Quartz bracket for hydrothermal reaction

By designing a quartz bracket, the problem of limited placement of substrate materials in traditional hydrothermal reactions was solved, achieving more efficient hydrothermal reactions and more stable material preparation.

CN223324561UActive Publication Date: 2025-09-12CNBM RESEARCH INSTITUTE FOR ADVANCED GLASS MATERIALS GROUP CO LTD
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Patent Information

Application Number
CN202421736148.7
Authority / Receiving Office
CN · China
Patent Type
Utility models(China)
Current Assignee / Owner
Filing Date
2024-07-22
Publication Date
2025-09-12
Estimated Expiration
2034-07-22

AI Technical Summary

Technical Problem

In traditional hydrothermal reactions, the placement of substrate materials is limited by the size of the reactor, resulting in a limited effective area for the deposition reaction.

Method used

A bracket made of quartz material is designed, which has spaced-apart side plates and a support plate. The support plate is provided with a small sample placement slot and a lifting lug for easy lifting. The bracket is suitable for a hydrothermal reactor.

Benefits of technology

The efficiency and effect of the hydrothermal reaction are improved, the stability and durability of the scaffold under high temperature and high pressure conditions are ensured, and it is suitable for a variety of chemical syntheses and material preparations.

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Abstract

The utility model provides a quartz bracket for hydrothermal reaction, which is characterized in that the quartz bracket comprises a main body (1), the main body (1) comprises a pair of side plates (2) which are spaced at a certain distance and are longitudinally distributed, a group of supporting plates (3) which are distributed in parallel are distributed between the two side plates (2), and a small sample placing groove (4) is arranged on the upper surface of each supporting plate (3). The quartz bracket provided by the utility model has the characteristics of simple structure, low cost and convenience in operation, provides an efficient experimental tool for the hydrothermal reaction field, and is beneficial to promoting the development and application of related science and technology.
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Description

Technical Field

[0001] The utility model belongs to the technical field of hydrothermal reaction, in particular to a quartz support for hydrothermal reaction. Background Art

[0002] As a valuable method in the field of chemical synthesis and material preparation, hydrothermal reaction technology has been widely used in laboratories and industrial production. It can synthesize compounds and materials that are difficult to prepare under standard or conventional conditions. In particular, hydrothermal deposition, as an emerging synthetic method, has received widespread attention in recent years, showing great potential in synthesizing nanomaterials, thin films and nanoparticles. The core mechanism of hydrothermal deposition is to use specific conditions in high-temperature and high-pressure aqueous solutions, such as substance concentration, temperature and pressure, to promote the deposition of substances in the solution on the substrate surface, thereby forming the desired thin film or nanostructure. However, there are certain limitations in the traditional hydrothermal reaction process, especially in the placement of the substrate material. The substrate material can usually only be placed at the bottom of the reactor, which results in the effective area of ​​the deposition reaction being strictly limited by the size of the reactor. Utility Model Content

[0003] The utility model aims to overcome the deficiencies in the prior art and provides a quartz support for hydrothermal reaction.

[0004] This application provides the following technical solutions:

[0005] A quartz support for hydrothermal reaction, characterized in that it includes a main body, the main body includes a pair of side plates spaced a certain distance apart and distributed longitudinally, a group of parallel support plates are distributed between the two side plates, and a small sample placement groove is provided on the upper surface of each support plate.

[0006] On the basis of the above technical solutions, the following further technical solutions can be provided:

[0007] The distances between the two adjacent support plates are the same.

[0008] The shapes and areas of the small sample placement grooves on the various support plates may be the same or different.

[0009] The main body is made of quartz material.

[0010] There is also an integrally formed lifting lug on the top of the support plate.

[0011] Utility model advantages:

[0012] The quartz support of this invention not only provides a simple and cost-effective solution, but also, through its adjustable groove size, can meet the needs of different hydrothermal reaction experiments, thereby improving experimental efficiency and effectiveness. Furthermore, the vertical and parallel side panels and support plate design ensure the stability and durability of the entire support during the hydrothermal reaction process, providing more support for hydrothermal deposition material preparation. BRIEF DESCRIPTION OF THE DRAWINGS

[0013] Figure 1 It is the main view of the utility model;

[0014] Figure 2 It is a three-dimensional structural diagram of the utility model. DETAILED DESCRIPTION

[0015] like Figure 1-2 As shown, a quartz support for hydrothermal reaction includes a main body 1 that can be placed in a hydrothermal reaction environment. The main body 1 is made of quartz material as a whole.

[0016] The main body 1 comprises a pair of longitudinally spaced side panels 2. A set of parallel support panels 3 are fixedly connected between the side panels 2, with the spacing between adjacent support panels 3 being the same as that between the upper and lower support panels 3. A small rectangular sample placement slot 4 is provided on the top surface of each support panel 3.

[0017] Because the upper and lower support plates are parallel to ensure structural uniformity and symmetry, the main body forms a stable frame structure. The uppermost support plate 3 is spaced a certain distance from the top surface of the support plate 3. The lowermost support plate 3 is spaced a certain distance from the bottom surface of the support plate 3.

[0018] The main body is made of quartz material to ensure chemical stability and mechanical strength under high temperature and high pressure conditions. The use of quartz material not only provides high temperature and corrosion resistance, but also ensures matching of thermal expansion coefficients between components, thereby maintaining structural integrity during the hydrothermal reaction process.

[0019] An integrally formed lifting lug 2a is provided at the top of each side plate 2 to facilitate connection of a lifting device to the main body, thereby steadily lifting the main body and taking it out of or putting it into the reactor.

[0020] The application operation process of the quartz support of the utility model in the hydrothermal reaction is as follows:

[0021] First, the substrate material to be reacted is precisely placed in groove 3 on support plate 2. Once the substrate material is securely positioned, the entire quartz support is placed vertically into a hydrothermal reactor. Once the support is positioned, the reaction is initiated and conducted according to predetermined hydrothermal reaction conditions, such as temperature, pressure, and time. After the reaction is complete, the quartz support is removed from the reactor, and the reacted substrate material is removed from groove 3 for subsequent cleaning, analysis, and characterization.

[0022] Through this process, the quartz support of this utility model not only simplifies the hydrothermal reaction process but also, through its unique design, improves the efficiency of the hydrothermal reaction and the uniformity of the reaction products. Furthermore, the high-temperature and corrosion-resistant properties of the quartz material ensure the stability and durability of the support during the hydrothermal reaction, making it suitable for a variety of chemical synthesis and material preparation processes.

Claims

1. A quartz support for hydrothermal reaction, characterized in that: The invention comprises a main body (1), wherein the main body (1) comprises a pair of side plates (2) spaced a certain distance apart and distributed longitudinally, a group of support plates (3) distributed in parallel are distributed between the side plates (2), and a small sample placement groove (4) is provided on the upper surface of each support plate (3); the spacing between two adjacent support plates (3) is the same; and an integrally formed hanging ear (2a) is provided on the top of each support plate (3).

2. The quartz support for hydrothermal reaction according to claim 1, characterized in that: The shapes and areas of the small sample placement grooves (4) on the various support plates (3) may be the same or different.

3. The quartz support for hydrothermal reaction according to claim 1, characterized in that: The main body (1) is made of quartz material.