Aromatherapy cup wax and preparation method thereof

By using raw materials such as plant wax, stabilizers, flavors, emulsifiers and paraffin, combined with high shear homogeneous emulsification technology, a stable emulsified wax gel is formed, which solves the problems of high-temperature oil output, low-temperature cracking, unstable combustion and imperfect fragrance of aromatherapy cup wax, and candle preparation with reduced costs and structural homogeneity.

CN119529944APending Publication Date: 2025-02-28QINGDAO KINGKING APPL CHEM CO LTD
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Patent Information

Application Number
CN202411857444.7
Authority / Receiving Office
CN · China
Patent Type
Applications(China)
Current Assignee / Owner
Filing Date
2024-12-16
Publication Date
2025-02-28

AI Technical Summary

Technical Problem

The existing aromatherapy cup wax has problems such as oil output at high temperatures, cracking at low temperatures, unstable combustion and imperfect fragrance. The traditional filling method has caused the candle to be costly and uneven structure, affecting the fragrance volatility and thermal stability.

Method used

The raw materials such as plant wax, stabilizers, flavors, emulsifiers and paraffin are used to process them through a high-shear homogenized emulsifier to form a stable emulsified wax gel, control the temperature of the wax liquid to maintain the crystalline state, disperse into microcrystalline particles, and emulsify and stabilize with non-ionic surfactants.

Benefits of technology

It solves the problem that aromatherapy cup wax is not prone to oil when stored at high temperature, does not crack at low temperatures, has stable combustion and thorough fragrance, reduces costs and avoids the cooling and shrinkage of traditional candles and internal hollowing problems.

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Abstract

The invention discloses aromatherapy cup wax and a preparation method thereof. The aromatherapy cup wax consists of the following raw materials in parts by weight: 75-90 parts of vegetable wax, 0.1-5 parts of a stabilizer, 1-15 parts of essence and 0.5-10 parts of an emulsifier or 20-90 parts of vegetable wax, 0.1-5 parts of a stabilizer, 1-15 parts of essence, 0.5-10 parts of an emulsifier, 5-75 parts of paraffin and 1-10 parts of soft wax. The preparation method comprises the following steps: melting vegetable wax and mixing with a stabilizer or mixing with paraffin, soft wax and the stabilizer to obtain a mixed solution A, adding an emulsifier into the mixed solution A, stirring and melting to obtain a mixed solution B, adding essence, fully stirring to obtain a wax solution, adding the wax solution into a high-speed stirring and high-shear reactor, stirring at a high speed, and exhausting in vacuum to obtain the aromatherapy cup wax. And filling into a cup to obtain the cup wax. The formula of the aromatherapy cup wax is adjusted, the emulsifier is added, and the wax which begins to crystallize and separate out is dispersed into microcrystal particles in a high-speed stirring and high-shear mode, so that low-melting-point components are not easy to separate out in the high-temperature storage process of the aromatherapy candle, and the problem of cracking is avoided when the aromatherapy candle is stored at low temperature.
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Description

Technical Field

[0001] The invention relates to the technical field of daily chemical products, and in particular to an aromatherapy cup wax and a preparation method thereof. Background Art

[0002] As a product that can create different styles of atmosphere, more and more consumers are beginning to use scented candles as daily consumer goods to improve their quality of life. Therefore, the market has put forward higher and higher performance requirements for scented cup candles. In particular, the requirements for its fragrance are constantly increasing. This requires that a higher and higher proportion of fragrances be added to scented cup candles. However, with the increase in the proportion of fragrances in cup candles, cup candle products on the market often have serious problems such as high-temperature oiling and whitening after oiling. If the general solution is used to increase the proportion of high-melting-point wax in the formula, although the oiling problem can be solved, there are contradictory problems such as low-temperature cracking, poor appearance, and poor combustion.

[0003] At present, most of the cup waxes on the market are directly filled after mixing and melting the raw materials (paraffin wax, plant wax, etc.). The cup wax filled in this way is called solid wax; this kind of wax is generally solid and dense, and the consumables increase, so the cost increases. In addition, due to the large cooling shrinkage during the production process, there are often many non-homogeneous structures such as depressions and tunnels inside. This structure will have an adverse effect on the aroma volatilization and thermal stability of the wax column, such as: unstable flames, incomplete aroma volatilization, and oily appearance during the combustion process.

[0004] Patent CN110591826B discloses a foaming cup wax and its production method, and discloses that the specific ingredients of the foaming cup wax are 10-20 parts of soybean wax; 25-30 parts of palm wax; 5-10 parts of soft wax; 30-40 parts of paraffin wax; 1-5 parts of essence; and specifically discloses that the production method is: the raw materials are melted, mixed, and air is introduced, and foamed in a foaming machine by high shear dispersion to obtain the final product. Although the foaming wax obtained by the above patent can solve the problems of uneven bubbles and improve the appearance, the candles obtained by this foaming wax process have a significantly lower density than ordinary candles, and collapse when burning, which will affect the burning stability of the candles. At the same time, with the increase in the proportion of essence, the problem of oil release when the foaming wax obtained by this process is stored at high temperatures will become more and more serious. Summary of the invention

[0005] Purpose of the invention: The purpose of the present invention is to overcome the deficiencies of the above-mentioned prior art and to provide a scented cup wax and a preparation method thereof.

[0006] To achieve the above purpose, the technical solution provided by the present invention is as follows:

[0007] The invention discloses an aromatherapy cup wax, which is composed of the following raw materials in parts by weight: 75-90 parts of plant wax, 0.1-5 parts of stabilizer, 1-15 parts of essence, 0.5-10 parts of emulsifier, and preferably 1-3 parts of emulsifier; wherein the emulsifier is a nonionic surfactant, and the nonionic surfactant is glycerol fatty acid ester, polyglycerol fatty acid ester, octadecyl alcohol, polyoxyethylene stearate or polyoxyethylene palmitate; and the stabilizer is 2-(2-hydroxy-5-benzyl)benzotriazole.

[0008] The invention discloses an aromatherapy cup wax, which is composed of the following raw materials in parts by weight: 20-90 parts of plant wax, 0.1-5 parts of stabilizer, 1-15 parts of essence, 0.5-10 parts of emulsifier, preferably 1-3 parts of emulsifier, 5-75 parts of paraffin wax, and 1-10 parts of soft wax; wherein the emulsifier is a nonionic surfactant, which is glycerol fatty acid ester, polyglycerol fatty acid ester, octadecyl alcohol, polyoxyethylene stearate or polyoxyethylene palmitate; and the stabilizer is 2-(2-hydroxy-5-benzyl)benzotriazole.

[0009] The vegetable wax is soybean wax, palm wax, beeswax, coconut wax, rice bran wax, rapeseed wax or shea wax.

[0010] A method for preparing an aromatherapy cup wax comprises the following steps:

[0011] Step 1: Melt the vegetable wax at T1 to obtain a vegetable wax liquid, add a stabilizer and mix at temperature T2 to obtain a mixed liquid A;

[0012] Step 2: Add emulsifier to mixed solution A at temperature T3 and stir until completely melted to obtain mixed solution B;

[0013] Step 3: Add essence to the mixed liquid B at temperature T4 and stir thoroughly to obtain wax liquid;

[0014] Step 4: the wax liquid is added into a high-speed stirring high-shear reactor at temperature T5, the system temperature is controlled between 30 and 60°C, preferably between 30 and 50°C, high-speed stirring is performed, vacuum exhaust is performed, the stirring speed is 500 to 20,000 rpm, and the stirring time is 2 to 30 min;

[0015] Step 5: Fill the wax liquid into the cup to obtain cup wax.

[0016] A method for preparing an aromatherapy cup wax comprises the following steps:

[0017] Step 1: paraffin wax, soft wax and stabilizer are mixed and melted at temperature T6 to obtain paraffin liquid;

[0018] Step 2: The plant wax is melted at temperature T1 to obtain plant wax liquid;

[0019] Step 3: mixing the paraffin liquid in step 1 and the plant wax liquid in step 2 at temperature T2 to obtain a mixed liquid A;

[0020] Step 4: Add emulsifier to mixed solution A at temperature T3 and stir until completely melted to obtain mixed solution B;

[0021] Step 5: Add essence to the mixed liquid B at temperature T4 and stir thoroughly to obtain wax liquid;

[0022] Step 6: Add the wax liquid into a high-speed stirring high-shear reactor at temperature T5, control the system temperature between 30 and 60° C., preferably between 30 and 50° C., perform high-speed stirring, vacuum exhaust, stirring speed of 500 to 20,000 rpm, and stirring time of 2 to 30 min;

[0023] Step 7: Fill the wax liquid into the cup to get cup wax.

[0024] The temperature range of T1 is 60-80°C, and the temperature range of T2 is 70-85°C.

[0025] The temperature range of T3 is 70-85°C, and the temperature range of T4 is 70-85°C.

[0026] The T5 temperature range is 60-75°C.

[0027] The T6 temperature range is 85-100°C.

[0028] The high-speed stirring high-shear reactor is a high-shear homogenizing emulsifier or a high-shear homogenizing emulsifying pump / mixing pump.

[0029] Beneficial effects: The present invention discloses an aromatherapy cup wax and a preparation method thereof. The aromatherapy cup wax is composed of the following raw materials in parts by weight: 75-90 parts of plant wax, 0.1-5 parts of stabilizer, 1-15 parts of essence, 0.5-10 parts of emulsifier or 20-90 parts of plant wax, 0.1-5 parts of stabilizer, 1-15 parts of essence, 0.5-10 parts of emulsifier, 5-75 parts of paraffin wax, and 1-10 parts of soft wax; and discloses a preparation method of the aromatherapy cup wax, wherein the plant wax is melted and mixed with the stabilizer or mixed with paraffin wax, soft wax, and stabilizer to obtain a mixed liquid A, an emulsifier is added to the mixed liquid A, and the mixed liquid B is melted by stirring to obtain a mixed liquid B, and the essence is added and stirred to obtain a wax liquid, and the wax liquid is added to a high-speed stirring and high-shear reactor, stirred at a high speed, and vacuum-exhausted, and filled into a cup to obtain the cup wax. In the process of gradually cooling the wax liquid, the present invention controls the temperature of the wax liquid to keep it in a state of slowly forming crystals, disperses the wax that begins to crystallize into microcrystalline particles by high-speed stirring and high shearing, and uses a non-ionic surfactant as an emulsifier to stabilize the formed wax microcrystalline particles. The emulsifier has the functions of dispersing and stabilizing the gel microcrystalline particles and solubilizing the solvent with higher polarity in the essence, so the scented candle prepared by the present invention is not easy to oil out during high-temperature storage, and avoids cracking at low temperatures. Since the candle is filled at a relatively low temperature when it has already crystallized, the wax body does not shrink significantly and internal cavities are not generated after filling, thereby avoiding the problems of combustion collapse and self-extinguishing caused by adding wax when ordinary filled candles are not cooled enough. DETAILED DESCRIPTION

[0030] The present invention is further illustrated below in conjunction with specific embodiments. The embodiments are implemented based on the technical solutions of the present invention. It should be understood that these embodiments are only used to illustrate the present invention and are not used to limit the scope of the present invention.

[0031] Example 1

[0032] A scented cup wax consists of 30 parts of vegetable wax, 0.2 parts of a stabilizer, 8 parts of essence, 2 parts of an emulsifier, 58.8 parts of paraffin wax and 1 part of soft wax; the vegetable wax is soybean wax, palm wax, beeswax, coconut wax, rice bran wax, rapeseed wax or shea wax; the stabilizer is 2-(2-hydroxy-5-benzyl)benzotriazole; and the emulsifier is glycerol fatty acid ester.

[0033] The preparation method of the aromatherapy cup wax comprises the following steps:

[0034] Step 1: Melt paraffin, soft wax and stabilizer at 85-100℃ to obtain paraffin liquid

[0035] Step 2: Melt the plant wax at 60-80°C to obtain plant wax liquid

[0036] Step 3: Mix the paraffin liquid obtained in step 1 and the plant wax liquid obtained in step 2 at 70-85°C to obtain a mixed solution A.

[0037] Step 4: Take the mixed solution A obtained in step 3, add the emulsifier at 70-85°C, and stir until completely melted to obtain mixed solution B

[0038] Step 5: Take the mixed solution B obtained in step 4 and add the essence at 70-85°C and stir thoroughly

[0039] Step 6: Take the wax liquid obtained in step 5 and add it to a high-shear homogenizer at 60-75°C, control the system temperature between 30-50°C, and then stir it at a high speed, with a stirring speed of 2000-10000 rpm and a stirring time of 2-30min to obtain a homogenous wax liquid. During this stirring process, the stirring speed and temperature need to be controlled to avoid obvious bubbles from mixing in the wax gel system. To avoid the generation of bubbles, the reactor can exhaust the air in the system by providing negative pressure through vacuuming.

[0040] Step 7: After the wax liquid dispersed by the high-shear homogenizer forms a stable emulsified wax gel, the wax liquid is filled into a cup to obtain a cup wax.

[0041] Example 2

[0042] A scented cup wax is composed of 89.8 parts of plant wax, 0.2 parts of a stabilizer, 8 parts of essence and 2 parts of an emulsifier; the plant wax is soybean wax, palm wax, beeswax, coconut wax, rice bran wax, rapeseed wax or shea wax; the stabilizer is 2-(2-hydroxy-5-benzyl)benzotriazole; and the emulsifier is polyglycerol fatty acid ester.

[0043] The preparation method of the aromatherapy cup wax comprises the following steps:

[0044] Step 1: Melting the vegetable wax at 60-80° C. to obtain a vegetable wax liquid, adding a stabilizer and mixing at 70-85° C. to obtain a mixed liquid A;

[0045] Step 2: Add emulsifier to mixed solution A at 70-85°C and stir until completely melted to obtain mixed solution B;

[0046] Step 3: Add essence to the mixed solution B at 70-85°C and stir thoroughly to obtain wax liquid;

[0047] Step 4: Add the wax liquid to a high shear homogenizing emulsifier pump at 60-75°C, control the system temperature between 30-50°C, and then stir at high speed at 2000-10000 rpm, and control the stirring time at 2-30 min to obtain a homogenous wax liquid. During this stirring process, the stirring speed and temperature need to be controlled to avoid obvious bubbles being mixed in the wax gel system. To avoid the generation of bubbles, the reactor can exhaust the air in the system by providing negative pressure through vacuum pumping;

[0048] Step 5: After the wax liquid dispersed by the high shear homogenizing emulsifier pump forms a stable emulsified wax gel, the wax liquid is filled into the cup to obtain the cup wax.

[0049] Example 3

[0050] A scented cup wax consists of 20 parts of vegetable wax, 5 parts of a stabilizer, 1 part of essence, 1 part of an emulsifier, 63 parts of paraffin wax and 10 parts of soft wax; the vegetable wax is soybean wax, palm wax, beeswax, coconut wax, rice bran wax, rapeseed wax or shea wax; the stabilizer is 2-(2-hydroxy-5-benzyl)benzotriazole; and the emulsifier is octadecyl alcohol.

[0051] The preparation method of the aromatherapy cup wax comprises the following steps:

[0052] Step 1: Melt paraffin, soft wax and stabilizer at 85-100℃ to obtain paraffin liquid

[0053] Step 2: Melt the plant wax at 60-80°C to obtain plant wax liquid

[0054] Step 3: Mix the paraffin liquid obtained in step 1 and the plant wax liquid obtained in step 2 at 70-85°C to obtain a mixed solution A.

[0055] Step 4: Take the mixed solution A obtained in step 3, add the emulsifier at 70-85°C, and stir until completely melted to obtain mixed solution B

[0056] Step 5: Take the mixed solution B obtained in step 4 and add the essence at 70-85°C and stir thoroughly

[0057] Step 6: Take the wax liquid obtained in step 5 and add it to a high-shear homogenizer at 60-75°C, control the system temperature between 30-50°C, and then stir it at a high speed, with a stirring speed of 2000-10000 rpm and a stirring time of 2-30min to obtain a homogenous wax liquid. During this stirring process, the stirring speed and temperature need to be controlled to avoid obvious bubbles from mixing in the wax gel system. To avoid the generation of bubbles, the reactor can exhaust the air in the system by providing negative pressure through vacuuming.

[0058] Step 7: After the wax liquid dispersed by the high-shear homogenizer forms a stable emulsified wax gel, the wax liquid is filled into a cup to obtain a cup wax.

[0059] Example 4

[0060] A scented cup wax consists of 20 parts of vegetable wax, 0.1 parts of a stabilizer, 15 parts of essence, 3 parts of an emulsifier, 51.9 parts of paraffin wax and 10 parts of soft wax; the vegetable wax is soybean wax, palm wax, beeswax, coconut wax, rice bran wax, rapeseed wax or shea wax; the stabilizer is 2-(2-hydroxy-5-benzyl)benzotriazole; and the emulsifier is polyoxyethylene stearate.

[0061] The preparation method of the aromatherapy cup wax comprises the following steps:

[0062] Step 1: Melt paraffin, soft wax and stabilizer at 85-100℃ to obtain paraffin liquid

[0063] Step 2: Melt the plant wax at 60-80°C to obtain plant wax liquid

[0064] Step 3: Mix the paraffin liquid obtained in step 1 and the plant wax liquid obtained in step 2 at 70-85°C to obtain a mixed solution A.

[0065] Step 4: Take the mixed solution A obtained in step 3, add the emulsifier at 70-85°C, and stir until completely melted to obtain mixed solution B

[0066] Step 5: Take the mixed solution B obtained in step 4 and add the essence at 70-85°C and stir thoroughly

[0067] Step 6: Take the wax liquid obtained in step 5 and add it to a high-shear homogenizer at 60-75°C, control the system temperature between 30-50°C, and then stir it at a high speed, with a stirring speed of 2000-10000 rpm and a stirring time of 2-30min to obtain a homogenous wax liquid. During this stirring process, the stirring speed and temperature need to be controlled to avoid obvious bubbles from mixing in the wax gel system. To avoid the generation of bubbles, the reactor can exhaust the air in the system by providing negative pressure through vacuuming.

[0068] Step 7: After the wax liquid dispersed by the high-shear homogenizer forms a stable emulsified wax gel, the wax liquid is filled into a cup to obtain a cup wax.

[0069] Example 5

[0070] A scented cup wax consists of 20 parts of vegetable wax, 1 part of stabilizer, 1 part of essence, 1 part of emulsifier, 75 parts of paraffin wax and 2 parts of soft wax; the vegetable wax is soybean wax, palm wax, beeswax, coconut wax, rice bran wax, rapeseed wax or shea wax; the stabilizer is 2-(2-hydroxy-5-benzyl)benzotriazole; and the emulsifier is polyoxyethylene palmitate.

[0071] The preparation method of the aromatherapy cup wax comprises the following steps:

[0072] Step 1: Melt paraffin, soft wax and stabilizer at 85-100℃ to obtain paraffin liquid

[0073] Step 2: Melt the plant wax at 60-80°C to obtain plant wax liquid

[0074] Step 3: Mix the paraffin liquid obtained in step 1 and the plant wax liquid obtained in step 2 at 70-85°C to obtain a mixed solution A.

[0075] Step 4: Take the mixed solution A obtained in step 3, add the emulsifier at 70-85°C, and stir until completely melted to obtain mixed solution B

[0076] Step 5: Take the mixed solution B obtained in step 4 and add the essence at 70-85°C and stir thoroughly

[0077] Step 6: Take the wax liquid obtained in step 5 and add it to a high-shear homogenizer at 60-75°C, control the system temperature between 30-50°C, and then stir it at a high speed, with a stirring speed of 2000-10000 rpm and a stirring time of 2-30min to obtain a homogenous wax liquid. During this stirring process, the stirring speed and temperature need to be controlled to avoid obvious bubbles from mixing in the wax gel system. To avoid the generation of bubbles, the reactor can exhaust the air in the system by providing negative pressure through vacuuming.

[0078] Step 7: After the wax liquid dispersed by the high-shear homogenizer forms a stable emulsified wax gel, the wax liquid is filled into a cup to obtain a cup wax.

[0079] Comparative Example 6

[0080] A scented cup wax consists of 30 parts of vegetable wax, 0.2 parts of a stabilizer, 8 parts of essence, 1 part of soft wax and the remainder of paraffin wax; the vegetable wax is soybean wax, palm wax, beeswax, coconut wax, rice bran wax, rapeseed wax or shea wax, and the stabilizer is 2-(2-hydroxy-5-benzyl)benzotriazole.

[0081] The preparation method of the aromatherapy cup wax comprises the following steps:

[0082] Step 1: melt paraffin wax, soft wax and stabilizer at 85-100°C to obtain paraffin liquid;

[0083] Step 2: Melt the plant wax at 60-80° C. to obtain a plant wax liquid;

[0084] Step 3: Mix the paraffin liquid obtained in step 1 and the plant wax liquid obtained in step 2 at 70-85° C. to obtain a mixed solution A;

[0085] Step 4: Take the mixed solution A obtained in step 3, add essence at 70-85°C, stir until completely melted, and obtain mixed solution B. Fill the wax liquid into the cup normally to obtain cup wax.

[0086] Comparative Example 7

[0087] A scented cup wax is composed of 91.8 parts of plant wax, 0.2 parts of a stabilizer and 8 parts of essence; the plant wax is soybean wax, palm wax, beeswax, coconut wax, rice bran wax, rapeseed wax or shea wax, and the stabilizer is 2-(2-hydroxy-5-benzyl)benzotriazole.

[0088] The preparation method of the aromatherapy cup wax comprises the following steps:

[0089] Step 1: Take a stabilizer;

[0090] Step 2: Melt the plant wax at 60-80° C. to obtain a plant wax liquid;

[0091] Step 3: Mix the stabilizer obtained in step 1 and the plant wax liquid obtained in step 2 at 70-85° C. to obtain a mixed solution A;

[0092] Step 4: Take the mixed solution A obtained in step 3, add essence at 70-85°C, stir until completely melted, and obtain mixed solution B. Fill the wax liquid into the cup normally to obtain cup wax.

[0093] Comparative Example 8

[0094] A scented cup wax is composed of 30 parts of vegetable wax, 8 parts of essence, 1 part of soft wax and the rest of paraffin wax; the vegetable wax is soybean wax, palm wax, beeswax, coconut wax, rice bran wax, rapeseed wax or shea wax.

[0095] The preparation method of the aromatherapy cup wax comprises the following steps:

[0096] Step 1: Take paraffin wax and melt the soft wax at 85-100°C to obtain paraffin liquid;

[0097] Step 2: Melt the plant wax at 60-80° C. to obtain a plant wax liquid;

[0098] Step 3: Mix the paraffin liquid obtained in step 1 and the plant wax liquid obtained in step 2 at 70-85° C. to obtain a mixed solution A;

[0099] Step 4: Take the mixed solution A obtained in step 3, add essence at 70-85°C, stir until completely melted, and obtain mixed solution B. Fill the wax liquid into the cup normally to obtain cup wax.

[0100] The aromatherapy cup wax prepared in Examples 1 to 5 and Comparative Examples 6 to 8 were used for performance testing, and the results are shown in Table 1 below:

[0101] Table 1 Performance test of Examples 1 to 5 and Comparative Examples 6 to 8

[0102]

[0103] As can be seen from Table 1, in the candles of Examples 1 to 5, nonionic surfactants are used as emulsifiers to stabilize the wax crystal microparticles formed, thereby maintaining uniform and tiny microcrystalline particles, so that the surface of the wax body shows a delicate and silky texture and touch, providing users with a better use experience, and the wax that begins to crystallize and precipitate is dispersed into microcrystalline particles by high-speed stirring and high-shearing. At the same time, the emulsifier has the functions of dispersing and stabilizing the gel microcrystalline particles and solubilizing the solvent with higher polarity in the flavor. Compared with Comparative Examples 6 to 8, the candles prepared in Examples 1 to 5 are not easy to oil out in a high temperature environment and do not crack at a low temperature. Since the temperature in the can is lower than that in the normal can, there is no obvious shrinkage and internal voids after canning, thereby avoiding the problems of burning collapse, poor fragrance effect and self-extinguishing of ordinary canned candles.

[0104] The above specific implementation methods further describe the purpose, technical solutions and beneficial effects of the present application in detail. It should be understood that the above are only specific implementation methods of the present application and are not used to limit the protection scope of the present application. Any modifications, equivalent substitutions, improvements, etc. made on the basis of the technical solutions of the present application should be included in the protection scope of the present application.

Claims

1. A scented cup wax, characterized in that: The aromatherapy cup wax is composed of the following raw materials in parts by weight: 75-90 parts of plant wax, 0.1-5 parts of stabilizer, 1-15 parts of essence, and 0.5-10 parts of emulsifier; wherein the emulsifier is a nonionic surfactant, the nonionic surfactant is glycerol fatty acid ester or polyglycerol fatty acid ester, and the stabilizer is 2-(2-hydroxy-5-benzyl)benzotriazole.

2. A scented cup candle, characterized in that: The aromatherapy cup wax is composed of the following raw materials in parts by weight: 20 to 90 parts of plant wax, 0.1 to 5 parts of stabilizer, 1 to 15 parts of essence, 0.5 to 10 parts of emulsifier, 5 to 75 parts of paraffin wax, and 1 to 10 parts of soft wax; wherein the emulsifier is a nonionic surfactant, and the nonionic surfactant is glycerol fatty acid ester, polyglycerol fatty acid ester, octadecyl alcohol, polyoxyethylene stearate or polyoxyethylene palmitate; and the stabilizer is 2-(2-hydroxy-5-benzyl)benzotriazole.

3. The aromatherapy cup wax according to claim 1 or 2, characterized in that: The vegetable wax is soybean wax, palm wax, beeswax, coconut wax, rice bran wax, rapeseed wax or shea wax.

4. A method for preparing the aromatherapy cup wax according to claim 1, characterized in that: The following steps are involved: Step 1: Melt the vegetable wax at T1 to obtain a vegetable wax liquid, add a stabilizer and mix at temperature T2 to obtain a mixed liquid A; Step 2: Add emulsifier to mixed solution A at temperature T3 and stir until completely melted to obtain mixed solution B; Step 3: Add essence to the mixed liquid B at temperature T4 and stir thoroughly to obtain wax liquid; Step 4: the wax liquid is added into a high-speed stirring high-shear reactor at a temperature of T5, the system temperature is controlled between 30 and 60°C, high-speed stirring is performed, vacuum exhaust is performed, the stirring speed is 500 to 20,000 rpm, and the stirring time is 2 to 30 min; Step 5: Fill the wax liquid into the cup to obtain cup wax.

5. A method for preparing the aromatherapy cup wax according to claim 2, characterized in that: The following steps are involved: Step 1: paraffin wax, soft wax and stabilizer are mixed and melted at temperature T6 to obtain paraffin liquid; Step 2: The plant wax is melted at temperature T1 to obtain plant wax liquid; Step 3: mixing the paraffin liquid in step 1 and the plant wax liquid in step 2 at temperature T2 to obtain a mixed liquid A; Step 4: Add emulsifier to mixed solution A at temperature T3 and stir until completely melted to obtain mixed solution B; Step 5: Add essence to the mixed liquid B at temperature T4 and stir thoroughly to obtain wax liquid; Step 6: Add the wax liquid into a high-speed stirring high-shear reactor at temperature T5, control the system temperature between 30 and 60° C., perform high-speed stirring, vacuum exhaust, stirring speed of 500 to 20,000 rpm, and stirring time of 2 to 30 min; Step 7: Fill the wax liquid into the cup to get cup wax.

6. The preparation method according to claim 4 or 5, characterized in that: The temperature range of T1 is 60-80°C, and the temperature range of T2 is 70-85°C.

7. The preparation method according to claim 4 or 5, characterized in that: The temperature range of T3 is 70-85°C, and the temperature range of T4 is 70-85°C.

8. The preparation method according to claim 4 or 5, characterized in that: The T5 temperature range is 60-75°C.

9. The preparation method according to claim 5, characterized in that: The T6 temperature range is 85-100°C.

10. The preparation method according to claim 4 or 5, characterized in that: The high-speed stirring high-shear reactor is a high-shear homogenizing emulsifier or a high-shear homogenizing emulsifying pump / mixing pump.

Citation Information

Patent Citations

  • A foaming cup wax and its production method

    CN110591826B