Tar and ammonia water separation device and separation method thereof

Abstract

The tar and ammonia water separation device comprises a working shell, a plurality of supporting legs are fixedly connected to the periphery of the outer wall of the bottom end of the working shell, one side of the bottom end of the working shell communicates with an oil discharging pipe, and a feeding shell is fixedly connected to the top of the working shell. The rotating separation assembly comprises a motor fixedly connected to the bottom of the working shell, the output end of the motor is fixedly connected with a rotating shaft, one end of the rotating shaft penetrates through the feeding shell and extends into the feeding shell, a specific solvent is poured into a conical filter sleeve plate, then a mixture is discharged into the feeding shell, and the specific solvent is separated from the feeding shell. The conical filter sleeve plate filters impurities in the mixture, the motor is started, the rotating motor drives the rotating shaft to rotate, and the rotating shaft drives the special-shaped stirring blades to rotate, so that the mixture is mixed with the specific solvent, ammonia water in the mixture reacts with the specific solvent, and ammonia salt precipitates are generated.

Description

Technical Field

[0001] The present invention relates to the technical field of chemical equipment, and specifically relates to a tar-ammonia water separation device and a separation method thereof. Background Art

[0002] With the development of the coking production process, coking plants have increasingly paid attention to the separation of tar-ammonia water. Existing devices usually mix the mixture with a specific solvent. Organic solvents such as methanol or ethyl acetate can be used in the specific solvent to react with the ammonia water in the mixture to produce ammonium salt precipitation, and then filter it out to obtain pure tar.

[0003] However, during the separation of tar-ammonia water by existing devices, since impurities such as tar slag are generated after the mixture is mixed with the solvent, these impurities will block the filter holes of the filter screen, thereby reducing the flow efficiency of the mixture and affecting the reaction efficiency between the mixture and the solvent. Summary of the Invention

[0004] The purpose of the present invention is to provide a tar-ammonia water separation device and a separation method thereof to solve the problems raised in the above background art.

[0005] To solve the above technical problems, the present invention is realized through the following technical solutions:

[0006] The present invention is a tar-ammonia water separation device and a separation method thereof, including a working shell. A plurality of support feet are respectively fixedly connected to the outer periphery of the bottom end of the working shell. A drain pipe is communicated with one side of the bottom end of the working shell. A feeding shell is fixedly connected to the top of the working shell. The tar-ammonia water separation device further includes:

[0007] A rotating separation component, which includes a motor fixedly connected to the bottom of the working shell. The output end of the motor is fixedly connected to a rotating shaft. One end of the rotating shaft penetrates through the feeding shell and extends into the interior of the feeding shell. A plurality of oil holes are respectively opened in the outer periphery of the bottom end of the feeding shell. A conical filter sleeve plate is fixedly connected to the bottom of the feeding shell. A stirring component is arranged on the outer wall of the rotating shaft.

[0008] Further, the stirring component includes a plurality of special-shaped stirring blades fixedly connected to the outer periphery of the top end of the rotating shaft. Square shells are respectively fixedly connected to both sides of the special-shaped stirring blades. A square block is sleeved and slidably connected to the inner wall of the square shell. A power spring is fixedly connected to one side of the square block. One end of the power spring is fixedly connected to one side of the inner wall of the square shell.

[0009] Further, a rubber rod is fixedly connected to the side of the square block away from the power spring. A trachea is communicated with one end of the square shell. The end of the trachea away from the square shell is fixedly connected to a sleeve piece. The outer wall of the sleeve piece is sleeved and rotatably connected to a heating box. The bottom of the heating box is fixedly connected to the inner wall bottom of the feeding shell. A heating plate is fixedly connected to the inner wall bottom of the heating box.

[0010] Furthermore, a heating assembly is provided on the top of the heating plate, and the heating assembly includes several first return springs fixedly connected around the top of the heating plate, the top of the first return spring is fixedly connected to a lifting plate, the outer wall of the lifting plate is sleeved and slidably connected to a square box, the bottom of the square box is connected to the top of the second return spring, and rotating plates are rotatably connected to both sides of the top of the lifting plate, and a slider is rotatably connected to the end of the rotating plate away from the lifting plate, and a cross bar is sleeved and slidably connected to the inner wall of the slider.

[0011] Furthermore, both ends of the cross bar are fixedly connected to the inner cavity of the square box, a second return spring is fixedly connected between the two sliders, a rubber block is fixedly connected to the side of the slider away from the second return spring, and first arc springs are fixedly connected to both sides of the inner wall of the square box respectively. One end of the first arc spring is fixedly connected to a square plate stirring blade, and the middle end of the square plate stirring blade passes through and is rotatably connected to the inner wall of the square box.

[0012] Furthermore, a lifting assembly is provided on the top of the heating box, and the lifting assembly includes several vertical tubes connected to the four sides of the heating box near the top of the square box. The inner wall of the vertical tube is sleeved and slidably connected with a lifting block, the top of the lifting block is fixedly connected with a vertical rod, and the outer wall of the top end of the vertical rod is sleeved and fixedly connected with a clamping block.

[0013] Furthermore, a pull rope is fixedly connected to one side of the bottom of the block, and a telescopic sleeve is fixedly connected to the end of the pull rope away from the block. A buoyancy ring is fixedly connected to the top of the telescopic sleeve. The outer wall of the buoyancy ring is sleeved and slidably connected to the inner wall of the feed shell, and several bent rods are fixedly connected around the inner wall of the buoyancy ring.

[0014] Furthermore, a cleaning assembly is provided at one end of the bent rod, and the cleaning assembly includes a buoyancy arc sleeve fixedly connected to the end of the bent rod away from the buoyancy ring, and slides are respectively provided at both ends of the inner wall of the buoyancy arc sleeve and slidably connected, and a second arc spring is fixedly connected between the two slides, and the second arc spring is provided inside the buoyancy arc sleeve, and the side of the slide away from the second arc spring is fixedly connected to the arc rod.

[0015] Furthermore, the bottom of the buoyancy arc sleeve is connected to an inclined tube, the bottom of the inclined tube is connected to an arc shell, the inner wall of the arc shell is sleeved and slidably connected with an arc cleaning block, one side of the arc cleaning block is fixedly connected to a plurality of extrusion springs, one end of the extrusion spring is fixedly connected to one side of the inner wall of the arc shell, the side of the arc cleaning block away from the extrusion spring is fixedly connected to a plurality of rubber semicircular blocks, and one side of the outer wall of the clamping block is fixedly connected to one end of the vertical rod.

[0016] A tar-ammonia water separation device and a separation method thereof, the tar-ammonia water separation method comprising the following steps:

[0017] Step 1: Pour a specific solvent into the conical filter sleeve plate, and then discharge the mixture into the feeding shell. The conical filter sleeve plate filters impurities in the mixture. Start the motor, the rotating motor drives the rotating shaft to rotate, the rotating shaft drives the special-shaped stirring blade to rotate, and the special-shaped stirring blade drives the square shell to rotate. The centrifugal force generated during the rotation of the square shell causes the square block to move outward from the square shell. The square block drives the rubber rod to move, and the heating plate heats the mixture on the top of the heating box.

[0018] Step 2: During the process of the rubber rod knocking on the conical filter sleeve plate, the square block stretches the power spring. Under the action of the reaction force generated during the elastic deformation of the power spring, the square block moves in the reverse direction. During the movement of the square block, the gas inside the square shell is discharged into the heating box through the air pipe. After the gas enters the heating box, it then enters the square box through the heating box. The gas causes the lifting plate inside the square box to move upward, and the lifting plate drives the rotating plate to move upward. Restricted by the cross bar, during the upward movement of the rotating plate, the slider moves horizontally. The two sliders move in opposite directions. The slider drives the rubber block to move and squeezes the square plate stirring blade. The square plate stirring blade is squeezed to produce a semi-circular rotation. The two sliders move away from each other and stretch the second return spring. Under the elastic force of the second return spring, the slider can move reciprocally.

[0019] Step 3:

[0020] When the mixture enters the feeding shell, the mixture causes the buoyancy arc-shaped sleeve to move upward. And under the elastic force of the second arc-shaped spring, during the upward movement of the buoyancy arc-shaped sleeve, the second arc-shaped spring will contract. The second arc-shaped spring drives the sliding plate to move. The two sliding plates move closer to each other. The sliding plate drives the arc-shaped rod to enter the inside of the buoyancy arc-shaped sleeve, so that the buoyancy arc-shaped sleeve can always fit against the inner wall of the conical filter sleeve plate. During the process of the two sliding plates moving closer to each other, the gas inside the buoyancy arc-shaped sleeve enters the inside of the arc-shaped shell through the inclined pipe. The air pressure pushes the arc-shaped cleaning block inside the arc-shaped shell to move, and the arc-shaped cleaning block drives the rubber semi-circular block to move. During the movement of the arc-shaped cleaning block, the extrusion spring is stretched. Under the elastic action of the extrusion spring, the arc-shaped cleaning block drives the rubber semi-circular block to move reciprocally.

[0021] Step 4:

[0022] During the upward movement of the buoyancy arc-shaped sleeve, the buoyancy arc-shaped sleeve drives the bent rod to move upward, and the bent rod drives the buoyancy ring to move upward. The buoyancy ring drives the telescopic sleeve to rise. The telescopic sleeve can block the oil hole at the feeding shell. And the gas inside the heating box will also move into the vertical pipe. The gas causes the lifting block inside the vertical pipe to move upward, the lifting block drives the vertical rod to move upward, the vertical rod drives the buoyancy arc-shaped sleeve to rise, and the vertical rod drives the clamping block to rise. The clamping block drives the pull rope to rise. The pull rope is stretched, causing the movable end of the telescopic sleeve to move upward. During the upward movement of the telescopic sleeve, it no longer blocks the oil hole, so that the pure tar enters the inside of the working shell through the oil hole, and then the tar is discharged outward through the drain pipe at the working shell.

[0023] The present invention has the following beneficial effects:

[0024] (1) Pour a specific solvent into the conical filter sleeve plate, and then discharge the mixture into the feeding shell. The conical filter sleeve plate filters impurities in the mixture. Start the motor, and the rotating motor drives the rotating shaft to rotate. The rotating shaft drives the special-shaped stirring blade to rotate, so that the mixture is mixed with the specific solvent. Ammonia water in the mixture reacts with the specific solvent to produce ammonium salt precipitation. Moreover, the special-shaped stirring blade drives the square shell to rotate. The centrifugal force generated during the rotation of the square shell makes the square block move towards the outside of the square shell. The square block drives the rubber rod to move, thereby knocking on the conical filter sleeve plate. The generated vibration makes the conical filter sleeve plate shake slightly, preventing the filter holes of the conical filter sleeve plate from being blocked by impurities, and thus improving the efficiency of ammonium salt precipitation. The heating plate heats the mixture on the top of the heating box, further improving the efficiency of ammonium salt precipitation.

[0025] (2) During the process of the rubber rod knocking on the conical filter sleeve plate, the square block stretches the power spring. Under the elastic force of the power spring, the square block moves in the reverse direction. During the movement of the square block, the gas inside the square shell is discharged into the heating box through the air pipe, making the heat flow inside the heating box move. Laterally, it enhances the heating effect of the heat flow on the mixture. After the gas enters the heating box, the air pressure makes the lifting plate inside the square box move upward. The lifting plate drives the rotating plate to move upward. Due to the limitation of the cross bar, when the rotating plate moves upward, the slider moves horizontally. The two sliders move in opposite directions. The slider drives the rubber block to move, thereby squeezing the square plate stirring blade. The square plate stirring blade is squeezed to generate a semi-circular rotation, thereby disturbing the mixture inside the conical filter sleeve plate, making the mixture near the top of the heating box move upward, so that the mixture is heated more evenly, and further improving the heating effect of the mixture. During the process of the two sliders moving away from each other, the second reset spring is stretched. Under the elastic force of the second reset spring, the slider can move reciprocally, thereby enhancing the rotation frequency of the square plate stirring blade and improving the heating efficiency.

[0026] (3) After the mixture enters the interior of the feed housing, the mixture causes the buoyancy arc sleeve to move upward. The buoyancy arc sleeve cleans the inner wall joint of the conical filter sleeve plate to prevent the filter holes of the conical filter sleeve plate from being blocked by impurities. And due to the elastic deformation of the second arc spring, during the upward movement of the buoyancy arc sleeve, the second arc spring will contract. The second arc spring drives the slide plate to move, and the two slide plates move closer to each other. The slide plate drives the arc rod to enter the interior of the buoyancy arc sleeve, enabling the buoyancy arc sleeve to always fit against the inner wall of the conical filter sleeve plate, enhancing the cleaning effect. Additionally, during the process of the two slide plates moving closer to each other, the air pressure inside the buoyancy arc sleeve enters the interior of the arc housing through the inclined tube. The air pressure pushes the arc cleaning block inside the arc housing to move, and the arc cleaning block drives the rubber semi-circular block to move, thereby causing the rubber semi-circular block to strike the outer wall of the conical filter sleeve plate, making the conical filter sleeve plate vibrate, and further preventing the filter holes of the conical filter sleeve plate from being blocked by impurities. During the movement of the arc cleaning block, the extrusion spring is stretched. Under the elastic force of the extrusion spring, the arc cleaning block drives the rubber semi-circular block to move reciprocally, thereby enhancing the knocking frequency of the rubber semi-circular block on the conical filter sleeve plate, further enhancing the anti-blocking effect of the conical filter sleeve plate, and enhancing the reaction efficiency of the mixture.

[0027] (4) During the upward movement of the buoyancy arc sleeve, the buoyancy arc sleeve drives the bent rod to move upward, and the bent rod drives the buoyancy ring to move upward. The buoyancy ring improves the lifting effect of the buoyancy arc sleeve, and the buoyancy ring drives the telescopic sleeve to rise. The setting of the telescopic sleeve can block the oil hole at the feed housing to prevent the mixture from leaking, extending the reaction time. Moreover, the gas inside the heating box will also move into the interior of the vertical tube. The air pressure causes the lifting block inside the vertical tube to move upward, and the lifting block drives the vertical rod to move upward. The vertical rod drives the buoyancy arc sleeve to rise, enhancing the stability of the lifting of the buoyancy arc sleeve. And the vertical rod drives the clamping block to rise, and the clamping block drives the pull rope to rise. The pull rope is stretched, causing the movable end of the telescopic sleeve to move upward. During the upward movement of the telescopic sleeve, it no longer blocks the oil hole, so that pure tar enters the interior of the working housing through the oil hole. Subsequently, the tar is discharged outward through the drain pipe at the working housing, controlling the mixing time between the mixture and the specific solvent, and indirectly improving the purity of the tar.

[0028] Of course, it is not necessary for any product implementing the present invention to simultaneously achieve all the above-mentioned advantages. BRIEF DESCRIPTION OF THE DRAWINGS

[0029] In order to more clearly illustrate the technical solutions of the embodiments of the present invention, the following will briefly introduce the drawings required for describing the embodiments. Obviously, the drawings in the following description are only some embodiments of the present invention. For those of ordinary skill in the art, without creative efforts, other drawings can be obtained based on these drawings.

[0030] Figure 1Schematic diagram of the overall side top view of the present invention;

[0031] Figure 2 Schematic diagram of the overall half-section side structure of the present invention;

[0032] Figure 3 Schematic diagram of the internal top view structure of the present invention;

[0033] Figure 4 Schematic diagram of the internal half-section structure of the present invention;

[0034] Figure 5 Schematic diagram of the exploded side structure of the stirring component of the present invention;

[0035] Figure 6 Schematic diagram of the half-section structure of the heating component of the present invention;

[0036] Figure 7 Schematic diagram of the side structure of the lifting component of the present invention;

[0037] [[ID=?]] Figure 8 Schematic diagram of the exploded structure of the cleaning component of the present invention;

[0038] Figure 9 For the present invention Figure 2 Enlarged view of A in;

[0039] Figure 10 For the present invention Figure 4 Enlarged view of B in;

[0040] Figure 11 For the present invention Figure 4 Enlarged view of C in.

[0041] In the drawings, the list of components represented by each reference numeral is as follows:

[0042] In the figure: 1, working shell; 2, support feet; 3, drain pipe; 4, feeding shell; 5, rotating separation component; 51, motor; 52, rotating shaft; 53, oil hole; 54, conical filter sleeve plate; 55, stirring component; 56, heating component; 57, lifting component; 58, cleaning component; 551, special-shaped stirring blade; 552, square shell; 553, square block; 554, power spring; 555, rubber rod; 556, air pipe; 557, sleeve piece; 558, heating box; 559, heating plate; 561, first reset spring; 562, lifting plate; 563, square box; 564, rotating plate; 565, slider; 566, cross bar; 567, second reset spring; 568, rubber block; 569, first arc spring; 5610, square plate stirring blade; 571, vertical pipe; 572, lifting block; 573, vertical rod; 574, clamping block; 575, pull rope; 576, telescopic sleeve; 577, buoyancy ring; 578, bent rod; 581, buoyancy arc sleeve; 582, second arc spring; 583, sliding plate; 584, arc rod; 585, inclined pipe; 586, arc shell; 587, extrusion spring; 588, arc cleaning block; 589, rubber semi-circular block. Detailed implementation mode

[0043] Next, the technical solutions in the embodiments of the present invention will be clearly and completely described in conjunction with the accompanying drawings in the embodiments of the present invention. Obviously, the described embodiments are only a part of the embodiments of the present invention, rather than all the embodiments. Based on the embodiments of the present invention, all other embodiments obtained by those of ordinary skill in the art without creative efforts shall fall within the protection scope of the present invention.

[0044] Example 1, please refer to Figures 1-11 As shown in the figure, the embodiment of the present application provides a tar-ammonia water separation device, including a working shell 1. A plurality of support feet 2 are respectively fixedly connected to the outer periphery of the bottom end of the working shell 1. One side of the bottom end of the working shell 1 is communicated with a drain pipe 3. The purpose of this setting is to discharge tar. A feeding shell 4 is fixedly connected to the top of the working shell 1. The tar-ammonia water separation device further includes a rotating separation component 5. The rotating separation component 5 includes a motor 51 fixedly connected to the bottom of the working shell 1. The output end of the motor 51 is fixedly connected to a rotating shaft 52. One end of the rotating shaft 52 penetrates through the feeding shell 4 and extends into the interior of the feeding shell 4. A plurality of oil holes 53 are respectively opened around the outer wall bottom end of the feeding shell 4. A conical filter sleeve plate 54 is fixedly connected to the bottom of the feeding shell 4. The purpose of this setting is to filter impurities generated by the reaction of a specific solvent and a mixture. A stirring component 55 is arranged on the outer wall of the rotating shaft 52.

[0045] The stirring assembly 55 includes a plurality of special-shaped stirring blades 551 fixedly connected to the outer periphery of the top end of the rotating shaft 52. Square shells 552 are fixedly connected to both sides of the special-shaped stirring blades 551. A square block 553 is sleeved and slidably connected to the inner wall of the square shell 552. A power spring 554 is fixedly connected to one side of the square block 553, and one end of the power spring 554 is fixedly connected to one side of the inner wall of the square shell 552.

[0046] A rubber rod 555 is fixedly connected to the side of the square block 553 away from the power spring 554. The purpose of this setting is to prevent excessive knocking and protect the conical filter sleeve plate 54. One end of the square shell 552 communicates with an air pipe 556. A sleeve piece 557 is fixedly connected to the end of the air pipe 556 away from the square shell 552. A heating box 558 is sleeved and rotatably connected to the outer wall of the sleeve piece 557. The bottom of the heating box 558 is fixedly connected to the inner bottom of the feeding shell 4. A heating plate 559 is fixedly connected to the inner bottom of the heating box 558. The purpose of this setting is to raise the temperature.

[0047] A heating assembly 56 is arranged on the top of the heating plate 559. The heating assembly 56 includes a plurality of first return springs 561 fixedly connected to the periphery of the top of the heating plate 559. The purpose of this setting is to perform reset. A lifting plate 562 is fixedly connected to the top of the first return spring 561. A square box 563 is sleeved and slidably connected to the outer wall of the lifting plate 562. The bottom of the square box 563 communicates with the top of the second return spring 567. Rotating plates 564 are respectively rotatably connected to both sides of the top of the lifting plate 562. A slider 565 is rotatably connected to the end of the rotating plate 564 away from the lifting plate 562. A cross bar 566 is sleeved and slidably connected to the inner wall of the slider 565. The purpose of this setting is to prevent the slider 565 from falling off.

[0048] Both ends of the cross bar 566 are fixedly connected to the inner cavity of the square box 563. A second return spring 567 is fixedly connected between the two sliders 565. A rubber block 568 is fixedly connected to the side of the slider 565 away from the second return spring 567. First arc-shaped springs 569 are respectively fixedly connected to both sides of the inner wall of the square box 563. The purpose of this setting is to facilitate the reciprocating movement of the square plate stirring blade 5610. One end of the first arc-shaped spring 569 is fixedly connected to the square plate stirring blade 5610. The middle end of the square plate stirring blade 5610 penetrates and is rotatably connected to the inner wall of the square box 563.

[0049] Pour a specific solvent inside the conical filter sleeve plate 54, and then drain the mixture into the inside of the feed housing 4. The conical filter sleeve plate 54 filters the impurities in the mixture. Start the motor 51, the motor 51 drives the rotating shaft 52 to rotate, the rotating shaft 52 drives the special-shaped stirring blade 551 to rotate, so that the mixture is mixed with the specific solvent, the ammonia water in the mixture reacts with the specific solvent to produce ammonium salt precipitation, and the special-shaped stirring blade 551 drives the square shell 552 to rotate. The centrifugal force generated during the rotation of the square shell 552 causes the square block 553 to move outward from the square shell 552. The square block 553 drives the rubber rod 555 to move, thereby knocking on the conical filter sleeve plate 54. The generated vibration causes the conical filter sleeve plate 54 to shake slightly, preventing the filter holes of the conical filter sleeve plate 54 from being blocked by impurities, enhancing the efficiency of ammonium salt precipitation, and the heating plate 559 can heat the mixture on the top of the heating box 558, further accelerating the efficiency of ammonium salt precipitation.

[0050] During the process of the rubber rod 555 knocking on the conical filter sleeve plate 54, the square block 553 stretches the power spring 554. Under the action of the reaction force generated during the elastic deformation of the power spring 554, the square block 553 moves in the reverse direction. During the movement of the square block 553, the gas inside the square shell 552 is discharged into the inside of the heating box 558 through the air pipe 556, causing the heat flow inside the heating box 558 to move, which laterally enhances the heating effect of the heat flow on the mixture. After the gas enters the inside of the heating box 558, it enters the inside of the square box 563 through the heating box 558. The gas causes the lifting plate 562 inside the square box 563 to move upward. The lifting plate 562 drives the rotating plate 564 to move upward. Limited by the cross bar 566, during the upward movement of the rotating plate 564, the slider 565 moves horizontally. The two sliders 565 move in opposite directions. The slider 565 drives the rubber block 568 to move and squeezes the square plate stirring blade 5610. The square plate stirring blade 5610 is squeezed to produce a semi-circular rotation, thereby disturbing the mixture inside the conical filter sleeve plate 54, causing the mixture near the top of the heating box 558 to move upward, making the mixture heated more evenly, and further improving the heating effect of the mixture. The two sliders 565 move away from each other and stretch the second return spring 567. Under the elastic force of the second return spring 567, the slider 565 can move reciprocally, enhancing the rotation frequency of the square plate stirring blade 5610 and laterally improving the heating efficiency.

[0051] Example 2, a lifting component 57 is arranged on the top of the heating box 558. The lifting component 57 includes a plurality of vertical pipes 571 connected to the periphery of the top of the heating box 558 close to the square box 563. The inner wall of the vertical pipe 571 is sleeved and slidably connected with a lifting block 572. The top of the lifting block 572 is fixedly connected with a vertical rod 573. The outer wall of the top of the vertical rod 573 is sleeved and fixedly connected with a clamping block 574.

[0052] A pull rope 575 is fixedly connected to one side of the bottom of the block 574, and a telescopic sleeve 576 is fixedly connected to the end of the pull rope 575 away from the block 574. The purpose of this arrangement is to enable automatic telescopic expansion and contraction. A buoyancy ring 577 is fixedly connected to the top of the telescopic sleeve 576. The outer wall of the buoyancy ring 577 is sleeved and slidably connected to the inner wall of the feed shell 4. Several bent rods 578 are fixedly connected around the inner wall of the buoyancy ring 577.

[0053] A cleaning assembly 58 is provided at one end of the bent rod 578, and the cleaning assembly 58 includes a buoyancy arc sleeve 581 fixedly connected to the end of the bent rod 578 away from the buoyancy ring 577, and slides 583 are respectively provided at both ends of the inner wall of the buoyancy arc sleeve 581 and slidably connected, and a second arc spring 582 is fixedly connected between the two slides 583, and the second arc spring 582 is provided inside the buoyancy arc sleeve 581, and an arc rod 584 is fixedly connected to the side of the slide 583 away from the second arc spring 582. The purpose of this arrangement is to enable the arc rod 584 to slide in the buoyancy arc sleeve 581.

[0054] The bottom of the buoyancy arc sleeve 581 is connected to an inclined tube 585, and the bottom of the inclined tube 585 is connected to an arc shell 586. The inner wall of the arc shell 586 is sleeved and slidably connected with an arc cleaning block 588. One side of the arc cleaning block 588 is fixedly connected to a plurality of extrusion springs 587. One end of the extrusion spring 587 is fixedly connected to one side of the inner wall of the arc shell 586. The side of the arc cleaning block 588 away from the extrusion spring 587 is fixedly connected to a plurality of rubber semicircular blocks 589. The outer wall side of the clamping block 574 is fixedly connected to one end of the vertical rod 573.

[0055] A tar-ammonia water separation method, applied to the tar-ammonia water separation device, comprises the following steps:

[0056] Step 1: Pour a specific solvent into the interior of the conical filter sleeve plate 54, and then discharge the mixture into the interior of the feed shell 4. The conical filter sleeve plate 54 filters impurities in the mixture, and the motor 51 is started. The motor 51 drives the rotating shaft 52 to rotate, and the rotating shaft 52 drives the special-shaped stirring blades 551 to rotate, and the special-shaped stirring blades 551 drive the square shell 552 to rotate. The centrifugal force generated by the square shell 552 during the rotation process causes the block 553 to move to the outside of the square shell 552, and the block 553 drives the rubber rod 555 to move. At the same time, the heating plate 559 heats the mixture on the top of the heating box 558.

[0057] Step 2: During the process of the rubber rod 555 knocking on the conical filter sleeve plate 54, the square block 553 stretches the power spring 554. Under the action of the reaction force generated during the elastic deformation of the power spring 554, the square block 553 moves in the reverse direction. During the movement of the square block 553, the gas inside the square shell 552 is discharged into the interior of the heating box 558 through the air pipe 556. After the gas enters the interior of the heating box 558, it then enters the interior of the square box 563 through the heating box 558. The gas causes the lifting plate 562 inside the square box 563 to move upward. The lifting plate 562 drives the rotating plate 564 to move upward. Restricted by the cross bar 566, during the upward movement of the rotating plate 564, the slider 565 moves horizontally. The two sliders 565 move in opposite directions. The slider 565 drives the rubber block 568 to move and squeezes the square plate stirring blade 5610. The square plate stirring blade 5610 is squeezed to produce a semi-circular rotation. The two sliders 565 move away from each other and stretch the second return spring 567. Under the elastic force of the second return spring 567, the slider 565 can move reciprocally.

[0058] Step 3: When the mixture enters the interior of the feeding shell 4, the mixture causes the buoyancy arc-shaped sleeve 581 to move upward. And under the elastic force of the second arc-shaped spring 582, during the upward movement of the buoyancy arc-shaped sleeve 581, the second arc-shaped spring 582 will contract. The second arc-shaped spring 582 drives the sliding plate 583 to move. The two sliding plates 583 move closer to each other. The sliding plate 583 drives the arc-shaped rod 584 to enter the interior of the buoyancy arc-shaped sleeve 581, enabling the buoyancy arc-shaped sleeve 581 to always fit against the inner wall of the conical filter sleeve plate 54. During the process of the two sliding plates 583 moving closer to each other, the gas inside the buoyancy arc-shaped sleeve 581 enters the interior of the arc-shaped shell 586 through the inclined pipe 585. The air pressure pushes the arc-shaped cleaning block 588 inside the arc-shaped shell 586 to move. The arc-shaped cleaning block 588 drives the rubber semi-circular block 589 to move. During the movement of the arc-shaped cleaning block 588, the extrusion spring 587 is stretched. Under the elastic action of the extrusion spring 587, the arc-shaped cleaning block 588 drives the rubber semi-circular block 589 to move reciprocally.

[0059] Step 4: During the upward movement of the buoyancy arc sleeve 581, the buoyancy arc sleeve 581 drives the bent rod 578 to move upward, and the bent rod 578 drives the buoyancy ring 577 to move upward. The buoyancy ring 577 drives the telescopic sleeve 576 to rise. The telescopic sleeve 576 can block the oil hole 53 at the feeding shell 4, and the gas inside the heating box 558 will also move into the vertical pipe 571. The gas causes the lifting block 572 inside the vertical pipe 571 to move upward. The lifting block 572 drives the vertical rod 573 to move upward. The vertical rod 573 drives the buoyancy arc sleeve 581 to rise, and the vertical rod 573 drives the clamping block 574 to rise. The clamping block 574 drives the pull rope 575 to rise. The pull rope 575 is stretched, causing the movable end of the telescopic sleeve 576 to move upward. During the upward movement of the telescopic sleeve 576, it no longer blocks the oil hole 53, allowing pure tar to enter the interior of the working shell 1 through the oil hole 53. Subsequently, the tar is discharged outward through the drain pipe 3 at the working shell 1.

[0060] During use, when the mixture enters the interior of the feeding shell 4, the mixture causes the buoyancy arc sleeve 581 to move upward, enabling the buoyancy arc sleeve 581 to clean the inner wall fitting portion of the conical filter sleeve plate 54, preventing impurities from blocking the filter holes of the conical filter sleeve plate 54. Due to the elastic deformation of the second arc spring 582, during the upward movement of the buoyancy arc sleeve 581, the second arc spring 582 will contract, and the second arc spring 582 drives the sliding plate 583 to move. The two sliding plates 583 move closer to each other. The sliding plate 583 drives the arc rod 584 into the interior of the buoyancy arc sleeve 581, enabling the buoyancy arc sleeve 581 to always fit against the inner wall of the conical filter sleeve plate 54, enhancing the cleaning effect. During the process of the two sliding plates 583 moving closer to each other, the gas inside the buoyancy arc sleeve 581 enters the interior of the arc shell 586 through the inclined pipe 585. The air pressure drives the arc cleaning block 588 inside the arc shell 586 to move. The arc cleaning block 588 drives the rubber semi-circular block 589 to move, thereby causing the rubber semi-circular block 589 to strike the outer wall of the conical filter sleeve plate 54, causing the conical filter sleeve plate 54 to vibrate, further preventing impurities from blocking the filter holes of the conical filter sleeve plate 54. During the movement of the arc cleaning block 588, the extrusion spring 587 is stretched. Under the elastic force of the extrusion spring 587, the arc cleaning block 588 drives the rubber semi-circular block 589 to move reciprocally, thereby enhancing the knocking frequency of the rubber semi-circular block 589 on the conical filter sleeve plate 54, further enhancing the anti-blocking effect of the conical filter sleeve plate 54 and enhancing the reaction efficiency of the mixture.

[0061] During the upward movement of the buoyancy arc sleeve 581, the buoyancy arc sleeve 581 drives the curved rod 578 to move upward, and the curved rod 578 drives the buoyancy ring 577 to move upward. By setting the buoyancy ring 577, the buoyancy is enhanced, improving the lifting effect of the buoyancy arc sleeve 581. Moreover, the movement of the buoyancy ring 577 can drive the telescopic sleeve 576 to rise. The telescopic sleeve 576 can block the oil hole 53 at the feeding shell 4 to prevent the mixture from leaking out, thereby prolonging the reaction time. The gas inside the heating box 558 will move into the interior of the vertical pipe 571, and the air pressure causes the lifting block 572 inside the vertical pipe 571 to move upward. The lifting block 572 drives the vertical rod 573 to move upward, and the vertical rod 573 drives the buoyancy arc sleeve 581 to rise, enhancing the stability of the lifting of the buoyancy arc sleeve 581. The vertical rod 573 drives the latch 574 to rise, and the latch 574 drives the pull rope 575 to rise. The pull rope 575 is stretched, causing the movable end of the telescopic sleeve 576 to move upward. During the upward movement of the telescopic sleeve 576, it no longer blocks the oil hole 53, so that the pure tar enters the interior of the working shell 1 through the oil hole 53. Subsequently, the tar is discharged outward through the drain pipe 3 at the working shell 1, controlling the mixing time between the mixture and the specific solvent, which is beneficial to improving the purity of the tar.

[0062] The preferred embodiments of the present invention disclosed above are only used to help explain the present invention. The preferred embodiments do not describe all the details in detail, nor do they limit the invention to the specific embodiments described. Obviously, many modifications and changes can be made according to the content of this specification. This specification selects and specifically describes these embodiments to better explain the principle and practical application of the present invention, so that those skilled in the relevant technical field can understand and utilize the present invention well. The present invention is only limited by the claims and their full scope and equivalents.

Claims

1. A tar and ammonia separation device, characterized in that, It includes a working shell (1), and several supporting feet (2) are respectively and fixedly connected to the outer periphery of the bottom end outer wall of the working shell (1). An oil discharge pipe (3) is communicated with one side of the bottom end of the working shell (1). A feeding shell (4) is fixedly connected to the top of the working shell (1). The tar-ammonia separation device further includes: A rotating separation component (5), the rotating separation component (5) includes a motor (51) fixedly connected to the bottom of the working shell (1). The output end of the motor (51) is fixedly connected to a rotating shaft (52). One end of the rotating shaft (52) penetrates through the feeding shell (4) and extends into the interior of the feeding shell (4). A plurality of oil holes (53) are respectively opened in the outer periphery of the bottom end of the outer wall of the feeding shell (4). A conical filter sleeve plate (54) is fixedly connected to the bottom of the feeding shell (4). A stirring component (55) is arranged on the outer wall of the rotating shaft (52).

2. The tar-ammonia separation device according to claim 1, characterized in that, The stirring component (55) includes several special-shaped stirring blades (551) fixedly connected to the outer periphery of the top end outer wall of the rotating shaft (52). Square shells (552) are respectively fixedly connected to both sides of the special-shaped stirring blades (551). A square block (553) is sleeved and slidably connected to the inner wall of the square shell (552). A power spring (554) is fixedly connected to one side of the square block (553). One end of the power spring (554) is fixedly connected to one side of the inner wall of the square shell (552).

3. The tar-ammonia separation device according to claim 2, characterized in that, A rubber rod (555) is fixedly connected to the side of the square block (553) away from the power spring (554). An air pipe (556) is communicated with one end of the square shell (552). A sleeve piece (557) is fixedly connected to the end of the air pipe (556) away from the square shell (552). A heating box (558) is sleeved and rotatably connected to the outer wall of the sleeve piece (557). The bottom of the heating box (558) is fixedly connected to the inner wall bottom of the feeding shell (4). A heating plate (559) is fixedly connected to the inner wall bottom of the heating box (558).

4. The tar-ammonia water separation device according to claim 3, characterized in that, A heating component (56) is arranged on the top of the heating plate (559). The heating component (56) includes several first return springs (561) fixedly connected to the outer periphery of the top of the heating plate (559). A lifting plate (562) is fixedly connected to the top of the first return springs (561). A square box (563) is sleeved and slidably connected to the outer wall of the lifting plate (562). The bottom of the square box (563) is communicated with the top of the second return spring (567). Rotating plates (564) are respectively rotatably connected to both sides of the top of the lifting plate (562). A slider (565) is rotatably connected to the end of the rotating plate (564) away from the lifting plate (562). A cross bar (566) is sleeved and slidably connected to the inner wall of the slider (565).

5. The tar-ammonia water separation device according to claim 4, characterized in that, Both ends of the cross bar (566) are fixedly connected to the inner cavity of the square box (563). A second return spring (567) is fixedly connected between the two sliders (565). A rubber block (568) is fixedly connected to the side of the slider (565) away from the second return spring (567). On both sides of the inner wall of the square box (563), a first arc spring (569) is respectively fixedly connected. One end of the first arc spring (569) is fixedly connected to a square plate stirring blade (5610). The middle end of the square plate stirring blade (5610) penetrates and is rotatably connected to the inner wall of the square box (563).

6. The tar-ammonia separation device according to claim 5, wherein A lifting component (57) is arranged on the top of the heating box (558). The lifting component (57) includes a plurality of vertical pipes (571) communicated around the top of the heating box (558) close to the square box (563). A lifting block (572) is sleeved and slidably connected to the inner wall of the vertical pipe (571). A vertical rod (573) is fixedly connected to the top of the lifting block (572). A clamping block (574) is sleeved and fixedly connected to the outer wall of the top end of the vertical rod (573).

7. The tar-ammonia separation device according to claim 6, characterized in that, One side of the bottom of the clamping block (574) is fixedly connected to a pull rope (575). One end of the pull rope (575) away from the clamping block (574) is fixedly connected to a telescopic sleeve (576). A buoyancy ring (577) is fixedly connected to the top of the telescopic sleeve (576). The outer wall of the buoyancy ring (577) is sleeved and slidably connected to the inner wall of the feeding shell (4). A plurality of bent rods (578) are respectively fixedly connected to the periphery of the inner wall of the buoyancy ring (577).

8. A tar and ammonia water separation device according to claim 7, characterized in that, One end of the bent rod (578) is provided with a cleaning component (58). The cleaning component (58) includes a buoyancy arc sleeve (581) fixedly connected to the end of the bent rod (578) away from the buoyancy ring (577). Two sliding plates (583) are respectively sleeved and slidably connected to both ends of the inner wall of the buoyancy arc sleeve (581). A second arc spring (582) is fixedly connected between the two sliding plates (583). The second arc spring (582) is arranged inside the buoyancy arc sleeve (581). An arc rod (584) is fixedly connected to the side of the sliding plate (583) away from the second arc spring (582).

9. The tar-ammonia separation device according to claim 8, characterized in that, The bottom of the buoyancy arc sleeve (581) is communicated with an inclined pipe (585). The bottom of the inclined pipe (585) is communicated with an arc shell (586). An arc cleaning block (588) is sleeved and slidably connected to the inner wall of the arc shell (586). A plurality of extrusion springs (587) are fixedly connected to one side of the arc cleaning block (588). One end of the extrusion spring (587) is fixedly connected to one side of the inner wall of the arc shell (586). A plurality of rubber semi - circular blocks (589) are fixedly connected to the side of the arc cleaning block (588) away from the extrusion springs (587). One side of the outer wall of the clamping block (574) is fixedly connected to one end of the vertical rod (573).

10. A method for separating tar and ammonia water, characterized in that, Applied to the tar - ammonia separation device according to any one of claims 1 - 9, comprising: Step 1: Pour a specific solvent into the inside of the conical filter sleeve plate (54), and then discharge the mixture into the inside of the feed housing (4). The conical filter sleeve plate (54) filters impurities in the mixture. Start the motor (51), and the motor (51) drives the rotating shaft (52) to rotate. The rotating shaft (52) drives the special-shaped stirring blade (551) to rotate, and the special-shaped stirring blade (551) drives the square shell (552) to rotate. The centrifugal force generated during the rotation of the square shell (552) causes the square block (553) to move outward from the square shell (552). The square block (553) drives the rubber rod (555) to move. At the same time, the heating plate (559) heats the mixture on the top of the heating box (558). Step 2: During the process of the rubber rod (555) knocking on the conical filter sleeve plate (54), the square block (553) stretches the power spring (554). Under the action of the reaction force generated during the elastic deformation of the power spring (554), the square block (553) moves in the reverse direction. During the movement of the square block (553), the gas inside the square shell (552) is discharged into the inside of the heating box (558) through the air pipe (556). After the gas enters the inside of the heating box (558), it then enters the inside of the square box (563) through the heating box (558). The gas causes the lifting plate (562) inside the square box (563) to move upward. The lifting plate (562) drives the rotating plate (564) to move upward. Limited by the cross bar (566), during the upward movement of the rotating plate (564), the slider (565) moves horizontally. The two sliders (565) move in opposite directions. The slider (565) drives the rubber block (568) to move and squeezes the square plate stirring blade (5610). The square plate stirring blade (5610) is squeezed to produce a semi-circular rotation. The two sliders (565) move away from each other and stretch the second return spring (567). Under the elastic force of the second return spring (567), the slider (565) can move reciprocally. Step 3: After the mixture enters the interior of the feed housing (4), the mixture causes the buoyancy arc sleeve (581) to move upward. Under the elastic force of the second arc spring (582), during the upward movement of the buoyancy arc sleeve (581), the second arc spring (582) will contract. The second arc spring (582) drives the sliding plate (583) to move. The two sliding plates (583) move closer to each other. The sliding plate (583) drives the arc rod (584) into the interior of the buoyancy arc sleeve (581), enabling the buoyancy arc sleeve (581) to always fit against the inner wall of the conical filter sleeve plate (54). During the process of the two sliding plates (583) moving closer to each other, the gas inside the buoyancy arc sleeve (581) enters the interior of the arc housing (586) through the inclined tube (585). The air pressure pushes the arc cleaning block (588) inside the arc housing (586) to move. The arc cleaning block (588) drives the rubber semi-circular block (589) to move. During the movement of the arc cleaning block (588), the extrusion spring (587) is stretched. Under the elastic action of the extrusion spring (587), the arc cleaning block (588) drives the rubber semi-circular block (589) to move reciprocally. Step 4: During the upward movement of the buoyancy arc sleeve (581), the buoyancy arc sleeve (581) drives the bent rod (578) to move upward. The bent rod (578) drives the buoyancy ring (577) to move upward. The buoyancy ring (577) drives the telescopic sleeve (576) to rise. The telescopic sleeve (576) can block the oil hole (53) at the feed housing (4). Moreover, the gas inside the heating box (558) will also move into the vertical tube (571). The gas causes the lifting block (572) inside the vertical tube (571) to move upward. The lifting block (572) drives the vertical rod (573) to move upward. The vertical rod (573) drives the buoyancy arc sleeve (581) to rise. And the vertical rod (573) drives the clamping block (574) to rise. The clamping block (574) drives the pull rope (575) to rise. The pull rope (575) is stretched, causing the movable end of the telescopic sleeve (576) to move upward. During the upward movement of the telescopic sleeve (576), it no longer blocks the oil hole (53). Thus, the pure tar enters the interior of the working housing (1) through the oil hole (53). Subsequently, the tar is discharged outward through the drain pipe (3) at the working housing (1).

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