Reaction kettle shaking device for preparing powder catalyst by sol-gel method

Abstract

The invention discloses a reaction kettle shake-up device for preparing a powder catalyst by a sol-gel method, and relates to the technical field of powder catalyst preparation equipment, the reaction kettle shake-up device comprises a bottom plate, a supporting platform, a first limiting plate, a second limiting plate, an annular electromagnet, a gear ring and a first motor, the bottom plate and the side, away from the first supporting plate, of the supporting platform are connected through a disturbance assembly, a circumferential shaking assembly is installed at the bottom of a first limiting plate, an annular permanent magnet is installed at the top of the reaction kettle, and an annular electromagnet is installed at the bottom of a second limiting plate; through reciprocating oscillation of the reaction kettle between the first limiting plate and the second limiting plate, in cooperation with deflection circular motion and reciprocating swing in the vertical direction, the shaking speed and the shaking uniformity of a reagent in the reaction kettle can be increased, and by adjusting the intermittent power supply frequency of an annular electromagnet and the rotating speed of a first motor and a second motor, the shaking uniformity of the reagent in the reaction kettle can be improved. And the shaking speed and the shaking uniformity in the reaction kettle can be adjusted.

Description

Technical Field

[0001] The invention relates to the technical field of powder catalyst preparation equipment, in particular to a reaction kettle shaking device for preparing powder catalyst by a sol-gel method. Background Art

[0002] The sol-gel method is a method for preparing solid materials, in which a precursor solution is hydrolyzed and polymerized in a liquid phase to form a sol, and then a gel is formed by evaporating the solvent or curing at low temperature. Since the sol-gel method was discovered in the 1940s, it has undergone decades of development and has become one of the important methods for preparing solid materials. The sol-gel method has the advantages of low preparation temperature, high purity, small particle size, and uniform particles. At present, the sol-gel method has been widely used in the preparation of ceramics, glass, composite materials, catalysts and other material fields, and has become an important branch in the field of materials science. Obtaining dry gel is an important step in the preparation of powder catalysts. It takes 5 to 10 hours of shaking operation to obtain the dry gel process, and the shaking operation has a great influence on the shaking uniformity of the dry gel.

[0003] In the prior art, a shaking table and a unidirectional tilting rotating device are mainly used to shake the reactor, but the shaking trajectory is fixed, the speed and uniformity of the shaking process are not very good, and the shaking of the entire reactor cannot be completed by manpower and simple equipment alone. Therefore, there is an urgent need for a reactor shaking device for preparing powder catalysts by a sol-gel method. Summary of the invention

[0004] The object of the present invention is to provide a reaction kettle shaking device for preparing powder catalyst by sol-gel method, thereby solving the problems in the background technology.

[0005] To achieve the above object, the present invention provides the following technical solutions:

[0006] A shaking device for a reactor for preparing a powder catalyst by a sol-gel method comprises a bottom plate, a supporting platform, a first limiting plate, a second limiting plate, an annular electromagnet, a gear ring and a first motor, wherein a second supporting plate is installed on a top side of the bottom plate, a first supporting plate is installed on a bottom side of the supporting platform, the first supporting plate and the second supporting plate are rotatably connected, the bottom plate and the supporting platform are connected at a side away from the first supporting plate through a disturbance component, a plurality of groups of guide components are connected between the bottom plate and the supporting platform, a spherical head is installed at the bottom of the first limiting plate, a support seat is installed at the top of the supporting platform, the spherical head and the support seat are rotatably matched, a gear ring installed on the supporting platform is arranged on the outer side of the support seat, a circumferential shaking component is installed at the bottom of the first limiting plate, the axial shaking component is meshed with the gear ring, a plurality of groups of supporting components are installed on a side of the first limiting plate away from the circumferential shaking component, the supporting component is meshed with the gear ring, and the support component is used to maintain the first limiting plate as a whole The cam is provided with a plurality of guide posts on the two ends of the guide post, and a pair of guide posts is provided on each of the two guide posts, and a side plate is slidably matched with the side plate. Guide holes are provided on the two ends of the guide post, and the guide holes are slidably matched with the guide posts to fix and guide the movement of the side plate between the first limit plate and the second limit plate. A U-shaped bent plate is installed between the bottoms of the two side plates on the two ends of the side plates, and threaded holes are provided between the guide holes on the two ends of the side plates, and bolts are rotatably installed in the threaded holes on the side plates, a reactor is placed on the U-shaped bent plate, arc plates are provided on both sides of the reactor, and the arc plates are rotatably matched with the bolts, an annular permanent magnet is installed on the top of the reactor, and an annular electromagnet is installed on the bottom of the second limit plate, and several groups of first springs are connected between the bottom of the U-shaped bent plate and the first limit plate, and a controller is installed on the support platform.

[0007] Furthermore, the disturbance assembly includes a second motor, a guide groove plate, a disc and a cylindrical pin. The second motor is fixedly mounted on the base plate through a mounting platform. A disc is mounted on the output end of the second motor. A cylindrical pin is mounted on the upper edge of the disc. A horizontally arranged guide groove plate is fixedly mounted on the bottom of the support platform, and the cylindrical pin is slidably engaged with the guide groove plate.

[0008] Furthermore, the circumferential shaking assembly includes a first motor and a driving gear, the first motor is horizontally installed on one side of the bottom of the first limiting plate, the output end of the first motor is installed with a driving gear, and the driving gear is meshed with the gear ring.

[0009] Furthermore, the first limiting plate is inclined, and the inclination angle between the first limiting plate and the supporting platform is 10° to 20°.

[0010] Furthermore, a support component symmetrical to the first motor is disposed at the bottom of the first limiting plate with respect to the spherical head, and a pair of support components are also symmetrically disposed on a side of the first limiting plate away from the first motor.

[0011] Furthermore, the support assembly includes a first mounting block, a bracket, a second spring and a roller, the first mounting block is fixedly mounted on the bottom of the first limit plate, a positioning block is mounted on the top of the bracket, a first guide sleeve is mounted on the positioning block, a first guide rod is mounted on the bottom of the first mounting block, the first guide rod and the first guide sleeve are slidably matched, a second spring is connected between the first mounting block and the positioning block, the second spring is in a compressed state, a roller is rotatably mounted on the bottom of the bracket, and the roller is engaged with the gear ring.

[0012] Furthermore, the guide assembly includes a second mounting block, a connecting block, a second guide rod and a second guide sleeve. The second mounting blocks are respectively installed on the bottom of the support platform and the top of the base plate. The connecting block is rotatably installed on the second mounting block. The second guide rod and the second guide sleeve are respectively installed between the connecting blocks on both sides. The second guide rod and the second guide sleeve are slidably matched.

[0013] Compared with the prior art, the present invention has the following beneficial effects:

[0014] The present invention provides a reactor shaking device for preparing powdered catalyst by a sol-gel method. The reactor can accelerate the shaking speed and the shaking uniformity of the reagents in the reactor by reciprocating the reactor between a first limit plate and a second limit plate, in coordination with deflected circular motion and reciprocating swinging in the vertical direction. The shaking speed and the shaking uniformity in the reactor can be adjusted by adjusting the frequency of the intermittent power supply of the annular electromagnet and the rotation speed of the first motor and the second motor. BRIEF DESCRIPTION OF THE DRAWINGS

[0015] Figure 1 It is a schematic diagram of the overall structure of the present invention;

[0016] Figure 2 It is a schematic diagram of the installation of the side plate and the guide column of the present invention;

[0017] Figure 3 It is a schematic diagram of the support assembly structure of the present invention;

[0018] Figure 4 It is a structural schematic diagram of the A region of the present invention;

[0019] Figure 5 It is a schematic diagram of the structure of the guide assembly of the present invention.

[0020] In the figure: 1, bottom plate; 11, first support plate; 12, second support plate; 13, first limit plate; 14, second limit plate; 15, guide column; 16, guide hole; 17, side plate; 18, arc plate; 19, bolt; 2, support platform; 21, U-shaped bent plate; 22, first spring; 23, annular electromagnet; 24, annular permanent magnet; 25, spherical head; 26, support seat; 27, gear ring; 28, first motor; 29, drive gear ; 3. Support assembly; 31. First mounting block; 32. Bracket; 33. Positioning block; 34. First guide sleeve; 35. First guide rod; 36. Second spring; 37. Roller; 4. Reactor; 41. Mounting table; 42. Second motor; 43. Guide groove plate; 44. Disc; 45. Cylindrical pin; 5. Guide assembly; 51. Second mounting block; 52. Connecting block; 53. Second guide rod; 54. Second guide sleeve; 6. Controller. DETAILED DESCRIPTION

[0021] The following will be combined with the drawings in the embodiments of the present invention to clearly and completely describe the technical solutions in the embodiments of the present invention. Obviously, the described embodiments are only part of the embodiments of the present invention, not all of the embodiments. Based on the embodiments of the present invention, all other embodiments obtained by ordinary technicians in this field without creative work are within the scope of protection of the present invention.

[0022] like Figures 1 to 5As shown, a reactor shaking device for preparing powder catalyst by sol-gel method comprises a bottom plate 1, a support platform 2, a first limit plate 13, a second limit plate 14, an annular electromagnet 23, a gear ring 27 and a first motor 28. A second support plate 12 is installed on the top side of the bottom plate 1, and a first support plate 11 is installed on the bottom side of the support platform 2. The first support plate 11 and the second support plate 12 are rotatably connected. The bottom plate 1 and the side of the support platform 2 away from the first support plate 11 are connected by a disturbance component. The support platform 2 is driven to reciprocate up and down around the bottom plate 1 relative to the connection between the first support plate 11 and the second support plate 12 by the disturbance component, thereby driving the support platform 2 as a whole to achieve a small range of reciprocating shaking operation. , a plurality of guide components 5 are connected between the bottom plate 1 and the support platform 2, and the guide components 5 can provide guidance for the relative rotation between the bottom plate 1 and the support platform 2. A spherical head 25 is installed at the bottom of the first limit plate 13, and a support seat 26 is installed at the top of the support platform 2. The spherical head 25 and the support seat 26 rotate together to support the first limit plate 13. A gear ring 27 installed on the support platform 2 is arranged on the outer side of the support seat 26. A circumferential shaking component is installed at the bottom of the first limit plate 13, and the axial shaking component is meshed with the gear ring 27. A plurality of support components 3 are installed on the side of the first limit plate 13 away from the circumferential shaking component, and the support component 3 is meshed with the gear ring 27. The support assembly 3 is used to maintain the overall stability of the first limit plate 13 while supporting the bottom of the first limit plate 13 away from one side of the circumferential shaking assembly, so that the circumferential shaking assembly and the gear ring 27 are closely matched. The first limit plate 13 and the second limit plate 14 are parallel to each other. The second limit plate 14 is located at the top of the first limit plate 13 and is connected to the first limit plate 13 through two pairs of guide columns 15 on both sides. A side plate 17 is slidably matched on a pair of guide columns 15 on one side. Guide holes 16 are provided on both sides of the side plate 17. The guide holes 16 are slidably matched with the guide columns 15 to fix and guide the movement of the side plate 17 between the first limit plate 13 and the second limit plate 14. A U-shaped bent plate 2 is installed between the bottoms of the side plates 17 on both sides. 1, a threaded hole is arranged between the guide holes 16 on both sides of the side plate 17, a bolt 19 is rotatably installed in the threaded hole on the side plate 17, a reactor 4 is placed on the U-shaped bent plate 21, arc plates 18 are arranged on both sides of the reactor 4, the arc plates 18 are rotatably matched with the bolts 19, and the arc plates 18 on both sides of the reactor 4 can be tightly attached to the reactor 4 through the bolts 19 and the threaded holes on the side plate 17, so as to realize the fixing of the reactor 4 on the side plates 17 and the U-shaped bent plate 21 on both sides, an annular permanent magnet 24 is installed on the top of the reactor 4, an annular electromagnet 23 is installed on the bottom of the second limiting plate 14, and a plurality of groups of first springs 22 are connected between the bottom of the U-shaped bent plate 21 and the first limiting plate 13,The intermittently powered on and off annular electromagnet 23 cooperates with the first spring 22 to achieve vertical shaking interference on the reactor 4. After the annular electromagnet 23 is powered on, the annular electromagnet 23 attracts the annular permanent magnet 24 so that the whole composed of the side plate 17, the U-shaped bent plate 21 and the reactor 4 moves vertically upward along the extension direction of the guide column 15, and the first spring 22 is stretched; after the annular electromagnet 23 is powered off, the annular electromagnet 23 and the annular permanent magnet 24 lose their attraction. Under the retraction effect of the first spring 22, the reactor 4 shakes between the first limit plate 13 and the second limit plate 14 along the extension direction of the guide column 15, thereby interfering with the shaking process in the reactor 4 and accelerating the speed of the shaking process. A controller 6 is installed on the support platform 2, and the controller 6 is used to control and adjust the power supply and output power of the electrical components in the device.

[0023] The disturbance component includes a second motor 42, a guide groove plate 43, a disc 44 and a cylindrical pin 45. The second motor 42 is fixedly mounted on the base plate 1 through a mounting platform 41. A disc 44 is mounted on the output end of the second motor 42. A cylindrical pin 45 is mounted on the upper edge of the disc 44. A horizontally arranged guide groove plate 43 is fixedly mounted on the bottom of the support platform 2. The cylindrical pin 45 is slidably matched with the guide groove plate 43. The disc 44 and the cylindrical pin 45 are driven to rotate by the second motor 42. Under the guidance of the sliding match between the cylindrical pin 45 and the guide groove plate 43, the support platform 2 and the guide groove plate 43 are driven to swing in the vertical direction, thereby realizing the reciprocating swing of the support platform 2 relative to the base plate 1.

[0024] The circumferential shaking assembly includes a first motor 28 and a driving gear 29. The first motor 28 is horizontally installed on one side of the bottom of the first limit plate 13. The output end of the first motor 28 is installed with the driving gear 29. The driving gear 29 is engaged with the gear ring 27. The first limit plate 13 can be driven by the first motor 28 to perform circular rotation as a whole under the support of the support seat 26 and the spherical head 25.

[0025] The first limit plate 13 is inclined, and the inclination angle between the first limit plate 13 and the support platform 2 is 10° to 20°. Preferably, the inclination angle between the first limit plate 13 and the support platform 2 is 15° for the guide column. The inclined first limit plate 13 cooperates with the circumferential shaking component to fully shake the reagents in the reactor 4.

[0026] A support assembly 3 symmetrical to the first motor 28 is arranged at the bottom of the first limit plate 13 about the spherical head 25. The driving gear 29 can be tightly attached to the gear ring 27 through the elastic support of the support assembly 3. A pair of support assemblies 3 are also symmetrically arranged on the side of the first limit plate 13 away from the first motor 28. The symmetrically arranged support assemblies 3 can prevent the first limit plate 13 from tipping over.

[0027] The support assembly 3 includes a first mounting block 31, a bracket 32, a second spring 36 and a roller 37. The first mounting block 31 is fixedly mounted on the bottom of the first limit plate 13. A positioning block 33 is mounted on the top of the bracket 32. A first guide sleeve 34 is mounted on the positioning block 33. A first guide rod 35 is mounted on the bottom of the first mounting block 31. The first guide rod 35 slides with the first guide sleeve 34. A second spring 36 is connected between the first mounting block 31 and the positioning block 33. The second spring 36 is in a compressed state, so that the first mounting block 31 and the positioning block 33 have a tendency to move away from each other in a free state. A roller 37 is rotatably mounted on the bottom of the bracket 32. The roller 37 meshes with the gear ring 27, so as to realize pre-tightening of the meshing between the driving gear 29 and the gear ring 27 while preventing the first limit plate 13 from tipping over, so that the circumferential rotation of the first limit plate 13 remains stable.

[0028] The guide assembly 5 includes a second mounting block 51, a connecting block 52, a second guide rod 53 and a second guide sleeve 54. The second mounting blocks 51 are respectively installed at the bottom of the support platform 2 and the top of the base plate 1. The connecting block 52 is rotatably installed on the second mounting block 51. The second guide rod 53 and the second guide sleeve 54 are respectively installed between the connecting blocks 52 on both sides. The second guide rod 53 and the second guide sleeve 54 are slidably matched to realize guidance for the relative rotation of the base plate 1 and the support platform 2 to prevent the support platform 2 from tipping over relative to the base plate 1.

[0029] When the device is working, the controller 6 drives the annular electromagnet 23 to intermittently turn on and off the power, and cooperates with the first spring 22 to realize the reciprocating oscillation of the reactor 4 between the first limit plate 13 and the second limit plate 14; the controller 6 energizes the first motor 28 to realize the engagement of the driving gear 29 and the gear ring 27 to drive the reactor 4 to perform a deflection circular motion; the controller 6 energizes the second motor 42 to realize the reciprocating swing of the support platform 2 relative to the bottom plate 1; the reciprocating oscillation of the reactor 4 between the first limit plate 13 and the second limit plate 14, in conjunction with the deflection circular motion and the reciprocating swing in the vertical direction, can accelerate the shaking speed and uniformity of the reagents in the reactor 4.

[0030] Heating tubes are embedded in the bottom and sides of the reactor 4, and the materials in the reactor 4 can be heated during the shaking process through the heating tubes. Exhaust holes are provided on the top cover plate of the reactor. By continuously heating during the shaking process, the solvent in the material can be discharged through the exhaust holes, so that the material solution is converted into a solid state. The addition and discharging operations can be performed by removing the reactor 4.

[0031] It should be noted that, in this article, relational terms such as first and second, etc. are only used to distinguish one entity or operation from another entity or operation, and do not necessarily require or imply any such actual relationship or order between these entities or operations. Moreover, the terms "include", "comprise" or any other variants thereof are intended to cover non-exclusive inclusion, so that a process, method, article or device including a series of elements includes not only those elements, but also other elements not explicitly listed, or also includes elements inherent to such process, method, article or device.

[0032] Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that various changes, modifications, substitutions and variations may be made to the embodiments without departing from the principles and spirit of the present invention, and that the scope of the present invention is defined by the appended claims and their equivalents.

Claims

1. A reactor shaking device for preparing powder catalyst by sol-gel method, comprising a bottom plate (1), a support platform (2), a first limit plate (13), a second limit plate (14), an annular electromagnet (23), a gear ring (27) and a first motor (28), characterized in that: The bottom plate (1) and the support platform (2) are connected via a disturbance component at a side away from the first support plate (11); a plurality of guide components (5) are connected between the bottom plate (1) and the support platform (2); a spherical head (25) is installed at the bottom of the first limit plate (13); a support seat (26) is installed at the top of the support platform (2); the spherical head (25) and the support seat (26) are rotatably matched; a support seat (26) is installed on the support platform (2) on the outer side thereof. The first limit plate (13) is provided with a circumferential shaking assembly at the bottom, and the axial shaking assembly is meshed with the gear ring (27). The first limit plate (13) and the second limit plate (14) are parallel to each other. The second limit plate (14) is located at the top of the first limit plate (13) and is connected to the first limit plate (13) through two pairs of guide columns (15) on both sides. A side plate (17) is slidably matched on a pair of guide columns (15) on one side. The side plate (17) Guide holes (16) are arranged on both sides of the upper plate, and the guide holes (16) are slidably matched with the guide columns (15) to provide fixed guidance for the movement of the side plate (17) between the first limiting plate (13) and the second limiting plate (14). A U-shaped bent plate (21) is installed between the bottoms of the side plates (17) on both sides. A threaded hole is arranged between the guide holes (16) on both sides of the side plate (17), and bolts (19) are rotatably installed in the threaded holes on the side plate (17). The U-shaped bent plate (21) ) is placed on a reactor (4), arc plates (18) are arranged on both sides of the reactor (4), the arc plates (18) are rotatably matched with bolts (19), an annular permanent magnet (24) is installed on the top of the reactor (4), an annular electromagnet (23) is installed on the bottom of the second limiting plate (14), a plurality of groups of first springs (22) are connected between the bottom of the U-shaped bent plate (21) and the first limiting plate (13), and a controller (6) is installed on the support platform (2).

2. The device for shaking a reactor for preparing a powder catalyst by a sol-gel method according to claim 1, characterized in that: A second support plate (12) is installed on the top side of the base plate (1), and a first support plate (11) is installed on the bottom side of the support platform (2). The first support plate (11) and the second support plate (12) are rotatably connected. A plurality of groups of support assemblies (3) are installed on the side of the first limit plate (13) away from the circumferential shaking assembly. The support assemblies (3) are meshed with the gear ring (27). The support assemblies (3) are used to maintain the overall stability of the first limit plate (13) while supporting the side of the bottom of the first limit plate (13) away from the circumferential shaking assembly.

3. The device for shaking a reaction kettle for preparing a powder catalyst by a sol-gel method according to claim 2, characterized in that: The disturbance component comprises a second motor (42), a guide groove plate (43), a disc (44) and a cylindrical pin (45); the second motor (42) is fixedly mounted on the base plate (1) via a mounting platform (41); a disc (44) is mounted on the output end of the second motor (42); a cylindrical pin (45) is mounted on the upper edge of the disc (44); a horizontally arranged guide groove plate (43) is fixedly mounted on the bottom of the support platform (2); and the cylindrical pin (45) is slidably matched with the guide groove plate (43).

4. The device for shaking a reactor for preparing a powder catalyst by a sol-gel method according to claim 3, characterized in that: The circumferential shaking assembly comprises a first motor (28) and a driving gear (29), wherein the first motor (28) is horizontally mounted on one side of the bottom of the first limiting plate (13), and the output end of the first motor (28) is mounted with the driving gear (29), and the driving gear (29) is meshed with the gear ring (27).

5. The device for shaking a reaction kettle for preparing a powder catalyst by a sol-gel method according to claim 4, characterized in that: The first limiting plate (13) is arranged to be inclined, and the inclination angle between the first limiting plate (13) and the supporting platform (2) is 10° to 20°.

6. The device for shaking a reactor for preparing a powder catalyst by a sol-gel method according to claim 5, characterized in that: A support assembly (3) symmetrical to the first motor (28) is arranged at the bottom of the first limit plate (13) relative to the spherical head (25), and a pair of support assemblies (3) are also symmetrically arranged on a side of the first limit plate (13) away from the first motor (28).

7. The device for shaking a reaction kettle for preparing a powder catalyst by a sol-gel method according to claim 6, characterized in that: The support assembly (3) comprises a first mounting block (31), a bracket (32), a second spring (36) and a roller (37); the first mounting block (31) is fixedly mounted on the bottom of the first limiting plate (13); a positioning block (33) is mounted on the top of the bracket (32); a first guide sleeve (34) is mounted on the positioning block (33); a first guide rod (35) is mounted on the bottom of the first mounting block (31); the first guide rod (35) and the first guide sleeve (34) are slidably matched; a second spring (36) is connected between the first mounting block (31) and the positioning block (33); the second spring (36) is in a compressed state; a roller (37) is rotatably mounted on the bottom of the bracket (32); the roller (37) is meshed with the gear ring (27).

8. The device for shaking a reactor for preparing a powder catalyst by a sol-gel method according to claim 7, characterized in that: The guide assembly (5) comprises a second mounting block (51), a connecting block (52), a second guide rod (53) and a second guide sleeve (54); the second mounting block (51) is respectively mounted on the bottom of the support platform (2) and the top of the base plate (1); the connecting block (52) is rotatably mounted on the second mounting block (51); the second guide rod (53) and the second guide sleeve (54) are respectively mounted between the connecting blocks (52) on both sides; the second guide rod (53) and the second guide sleeve (54) are slidably matched.

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