42-extraction device; 421-extraction rod; 4211-rod body; 4212-extraction cone; 4213-extraction platform; 4214-extraction external thread part; 4215-extraction inner inclined surface; 4216-extraction internal thread part; 422-extraction locking nut; 423-extraction joint; 4231-extraction external inclined surface; 4232-joint thread; 4233-joint hand part; 4234-joint inclined surface; 424-extraction air pipe; 43-first gas collecting device; 431-first gas collecting tank body; 4311-including tank body shell; 4312-tank body boss; 4313-tank body thread; 4314-tank body inclined surface; 4315-tank body first joint mounting position; 4316-tank body second joint mounting position; 432-first gas collecting sealing ring; 433-first gas collecting upper cover; 434-first gas collecting adapter; 4341-adapter first thread; 4342-adapter first inclined surface; 4343-adapter second thread; 4344-adapter second inclined surface; 435-first gas collecting joint; 436-first gas collecting air pipe; 44-on-off valve; 45-second gas collecting device; 451-second gas collecting tank body; 452-second gas collecting sealing ring; 453-second gas collecting upper cover; 454-second gas collecting joint; 455-second gas collecting air pipe; 5-filtration system; 51-filtration stand; 52-filtration flat plate; 53-filtration bottle; 54-filtration cover; 55-filtration joint; 56-connection air pipe; 57-outlet air pipe; 6-electric control system. DETAILED DESCRIPTION
[0054] DETAILED DESCRIPTION Figures 1-26As shown, the specific embodiment adopts the following technical scheme: it comprises a digestion system 1, a base system 2, a module system 3, an extraction system 4, a filtering system 5, and an electric control system 6. The base system 2 is arranged at the bottom of the whole multifunctional inorganic sample processing workstation and is in contact with the ground, serving as the base of the whole multifunctional inorganic sample processing workstation for mounting other systems. The digestion system 1 is mounted above the base system 2 and can digest samples to be analyzed. The module system 3 is mounted on the base system 2 and can drive the module slider on the module system 3 to slide up and down through the driving of a motor. The extraction system 4 is fixedly mounted on the module system 3 and can move up and down along the module system 3 to extract acid gas digested in the digestion tank of the digestion system 1. The filtering system 5 is arranged on the side of the base system 2 and is connected with the extraction system 4 to filter the acid gas extracted by the extraction system 4. The electric control system 6 is arranged on the back side of the module system 3 and is fixedly mounted with the base system 2, mainly for motion control of the multifunctional inorganic sample processing workstation. The above constitutes a whole multifunctional inorganic sample processing workstation.
[0055] The digestion system 1 comprises a digestion instrument 11 and a digestion tank 12. The digestion instrument 11 is arranged above the base system 2 and can be a cylinder or a cuboid. The digestion instrument 11 can heat the sample to be analyzed and complete the pretreatment of digestion. A series of digestion holes 111 are arranged on the upper part of the digestion instrument 11. The specific number and arrangement of the digestion holes 111 are not limited and are within the protection scope of the patent. The digestion tank 12 is in the shape of a cylinder and can contain the sample to be analyzed and acidic liquid. The digestion tank 12 is inserted into the digestion hole 111. The sample in the digestion tank 12 can be digested after the heating disc of the digestion instrument 11 is heated. The base system 2 comprises a foot cup 21, an aluminum profile base 22, a base working platform 23, and a locking device 24. The foot cup 21 is arranged at the lower part of the base system 2 and is fixed on the aluminum profile base 22 by bolts. The number of the foot cups 21 is not limited. The locking height of each foot cup 21 can be adjusted to adjust the levelness of the base system 2. The aluminum profile base 22 is installed together by aluminum profiles with different sizes in the horizontal and vertical directions. The specific installation structure is not limited. The aluminum profile base 22 supports and fixes the entire base system 2. The base working platform 23 is in the shape of a flat plate and is fixed on the aluminum profile base 22 by bolts to form a whole. The base working platform 23 comprises a water blocking groove 231, a U-shaped groove 232, and a module installation position 233. The water blocking groove 231 is arranged around the base working platform 23 and is in the shape of a protrusion. If liquid flows out of the base working platform 23, the water blocking groove 231 can block the liquid. The U-shaped groove 232 is arranged at the front ends of the base working platform 23 and is in the shape of a U. The U-shaped groove 232 is used to assemble the locking device 24 and allows the locking device 24 to slide upwards. The module installation position 233 is used to install the module system 3. The locking device 24 is clamped on the U-shaped groove 232. The locking device 24 comprises a locking bracket 241, a locking pressing plate 242, a locking push rod 243, a locking pressing pad 244, a first locking pressing rod 245, a locking optical shaft 246, and a second locking pressing rod 247. The locking bracket 241 is in the shape of an L. The locking pressing plate 242 is in the shape of a flat plate and is arranged below the locking bracket 241. The locking push rod 243 is fixedly installed with the locking bracket 241. The front end of the locking push rod 243 is fixed with the locking pressing pad 244. The locking pressing pad 244 has a certain elasticity. The first locking pressing rod 245 is arranged at the rear end of the locking push rod 243. After the first locking pressing rod 245 is pressed down, the locking pressing pad 244 of the working locking device 24 can contact the digestion instrument 11. The locking optical shaft 246 is in the shape of a cylinder. One end of the locking optical shaft 246 is sleeved on the locking bracket 241. The other end of the locking optical shaft 246 penetrates through the base working platform 23 and is screwed into the locking pressing plate 242. One end of the second locking pressing rod 247 is sleeved on the locking bracket 241. The other end of the second locking pressing rod 247 penetrates through the base working platform 23 and is screwed into the locking pressing plate 242. The handle of the second locking pressing rod 247 is rotated.The locking pressure plate 242 can be pressed on the base workbench 23, and then the locking pressure pad 244 on both sides of the digestion instrument 11 is pressed against the digestion instrument 11 by pressing the first locking pressure rod 245, so that the digestion instrument 11 is relatively fixed on the base system 2; the module system 3 comprises a module cover 31, a module cover plate 32, a module stand 33, a module 34, a module sliding block 35, a module motor 36, a speed reducer 37, a shaft coupling 38, a cooling fan 39, and a decorative cover 310, the module cover 31 is arranged outside the module system 3 and is fixedly installed on the base workbench 23 by bolts, which prevents dust and acid gas corrosion from entering the module 34 and other components in the module system 3, the module cover plate 32 is arranged on the module cover 31 by bolt cover, which prevents dust and acid gas corrosion from entering the module 34 and other components in the module system 3, the specific material of the module stand 33 is not limited, including iron plate, aluminum plate or other materials, which are welded or assembled together by different sizes of plates to form a whole and are installed on the module installation position 233, so that the module stand 33 is perpendicular to the base workbench 23, the module 34 is fixedly installed on the module stand 33 by bolts, the module 34 has a lead screw, a bearing and a lead screw sleeve, the rotation of the lead screw can drive the up-down movement of the lead screw sleeve, the module sliding block 35 is fixedly installed with the lead screw sleeve in the module 34 by bolts and moves up and down with the lead screw sleeve, the module motor 36 can be a servo motor or a stepping motor, and the specific motor type is not limited, which is arranged above the module stand 33, the speed reducer 37 is fixedly installed below the module motor 36, the output shaft sleeve of the module motor 36 is arranged in the speed reducer 37, when the module motor 36 rotates at a certain speed, the speed is transmitted to the speed reducer 37, which can reduce the speed by a speed reduction ratio, so as to reduce the speed and increase the torque of the motor, one end of the shaft coupling 38 is sleeved on the output shaft of the speed reducer 37, and the other end is sleeved on the lead screw of the module 34, so that the speed reducer 37 and the module 34 are connected to form a whole, and the speed of the module motor 36 can be transmitted to the lead screw of the module 34, so that the module sliding block 35 moves according to the set distance, in another embodiment, the speed reducer 37 can be removed, so that the output shaft of the module motor 36 is directly sleeved with the shaft coupling 38, so that the speed of the module motor 36 is directly transmitted to the lead screw of the module 34, both of which are within the protection scope of the patent, the cooling fan 39 is arranged on the upper end of the module cover 31, and the heat generated by the module 34, the module motor 36 and the speed reducer 37 can be quickly discharged to the outside through the movement of the cooling fan 39, so as to effectively play a heat dissipation role, and the decorative cover 310 is fixedly installed on the module cover 31 by bolts, which can shield the extraction system 4 and play a role in beauty and decoration; the extraction system 4 comprises an extraction frame 41, an extraction device 42, a first gas collecting device 43, an on-off valve 44 and a second gas collecting device 45,The extraction frame 41 is fixedly installed on the module system 3 by bolts, and is the base body of the whole extraction system 4 for mounting and fixing other parts. The extraction frame 41 comprises a first connecting plate 411, a second connecting plate 412, a first working platform 413, a second working platform 414, a stand column 415, a third working platform 416 and a side cover plate 417. The first connecting plate 411 is flat and is arranged at the rear end of the extraction frame 41 and has a plurality of first screw holes 4111 for fixedly connecting the module slider 35 by bolts. The second connecting plate 412 is flat and is arranged at two sides of the first connecting plate 411 and is fixedly connected with the first connecting plate 411 by bolts. The first working platform 413 is flat and comprises a first connecting plate mounting position 4131, a second connecting plate mounting position 4132, a stand column mounting position 4133, a sunken platform 4134, locking screw holes 4135 and a second gas gathering device mounting position 4136. The first connecting plate mounting position 4131 is used for bolt mounting of the first connecting plate 411. The second connecting plate mounting position 4132 is used for bolt mounting of the second connecting plate 412. The stand column mounting position 4133 is used for bolt mounting of the stand column 415. The sunken platform 4134 is arranged at the middle part of the first working platform 413 and is a hollow recess, so that the second working platform 414 can be clamped and mounted in the sunken platform 4134. The locking screw holes 4135 are arranged on the sunken platform 4134 in a circumferential direction and are used for locking the second working platform 414 on the first working platform 413 by bolts. The second gas gathering device mounting position 4136 is a circular hole and is used for mounting the second gas gathering device 45. The second working platform 414 is annular and is arranged on the sunken platform 4134 of the first working platform 413. The second working platform 414 comprises an extraction device mounting position 4141 and an arc-shaped groove 4142. The extraction device mounting position 4141 is a circular opening and has a sunken platform at the lower part for mounting the extraction device 42. The arc-shaped groove 4142 is an arc-shaped groove, and the bolts are screwed and locked through the arc-shaped groove 4142 and the locking screw holes 4135. Because the arc-shaped groove 4142 has a certain arc length, the second working platform 414 can rotate at a certain angle on the first working platform 413, so that the flexibility of the second working platform 414 is enhanced, and the extraction device 42 can be accurately inserted into the digestion tank 12. The stand column 415 is a cylindrical body and has screw holes at the upper and lower ends. The lower end is locked with the first working platform 413 by bolts, and the upper end is locked with the third working platform 416 by bolts, so that the first working platform 413 and the third working platform 416 form an integral whole. The length of the stand column 415 can be adjusted according to actual conditions. The third working platform 416 is flat and is arranged on the upper part of the stand column 415. The third working platform 416 is provided with a first gas gathering device mounting position 4161 for placing the second gas gathering device 45. The number, diameter and position of the first gas gathering device mounting position 4161 are not limited and can be adjusted according to actual conditions.The side cover plate 417 is clamped in the first work platform 413 and the third work platform 416, and a plurality of switch valve installation positions 4171 are arranged on the side cover plate 417 for installing the switch valve 44; the number of the extraction device 42 is determined according to the number of the digestion tank 12, and the specific number and arrangement mode are not limited, which are all within the protection scope of the patent; the extraction device 42 is fixed on the second work platform 414 and comprises an extraction rod 421, an extraction locking nut 422, an extraction connector 423 and an extraction air pipe 424. The extraction rod 421 is annular, and the diameter is slightly smaller than the inner hole diameter of the digestion tank 12. The extraction rod 421 comprises a rod body 4211, an extraction cone part 4212, an extraction platform 4213, an extraction external thread part 4214, an extraction internal inclined surface 4215 and an extraction internal thread part 4216. The rod body 4211 is annular and is made of a material resistant to high temperature, acid and corrosion, and has slight elasticity. A through hole penetrating upward and downward is arranged in the middle of the rod body 4211. The extraction cone part 4212 is arranged at the lower part of the rod body 4211 and is conical, which is beneficial to the extraction of acid gas. The extraction platform 4213 is a boss arranged at the upper part of the rod body 4211, and the upper surface thereof is in contact with the extraction device installation position 4141, so as to ensure the perpendicularity of the extraction rod 421. The extraction external thread part 4214 is arranged at the upper external end of the extraction rod 421. The extraction internal inclined surface 4215 is arranged at the upper internal side of the extraction rod 421 and is conical. The extraction internal thread part 4216 is arranged at the upper internal side of the extraction rod 421 and the upper part of the extraction internal inclined surface 4215. A plurality of extraction rods 421 pass through the second work platform 414, and the extraction locking nut 422 is used for thread locking the extraction rod 421, so as to press the extraction rod 421 against the second work platform 414. The extraction connector 423 is used for tightly locking the extraction air pipe 424 in the extraction rod 421. The extraction connector 423 is made of a material resistant to high temperature, acid and corrosion, and has slight elasticity. The extraction connector 423 comprises an extraction external inclined surface 4231, a connector thread 4232, a connector hand part 4233 and a connector inclined surface 4234. The extraction external inclined surface 4231 is arranged at the lower part of the extraction connector 423 and is conical. After the extraction external inclined surface 4231 is threadedly fastened with the extraction rod 421, the extraction external inclined surface 4231 is in close contact with the extraction internal inclined surface 4215. The connector thread 4232 is arranged at the lower external side of the extraction connector 423 and can be threadedly matched with the extraction internal thread part 4216. The connector hand part 4233 is arranged at the upper part of the extraction connector 423 and is used for screwing the extraction connector 423 into the extraction rod 421. The connector inclined surface 4234 is arranged at the upper part of the extraction connector 423 and is a small inclined surface, which is used for smoothly inserting the extraction air pipe 424 into the extraction connector 423. The extraction air pipe 424 is tubular, and the specific length thereof can be adjusted according to actual conditions. The extraction air pipe 424 is made of a material resistant to high temperature, acid and corrosion.The extraction rod 421 is inserted into the interior of the rod body 4211, and then screwed with the extraction inner threaded portion 4216 through the joint threads 4232 of the extraction joint 423, and finally the extraction outer bevel 4231 and the extraction inner bevel 4215 are in contact with each other. Since the materials of the extraction rod 421 and the extraction joint 423 have a certain elasticity, the extraction outer bevel 4231 and the extraction inner bevel 4215 form an effective sealing relationship, and the extraction joint 423 and the extraction gas pipe 424 also form an effective sealing relationship. Therefore, the gas extracted from the extraction cone portion 4212 can only be extracted from the extraction gas pipe 424; the number of the first gas gathering device 43 is determined according to the number of the extraction device 42, and the specific number and arrangement manner are not limited, which are all within the protection scope of the patent. The extraction gas pipes 424 on the extraction device 42 can be collected together and fixed on the third working platform 416. The first gas gathering device 43 includes a first gas gathering tank body 431, a first gas gathering sealing ring 432, a first gas gathering upper cover 433, a first gas gathering adapter 434, a first gas gathering joint 435, and a first gas gathering pipe 436. The first gas gathering tank body 431 is a cylindrical inner space. The first gas gathering tank body 431 includes a tank body shell 4311, a tank body boss 4312, tank body threads 4313, a tank body bevel 4314, a tank body first joint mounting position 4315, and a tank body second joint mounting position 4316. The tank body shell 4311 is the base body of the entire first gas gathering device 43, for mounting other components. The tank body boss 4312 is arranged in the middle of the first gas gathering tank body 431, so that the first gas gathering device 43 can be placed on the first gas gathering device mounting position 4161. The tank body threads 4313 are arranged at the upper end of the first gas gathering tank body 431. The tank body bevel 4314 is arranged at the lower part of the first gas gathering tank body 431, which is a bevel, so that the acidic liquid gathered in the first gas gathering tank body 431 can flow to the middle along the tank body bevel 4314. The tank body first joint mounting position 4315 is internally provided with threads and a bevel, which can be in contact with and threadedly connected with the extraction gas pipe 424 and the extraction joint 423 to form an effective sealing relationship therebetween. The tank body second joint mounting position 4316 is internally provided with threads and a bevel, which can be threadedly connected with the first gas gathering joint 435 to form an effective sealing relationship therebetween. The first gas gathering sealing ring 432 is made of corrosion-resistant silica gel material and has a certain elasticity, which is in the form of a ring and is arranged in the upper clamping groove of the first gas gathering tank body 431. The first gas gathering upper cover 433 is provided with threads at the lower part, which can be threadedly connected with the first gas gathering tank body 431 to press the first gas gathering sealing ring 432 tightly on the first gas gathering tank body 431, so as to form an effective sealing on the upper part of the first gas gathering tank body 431. The first gas gathering adapter 434 is in the form of L and internally has an L-shaped through hole, which is assembled with the first gas gathering tank body 431. The upper part of the first gas gathering adapter 434 is provided with an adapter first thread 4341 and an adapter first bevel 4342, so that after being threadedly connected with the tank body second joint mounting position 4316, an effective sealing relationship is formed.The lower part of the first gas gathering adapter 434 is provided with an adapter second thread 4343 and an adapter second bevel 4344, so that after being assembled with the first gas adapter 435 and the first gas pipe 436, an effective sealing relationship is formed. The first gas adapter 435 has a structure similar to that of the extraction adapter 423, except that the size is adjusted according to the actual situation, which will not be described in this patent. The first gas pipe 436 is a tubular structure, and its specific structure is consistent with that of the extraction gas pipe 424, except that the size is adjusted according to the actual situation, which will not be described in this patent. The on-off valve 44 is made of high-temperature-resistant, acid-resistant and corrosion-resistant materials, and the specific material is not limited. The number is consistent with the first gas device 43, and can be adjusted according to the actual situation. One end is connected with the first gas pipe 436, and the other end is connected with the gas inlet pipe of the second gas device 45. The upper part is provided with an openable valve, which can open or close the cavity inside the on-off valve 44, so that the on-off valve 44 can form a connected or closed state. The second gas device 45 can collect the first gas pipes 436 of the first gas device 43 together and is arranged on the second gas device mounting position 4136. The second gas device 45 includes a second gas tank body 451, a second gas sealing ring 452, a second gas upper cover 453, a second gas adapter 454, and a second gas pipe 455. The structure of the second gas tank body 451 is similar to that of the first gas tank body 431. The structure of the second gas sealing ring 452 is similar to that of the first gas sealing ring 432 and is arranged in the clamping groove of the second gas tank body 451. The structure of the second gas upper cover 453 is similar to that of the first gas upper cover 433. The second gas sealing ring 452 is pressed tightly on the second gas tank body 451 by threads. The upper end is provided with a plurality of threaded holes, so that the corresponding first gas adapter 435 can fix, seal and press the first gas pipe 436 tightly on the second gas upper cover 453. The second gas adapter 454 is arranged at the lower part of the second gas tank body 451 and can press the second gas pipe 455 tightly on the second gas tank body 451 by threads, forming an effective fixing and sealing relationship. The filtering system 5 is arranged on the side of the base system 2 and is connected with the extraction system 4. It can filter the acid gas extracted from the extraction system 4. The filtering system 5 includes a filtering column 51, a filtering flat plate 52, a filtering bottle 53, a filtering cover 54, a filtering adapter 55, a connecting gas pipe 56, and an outlet gas pipe 57. The filtering column 51 is a cylindrical body with threads at the upper and lower ends. The lower end is bolted to the base working platform 23, and the upper end is bolted to the filtering flat plate 52. The filtering flat plate 52 is a flat plate with a plurality of circular holes of a certain diameter. The filtering bottle 53 is a cylindrical shape and is placed in the circular hole of the filtering flat plate 52. The filtering cover 54 is screwed on the filtering bottle 53 and is provided with a plurality of threaded holes at the upper part.The filter joint 55 can seal the second gas collecting tube 455, the connecting tube 56 and the gas outlet tube 57 to the filter cover 54 by screwing, the connecting tube 56 connects the filter bottles 53 in a communicating state, and the gas outlet tube 57 is the gas outlet tube of the filter system 5, which is connected to the external air extraction equipment tube.
[0056] The workflow of the embodiment is as follows: a. Press the corresponding button of the electric control system 6 to return each component to the initial position, return the extraction system 4 to the upper end of the module system 3, then place the digestion instrument 11 in the middle of the base system 2, then slide the locking devices 24 at both ends along the U-shaped groove 232 to the sidewalls of the digestion instrument 11, rotate the second locking pressure rod 247 to fix the locking devices 24 on the base working platform 23, then press the first locking pressure rod 245 to press the locking pressure pad 244 against the digestion instrument 11, so that the digestion instrument 11 is fixed on the base working platform 23, then pour different kinds of pickling filtrate into the plurality of filter bottles 53, connect the gas outlet pipe 57 with the external air extractor, then check the connection of the corresponding gas pipes of the digestion instrument to ensure the sealing of the whole system; b. Then place the sample to be detected on the digestion tank 12, pour acid solution into the digestion tank 12, and place the digestion tank 12 in the corresponding digestion hole 111 of the digestion instrument 11; c. Press the corresponding button of the electric control system 6 to start, and the external air extractor works according to the program setting logic to continuously extract the gas in the gas outlet pipe 57, the module motor 36 on the module 34 moves to drive the module sliding block 35 to quickly descend, so that the extraction system 4 quickly moves downward, and the extraction device 42 extends into the inner hole of the digestion tank 12 until it is above the liquid level of the acid solution in the digestion tank 12. The digestion instrument 11 generates heat during work to raise the temperature of the digestion tank 12, and the acid solution in the digestion tank 12 digests the sample to be detected after heating, and the acid solution generates acid gas after heating; d. The extraction force generated by the external air extractor causes the extraction device 42 to continuously extract the high-temperature acid gas in the digestion tank 12, and the taper of the extraction cone portion 4212 causes the acid gas generated after the acid solution volatilizes to gather as much as possible in the inner hole of the rod body 4211. The acid gas is extracted upward to the extraction gas pipe 424, and the acid gas generated by the plurality of extraction devices 42 enters the first gas gathering device 43 through the gas pipe. Since the temperature of the first gas gathering device 43 is room temperature, part of the acid gas is liquefied into acid solution, flows to the middle hole of the tank body outer shell 4311 through the tank body slope 4314, then flows away along the first gas gathering adapter 434, enters the first gas gathering gas pipe 436, and the acid gas that is not liquefied is extracted into the first gas gathering adapter 434 under the action of the extraction force of the external air extractor, and then enters the first gas gathering gas pipe 436; e. Since the installation height of the second gas gathering device 45 is lower than that of the first gas gathering device 43, the acid gas and acid solution flowing out of the plurality of first gas gathering devices 43 can smoothly flow into the second gas gathering device 45 to form a gathering form. In the second gas gathering device 45, more acid gas is liquefied, and part of the acid gas is in a gaseous state, then flows into the filter bottle 53 through the second gas gathering gas pipe 455.f. After the acidic gas and acid liquid flow from the second gas-gathering device 45 to the filter bottle 53, multiple filter bottles 53 filter the acidic gas and acid liquid. On the one hand, the acidic gas is liquefied, and on the other hand, the acid liquid and the filtered liquid in the filter bottle undergo a chemical reaction to reach a neutral state, ensuring that the gas drawn from the gas outlet pipe 57 is neutralized gas and will not pollute the environment. g. As the acid liquid in the digestion tank 12 continues to evaporate, the liquid level of the acid liquid in the digestion tank 12 continues to decrease. At this time, the module motor 36 on the module 34 moves, driving the module slider 35 to slowly descend. This causes the extraction device 42 to descend along with the acid liquid level, ensuring that the acid gas generated in the digestion vessel 12 can be extracted in a timely manner. This ensures that the acid gas generated in the digestion vessel 12 is removed before liquefaction, guaranteeing the purity of the acid liquid in the digestion vessel 12 and ensuring the reliability of the sample digestion. After digestion by the digester 11, the module motor 36 on the module 34 moves, driving the module slider 35 to rise rapidly, causing the extraction device 42 on the extraction system 4 to leave the digester 11 and return to its initial position, completing the entire process of the multifunctional inorganic sample processing workstation.
[0057] Specific implementation method two: such as Figure 27 As shown, the difference between this specific embodiment and specific embodiment one is that the digester 11 is a cuboid structure design, while the other structural principles and connection relationships are the same as in specific embodiment one.
[0058] The multifunctional inorganic sample processing workstation has novel structure, is accurate and reliable, has high efficiency of acid removal, high stability and reliability, reduces labor intensity, can extract, gather and filter acid gas in real time, avoids environmental pollution, can drive the extraction device to move slowly downward with the liquid level of the acid liquid in the digestion tank through the module motor drive on the module system, can effectively extract the acid gas generated in the digestion tank in time, realizes flexibility of acid gas extraction, can gather the acid gas in the extraction pipe of the extraction device into the first gas gathering device, gathers the acid gas and acid liquid into the second gas gathering device after the first gas gathering device gathers the acid gas and acid liquid, and the whole process does not discharge the acid gas and acid liquid in the air, avoiding air pollution, the setting of the switch valve can open or close a certain first gas gathering device, thus reducing the number of digestion tanks during digestion and improving the use efficiency of the digestion instrument, the joint and the gas gathering tank body are made of corrosion-resistant and elastic materials, the gas pipe can be effectively fixed and sealed in the gas gathering tank body through the joint after being inserted into the gas gathering tank, forming an effective sealing relationship, the locking pressure rod of the locking device can quickly fix the digestion instrument on the working platform, the working platform of the extraction device can be replaced and installed, the digestion instrument of different sizes and different hole numbers can be adapted, the flexibility of the multifunctional inorganic sample processing workstation is improved, multiple filters are arranged in the filtering system, ensuring that the acid gas and acid liquid are completely neutralized and filtered, and the environment is not polluted, and the extraction device outside the multifunctional inorganic sample processing workstation adopts a negative pressure extraction mode, so that the acid gas generated in the extraction device can be quickly extracted.
[0059] The basic principles and main features of the present application are shown and described above, and the advantages of the present application are shown and described above. It should be understood by those skilled in the art that the present application is not limited to the above examples, and the above examples and descriptions in the specification are only to illustrate the principles of the present application. Without departing from the spirit and scope of the present application, various changes and improvements can be made to the present application, and these changes and improvements all fall within the scope of the present application. The scope of protection of the present application is defined by the appended claims and their equivalents.
Claims
1. A multi-functional inorganic sample processing work station, characterized by: It includes digestion system (1), base system (2), module system (3), extraction system (4), filter system (5), electric control system (6), the base system (2) is located at the bottom of the whole multifunctional inorganic sample processing workstation, and is in contact with the ground, the digestion system (1) is installed on the top of the base system (2), the module system (3) is installed on the base system (2), the extraction system (4) is fixedly installed on the module system (3) by bolt, the filter system (5) is installed on the side of the base system (2) and is connected with the extraction system (4) pipe, the electric control system (6) is arranged on the back side of the module system (3) and is fixedly installed with the base system (2) together. The extraction system (4) includes a first gas gathering device (43), the first gas gathering device (43) includes a first gas gathering tank body (431), a first gas gathering sealing ring (432), a first gas gathering upper cover (433), a first gas gathering adapter (434), a first gas gathering connector (435) and a first gas gathering pipe (436), the first gas gathering tank body (431) is a cylindrical inner space, the first gas gathering tank body (431) includes a tank body shell (4311), a tank body boss (4312), a tank body thread (4313), a tank body inclined surface (4314), a tank body first connector mounting position (4315) and a tank body second connector mounting position (4316), the tank body shell (4311) is the base body of the whole first gas gathering device (43), the tank body boss (4312) is arranged on the middle boss of the first gas gathering tank body (431), the tank body thread (4313) is arranged on the upper end of the first gas gathering tank body (431), the tank body inclined surface (4314) is arranged on the lower part of the first gas gathering tank body (431) and is a inclined surface, the tank body first connector mounting position (4315) is internally provided with a thread and an inclined surface, the tank body second connector mounting position (4316) is internally provided with a thread and an inclined surface, the first gas gathering sealing ring (432) is made of corrosion-resistant silica gel material and is in the form of a circular ring and is arranged in the upper clamping groove of the first gas gathering tank body (431), the first gas gathering upper cover (433) is provided with a thread at the lower part and is connected with the first gas gathering tank body (431) through the thread, the first gas gathering adapter (434) is in the form of L and is internally provided with an L-shaped through hole and is assembled with the first gas gathering tank body (431), the upper part of the first gas gathering adapter (434) is provided with an adapter first thread (4341) and an adapter first inclined surface (4342), the lower part of the first gas gathering adapter (434) is provided with an adapter second thread (4343) and an adapter second inclined surface (4344), and the first gas gathering pipe (436) is in the form of a pipe.
2. The multi-functional inorganic sample processing station of claim 1, wherein: The digestion system (1) includes a digestion instrument (11) and a digestion tank (12), the digestion instrument (11) is arranged on the top of the base system (2), and a series of digestion holes (111) are arranged on the upper part of the digestion instrument (11), the digestion tank (12) is in the form of a cylinder and is inserted into the digestion hole (111).
3. The multi-functional inorganic sample processing station of claim 1, wherein: The base system (2) includes a foot cup (21), an aluminum profile chassis (22), a base work platform (23), a locking device (24), the foot cup (21) is arranged at the lower part of the base system (2) and is fixed on the aluminum profile chassis (22) by bolts, the aluminum profile chassis (22) is installed together horizontally and vertically by aluminum profiles of different sizes, the base work platform (23) is in the form of a flat plate and is fixedly installed on the aluminum profile chassis (22) to form an integral whole, the base work platform (23) includes a water baffle (231), a U-shaped groove (232) and a module installation position (233), the water baffle (231) is arranged around the base work platform (23) and is in the form of a protrusion, the U-shaped groove (232) is arranged at the two ends of the front side of the base work platform (23) and is in the form of a U shape, the locking device (24) is clamped on the U-shaped groove (232), the locking device (24) includes a locking bracket (241), a locking pressing plate (242), a locking push rod (243), a locking pressing pad (244), a first locking pressing rod (245), a locking optical shaft (246) and a second locking pressing rod (247), the locking bracket (241) is in the form of an L shape, the locking pressing plate (242) is in the form of a flat plate and is arranged below the locking bracket (241), the locking push rod (243) is fixedly installed together with the locking bracket (241), the front end of the locking push rod (243) is fixed with the locking pressing pad (244), the first locking pressing rod (245) is arranged at the rear end of the locking push rod (243), the locking optical shaft (246) is in the form of a cylinder, one end of the locking optical shaft (246) is sleeved on the locking bracket (241), the other end of the locking optical shaft (246) penetrates through the base work platform (23) and is screwed into the locking pressing plate (242), one end of the second locking pressing rod (247) is sleeved on the locking bracket (241), the other end of the second locking pressing rod (247) penetrates through the base work platform (23) and is screwed into the locking pressing plate (242), and the handle of the second locking pressing rod (247) is rotated.
4. The multi-functional inorganic sample processing station of claim 1, wherein: The module system (3) includes a module cover (31), a module cover plate (32), a module column (33), a module (34), a module slider (35), a module motor (36), a reducer (37), a shaft coupling (38), a cooling fan (39), a decorative cover (310), the module cover (31) is provided outside the module system (3), and is fixedly installed on the base workbench (23) by bolts, the module cover plate (32) is provided on the module cover (31) by bolt cover, the module column (33) is installed on the module installation site (233), so that the module column (33) and the base workbench (23) form a vertical relationship, the module (34) is fixedly installed on the module column (33) by bolts, the module slider (35) and the screw rod sleeve in the module (34) are fixedly installed together by bolts, the module motor (36) is installed above the module column (33), the reducer (37) is fixedly installed below the module motor (36), the output shaft sleeve of the module motor (36) is installed in the reducer (37), one end of the shaft coupling (38) is sleeved on the output shaft of the reducer (37), the other end is sleeved on the screw rod of the module (34), so that the reducer (37) and the module (34) are connected to form a whole, the cooling fan (39) is installed on the upper end of the module cover (31), and the decorative cover (310) is fixed on the module cover (31) by bolts.
5. The multi-functional inorganic sample processing station of claim 2, wherein: The extraction system (4) includes an extraction frame (41), an extraction device (42), a first gas gathering device (43), a switch valve (44), a second gas gathering device (45), the extraction frame (41) is fixedly installed on the module system (3) by bolts, and is the base body of the entire extraction system (4); the extraction frame (41) includes a first connecting plate (411), a second connecting plate (412), a first working platform (413), a second working platform (414), a stand (415), a third working platform (416), and a side cover plate (417); the first connecting plate (411) is flat, is arranged at the rear end of the extraction frame (41), has a plurality of first screw holes (4111) on the top, and is fixedly connected with the module slider (35) through bolts; the second connecting plate (412) is flat, is arranged in two, is arranged on the two sides of the first connecting plate (411), and is fixedly connected with the first connecting plate (411) through bolts; the first working platform (413) is flat, and the first working platform (413) includes a first connecting plate mounting position (4131), a second connecting plate mounting position (4132), a stand mounting position (4133), a sunken table (4134), a locking screw hole (4135), and a second gas gathering device mounting position (4136); the sunken table (4134) is arranged in the middle of the first working platform (413) and is a hollow recess; the locking screw holes (4135) are uniformly distributed on the sunken table (4134) in a circumferential direction, and the second working platform (414) can be pressed tightly on the first working platform (413) through bolt locking; the second gas gathering device mounting position (4136) is a circular hole; the second working platform (414) is annular, is arranged on the sunken table (4134) of the first working platform (413), and includes an extraction device mounting position (4141) and an arc-shaped groove (4142); the extraction device mounting position (4141) is a circular opening, and the lower part has a sunken table; the arc-shaped groove (4142) is an arc-shaped slot, bolts pass through the arc-shaped groove (4142) and are threadedly locked with the locking screw holes (4135); the stand (415) is a cylinder, screw holes are arranged at the upper end and the lower end, the lower part is locked with the first working platform (413) through bolts, and the upper part is locked with the third working platform (416) through bolts; the third working platform (416) is flat, is arranged on the upper part of the stand (415), and the third working platform (416) is provided with a first gas gathering device mounting position (4161); and the side cover plate (417) is clamped in the first working platform (413) and the third working platform (416), and the side cover plate (417) is provided with a plurality of switch valve mounting positions (4171).
6. The multi-functional inorganic sample processing station of claim 1, wherein: The extraction device (42) comprises an extraction rod (421), an extraction locking nut (422), an extraction joint (423) and an extraction air pipe (424). The extraction rod (421) is annular, and its diameter is slightly smaller than the inner hole diameter of the digestion tank (12). The extraction rod (421) comprises a rod body (4211), an extraction cone (4212), an extraction platform (4213), an extraction outer threaded part (4214), an extraction inner inclined surface (4215) and an extraction inner threaded part (4216). The rod body (4211) is annular, and is made of a high-temperature-resistant, acid-resistant and corrosion-resistant material. A through hole penetrates the rod body (4211) from top to bottom. The extraction cone (4212) is arranged at the lower part of the rod body (4211), and is conical. The extraction platform (4213) is a boss at the upper part of the rod body (4211), and its upper surface is in contact with the extraction device mounting position (4141). The extraction outer threaded part (4214) is arranged at the upper outer end of the extraction rod (421). The extraction inner inclined surface (4215) is arranged at the upper inner side of the extraction rod (421), and is a conical inclined surface. The extraction inner threaded part (4216) is arranged at the upper inner side of the extraction rod (421) and the upper part of the extraction inner inclined surface (4215). A plurality of extraction rods (421) pass through the second working platform (414). The extraction joint (423) comprises an extraction outer inclined surface (4231), a joint thread (4232), a joint hand twisting part (4233) and a joint inclined surface (4234). The extraction outer inclined surface (4231) is arranged at the lower part of the extraction joint (423), and is a conical inclined surface. The joint thread (4232) is arranged at the lower outer side of the extraction joint (423). The joint hand twisting part (4233) is arranged at the upper part of the extraction joint (423). The joint inclined surface (4234) is arranged at the upper part of the extraction joint (423), and is a small inclined surface. The extraction air pipe (424) is tubular, and is made of a high-temperature-resistant, acid-resistant and corrosion-resistant material. The extraction air pipe (424) is inserted into the extraction joint (423), and extends into the interior of the rod body (4211).
7. The multi-functional inorganic sample processing station of claim 5, wherein: The on-off valve (44) is made of a high-temperature-resistant, acid-resistant and corrosion-resistant material, and its number is consistent with that of the first gas gathering device (43). One end of the on-off valve (44) is connected with the first gas gathering air pipe (436), and the other end is connected with the air inlet pipe of the second gas gathering device (45). An upper part of the on-off valve (44) is provided with an openable and closable valve.
8. The multi-functional inorganic sample processing station of claim 5, wherein: The second gas gathering device (45) comprises a second gas gathering tank body (451), a second gas gathering sealing ring (452), a second gas gathering upper cover (453), a second gas gathering connector (454) and a second gas gathering pipe (455). The second gas gathering tank body (451) is similar in structure to the first gas gathering tank body (431). The second gas gathering sealing ring (452) is similar in structure to the first gas gathering sealing ring (432) and is arranged in a clamping groove of the second gas gathering tank body (451). The second gas gathering upper cover (453) is similar in structure to the first gas gathering upper cover (433) and is screwed to compress the second gas gathering sealing ring (452) on the second gas gathering tank body (451). The upper end of the second gas gathering upper cover (453) is provided with a plurality of threaded holes. The second gas gathering connector (454) is arranged at the lower part of the second gas gathering tank body (451).
9. The multi-functional inorganic sample processing station of claim 1, wherein: The filter system (5) comprises a filter column (51), a filter flat plate (52), a filter bottle (53), a filter cover (54), a filter connector (55), a connecting gas pipe (56) and an air outlet gas pipe (57). The filter column (51) is a cylinder and is provided with threads at the upper and lower ends. The lower end is bolted to the base workbench (23) and the upper end is bolted to the filter flat plate (52). The filter flat plate (52) is a flat plate. The filter bottle (53) is a cylinder and is placed in a round hole of the filter flat plate (52). The filter cover (54) is screwed to the filter bottle (53) and is provided with a plurality of threaded holes at the upper end.
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