Cream texture hair mud with keratin and preparation method of cream texture hair mud

Abstract

The invention relates to the technical field of daily cosmetics, in particular to cream texture hair mud with keratin and a preparation method of the cream texture hair mud. Comprising the following steps: sequentially adding a water-based emulsifier and a humectant into deionized water, and stirring at 70-80 DEG C for 1-1.5 hours to obtain a water phase for later use; melting beeswax at 70-80 DEG C, adding an oily emulsifier and petrolatum, and stirring for 1-1.5 hours to obtain an oil phase for later use; adding the oil phase into the water phase, and mixing for 30-40 minutes at 70-80 DEG C; cooling to 60-70 DEG C, sequentially adding the VP / VA copolymer, the conditioner, the bentonite, the essence and the preservative, stirring and mixing for 1-2 hours, cooling to room temperature, and sterilizing to obtain the cream texture mud with keratin; the keratin-containing cream-like texture hair mud has good antibacterial, hair-growing, hair-loss-preventing and shaping capacities, and also has the performance characteristics of safe components, higher moisturizing capacity and the like, and finally, the cream-like texture hair mud with keratin is obtained.

Description

Technical Field

[0001] The invention relates to the technical field of daily cosmetics, in particular to a frosty textured hair mud with keratin and a preparation method thereof. Background Art

[0002] In the modern hairdressing industry, hair clay is a common styling product that is widely used to shape and fix hairstyles. With the development of the times, traditional hair clay has been unable to meet the needs of consumers. In the prior art, a basic formula mixing method is usually used, but this method may cause the hair clay to be insufficient in terms of adhesion, styling ability or durability, and the hair clay contains a lot of wax and grease. Frequent use will induce oily scalp, and even cause bacterial infection of the scalp, causing acne and seborrheic dermatitis.

[0003] In summary, it is of great significance to prepare a creamy textured hair clay with keratin. Summary of the invention

[0004] The object of the present invention is to provide a cream-like textured hair clay with keratin and a preparation method thereof, so as to solve the problems raised in the above-mentioned background technology.

[0005] In order to solve the above technical problems, the present invention provides the following technical solutions:

[0006] A cream-like textured hair clay with keratin: the textured hair clay comprises the following raw materials, calculated by weight percentage: 3-8% beeswax, 2-4% aqueous emulsifier, 2-4% oily emulsifier, 1-3% VP / VA copolymer, 2-5% conditioner, 1-3% moisturizer, 1-2% petrolatum, 0.5-1.5% bentonite, 0.1-0.2% flavor, 0.1-0.3% preservative, and the rest is deionized water.

[0007] More optimally, the aqueous emulsifier includes one or two of ceteareth-30 and ceteareth-25; the oily emulsifier includes one or two of oleth-10 and hydroxypropyl distearyl dimethyl ammonium chloride;

[0008] The humectant includes one or more of maltitol, glycerin, and propylene glycol;

[0009] The preservatives include one or more of phenoxyethanol, methylparaben, chlorphenesin, and propylparaben.

[0010] More optimally, the conditioning agent includes polydimethylsiloxane and modified keratin / sodium carboxymethyl cellulose, and the mass ratio of the two is 0.5-1.5:1.5-3.5.

[0011] More optimally, the preparation method of the modified keratin / sodium carboxymethyl cellulose is:

[0012] S1: Preparation of modified keratin: Keratin powder and deionized water are mixed, polylysine and glyoxal are added in sequence, heated at 50-60° C. for 3-6 hours, filtered, and frozen at -20--45° C. for 48-50 hours to obtain modified keratin;

[0013] S2: Add sodium carboxymethyl cellulose to deionized water to obtain a sodium carboxymethyl cellulose solution, add modified keratin, stir evenly, add calcium silicate, polyacrylate, and potassium persulfate, stir evenly, and freeze at -20 to -80°C for 24 to 36 hours to obtain modified keratin / sodium carboxymethyl cellulose.

[0014] More optimally, the modified keratin comprises the following raw materials by weight: 4 to 6 parts of keratin powder, 50 to 60 parts of deionized water, 2 to 4 parts of polylysine, and 2 to 3 parts of glyoxal;

[0015] The modified keratin / sodium carboxymethyl cellulose comprises the following raw materials in parts by weight: 5-6 parts of sodium carboxymethyl cellulose, 30-40 parts of deionized water, 3-4 parts of modified keratin, 1-1.5 parts of calcium silicate, 2-2.5 parts of polyacrylate, and 0.5-0.8 parts of potassium persulfate.

[0016] In the scheme, keratin is a natural ingredient. Adding it to the hair mud can provide nourishment and protection for the hair while retaining the styling effect; in the aqueous phase solution for preparing the cream-like textured hair mud with keratin, modified keratin / carboxymethyl cellulose is added. The modified keratin is modified by a specific grafting reaction, a cross-linking reaction, etc. to modify the natural keratin to improve its solubility, stability and functionality. In the hair mud, the modified keratin can interact with the keratin in the hair to form a tighter bond, thereby enhancing the adhesion and styling effect of the hair mud. Carboxymethyl cellulose, as a water-soluble polymer compound, mainly plays the role of thickening, gelling and water retention in the hair mud. It can not only give the hair mud a good texture and spreadability, but also maintain the wetness and gloss of the hair. The combination of modified keratin and carboxymethyl cellulose will produce a synergistic effect. The modified keratin has a three-dimensional network structure. Through the embedding of carboxymethyl cellulose, it can be further grafted to produce a cross-linking effect, which can enhance the stability, adhesion and styling effect of the hair mud, while maintaining the natural gloss and softness of the hair. In addition, the combination of the two also enhances the biocompatibility of the hair mud, improves the texture and enhances moisturizing properties.

[0017] More optimally, the textured hair mud also includes 1-2% of a traditional Chinese medicine compound.

[0018] More optimally, the preparation method of the traditional Chinese medicine complex is:

[0019] S1: Preparation of Chinese medicine extract: sequentially add Polygonum multiflorum, ginseng, Chinese angelica, and Psoralea corylifolia to deionized water and soak for 2 to 3 hours to obtain mixture A; sequentially add Platycladus orientalis leaves, black beans, and black sesame to deionized water and soak for 1 to 1.5 hours to obtain mixture B; boil mixture A over high heat, then boil over medium heat for 1 to 2 hours, add mixture B and boil over low heat for 1 to 1.5 hours, filter, and obtain Chinese medicine extract;

[0020] S2: Preparation of Chinese medicine complex: Dissolve alcohol and artemisia annua oil uniformly by mixing and stirring, and then uniformly mix deionized water, Chinese medicine extract, tea polyphenols, dodecyl dimethyl tertiary amine, and polyglycerol-2 dipolyhydroxystearate to obtain the Chinese medicine complex.

[0021] In a further embodiment, in order to further reduce the growth of oily bacteria caused by wax and grease in hair mud, the present invention adds artemisia annua oil in the preparation of the traditional Chinese medicine complex. Its antibacterial and anti-inflammatory effects can reduce the growth of bacteria on the scalp to a certain extent, thereby improving scalp health and avoiding bacterial infection, acne and seborrheic dermatitis caused by oily hair mud.

[0022] More optimally, the mass ratio of mixture A to mixture B in the traditional Chinese medicine extract is (2-2.5):1;

[0023] The mixture A comprises the following components: by weight: 8 to 13 parts of Polygonum multiflorum, 5 to 8 parts of Ginseng, 3 to 5 parts of Angelica sinensis, 4 to 6 parts of Psoralea corylifolia, and 50 to 60 parts of deionized water;

[0024] The mixture B comprises the following components: by mass: 10 to 13 parts of black beans, 8 to 13 parts of black sesame seeds, 6 to 9 parts of Platycladus orientalis leaves, and 40 to 50 parts of deionized water;

[0025] The raw materials of the traditional Chinese medicine complex include the following components: by weight, 10 to 20 parts of alcohol, 1 to 2 parts of artemisia oil, 15 to 30 parts of deionized water, 3 to 5 parts of traditional Chinese medicine extract, 0.05 to 0.1 parts of tea polyphenols, 1.5 to 2 parts of dodecyl dimethyl tertiary amine, and 1 to 1.5 parts of polyglycerol-2 dipolyhydroxystearate.

[0026] Among them, the Chinese medicine extract added to the Chinese medicine complex has the effect of preventing hair loss and darkening hair. After the Chinese medicine extract is added to the hair mud, it can deeply nourish the scalp and hair roots, improve the blood circulation and nutritional status of the scalp, and promote the growth and repair of hair. At the same time, they can also effectively improve hair problems such as hair loss and gray hair, making the hair healthier, black and shiny. In addition, the addition of these Chinese medicines also enhances the nourishing effect and biological activity of the hair mud, making it more in line with modern people's pursuit of health and nature.

[0027] More optimally, a method for preparing a creamy textured hair mud having keratin comprises the following steps:

[0028] S1: (1) adding an aqueous emulsifier and a moisturizer to deionized water in sequence, stirring at 70 to 80° C. for 1 to 1.5 hours to obtain an aqueous phase for later use; (2) melting beeswax at 70 to 80° C., adding an oily emulsifier and petrolatum, stirring for 1 to 1.5 hours to obtain an oil phase for later use;

[0029] S2: Add the oil phase to the water phase, mix at 70-80°C for 30-40 minutes; cool to 60-70°C, add VP / VA copolymer, conditioner, bentonite, flavor, preservative in sequence, stir and mix for 1-2 hours, cool to room temperature, sterilize, and obtain textured mud.

[0030] More optimally, a method for preparing a frosty textured hair clay with keratin prepares a frosty textured hair clay with keratin.

[0031] Compared with the prior art, the present invention has the following beneficial effects:

[0032] (1) By adding modified keratin / carboxymethyl cellulose, the modified keratin has a stable three-dimensional structure. Through the embedding of carboxymethyl cellulose, the two produce a synergistic effect, which can enhance the stability, adhesion and styling effect of the hair mud while maintaining the natural luster and softness of the hair.

[0033] (2) In addition, in order to further improve the health and hair nourishing performance of the textured hair mud, a Chinese herbal medicine complex is further introduced into the scheme. Artemisia annua oil is added to the Chinese herbal medicine complex to inhibit bacterial growth and have antibacterial and anti-inflammatory effects. At the same time, Chinese herbal medicine extracts are also introduced into the Chinese herbal medicine complex. The addition of Polygonum multiflorum, ginseng, angelica, psoralea corylifolia, Platycladus orientalis leaves, black beans, and black sesame can effectively improve hair quality problems such as hair loss and gray hair, making hair healthier, black and shiny. DETAILED DESCRIPTION

[0034] The technical solutions in the embodiments of the present invention are described clearly and completely below. Obviously, the described embodiments are only part of the embodiments of the present invention, not all of them. Based on the embodiments of the present invention, all other embodiments obtained by ordinary technicians in this field without creative work are within the scope of protection of the present invention.

[0035] It should be noted that the following parts are by mass, and the purchase manufacturers of all raw materials involved in the present invention are exemplified without any special restrictions: In the following embodiments: beeswax purity 99%, CAS No. 8012-89-3, purchased from Shanghai Chunshi Biotechnology Co., Ltd.; cetearyl alcohol polyether-30 purity 99%, model O-30, purchased from Linyi Guoli Chemical Co., Ltd.; VP / VA copolymer purity 99%, CAS No. 25086-89-9, purchased from Tesco Chemical (Hubei) Co., Ltd.; oleyl alcohol polyether-10 purity 99%, CAS No. 24871-34-9, purchased from Nantong Chenrun Chemical Co., Ltd.; polydimethylsiloxane purity 99%, CAS No. 9016-00-6, purchased from From Shanxi Jinyang Pharmaceutical Excipients Co., Ltd.; maltitol purity 99%, CAS No. 585-88-6, purchased from Anhui Youtai Bioengineering Co., Ltd.; petrolatum purity 99%, CAS No. 8009-03-8, purchased from Kandis Chemical (Hubei) Co., Ltd.; polyisobutylene purity 99%, CAS No. 9003-27-4, purchased from Hebei Clavier Biotechnology Co., Ltd.; cetearyl alcohol polyether-25 purity 99%, CAS No. 68439-49-6, purchased from Hubei Baidu Chemical Co., Ltd.; phenoxyethanol purity 99%, CAS No. 122-99-6, purchased from Guangzhou Hengyu Chemical Co., Ltd.; bentonite purity 99%, CAS No. 1302-78-9, purchased from Shanghai Yuanye Biotechnology Co., Ltd.; methylparaben purity 99%, CAS No. 99-76-3, purchased from Xi'an Yutai Pharmaceutical Co., Ltd.; chlorphenesin purity 99%, CAS No. 104-29-0, purchased from Shanghai Dongfan Chemical Technology Co., Ltd.; propylene glycol purity 99.9%, CAS No. 57-55-6, purchased from Shanghai Fangye Chemical Co., Ltd.; hydroxypropyl distearyl dimethyl ammonium chloride, CAS No. 132467-76-6, purchased from Guangzhou Huazhiwang Chemical Co., Ltd.; propylparaben purity 99%, CAS No. 94-13-3, purchased from Zhengzhou Alpha Chemical Co., Ltd.; keratin purity 98%, CAS No. 68238-35-7, purchased from Xi'an Kangnuo Chemical Co., Ltd.; polylysine purity Purity 99%, CAS No. 25104-18-1, purchased from Beijing Purein Biochromatography Technology Co., Ltd.; glyoxal purity 99%, CAS No. 107-22-2, purchased from Nantong Runfeng Petrochemical Co., Ltd.; sodium carboxymethyl cellulose purity 99%, CAS No. 9004-32-4, purchased from Nanjing Songguan Biotechnology Co., Ltd.; calcium silicate purity 99%, CAS No. 1344-95-2, purchased from Langfang Qianyao Chemical Reagent Co., Ltd.; polyacrylate purity 99.5%, CAS No. 107-10-8, purchased from Jinan Renyuan Chemical Co., Ltd.; potassium persulfate purity 99%, CAS No. 7727-21-1, purchased from Shandong Xinhe New Materials Co., Ltd.; glycerol purity 99.5%, CAS No. 56-81-5, purchased from Shandong Yonglida New Materials Technology Co., Ltd.; tea polyphenols purity 98%, CAS No. 84650-60-2, purchased from Shaanxi Haochen Biotechnology Co., Ltd.; dodecyl dimethyl tertiary amine purity 99%, CAS No. 112-18-5, purchased from Shandong Panze Chemical Technology Co., Ltd.; artemisia annua oil purity 99%, CAS No. 63968-64-9, purchased from Jishui County Juyuantang Natural Fragrance Oil Co., Ltd.; polyglycerol-2 dipolyhydroxystearate purity 99%, CAS No. 156531-21-4, purchased from Hubei Xinkang Pharmaceutical Chemical Co., Ltd. .

[0036] Embodiment 1: A method for preparing a creamy textured hair clay having keratin, comprising the following steps:

[0037] Step 1: Preparation of Chinese medicine complex: (1) 10 parts of Polygonum multiflorum, 6.5 parts of ginseng, 4 parts of Angelica sinensis, and 5 parts of Psoralea corylifolia are added to 55 parts of deionized water and soaked for 2.5 hours to obtain mixture A; (2) 7.5 parts of Platycladus orientalis leaves, 11.5 parts of black beans, and 10.5 parts of black sesame are added to 45 parts of deionized water and soaked for 1.2 hours to obtain mixture B; (3) The mass ratio of mixture A to mixture B is 2.2:1, mixture A is boiled over high heat, then boiled over medium heat for 1.5 hours, mixture B is added and boiled over low heat for 1.2 hours, filtered, and a Chinese medicine extract is obtained; (4) 15 parts of alcohol and 1.5 parts of Artemisia annua oil are mixed and stirred to dissolve uniformly, 22.5 parts of deionized water, 4 parts of Chinese medicine extract, 0.075 parts of tea polyphenols, 1.75 parts of dodecyl dimethyl tertiary amine, and 1.2 parts of polyglycerol-2 dipolyhydroxystearate are added in turn, stirred uniformly, and a Chinese medicine complex is obtained;

[0038] Step 2: (1) Preparation of modified keratin: 5 parts of keratin powder and 55 parts of deionized water were mixed, and 3 parts of polylysine and 2.5 parts of glyoxal were added in sequence, heated at 55° C. for 4.5 hours, filtered, purified, and frozen at -35° C. for 49 hours to obtain modified keratin; (2) Preparation of modified keratin / sodium carboxymethyl cellulose: 5.5 parts of sodium carboxymethyl cellulose were added to 35 parts of deionized water to obtain a sodium carboxymethyl cellulose solution, 3.5 parts of modified keratin were added, stirred evenly, 1.2 parts of calcium silicate, 2.25 parts of polyacrylate, and 0.65 parts of potassium persulfate were added, stirred at 50° C. for 2 hours, cooled to room temperature, purified, and frozen at -50° C. for 30 hours to obtain modified keratin / sodium carboxymethyl cellulose;

[0039] Step 3: Preparation of a cream-like textured hair clay with keratin: (1) Add an aqueous emulsifier and a moisturizer to deionized water in sequence, stir at 75° C. for 1.25 hours to obtain a water phase for later use; (2) Melt beeswax at 75° C., add an oily emulsifier and petrolatum, stir for 1.25 hours to obtain an oil phase for later use; (3) Weigh the oil phase and the water phase in a mass ratio of 1.2:1.75; add the oil phase to the water phase, mix at 75° C. for 35 minutes, cool to 65° C., add VP / VA copolymer, conditioner, bentonite, fragrance, and preservative in sequence, stir and mix for 1.5 hours, cool to room temperature, and sterilize to obtain a textured hair clay;

[0040] In this embodiment, the raw materials of the textured hair mud include the following ingredients: by weight percentage, 5.5% beeswax, 3% aqueous emulsifier, 3% oily emulsifier, 2% VP / VA copolymer, 3.5% conditioning agent (polydimethylsiloxane, modified keratin / sodium carboxymethyl cellulose, the mass ratio of the two is 1:2.5), 2% moisturizer, 1.5% petrolatum, 1% bentonite, 0.15% flavor, 0.2% preservative, 1.5% Chinese medicine complex, and the rest is deionized water.

[0041] Embodiment 2: A method for preparing a creamy textured hair clay having keratin, comprising the following steps:

[0042] Step 1: Preparation of Chinese medicine complex: (1) 8 parts of Polygonum multiflorum, 5 parts of Ginseng, 3 parts of Angelica sinensis, and 4 parts of Psoralea corylifolia are added to 50 parts of deionized water and soaked for 2 hours to obtain mixture A; (2) 6 parts of Platycladus orientalis leaves, 10 parts of black beans, and 8 parts of black sesame are added to 40 parts of deionized water and soaked for 1 hour to obtain mixture B; (3) The mass ratio of mixture A to mixture B is 2:1, mixture A is boiled over high heat, then boiled over medium heat for 1 hour, mixture B is added and boiled over low heat for 1 hour, filtered, and a Chinese medicine extract is obtained; (4) 10 parts of alcohol and 1 part of Artemisia annua oil are mixed and stirred to dissolve uniformly, 15 parts of deionized water, 3 parts of Chinese medicine extract, 0.05 parts of tea polyphenols, 1.5 parts of dodecyl dimethyl tertiary amine, and 1 part of polyglycerol-2 dihydroxystearate are added in turn, stirred uniformly, and a Chinese medicine complex is obtained;

[0043] Step 2: (1) Preparation of modified keratin: 4 parts of keratin powder are mixed with 50 parts of deionized water, and 2 parts of polylysine and 2 parts of glyoxal are added in sequence, heated at 50°C for 3 hours, filtered, purified, and frozen at -20°C for 48 hours to obtain modified keratin; (2) Preparation of modified keratin / sodium carboxymethyl cellulose: 5 parts of sodium carboxymethyl cellulose are added to 30 parts of deionized water to obtain a sodium carboxymethyl cellulose solution, 3 parts of modified keratin are added, stirred evenly, 1 part of calcium silicate, 2 parts of polyacrylate, and 0.5 part of potassium persulfate are added, stirred at 50°C for 2 hours, cooled to room temperature, purified, and frozen at -20°C for 24 hours to obtain modified keratin / sodium carboxymethyl cellulose;

[0044] Step 3: Preparation of a cream-like textured hair clay with keratin: (1) Add an aqueous emulsifier and a moisturizer to deionized water in sequence, stir at 70°C for 1 hour to obtain an aqueous phase for later use; (2) Melt beeswax at 70°C, add an oily emulsifier and petrolatum, stir for 1 hour to obtain an oil phase for later use; (3) Add the oil phase at a mass ratio of 1.2:1.5 to the aqueous phase, mix at 70°C for 35 minutes; cool to 60°C, add VP / VA copolymer, conditioner, bentonite, fragrance, and preservative in sequence, stir and mix for 1 hour, cool to room temperature, and sterilize to obtain a textured hair clay.

[0045] In this embodiment, the raw materials of the textured hair mud include the following ingredients: by weight percentage, 3% beeswax, 2% aqueous emulsifier, 2% oily emulsifier, 1% VP / VA copolymer, 2% conditioning agent (polydimethylsiloxane, modified keratin / sodium carboxymethyl cellulose, the mass ratio of the two is 0.5:1.5), 1% moisturizer, 1% petrolatum, 0.5% bentonite, 0.1% flavor, 0.1% preservative, 1% Chinese medicine complex, and the rest is deionized water.

[0046] Embodiment 3: A method for preparing a creamy textured hair clay having keratin, comprising the following steps:

[0047] Step 1: Preparation of Chinese medicine complex: (1) 13 parts of Polygonum multiflorum, 8 parts of Ginseng, 5 parts of Angelica sinensis, and 6 parts of Psoralea corylifolia are added to 60 parts of deionized water and soaked for 3 hours to obtain mixture A; (2) 9 parts of Platycladus orientalis leaves, 13 parts of black beans, and 13 parts of black sesame are added to 50 parts of deionized water and soaked for 1.5 hours to obtain mixture B; (3) The mass ratio of mixture A to mixture B is 2.5:1, mixture A is boiled over high heat, then boiled over medium heat for 2 hours, mixture B is added and boiled over low heat for 1.5 hours, filtered, and a Chinese medicine extract is obtained; (4) 20 parts of alcohol and 2 parts of Artemisia annua oil are mixed and stirred to dissolve uniformly, 30 parts of deionized water, 5 parts of Chinese medicine extract, 0.1 parts of tea polyphenols, 2 parts of dodecyl dimethyl tertiary amine, and 1.5 parts of polyglycerol-2 dihydroxystearate are added in turn and stirred to obtain a Chinese medicine complex;

[0048] Step 2: (1) Preparation of modified keratin: 6 parts of keratin powder and 60 parts of deionized water are mixed, 4 parts of polylysine and 3 parts of glyoxal are added in sequence, heated at 60°C for 6 hours, filtered, purified, and frozen at -45°C for 50 hours to obtain modified keratin; (2) Preparation of modified keratin / sodium carboxymethyl cellulose: 6 parts of sodium carboxymethyl cellulose are added to 40 parts of deionized water to obtain a sodium carboxymethyl cellulose solution, 4 parts of modified keratin are added, stirred evenly, 1.5 parts of calcium silicate, 2.5 parts of polyacrylate, and 0.8 parts of potassium persulfate are added, stirred at 50°C for 2 hours, cooled to room temperature, purified, and frozen at -80°C for 36 hours to obtain modified keratin / sodium carboxymethyl cellulose;

[0049] Step 3: Preparation of a cream-like textured hair clay with keratin: (1) Add an aqueous emulsifier and a moisturizer to deionized water in sequence, stir at 80°C for 1.5 hours to obtain an aqueous phase for later use; (2) Melt beeswax at 80°C, add an oily emulsifier and petrolatum, stir for 1.5 hours to obtain an oil phase for later use; (3) Add the oil phase to the aqueous phase at a mass ratio of 1.2:2, mix at 80°C for 35 minutes; cool to 70°C, add VP / VA copolymer, conditioner, bentonite, fragrance, and preservative in sequence, stir and mix for 2 hours, cool to room temperature, and sterilize to obtain a textured hair clay.

[0050] In this embodiment, the raw materials of the textured hair mud include the following ingredients: by weight percentage, 8% beeswax, 4% aqueous emulsifier, 4% oily emulsifier, 3% VP / VA copolymer, 5% conditioner (polydimethylsiloxane, modified keratin / sodium carboxymethyl cellulose, the mass ratio of the two is 1.5:3.5), 3% moisturizer, 2% petrolatum, 1.5% bentonite, 0.2% flavor, 0.3% preservative, 2% Chinese medicine complex, and the rest is deionized water.

[0051] Comparative Example 1: Keratin / sodium carboxymethyl cellulose is not added, and the other processes remain unchanged, specifically:

[0052] Step 1: Preparation of Chinese medicine complex: (1) 10 parts of Polygonum multiflorum, 6.5 parts of ginseng, 4 parts of Angelica sinensis, and 5 parts of Psoralea corylifolia are added to 55 parts of deionized water and soaked for 2.5 hours to obtain mixture A; (2) 7.5 parts of Platycladus orientalis leaves, 11.5 parts of black beans, and 10.5 parts of black sesame are added to 45 parts of deionized water and soaked for 1.2 hours to obtain mixture B; (3) The mass ratio of mixture A to mixture B is 2.2:1, mixture A is boiled over high heat, then boiled over medium heat for 1.5 hours, mixture B is added and boiled over low heat for 1.2 hours, filtered, and a Chinese medicine extract is obtained; (4) 15 parts of alcohol and 1.5 parts of Artemisia annua oil are mixed and stirred to dissolve uniformly, 22.5 parts of deionized water, 4 parts of Chinese medicine extract, 0.075 parts of tea polyphenols, 1.75 parts of dodecyl dimethyl tertiary amine, and 1.2 parts of polyglycerol-2 dipolyhydroxystearate are added in turn, stirred uniformly, and a Chinese medicine complex is obtained;

[0053] Step 2: Preparation of a cream-like textured hair clay with keratin: (1) Add an aqueous emulsifier and a moisturizer to deionized water in sequence, stir at 75°C for 1.25 hours to obtain an aqueous phase for later use; (2) Melt beeswax at 75°C, add an oily emulsifier and petrolatum, stir for 1.25 hours to obtain an oil phase for later use; (3) Add the oil phase at a mass ratio of 1.2:1.75 to the aqueous phase, mix at 75°C for 35 minutes; cool to 65°C, add VP / VA copolymer, polydimethylsiloxane, bentonite, essence, and preservative in sequence, stir and mix for 1.5 hours, cool to room temperature, and sterilize to obtain a textured hair clay.

[0054] In this embodiment, the raw materials of the textured hair mud include the following ingredients: by weight percentage, 5.5% beeswax, 3% aqueous emulsifier, 3% oily emulsifier, 2% VP / VA copolymer, 3.5% polydimethylsiloxane, 2% moisturizer, 1.5% petrolatum, 1% bentonite, 0.15% flavor, 0.2% preservative, 1.5% traditional Chinese medicine compound, and the rest is deionized water.

[0055] Comparative Example 2: No Chinese medicine compound is added, and the other processes remain unchanged, specifically:

[0056] Step 1: (1) Preparation of modified keratin: 5 parts of keratin powder and 55 parts of deionized water are mixed, 3 parts of polylysine and 2.5 parts of glyoxal are added in sequence, heated at 55° C. for 4.5 hours, filtered, purified, and frozen at -35° C. for 49 hours to obtain modified keratin; (2) Preparation of modified keratin / sodium carboxymethyl cellulose: 5.5 parts of sodium carboxymethyl cellulose are added to 35 parts of deionized water to obtain a sodium carboxymethyl cellulose solution, 3.5 parts of modified keratin are added, stirred evenly, 1.2 parts of calcium silicate, 2.25 parts of polyacrylate, and 0.65 parts of potassium persulfate are added, stirred at 50° C. for 2 hours, cooled to room temperature, purified, and frozen at -50° C. for 30 hours to obtain modified keratin / sodium carboxymethyl cellulose;

[0057] Step 2: Preparation of a cream-like textured hair clay with keratin: (1) Add an aqueous emulsifier and a moisturizer to deionized water in sequence, stir at 75°C for 1.25 hours to obtain an aqueous phase for later use; (2) Melt beeswax at 75°C, add an oily emulsifier and petrolatum, stir for 1.25 hours to obtain an oil phase for later use; (3) Add the oil phase at a mass ratio of 1.2:1.75 to the aqueous phase, mix at 75°C for 35 minutes; cool to 65°C, add VP / VA copolymer, conditioner, bentonite, fragrance, and preservative in sequence, stir and mix for 1.5 hours, cool to room temperature, and sterilize to obtain a textured hair clay.

[0058] In this embodiment, the raw materials of the textured hair mud include the following ingredients: by weight percentage, 5.5% beeswax, 3% aqueous emulsifier, 3% oily emulsifier, 2% VP / VA copolymer, 3.5% conditioner (polydimethylsiloxane, modified keratin / sodium carboxymethyl cellulose, the mass ratio of the two is 1:2.5), 2% moisturizer, 1.5% petrolatum, 1% bentonite, 0.15% fragrance, 0.2% preservative, and the rest is deionized water.

[0059] Comparative Example 3: Artemisia annua oil is not added, and the rest of the process remains unchanged. Specifically:

[0060] Step 1: Preparation of Chinese medicine complex: (1) 10 parts of Polygonum multiflorum, 6.5 parts of Ginseng, 4 parts of Angelica sinensis, and 5 parts of Psoralea corylifolia are added to 55 parts of deionized water and soaked for 2.5 hours to obtain mixture A; (2) 7.5 parts of Platycladus orientalis leaves, 11.5 parts of black beans, and 10.5 parts of black sesame are added to 45 parts of deionized water and soaked for 1.2 hours to obtain mixture B; (3) The mass ratio of mixture A to mixture B is 2.2:1, mixture A is boiled over high heat, then boiled over medium heat for 1.5 hours, mixture B is added and boiled over low heat for 1.2 hours, filtered, and a Chinese medicine extract is obtained; (4) 15 parts of alcohol are mixed and stirred to dissolve uniformly, 22.5 parts of deionized water, 4 parts of Chinese medicine extract, 0.075 parts of tea polyphenols, 1.75 parts of dodecyl dimethyl tertiary amine, and 1.2 parts of polyglycerol-2 dipolyhydroxystearate are sequentially added and stirred to obtain a Chinese medicine complex;

[0061] Step 2: (1) Preparation of modified keratin: 5 parts of keratin powder and 55 parts of deionized water were mixed, and 3 parts of polylysine and 2.5 parts of glyoxal were added in sequence, heated at 55° C. for 4.5 hours, filtered, purified, and frozen at -35° C. for 49 hours to obtain modified keratin; (2) Preparation of modified keratin / sodium carboxymethyl cellulose: 5.5 parts of sodium carboxymethyl cellulose were added to 35 parts of deionized water to obtain a sodium carboxymethyl cellulose solution, 3.5 parts of modified keratin were added, stirred evenly, 1.2 parts of calcium silicate, 2.25 parts of polyacrylate, and 0.65 parts of potassium persulfate were added, stirred at 50° C. for 2 hours, cooled to room temperature, purified, and frozen at -50° C. for 30 hours to obtain modified keratin / sodium carboxymethyl cellulose;

[0062] Step 3: Preparation of a cream-like textured hair clay with keratin: (1) Add an aqueous emulsifier and a moisturizer to deionized water in sequence, stir at 75°C for 1.25 hours to obtain an aqueous phase for later use; (2) Melt beeswax at 75°C, add an oily emulsifier and petrolatum, stir for 1.25 hours to obtain an oil phase for later use; (3) Add the oil phase at a mass ratio of 1.2:1.75 to the aqueous phase, mix at 75°C for 35 minutes; cool to 65°C, add VP / VA copolymer, conditioner, bentonite, fragrance, and preservative in sequence, stir and mix for 1.5 hours, cool to room temperature, and sterilize to obtain a textured hair clay.

[0063] In this embodiment, the raw materials of the textured hair mud include the following ingredients: by weight percentage, 5.5% beeswax, 3% aqueous emulsifier, 3% oily emulsifier, 2% VP / VA copolymer, 3.5% conditioning agent (polydimethylsiloxane, modified keratin / sodium carboxymethyl cellulose, the mass ratio of the two is 1:2.5), 2% moisturizer, 1.5% petrolatum, 1% bentonite, 0.15% flavor, 0.2% preservative, 1.5% Chinese medicine complex, and the rest is deionized water.

[0064] Comparative Example 4: Keratin and sodium carboxymethyl cellulose were added separately, and the rest of the process remained unchanged. Specifically:

[0065] Step 1: Preparation of Chinese medicine complex: (1) 10 parts of Polygonum multiflorum, 6.5 parts of ginseng, 4 parts of Angelica sinensis, and 5 parts of Psoralea corylifolia are added to 55 parts of deionized water and soaked for 2.5 hours to obtain mixture A; (2) 7.5 parts of Platycladus orientalis leaves, 11.5 parts of black beans, and 10.5 parts of black sesame are added to 45 parts of deionized water and soaked for 1.2 hours to obtain mixture B; (3) The mass ratio of mixture A to mixture B is 2.2:1, mixture A is boiled over high heat, then boiled over medium heat for 1.5 hours, mixture B is added and boiled over low heat for 1.2 hours, filtered, and a Chinese medicine extract is obtained; (4) 15 parts of alcohol and 1.5 parts of Artemisia annua oil are mixed and stirred to dissolve uniformly, 22.5 parts of deionized water, 4 parts of Chinese medicine extract, 0.075 parts of tea polyphenols, 1.75 parts of dodecyl dimethyl tertiary amine, and 1.2 parts of polyglycerol-2 dipolyhydroxystearate are added in turn, stirred uniformly, and a Chinese medicine complex is obtained;

[0066] Step 2: Preparation of a cream-like textured hair clay with keratin: (1) Sodium carboxymethyl cellulose, an aqueous emulsifier, and a moisturizer are sequentially added to deionized water, and stirred at 75°C for 1.25 hours to obtain an aqueous phase for later use; (2) Beeswax is melted at 75°C, and an oily emulsifier and petrolatum are added, and stirred for 1.25 hours to obtain an oil phase for later use; (3) The oil phase is added to the aqueous phase at a mass ratio of 1.2:1.75, and mixed at 75°C for 35 minutes; the temperature is lowered to 65°C, and VP / VA copolymer, keratin, a conditioning agent, bentonite, a fragrance, and a preservative are sequentially added, and the mixture is stirred for 1.5 hours, cooled to room temperature, and sterilized to obtain a textured hair clay.

[0067] In this embodiment, the raw materials of the textured hair mud include the following ingredients: by weight percentage, 5.5% beeswax, 3% aqueous emulsifier, 3% oily emulsifier, 2% VP / VA copolymer, 3.5% conditioning agent (polydimethylsiloxane, modified keratin / sodium carboxymethyl cellulose, the mass ratio of the two is 1:2.5), 2% moisturizer, 0.3% sodium carboxymethyl cellulose, 1.5% petrolatum, 1% bentonite, 0.15% flavor, 0.2% preservative, 1.5% Chinese medicine compound, 0.5% keratin, and the rest is deionized water.

[0068] Testing experiment: The keratin cream-like textured hair clay prepared in Examples 1 to 3 and Comparative Examples 1 to 4 was subjected to the following performance tests: (1) Styling ability test: The sample was evenly applied to the hair and fully dried for 12 hours at room temperature. D represents poor, C represents fair, B represents good, and A represents very good; (2) Moisturizing ability test: The sample was evenly applied to the hair and fully dried for 12 hours at room temperature. D represents poor, C represents fair, B represents good, and A represents very good; (3) Antibacterial determination with reference to the patent "CN117064814A": The sample was dripped into the hair using the filter paper diffusion method and placed in a constant temperature incubator at 37°C for 24 hours to measure the antibacterial diameter.

[0069]

[0070] Table 1

[0071] Result analysis: According to the data analysis of Table 1 above, it can be seen that the present invention effectively enhances the stability, styling effect, biocompatibility, and moisturizing properties of the hair mud by adding modified keratin / carboxymethyl cellulose, and also improves the hair quality; by adding artemisia annua oil and the Chinese medicine extract in the Chinese medicine complex, the problems of hair loss, gray hair, and prevention of bacterial growth are effectively improved, making the hair healthier, black and shiny, that is, the present invention prepares a frosty textured hair mud with keratin.

[0072] Finally, it should be noted that the above description is only a preferred embodiment of the present invention and is not intended to limit the present invention. Although the present invention has been described in detail with reference to the aforementioned embodiments, those skilled in the art can still modify the technical solutions described in the aforementioned embodiments or replace some of the technical features therein by equivalents. Any modification, equivalent replacement, improvement, etc. made within the spirit and principle of the present invention shall be included in the protection scope of the present invention.

Claims

1. A creamy textured hair clay having keratin, characterized in that: The textured hair mud comprises the following raw materials, calculated by weight percentage: 3-8% beeswax, 2-4% aqueous emulsifier, 2-4% oily emulsifier, 1-3% VP / VA copolymer, 2-5% conditioner, 1-3% moisturizer, 1-2% petrolatum, 0.5-1.5% bentonite, 0.1-0.2% flavor, 0.1-0.3% preservative, and the rest is deionized water.

2. The keratin-containing cream-like textured hair clay according to claim 1, characterized in that: The aqueous emulsifier includes one or two of ceteareth-30 and ceteareth-25; the oily emulsifier includes one or two of oleth-10 and hydroxypropyl distearyl dimethyl ammonium chloride; the moisturizer includes one or more of maltitol, glycerin, and propylene glycol; the preservative includes one or more of phenoxyethanol, methylparaben, chlorphenesin, and propylparaben.

3. The keratin cream-like textured hair clay according to claim 1, characterized in that: The conditioning agent comprises polydimethylsiloxane and modified keratin / sodium carboxymethyl cellulose, and the mass ratio of the two is 0.5-1.5:1.5-3.

5.

4. The method for preparing a frosty textured hair clay having keratin according to claim 3, characterized in that: The preparation method of the modified keratin / sodium carboxymethyl cellulose: S1: Preparation of modified keratin: Keratin powder and deionized water are mixed, polylysine and glyoxal are added in sequence, heated at 50-60° C. for 3-6 hours, filtered, and frozen at -20--45° C. for 48-50 hours to obtain modified keratin; S2: Add sodium carboxymethyl cellulose to deionized water to obtain a sodium carboxymethyl cellulose solution, add modified keratin, stir evenly, add calcium silicate, polyacrylate, and potassium persulfate, stir evenly, and freeze at -20 to -80°C for 24 to 36 hours to obtain modified keratin / sodium carboxymethyl cellulose.

5. The method for preparing a frosty textured hair clay having keratin according to claim 4, characterized in that: The modified keratin comprises the following raw materials in parts by weight: 4 to 6 parts of keratin powder, 50 to 60 parts of deionized water, 2 to 4 parts of polylysine, and 2 to 3 parts of glyoxal; The modified keratin / sodium carboxymethyl cellulose comprises the following raw materials in parts by weight: 5-6 parts of sodium carboxymethyl cellulose, 30-40 parts of deionized water, 3-4 parts of modified keratin, 1-1.5 parts of calcium silicate, 2-2.5 parts of polyacrylate, and 0.5-0.8 parts of potassium persulfate.

6. The method for preparing a frosty textured hair clay having keratin according to claim 1, characterized in that: The textured hair mud also includes 1-2% of a traditional Chinese medicine compound.

7. The method for preparing a frosty textured hair clay having keratin according to claim 6, characterized in that: The preparation method of the traditional Chinese medicine complex is as follows: S1: Preparation of Chinese medicine extract: sequentially add Polygonum multiflorum, ginseng, Chinese angelica, and Psoralea corylifolia to deionized water and soak for 2 to 3 hours to obtain mixture A; sequentially add Platycladus orientalis leaves, black beans, and black sesame to deionized water and soak for 1 to 1.5 hours to obtain mixture B; boil mixture A over high heat, then boil over medium heat for 1 to 2 hours, add mixture B and boil over low heat for 1 to 1.5 hours, filter, and obtain Chinese medicine extract; S2: Preparation of Chinese medicine complex: Dissolve alcohol and artemisia annua oil uniformly by mixing and stirring, and then uniformly mix deionized water, Chinese medicine extract, tea polyphenols, dodecyl dimethyl tertiary amine, and polyglycerol-2 dipolyhydroxystearate to obtain the Chinese medicine complex.

8. The method for preparing a frosty textured hair clay having keratin according to claim 7, characterized in that: The mass ratio of mixture A to mixture B in the traditional Chinese medicine extract is (2-2.5):1; The mixture A comprises the following components: by weight: 8 to 13 parts of Polygonum multiflorum, 5 to 8 parts of Ginseng, 3 to 5 parts of Angelica sinensis, 4 to 6 parts of Psoralea corylifolia, and 50 to 60 parts of deionized water; The mixture B comprises the following components: by mass: 10 to 13 parts of black beans, 8 to 13 parts of black sesame seeds, 6 to 9 parts of Platycladus orientalis leaves, and 40 to 50 parts of deionized water; The raw materials of the traditional Chinese medicine complex include the following components: by weight, 10 to 20 parts of alcohol, 1 to 2 parts of artemisia oil, 15 to 30 parts of deionized water, 3 to 5 parts of traditional Chinese medicine extract, 0.05 to 0.1 parts of tea polyphenols, 1.5 to 2 parts of dodecyl dimethyl tertiary amine, and 1 to 1.5 parts of polyglycerol-2 dipolyhydroxystearate.

9. The method for preparing a frosty textured hair clay having keratin according to claim 6, characterized in that: A method for preparing a creamy textured hair clay having keratin comprises the following steps: S1: (1) adding an aqueous emulsifier and a moisturizer to deionized water in sequence, stirring at 70 to 80° C. for 1 to 1.5 hours to obtain an aqueous phase for later use; (2) melting beeswax at 70 to 80° C., adding an oily emulsifier and petrolatum, stirring for 1 to 1.5 hours to obtain an oil phase for later use; S2: Add the oil phase to the water phase, mix at 70-80°C for 30-40 minutes; cool to 60-70°C, add VP / VA copolymer, conditioner, bentonite, flavor, preservative in sequence, stir and mix for 1-2 hours, cool to room temperature, sterilize, and obtain textured mud.

10. The frosty textured hair clay with keratin prepared according to the method for preparing a frosty textured hair clay with keratin according to any one of claims 1 to 9.

Images