Device for producing atomic clock rubidium bubble by using rubidium chloride as raw material

Abstract

The embodiment of the invention provides a device for producing an atomic clock rubidium bubble by adopting rubidium chloride as a raw material, and relates to the technical field of atomic clock rubidium bubble production equipment. A device for producing atomic clock rubidium bubbles by adopting rubidium chloride as a raw material comprises a support, the top of the support is fixedly connected with a reaction kettle, the top of the support is fixedly connected with a fixing seat, and the inner wall of the fixing seat is fixedly connected with a cooling tank. A sliding rod slides in an arc-shaped groove, the sliding rod drives a positioning plate to approach a distillation crucible, and a chute plate guides the lifting sliding rod in the approaching process, so that the lifting sliding rod drives the positioning plate to descend, and the distillation crucible is positioned when the positioning plate descends and moves; materials are prevented from driving the distillation crucible to move in a chemical reaction, and the product quality and the safety in the production process are ensured.

Description

Technical Field

[0001] The invention belongs to the technical field of atomic clock rubidium bubble production equipment, and in particular relates to a device for producing atomic clock rubidium bubbles by using rubidium chloride as a raw material. Background Art

[0002] Rubidium has a wide range of uses due to its unique properties. It plays an important role in both traditional fields and new application fields, especially in high-tech fields. In traditional fields, such as catalysts, special glass, electronic devices, biomaterials, etc., and in new fields, such as rubidium atomic clocks, magnetohydrodynamic power generation, energy, etc., it has shown strong vitality. Metallothermal reduction is the simplest method for preparing metallic rubidium, and it is also the most mainstream method for preparing metallic rubidium. Rubidium chloride is used as the raw material and strongly reducing metal calcium is used as the reducing agent. The reduction is carried out at high temperature. The reduction reaction is carried out in an inert gas, and then the rubidium vapor is removed from the reaction device by vacuum distillation. The metallic rubidium vapor is guided to the condensation site under vacuum suction, condensed into droplets, and then flows into the collector.

[0003] In the prior art (the announcement number is CN220771853U, and the patent name is a patent application for a reaction chamber used in metal rubidium cesium production equipment), before starting work, valves one and two are closed, the main reaction chamber is evacuated, and then the crucible is placed in the feed bin. After the feed bin is closed, the feed bin is evacuated. After the two sides of valve one reach equilibrium, valve one is opened, the crucible is sent into the main reaction chamber and set below the material collecting device. After closing valve one, the crucible heating device is started to start the replacement reaction, and the generated metal rubidium cesium vapor is extracted through the material collecting device. After the reaction is completed, the discharge bin is evacuated. After the pressure on both sides of valve two is balanced, valve two is opened, the crucible is sent into the discharge bin, and valve two is closed again to keep the main reaction chamber in a vacuum state. After the crucible is cooled in the discharge bin, it can be taken out for the next step of recycling.

[0004] During the chemical reaction process of the existing device, the fluidity of the material and the change in gas pressure caused by the chemical reaction may cause the distillation crucible containing the material to shift, affecting the operational safety and product quality. In order to make the rubidium chloride fully react and effectively distill out the rubidium metal, it is necessary to ensure that the heating source can provide uniform heat distribution to prevent local overheating or insufficient heating, which directly affects the purity and yield of the rubidium metal. Under high temperature conditions, the rubidium chloride is easily agglomerated, which not only affects the reaction efficiency, but also causes waste of raw materials. Summary of the invention

[0005] The present application aims to solve at least one of the technical problems in the prior art that during the chemical reaction process, the fluidity of the material and the change in gas pressure caused by the chemical reaction may cause the distillation crucible containing the material to shift. To this end, the present application proposes a device for producing an atomic clock rubidium bubble using rubidium chloride as a raw material.

[0006] To achieve the above object, the specific technical scheme of the present invention is as follows: a device for producing rubidium bubbles of atomic clocks using rubidium chloride as a raw material, comprising a bracket, the top of which is fixedly connected to a reactor, the top of which is fixedly connected to a fixing seat, the inner wall of which is fixedly connected to a cooling tank, and further comprising: An automatic cover opening mechanism, the automatic cover opening mechanism includes a driving motor fixedly connected to the top of the bracket, the output end of the driving motor is fixedly connected to a spiral rotating rod, the outer wall of the spiral rotating rod is threadedly connected to a lifting frame, the top of the bracket is fixedly connected to a positioning rod, the top of the positioning rod passes through the bottom of the lifting frame and extends to the outside, the side wall of the lifting frame is fixedly connected to a sealing cover, the top of the bracket is fixedly connected to a fixed support frame, the side wall of the fixed support frame is fixedly connected to an arc-shaped guide plate, the outer wall of the arc-shaped guide plate is provided with a guide groove, the inner wall of the guide groove is slidably connected to the outer wall of the L-shaped rotating rod, and the bottom of the sealing cover is fixedly connected to a placement frame.

[0007] Preferably, a positioning mechanism is provided at the bottom end of the L-shaped rotating rod, and the positioning mechanism includes a guide plate fixedly connected to the bottom end of the L-shaped rotating rod, an arc-shaped groove is opened on the top of the guide plate, a sliding rod is slidably connected to the inner wall of the arc-shaped groove, the bottom end of the sliding rod is fixedly connected to a positioning plate, and a rolling ball is rollingly connected to the inner wall of the positioning plate.

[0008] Preferably, the positioning mechanism also includes a fixed plate fixedly connected to the side wall of the placement rack, a positioning slot is provided on the top of the fixed plate, the inner wall of the positioning slot is slidably connected to the side wall of the positioning plate, the top of the fixed plate is fixedly connected to an inclined slot plate, the side wall of the positioning plate is fixedly connected to a lifting slide rod, and the outer wall of the lifting slide rod is slidably connected to the inner wall of the inclined slot plate.

[0009] Preferably, the top of the bracket is fixedly connected to a support frame, the top of the support frame is provided with an inert gas supply tank, the bottom of the inert gas supply tank is fixedly connected to an inert gas output pipe, the exhaust port of the inert gas output pipe passes through the outer wall of the reactor and extends to the interior, the side wall of the reactor is connected to a distillation air inlet pipe, and the end of the distillation air inlet pipe away from the reactor passes through the top of the cooling tank and extends to the interior.

[0010] Preferably, the inner wall of the reactor is fixedly connected to a distillation cylinder, the outer wall of the distillation cylinder is sleeved with a heater, the outer wall of the reactor is connected to a vacuum tube 1, the outer wall of the vacuum tube 1 is fixedly connected to a vacuum tube valve, the end of the vacuum tube 1 away from the reactor is fixedly connected to a vacuum machine, the top of the vacuum machine is fixedly connected to a vacuum tube 2, and the end of the vacuum tube 2 away from the vacuum machine is connected to the interior of the cooling tank.

[0011] Preferably, the outer wall of the reactor is provided with a rotating reaction mechanism, and the rotating reaction mechanism includes a servo motor fixedly connected to the outer wall of the reactor, the output end of the servo motor is fixedly connected to a rotating part 1, the outer wall of the rotating part 1 is rotatably connected to a connecting rod, the end of the connecting rod away from the rotating part 1 is rotatably connected to a rotating part 2, and the top of the rotating part 2 is fixedly connected to an axial rod.

[0012] Preferably, the top of the central rod is connected to a driving gear, the top of the driving gear is meshingly connected to a driven gear, the top of the driven gear is fixedly connected to a placement plate, a distillation crucible is placed on the top of the placement plate, the outer wall of the placement plate is fixedly connected to an annular guide rail, and the outer wall of the annular guide rail is slidably connected to the side wall of the placement rack.

[0013] Preferably, the outer wall of the axis rod is provided with a collision mechanism, and the collision mechanism includes an oblique semicircular disk fixedly connected to the outer wall of the axis rod, the inner wall of the reactor is fixedly connected with a reset spring, the bottom end of the reset spring is fixedly connected with a connecting disk, the central axis of the connecting disk is fixedly connected with an L-shaped top rod, the inner wall of the reactor is fixedly connected with a positioning groove cylinder, the inner wall of the groove of the positioning groove cylinder is slidably connected to the outer wall of the L-shaped top rod, and the bottom of the oblique semicircular disk is arranged in contact with the outer wall of the L-shaped top rod.

[0014] Preferably, a reciprocating mechanism is provided at the top of the rotating member 1, and the reciprocating mechanism includes a rotating rod fixedly connected to the top of the rotating member 1, the outer wall of the rotating rod is fixedly connected to pulley 1, the outer wall of pulley 1 is sleeved with a belt, the inner wall of the belt is transmission-connected to pulley 2, the central axis of pulley 2 is fixedly connected to the rotating rod, the bottom end of the rotating rod passes through the top of the cooling tank and extends to the interior, the outer wall of pulley 2 is fixedly connected to a rotating column, the top of the rotating column is fixedly connected to a push block, the outer wall of the push block is arranged in contact with the side wall of the lifting plate, the top of the cooling tank is fixedly connected to a connecting spring, and the end of the connecting spring away from the cooling tank is fixedly connected to the bottom of the lifting plate.

[0015] Preferably, a lifting rod is fixedly connected to the bottom of the lifting plate, and the lifting rod passes through the top of the cooling tank and extends to the inside, and an impact rod is fixedly connected to the outer wall of the lifting rod, and a plurality of heat dissipation cooling plates are fixedly connected to the inner wall of the cooling tank, and the plurality of heat dissipation cooling plates are distributed at equal distances up and down, and the outer wall of the impact rod is arranged in contact with the top of the heat dissipation cooling plate, and the inner wall of the cooling tank is fixedly connected to a cooler.

[0016] The present invention discloses a device for producing rubidium bubbles for atomic clocks using rubidium chloride as a raw material: 1. The device for producing rubidium bubbles of atomic clocks using rubidium chloride as raw material drives the L-shaped rotating rod to descend during the descending process of the sealing cover. Since the guide groove guides the L-shaped rotating rod, when the sealing cover descends to close the reactor, the L-shaped rotating rod rotates 90°, and the L-shaped rotating rod drives the guide plate to rotate. Since the slide bar slides in the arc groove, the slide bar drives the positioning plate to approach the distillation crucible. During the approaching process, the inclined groove plate guides the lifting slide bar, so that the lifting slide bar drives the positioning plate to descend. When the positioning plate descends and moves, the distillation crucible is positioned to prevent the material from driving the distillation crucible to move during the chemical reaction, thereby ensuring the quality of the product and the safety of the production process. When the distillation crucible needs to be taken out, the positioning mechanism will release the positioning of the distillation crucible, and the positioning plate will rise and move away from the distillation crucible, so as to facilitate the removal of the distillation crucible.

[0017] 2. The device for producing rubidium bubbles of atomic clocks using rubidium chloride as raw material, the heater heats the distillation cylinder and then heats the material in the distillation crucible. After the placement frame drives the annular guide rail and the placement plate to descend, the driven gear engages with the driving gear, the servo motor drives the rotating part 1 to rotate, the rotating part 1 drives the rotating part 2 to move synchronously through the connecting rod, the rotating part 2 drives the shaft rod and the driving gear to rotate, the driving gear drives the driven gear to rotate, and the driven gear drives the placement plate and the distillation crucible to rotate, so that the material is heated more evenly and the distillation efficiency is high.

[0018] 3. The device for producing rubidium bubbles for atomic clocks using rubidium chloride as a raw material, when the axis rod rotates, the axis rod drives the inclined semicircular disk to rotate, and the inclined semicircular disk presses down the L-shaped push rod during rotation, and the L-shaped push rod descends in the notch of the positioning groove cylinder, and when the inclined semicircular disk is no longer in contact with the L-shaped push rod, the reset spring drives the connecting disk to reset, so that the connecting disk drives the L-shaped push rod to collide with the placement disk, thereby avoiding agglomeration of materials in chemical reactions, preventing material waste, and effectively improving the efficiency of forming metal vapor.

[0019] 4. The device for producing rubidium bubbles for atomic clocks using rubidium chloride as a raw material generates metal vapor after the material undergoes a reduction reaction. After starting the vacuum machine, the vacuum tube valve is closed so that the gas can only enter the cooling tank through the distillation air inlet pipe. The heat dissipation cooling plate and the cooler cool the metal vapor. The tilt of the heat dissipation cooling plate changes the flow direction of the metal vapor. At this time, the flowing metal vapor has a large inertia and collides with the heat dissipation cooling plate, increasing the contact area between the metal vapor and the heat dissipation cooling plate, making it easier to cool the metal vapor, thereby condensing the metal vapor into liquid and flowing into the cooling tank, thereby completing the production of metal rubidium. 5. In the device for producing rubidium bubbles for atomic clocks using rubidium chloride as a raw material, metal liquid will remain on the heat dissipation cooling plate during the cooling process, rotating member 1 drives rotating rod and pulley 1 to rotate, pulley 1 drives pulley 2 and rotating rod to rotate through a belt, the rotating rod drives the rotating column and the push block to rotate, the push block pushes the lifting plate to rise, after the push block is separated from the lifting plate, the connecting spring drives the lifting plate to reset and descend, so that the lifting plate drives the lifting rod to descend, the lifting rod drives the impact club to collide with the heat dissipation cooling plate, so that the metal liquid is separated from the heat dissipation cooling plate, which is convenient for collecting the metal liquid while improving the cooling efficiency of the heat dissipation cooling plate.

[0020] 6. The device uses rubidium chloride as a raw material to produce rubidium bubbles for atomic clocks. When the rotating rod rotates, it drives the guide column to rotate. Since the reciprocating groove guides the slider, when the guide column rotates, the slider moves along the reciprocating groove, so that the slider drives the scratch plate to reciprocate and rise and fall. The scratch plate scratches the cooler to prevent excessive metal liquid from remaining on the cooler and affecting its use, which is convenient for subsequent maintenance and cleaning, effectively prolonging the service life of the device, and further increasing the collection of metal liquid. BRIEF DESCRIPTION OF THE DRAWINGS

[0021] In order to more clearly illustrate the technical solutions of the embodiments of the present invention, the following briefly introduces the drawings required for use in the embodiments. It should be understood that the following drawings only show certain embodiments of the present invention and therefore should not be regarded as limiting the scope. For ordinary technicians in this field, other related drawings can be obtained based on these drawings without creative work.

[0022] Figure 1 It is a schematic diagram of the overall structure of the present invention; Figure 2 It is a schematic diagram of the structure of the reactor and cooling tank of the present invention; Figure 3 It is a cross-sectional view of the reactor structure of the present invention; Figure 4 It is a structural schematic diagram of the automatic cover opening mechanism of the present invention; Figure 5It is a schematic diagram of the positioning mechanism structure of the present invention; Figure 6 It is a schematic diagram of the structure of the rotary reaction mechanism of the present invention; Figure 7 For the present invention Figure 6 Enlarged view of point A in the middle; Figure 8 It is a cross-sectional view of the collision mechanism structure of the present invention; Fig. 9 It is a cross-sectional view of the internal structure of the cooling tank of the present invention; Fig.10 For the present invention Fig. 9 A magnified view of the structure at B in the middle; Fig.11 It is a cross-sectional view of the scratch mechanism structure of the present invention.

[0023] Explanation of the markings in the figure: 101, bracket; 102, reactor; 103, fixed seat; 104, cooling tank; 105, support frame; 106, inert gas supply tank; 107, inert gas output pipe; 108, distillation air inlet pipe; 11, distillation cylinder; 12, heater; 13, vacuum tube 1; 14, vacuum tube valve; 15, vacuum machine; 16, vacuum tube 2; 2, automatic cover opening mechanism; 201, drive motor; 202, Screw rod; 203, lifting frame; 204, positioning rod; 205, sealing cover; 206, L-shaped rod; 207, fixed support frame; 208, arc guide plate; 209, guide groove; 21, placement frame; 3, positioning mechanism; 301, guide plate; 302, arc groove; 303, slide rod; 304, positioning plate; 305, rolling ball; 31, fixed plate; 32, positioning notch; 33, inclined groove plate; 34, lifting slide rod; 4 , rotating reaction mechanism; 401, servo motor; 402, rotating part 1; 403, connecting rod; 404, rotating part 2; 405, axis rod; 406, driving gear; 407, driven gear; 408, placing plate; 409, annular guide rail; 410, distillation crucible; 5, collision mechanism; 501, oblique semicircular plate; 502, reset spring; 503, connecting plate; 504, L-shaped top rod; 505, positioning groove cylinder; 6 , reciprocating mechanism; 601, rotating rod; 602, pulley one; 603, belt; 604, pulley two; 605, rotating rod; 606, rotating column; 607, push block; 608, lifting plate; 609, connecting spring; 610, lifting rod; 611, impact club; 61, heat dissipation cooling plate; 62, cooler; 7, scratch mechanism; 701, guide column; 702, reciprocating groove; 703, slider; 704, scratch plate. DETAILED DESCRIPTION

[0024] In the following, only some exemplary embodiments are briefly described. As those skilled in the art will appreciate, the described embodiments may be modified in various ways without departing from the spirit or scope of the embodiments of the present invention. Therefore, the drawings and descriptions are considered to be exemplary and non-restrictive in nature.

[0025] In the description of the embodiments of the present invention, it should be understood that the terms "length", "vertical", "horizontal", "top", "bottom", etc. indicating the orientation or positional relationship are based on the orientation or positional relationship shown in the accompanying drawings, and are only for the convenience of describing the embodiments of the present invention and simplifying the description, rather than indicating or implying that the device or element referred to must have a specific orientation, be constructed and operated in a specific orientation, and therefore cannot be understood as a limitation on the embodiments of the present invention.

[0026] In addition, the terms "first" and "second" are used for descriptive purposes only and should not be understood as indicating or implying relative importance or implicitly indicating the number of the indicated technical features. Thus, a feature defined as "first" or "second" may explicitly or implicitly include one or more of the features. In the description of the embodiments of the present invention, the meaning of "plurality" is two or more, unless otherwise clearly and specifically defined.

[0027] In the embodiments of the present invention, unless otherwise clearly specified and limited, the terms "installed", "connected", "connected", "fixed" and the like should be understood in a broad sense, for example, it can be a fixed connection, a detachable connection, or an integral connection; it can be a mechanical connection, an electrical connection, or a communication; it can be a direct connection, or an indirect connection through an intermediate medium, and it can be the internal connection of two elements or the interaction relationship between two elements. For ordinary technicians in this field, the specific meanings of the above terms in the embodiments of the present invention can be understood according to specific circumstances.

[0028] The disclosure below provides many different embodiments or examples to implement different structures of the embodiments of the present invention. In order to simplify the disclosure of the embodiments of the present invention, the parts and settings of specific examples are described below. Of course, they are only examples, and the purpose is not to limit the embodiments of the present invention. In addition, the embodiments of the present invention can repeat reference numbers and / or reference letters in different examples, and this repetition is for the purpose of simplification and clarity, which itself does not indicate the relationship between the various embodiments and / or settings discussed.

[0029] like Figures 1 to 5 As shown, a device for producing rubidium bubbles for atomic clocks using rubidium chloride as a raw material of the present invention comprises a bracket 101, a reactor 102 is fixedly connected to the top of the bracket 101, a fixing seat 103 is fixedly connected to the top of the bracket 101, a cooling tank 104 is fixedly connected to the inner wall of the fixing seat 103, and further comprises: The automatic cover opening mechanism 2 comprises a driving motor 201 fixedly connected to the top of the bracket 101, a spiral rotating rod 202 fixedly connected to the output end of the driving motor 201, a lifting frame 203 threadedly connected to the outer wall of the spiral rotating rod 202, a positioning rod 204 fixedly connected to the top of the bracket 101, the top of the positioning rod 204 passes through the bottom of the lifting frame 203 and extends to the outside, a sealing cover 205 fixedly connected to the side wall of the lifting frame 203, a fixed support frame 207 fixedly connected to the top of the bracket 101, an arc-shaped guide plate 208 fixedly connected to the side wall of the fixed support frame 207, a guide groove 209 is provided on the outer wall of the arc-shaped guide plate 208, and the inner wall of the guide groove 209 is slidably connected to the outer wall of the L-shaped rotating rod 206, so as to start the driving motor 201 to drive the spiral rotating rod 202 to rotate, and the spiral rotating rod 202 drives the lifting frame 203 and the sealing cover 205 to descend during the rotation, and the bottom of the sealing cover 205 is fixedly connected to the placement frame 21.

[0030] The bottom end of the L-shaped rotating rod 206 is provided with a positioning mechanism 3, which includes a guide plate 301 fixedly connected to the bottom end of the L-shaped rotating rod 206, an arc groove 302 is provided on the top of the guide plate 301, a slide bar 303 is slidably connected to the inner wall of the arc groove 302, a positioning plate 304 is fixedly connected to the bottom end of the slide bar 303, and a ball 305 is rollingly connected to the inner wall of the positioning plate 304. The purpose of such arrangement is to enable the distillation crucible 410 to be rotated after being positioned. The positioning mechanism 3 also includes a fixed plate 31 fixedly connected to the side wall of the placement frame 21. A positioning notch 32 is provided on the top of the fixed plate 31. The inner wall of the positioning notch 32 is slidably connected to the side wall of the positioning plate 304. An inclined slot plate 33 is fixedly connected to the top of the fixed plate 31. A lifting slide bar 34 is fixedly connected to the side wall of the positioning plate 304. The outer wall of the lifting slide bar 34 is slidably connected to the inner wall of the inclined slot plate 33. When the L-shaped rotating rod 206 drives the guide plate 301 to rotate, the slide bar 303 slides in the arc slot 302. The slide bar 303 drives the positioning plate 304 to approach the distillation crucible 410. During the approach process, the inclined groove plate 33 guides the lifting slide bar 34, so that the lifting slide bar 34 drives the positioning plate 304 to descend. When the positioning plate 304 descends and moves, the distillation crucible 410 is positioned to prevent the material from driving the distillation crucible 410 to move during the chemical reaction, thereby ensuring the quality of the product and the safety of the production process. When the distillation crucible 410 needs to be taken out, the positioning mechanism 3 will release the positioning of the distillation crucible 410, and the positioning plate 304 will rise and move away from the distillation crucible 410, so as to facilitate the removal of the distillation crucible 410.

[0031] A support frame 105 is fixedly connected to the top of the bracket 101, and an inert gas supply tank 106 is arranged on the top of the support frame 105. An inert gas output pipe 107 is fixedly connected to the bottom of the inert gas supply tank 106. The exhaust port of the inert gas output pipe 107 penetrates the outer wall of the reactor 102 and extends to the interior. This is arranged so that the inert gas supply tank 106 can discharge high-purity argon gas for air replacement. A distillation air inlet pipe 108 is connected to the side wall of the reactor 102. The end of the distillation air inlet pipe 108 away from the reactor 102 penetrates the top of the cooling tank 104 and extends to the interior. This is arranged so that metal vapor can enter the cooling tank 104 through the distillation air inlet pipe 108.

[0032] The inner wall of the reactor 102 is fixedly connected to a distillation cylinder 11, the outer wall of the distillation cylinder 11 is sleeved with a heater 12, the outer wall of the reactor 102 is connected to a vacuum tube 13, the outer wall of the vacuum tube 13 is fixedly connected to a vacuum tube valve 14, the end of the vacuum tube 13 away from the reactor 102 is fixedly connected to a vacuum machine 15, the top of the vacuum machine 15 is fixedly connected to a vacuum tube 2 16, the end of the vacuum tube 2 16 away from the vacuum machine 15 is connected to the interior of the cooling tank 104, so that the reactor 102 and the cooling tank 104 form a vacuum state.

[0033] like Figures 6 to 8 As shown, the outer wall of the reactor 102 is provided with a rotating reaction mechanism 4, and the rotating reaction mechanism 4 includes a servo motor 401 fixedly connected to the outer wall of the reactor 102, the output end of the servo motor 401 is fixedly connected to a rotating member 1 402, the outer wall of the rotating member 1 402 is rotatably connected to a connecting rod 403, the end of the connecting rod 403 away from the rotating member 1 402 is rotatably connected to a rotating member 2 404, the top of the rotating member 2 404 is fixedly connected to an axis rod 405, the top of the axis rod 405 is connected to a driving gear 406, the top of the driving gear 406 is meshedly connected to a driven gear 407, and the top of the driven gear 407 is fixedly connected to a placement plate 408. A distillation crucible 410 is placed on the top of the placement plate 408, and the outer wall of the placement plate 408 is fixedly connected to a ring guide rail 409, and the outer wall of the ring guide rail 409 is slidably connected to the side wall of the placement frame 21. When the driven gear 407 is engaged with the driving gear 406, the servo motor 401 drives the rotating part 1 402 to rotate, and the rotating part 1 402 drives the rotating part 2 404 to move synchronously through the connecting rod 403, and the rotating part 2 404 drives the shaft rod 405 and the driving gear 406 to rotate, so that the driving gear 406 drives the driven gear 407 to rotate, and the driven gear 407 drives the placement plate 408 and the distillation crucible 410 to rotate.

[0034] The outer wall of the shaft rod 405 is provided with a collision mechanism 5, and the collision mechanism 5 includes an oblique semicircular disk 501 fixedly connected to the outer wall of the shaft rod 405, a reset spring 502 is fixedly connected to the inner wall of the reactor 102, a connecting disk 503 is fixedly connected to the bottom end of the reset spring 502, an L-shaped top rod 504 is fixedly connected to the central axis of the connecting disk 503, a positioning groove cylinder 505 is fixedly connected to the inner wall of the reactor 102, the inner wall of the notch of the positioning groove cylinder 505 is slidably connected to the outer wall of the L-shaped top rod 504, and the bottom of the oblique semicircular disk 501 is in contact with the outer wall of the L-shaped top rod 504. The purpose of this arrangement is that when the shaft rod 405 rotates, the shaft rod 405 drives the inclined semi-circular disk 501 to rotate, and the inclined semi-circular disk 501 presses down the L-shaped top rod 504 during rotation, and the L-shaped top rod 504 descends in the notch of the positioning groove cylinder 505. When the inclined semi-circular disk 501 is no longer in contact with the L-shaped top rod 504, the reset spring 502 drives the connecting disk 503 to reset, so that the connecting disk 503 drives the L-shaped top rod 504 to collide with the placement disk 408, thereby avoiding agglomeration of materials during chemical reactions, preventing material waste, and effectively improving the efficiency of forming metal vapor.

[0035] like Figures 9 and 10A reciprocating mechanism 6 is arranged on the top of the rotating member 1 402, and the reciprocating mechanism 6 includes a rotating rod 601 fixedly connected to the top of the rotating member 1 402, a pulley 1 602 is fixedly connected to the outer wall of the rotating rod 601, a belt 603 is sleeved on the outer wall of the pulley 1 602, a pulley 2 604 is connected to the inner wall of the belt 603, a rotating rod 605 is fixedly connected to the central axis of the pulley 2 604, the bottom end of the rotating rod 605 passes through the top of the cooling tank 104 and extends to the inside, and a rotating column 605 is fixedly connected to the outer wall of the pulley 2 604. 06, the top of the rotating column 606 is fixedly connected with a push block 607, the outer wall of the push block 607 is in contact with the side wall of the lifting plate 608, the top of the cooling tank 104 is fixedly connected with a connecting spring 609, the end of the connecting spring 609 away from the cooling tank 104 is fixedly connected to the bottom of the lifting plate 608, the bottom of the lifting plate 608 is fixedly connected with a lifting rod 610, the lifting rod 610 passes through the top of the cooling tank 104 and extends to the inside, the outer wall of the lifting rod 610 is fixedly connected with an impact ball rod 611, and this arrangement is for the rotating part to 402 drives the rotating rod 601 and the pulley 1 602 to rotate, the pulley 1 602 drives the pulley 2 604 and the rotating rod 605 to rotate through the belt 603, the rotating rod 605 drives the rotating column 606 and the pushing block 607 to rotate, the pushing block 607 pushes the lifting plate 608 to rise, after the pushing block 607 is separated from the lifting plate 608, the connecting spring 609 drives the lifting plate 608 to return to the original position and descend, so that the lifting plate 608 drives the lifting rod 610 to descend, and the lifting rod 610 drives the impact rod 611 to impact the heat dissipation cooling plate 61 The inner wall of the cooling tank 104 is fixedly connected with a plurality of heat dissipation cooling plates 61, and the plurality of heat dissipation cooling plates 61 are distributed at equal distances up and down. The tilting of the heat dissipation cooling plates 61 will change the flow direction of the metal vapor. At this time, the flowing metal vapor has a large inertia and will collide with the heat dissipation cooling plates 61, thereby increasing the contact area between the metal vapor and the heat dissipation cooling plates 61, which is convenient for cooling the metal vapor. The outer wall of the impact club 611 is in contact with the top of the heat dissipation cooling plate 61, and the inner wall of the cooling tank 104 is fixedly connected with a cooler 62.

[0036] like Fig.11As shown, during the condensation and recovery process of rubidium metal, incompletely condensed metal liquid is likely to remain on the surface of the cooler 62. If these residues are not cleaned for a long time, it will not only affect the long-term use effect of the cooler 62, but also may cause waste of resources and increase production costs. The outer wall of the rotating rod 605 is provided with a scratching mechanism 7, and the scratching mechanism 7 includes a guide column 701 fixedly connected to the outer wall of the rotating rod 605. The outer wall of the guide column 701 is provided with a reciprocating groove 702. The inner wall of the reciprocating groove 702 is slidably connected with a slider 703, and the end of the slider 703 away from the reciprocating groove 702 is fixedly connected with a scratching plate 70 4. The inner wall of the scratch plate 704 is slidably connected to the outer wall of the cooler 62. The purpose of this arrangement is to drive the guide column 701 to rotate during the rotation of the rotating rod 605. Since the reciprocating groove 702 guides the slider 703, when the guide column 701 rotates, the slider 703 moves along the reciprocating groove 702, so that the slider 703 drives the scratch plate 704 to reciprocate and rise and fall, and the scratch plate 704 scratches the cooler 62 to prevent excessive metal liquid from remaining on the cooler 62 and affecting its use, which is convenient for subsequent maintenance and cleaning, effectively extending the service life of the device, and further increasing the collection of metal liquid.

[0037] The working principle of the device for producing rubidium bubbles of atomic clocks using rubidium chloride as raw material is as follows: first, rubidium chloride is used as raw material, and strong reducing metal calcium is used as reducing agent and put into a distillation crucible 410, and the driving motor 201 is started to drive the spiral rotating rod 202 to rotate, and the spiral rotating rod 202 drives the lifting frame 203 and the sealing cover 205 during the rotation process. The reaction kettle 102 is lowered, and the sealing cover 205 seals the reaction kettle 102. The sealing of each connector is confirmed. The inert gas supply tank 106 discharges high-purity argon gas for air replacement. First, it is necessary to evacuate the air through the vacuum machine 15, then put in argon gas, and then evacuate the air again. Repeat the replacement several times to replace the gas in the reaction kettle 102 and the cooling tank 104 with argon gas. When the air replacement is completed, the inert gas output pipe 107 stops supplying gas to maintain the vacuum degree. After the replacement, high-temperature vacuum distillation is carried out in a vacuum and inert atmosphere to extract metallic rubidium, so that the melting point and boiling point of the metallic rubidium will be reduced after the chemical reaction of the material. During the descending process of the sealing cover 205, the L-shaped rotating rod 206 is driven to descend. Because the guide groove 209 guides the L-shaped rotating rod 206, when the sealing cover 205 descends to the reaction kettle 10 2 is closed, so that the L-shaped rotating rod 206 rotates 90°, and the L-shaped rotating rod 206 drives the guide plate 301 to rotate. As the sliding rod 303 slides in the arc groove 302, the sliding rod 303 drives the positioning plate 304 to approach the distillation crucible 410. During the approaching process, the inclined groove plate 33 guides the lifting sliding rod 34, so that the lifting sliding rod 34 drives the positioning plate 304 to descend. When the positioning plate 304 descends and moves, the distillation crucible 410 is positioned to prevent the material from driving the distillation crucible 410 to move during the chemical reaction, thereby ensuring the quality of the product and the safety of the production process. When the distillation crucible 410 needs to be taken out, the positioning mechanism 3 will release the positioning of the distillation crucible 410, and the positioning plate 304 will rise and move away from the distillation crucible 410, so as to facilitate the removal of the distillation crucible 410. The heater 12 heats the material in the distillation crucible 410 after heat treatment on the distillation cylinder 11. As the placement rack 21 drives the annular guide rail 409 and the placement plate 408 to descend, the driven gear 407 meshes with the driving gear 406, and the servo motor 401 drives the rotating member 1 402 to rotate. The rotating member 1 402 drives the rotating member 2 404 to move synchronously through the connecting rod 403. The rotating member 2 404 drives the shaft rod 405 and the driving gear 406 to rotate, so that the driving gear 406 drives the driven gear 407 to rotate, and the driven gear 407 drives the placement plate 408 and the distillation crucible 410 to rotate, so that the material is heated more evenly and the distillation efficiency is high. When the shaft rod 405 rotates, the shaft rod 405 drives the oblique semicircular disk 501 to rotate, and the oblique semicircular disk 501 presses down the L-shaped push rod 504 during rotation, and the L-shaped push rod 504 descends in the notch of the positioning groove cylinder 505. When the oblique semicircular disk 501 is no longer in contact with the L-shaped push rod 504, the reset spring 502 drives the connecting disk 503 to reset, so that the connecting disk 503 drives the L-shaped push rod 504 to collide with the placement disk 408, thereby avoiding agglomeration of materials in the chemical reaction, preventing material waste, and effectively improving the efficiency of forming metal vapor. After the reduction reaction of the material occurs, metal vapor will be generated. After the vacuum machine 15 is started, the vacuum tube valve 14 is closed so that the gas can only enter the cooling tank 104 through the distillation inlet pipe 108. The heat dissipation cooling plate 61 and the cooler 62 cool the metal vapor. The tilt of the heat dissipation cooling plate 61 changes the flow direction of the metal vapor. At this time, the flowing metal vapor has a large inertia and will collide with the heat dissipation cooling plate 61, so that the contact area between the metal vapor and the heat dissipation cooling plate 61 is increased, which is convenient for cooling the metal vapor, so that the metal vapor is condensed into liquid and flows into the cooling tank 104, so that the production of metal rubidium is completed; During the cooling process, the metal liquid will remain on the heat dissipation cooling plate 61, the rotating member 402 drives the rotating rod 601 and the pulley 1 602 to rotate, the pulley 1 602 drives the pulley 2 604 and the rotating rod 605 to rotate through the belt 603, the rotating rod 605 drives the rotating column 606 and the push block 607 to rotate, the push block 607 pushes the lifting plate 608 to rise, after the push block 607 is separated from the lifting plate 608, the connecting spring 609 drives the lifting plate 608 to return to the original position and descend, so that the lifting plate 608 drives the lifting rod 610 to descend, and the lifting rod 610 drives the impact rod 611 to collide with the heat dissipation cooling plate 61, so that the metal liquid can be cooled. The metal liquid is separated from the heat dissipation cooling plate 61, which is convenient for collecting the metal liquid and improving the cooling efficiency of the heat dissipation cooling plate 61. The rotating rod 605 drives the guide column 701 to rotate during the rotation, and the reciprocating groove 702 guides the slider 703. When the guide column 701 rotates, the slider 703 moves along the reciprocating groove 702, so that the slider 703 drives the scratch plate 704 to reciprocate and rise and fall, and the scratch plate 704 scratches the cooler 62 to prevent excessive metal liquid from remaining on the cooler 62 and affecting its use, which is convenient for subsequent maintenance and cleaning, effectively prolonging the service life of the device, and further increasing the collection of metal liquid.

[0038] It should be noted that the specific models and specifications of the vacuum machine 15, drive motor 201, heater 12, cooler 62 and servo motor 401 need to be selected and determined according to the actual specifications of the device, and the specific selection calculation method adopts the existing technology in this field, so it will not be repeated in detail.

[0039] The principles of the vacuum machine 15, the drive motor 201, the heater 12, the cooler 62 and the servo motor 401 are clear to those skilled in the art and will not be described in detail herein.

[0040] It is to be understood that the present invention is described by some embodiments, and it is known to those skilled in the art that various changes or equivalent substitutions may be made to these features and embodiments without departing from the spirit and scope of the present invention. In addition, under the teachings of the present invention, these features and embodiments may be modified to adapt to specific circumstances and materials without departing from the spirit and scope of the present invention.

Claims

1. A device for producing rubidium bubbles for atomic clocks using rubidium chloride as a raw material, comprising a support (101), a reactor (102) being fixedly connected to the top of the support (101), a fixing seat (103) being fixedly connected to the top of the support (101), and a cooling tank (104) being fixedly connected to the inner wall of the fixing seat (103), characterized in that: Also includes: An automatic cover opening mechanism (2), the automatic cover opening mechanism (2) comprising a driving motor (201) fixedly connected to the top of a support (101), the output end of the driving motor (201) being fixedly connected to a spiral rotating rod (202), the outer wall of the spiral rotating rod (202) being threadedly connected to a lifting frame (203), the top of the support (101) being fixedly connected to a positioning rod (204), the top end of the positioning rod (204) passing through the bottom of the lifting frame (203) and extending to the outside, The side wall of the lifting frame (203) is fixedly connected to a sealing cover (205), the top of the bracket (101) is fixedly connected to a fixed support frame (207), the side wall of the fixed support frame (207) is fixedly connected to an arc-shaped guide plate (208), the outer wall of the arc-shaped guide plate (208) is provided with a guide groove (209), the inner wall of the guide groove (209) is slidably connected to the outer wall of the L-shaped rotating rod (206), and the bottom of the sealing cover (205) is fixedly connected to a placement frame (21).

2. The device for producing rubidium bubbles for atomic clocks using rubidium chloride as a raw material according to claim 1, characterized in that: A positioning mechanism (3) is provided at the bottom end of the L-shaped rotating rod (206), and the positioning mechanism (3) comprises a guide plate (301) fixedly connected to the bottom end of the L-shaped rotating rod (206), an arc-shaped groove (302) is provided on the top of the guide plate (301), a sliding rod (303) is slidably connected to the inner wall of the arc-shaped groove (302), a positioning plate (304) is fixedly connected to the bottom end of the sliding rod (303), and a rolling ball (305) is rollably connected to the inner wall of the positioning plate (304).

3. The device for producing an atomic clock rubidium bubble using rubidium chloride as a raw material according to claim 2, characterized in that: The positioning mechanism (3) further comprises a fixed plate (31) fixedly connected to the side wall of the placement rack (21); a positioning notch (32) is provided on the top of the fixed plate (31); an inner wall of the positioning notch (32) is slidably connected to the side wall of the positioning plate (304); an inclined slot plate (33) is fixedly connected to the top of the fixed plate (31); a lifting slide rod (34) is fixedly connected to the side wall of the positioning plate (304); and an outer wall of the lifting slide rod (34) is slidably connected to the inner wall of the inclined slot plate (33).

4. The device for producing rubidium bubbles for atomic clocks using rubidium chloride as a raw material according to claim 3, characterized in that: The top of the support (101) is fixedly connected to a support frame (105), the top of the support frame (105) is provided with an inert gas supply tank (106), the bottom of the inert gas supply tank (106) is fixedly connected to an inert gas output pipe (107), the exhaust port of the inert gas output pipe (107) penetrates the outer wall of the reactor (102) and extends to the interior, the side wall of the reactor (102) is connected to a distillation air inlet pipe (108), and the end of the distillation air inlet pipe (108) away from the reactor (102) penetrates the top of the cooling tank (104) and extends to the interior.

5. The device for producing rubidium bubbles for atomic clocks using rubidium chloride as a raw material according to claim 4, characterized in that: The inner wall of the reactor (102) is fixedly connected to a distillation cylinder (11), the outer wall of the distillation cylinder (11) is sleeved with a heater (12), the outer wall of the reactor (102) is connected to a vacuum tube 1 (13), the outer wall of the vacuum tube 1 (13) is fixedly connected to a vacuum tube valve (14), the end of the vacuum tube 1 (13) away from the reactor (102) is fixedly connected to a vacuum machine (15), the top of the vacuum machine (15) is fixedly connected to a vacuum tube 2 (16), and the end of the vacuum tube 2 (16) away from the vacuum machine (15) is connected to the interior of the cooling tank (104).

6. The device for producing rubidium bubbles for atomic clocks using rubidium chloride as a raw material according to claim 5, characterized in that: The outer wall of the reaction kettle (102) is provided with a rotating reaction mechanism (4), and the rotating reaction mechanism (4) comprises a servo motor (401) fixedly connected to the outer wall of the reaction kettle (102), the output end of the servo motor (401) is fixedly connected to a rotating member 1 (402), the outer wall of the rotating member 1 (402) is rotatably connected to a connecting rod (403), one end of the connecting rod (403) away from the rotating member 1 (402) is rotatably connected to a rotating member 2 (404), and the top of the rotating member 2 (404) is fixedly connected to an axial rod (405).

7. The device for producing rubidium bubbles for atomic clocks using rubidium chloride as a raw material according to claim 6, characterized in that: The top of the shaft rod (405) is connected to a driving gear (406), the top of the driving gear (406) is meshingly connected to a driven gear (407), the top of the driven gear (407) is fixedly connected to a placement plate (408), a distillation crucible (410) is placed on the top of the placement plate (408), the outer wall of the placement plate (408) is fixedly connected to an annular guide rail (409), and the outer wall of the annular guide rail (409) is slidably connected to the side wall of the placement rack (21).

8. The device for producing rubidium bubbles for atomic clocks using rubidium chloride as a raw material according to claim 7, characterized in that: The outer wall of the shaft rod (405) is provided with a collision mechanism (5), and the collision mechanism (5) comprises an oblique semicircular disk (501) fixedly connected to the outer wall of the shaft rod (405); the inner wall of the reaction kettle (102) is fixedly connected with a return spring (502); the bottom end of the return spring (502) is fixedly connected with a connecting disk (503); the central axis of the connecting disk (503) is fixedly connected with an L-shaped top rod (504); the inner wall of the reaction kettle (102) is fixedly connected with a positioning groove cylinder (505); the inner wall of the notch of the positioning groove cylinder (505) is slidably connected to the outer wall of the L-shaped top rod (504); and the bottom of the oblique semicircular disk (501) is arranged in contact with the outer wall of the L-shaped top rod (504).

9. The device for producing rubidium bubbles for atomic clocks using rubidium chloride as a raw material according to claim 8, characterized in that: A reciprocating mechanism (6) is arranged on the top of the rotating member 1 (402), and the reciprocating mechanism (6) comprises a rotating rod (601) fixedly connected to the top of the rotating member 1 (402), the outer wall of the rotating rod (601) is fixedly connected to a pulley 1 (602), the outer wall of the pulley 1 (602) is sleeved with a belt (603), the inner wall of the belt (603) is transmission-connected to a pulley 2 (604), the central axis of the pulley 2 (604) is fixedly connected to a rotating rod (605), and the rotating rod (605) is fixedly connected to the central axis of the rotating rod (605). 05) passes through the top of the cooling tank (104) and extends into the interior, the outer wall of the pulley 2 (604) is fixedly connected with a rotating column (606), the top of the rotating column (606) is fixedly connected with a push block (607), the outer wall of the push block (607) is arranged in contact with the side wall of the lifting plate (608), the top of the cooling tank (104) is fixedly connected with a connecting spring (609), and the end of the connecting spring (609) away from the cooling tank (104) is fixedly connected to the bottom of the lifting plate (608).

10. The device for producing rubidium bubbles for atomic clocks using rubidium chloride as a raw material according to claim 9, characterized in that: The bottom of the lifting plate (608) is fixedly connected to a lifting rod (610), and the lifting rod (610) passes through the top of the cooling tank (104) and extends to the inside. The outer wall of the lifting rod (610) is fixedly connected to an impact rod (611), and the inner wall of the cooling tank (104) is fixedly connected to a plurality of heat dissipation cooling plates (61), and the plurality of heat dissipation cooling plates (61) are distributed at equal distances up and down. The outer wall of the impact rod (611) is arranged in contact with the top of the heat dissipation cooling plate (61), and the inner wall of the cooling tank (104) is fixedly connected to a cooler (62).

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