Device for measuring oil content of shale oil

By using a tumbler to turn the material and a cooling water circulation system in the shale oil content device, the problem of uneven sample heating was solved, resulting in more stable and accurate shale oil content determination and reduced operating costs.

CN224066745UActive Publication Date: 2026-03-31SOUTHWEST PETROLEUM UNIV
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Patent Information

Authority / Receiving Office
CN · China
Patent Type
Utility models(China)
Current Assignee / Owner
Filing Date
2025-04-22
Publication Date
2026-03-31

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Abstract

The utility model discloses a device for measuring the oil content of shale oil, which comprises a box body, the upper end of the box body is fixedly connected with a detector, the lower end of the detector is fixedly connected with an air pipe, the lower end of the air pipe is provided with a collecting box, a water pipe is sleeved outside the air pipe in a sealing manner, and the lower end of the water pipe is fixedly connected with a water flow pipe. A water pipe and a heat conduction box are hermetically connected to the water flow pipe, a heat conduction plate is fixedly connected to one side of the heat conduction box, a heat conduction block is fixedly connected to the interior of the heat conduction plate, heat dissipation strips are fixedly connected to the other side of the heat conduction plate, and a cooling box is arranged at the lower end of the heat conduction box. By means of the structure, cooling water in the water pipe can cool gas in the gas pipe to enable the gas to be condensed into water, the water flows to the collection box below through the gas pipe, collection is convenient, the cooling water can be reused through cooling circulation, and therefore the detected gas can be collected, experimental data are not affected, and the accuracy of an experiment is ensured.
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Description

Technical Field

[0001] This utility model relates to the field of shale oil content determination technology, and in particular to a device for determining shale oil content. Background Technology

[0002] Shale oil content is a core parameter for evaluating reservoir economics and development potential. Thermal detection, as one of the mainstream methods, involves programmed temperature rise to crack hydrocarbons and detect the amount of oil and gas released. It is widely used in geological exploration and laboratory analysis. However, clay minerals and organic matter in shale may undergo secondary reactions at high temperatures, causing the measured oil content to deviate from the true value. Parameters such as heating rate and carrier gas flow rate vary greatly among different equipment.

[0003] The patent application CN212228784U discloses a device for determining the oil content of shale oil. By setting an annular groove, and further setting it to be an inclined annular groove, it can quickly collect the condensate generated in the aluminum still and prevent it from flowing back, thereby effectively shortening the dry distillation time, improving the dry distillation efficiency, and saving more energy.

[0004] Traditional heating methods have temperature gradients, and uneven heating of samples can cause premature pyrolysis at the edges while the reaction in the center is delayed. Local overheating may trigger coking side reactions, requiring higher fuel input to maintain the same operating temperature, which directly increases operating costs. Reducing heat loss may also cause local low-temperature zones, resulting in incomplete combustion. Temperature fluctuations affect the stability of the detection. Utility Model Content

[0005] The purpose of this invention is to provide a device for determining the oil content of shale oil. By slowly turning the material in the combustion chamber with a shovel, the material can be burned more evenly and completely, improving the stability of the experiment and reducing labor costs.

[0006] To achieve the above objectives, a device for determining the oil content of shale oil is provided, comprising a housing, a protective shell fixedly connected to the upper end of the housing, an insulation layer fixedly connected inside the protective shell, a heating base fixedly connected to the bottom of the protective shell, a combustion chamber disposed at the upper end of the insulation layer, a fixing ring fixedly connected inside the combustion chamber, a tilting spade fixedly connected to the upper end of the fixing ring, a transmission column fixedly connected to the lower end of the fixing ring, a detector fixedly connected to the upper end of the housing, an air pipe fixedly connected to the lower end of the detector, a collection box disposed at the lower end of the air pipe, a water pipe sealed to the outside of the air pipe, a water flow pipe fixedly connected to the lower end of the water pipe, a water pipe and a heat conduction box sealed to the water flow pipe, a heat conduction plate fixedly connected to one side of the heat conduction box, a heat conduction block fixedly connected inside the heat conduction plate, a heat dissipation strip fixedly connected to the other side of the heat conduction plate, a cooling box disposed at the lower end of the heat conduction box, and a heat dissipation plate disposed inside the cooling box.

[0007] According to the device for determining the oil content of shale oil, the upper end of the protective shell is provided with a cover, the upper end of the cover is fixedly connected with a handle, the lower end of the box is fixedly connected with a base, one side of the box is movably fitted with an opening and closing port, and the other side of the box is fixedly connected with a No. 1 fan.

[0008] According to the device for determining the oil content of shale oil, a controller is fixedly connected to the upper end of the housing.

[0009] According to the device for determining the oil content of shale oil, two limiting strips are symmetrically opened on the lower edge of the cover. An air pipe is fixedly connected inside the cover. An air inlet is fixedly connected to one side of the air pipe. A sealing block is provided on the other side of the air pipe. An air pipe is fixedly connected to the other side of the sealing block. A detector is fixedly connected to the other side of the air pipe.

[0010] According to the device for determining the oil content of shale oil, a No. 1 sealing strip is provided on both sides of the upper end of the combustion chamber, a No. 2 sealing strip is fixedly connected to the outer end of the combustion chamber, and a No. 1 sealing strip is provided at the lower end of the No. 2 sealing strip.

[0011] According to the device for determining the oil content of shale oil, a drive shaft is movably mounted on the lower end of the drive column, and a No. 1 motor is fixedly connected to the lower end of the drive shaft.

[0012] According to the device for determining the oil content of shale oil, a sealing ring is fixedly connected to the upper end of the heat-conducting box, a water pipe is fixedly connected inside the sealing ring, a heat dissipation strip is fixedly connected to one side of the heat-conducting plate, and a second fan is fixedly connected to the other side of the heat dissipation strip.

[0013] According to the device for determining the oil content of shale oil, a water flow pipe is fixedly connected to the upper end of one side of the cooling box, a water pump is fixedly connected to the upper end of the water flow pipe, a second motor is fixedly connected to the other side of the water pump, and a water flow pipe is fixedly connected to the upper end of the water pump.

[0014] Beneficial effects:

[0015] 1. A protective shell is fixedly connected to the upper part of the chamber. An insulation layer is fixedly connected inside the protective shell. A heating base is fixedly connected to the bottom of the protective shell. A combustion chamber is set at the upper end of the insulation layer. A fixing ring is fixedly connected inside the combustion chamber. A flipping spatula is fixedly connected to the upper end of the fixing ring. During the combustion process, the material in the combustion chamber can be slowly turned over by the flipping spatula, which can make it burn more evenly and completely, improve the stability of the experiment, and reduce labor costs.

[0016] 2. A gas tube is fixedly connected to the lower end of the detector. A collection box is installed at the lower end of the gas tube. A water pipe is sealed outside the gas tube. A water flow pipe is fixedly connected to the lower end of the water pipe. The water flow pipe is sealed to a water pipe and a heat conduction box. A heat conduction plate is fixedly connected to one side of the heat conduction box, and a heat dissipation strip is fixedly connected to the other side of the heat conduction plate. A cooling box is installed at the lower end of the heat conduction box. The cooling water inside the water pipe can cool the gas inside the gas tube, causing the gas to condense into water. The water flows through the gas tube to the collection box below for easy collection. The cooling water can be reused through cooling circulation. In this way, the gas after detection can be collected without affecting the experimental data and ensuring the accuracy of the experiment.

[0017] Additional aspects and advantages of this invention will be set forth in part in the description which follows, and in part will be obvious from the description, or may be learned by practice of the invention. Attached Figure Description

[0018] The present invention will be further described below with reference to the accompanying drawings and embodiments;

[0019] Figure 1 This is a perspective view of a device for determining the oil content of shale oil proposed in this utility model;

[0020] Figure 2 This is a cross-sectional view of a device for determining the oil content of shale oil proposed in this utility model;

[0021] Figure 3 This is a perspective view of a shovel used in a device for determining the oil content of shale oil according to the present invention.

[0022] Figure 4 This is a perspective view of a heat-conducting box for a device used to determine the oil content of shale oil according to the present invention;

[0023] Figure 5 This is a perspective view of a cooling box for a device used to determine the oil content of shale oil according to the present invention.

[0024] Figure 6 The present utility model proposes Figure 2 Enlarged view of point A in the middle.

[0025] Legend:

[0026] 1. Handle; 2. Cover; 3. Protective shell; 4. Fixing ring; 5. Box body; 6. Base; 7. Opening / closing port; 8. Air pipe; 9. Detector; 10. Controller; 11. Fan No. 1; 12. Limiting strip; 13. Combustion chamber; 14. Insulation layer; 15. Heating seat; 16. Motor No. 1; 17. Air inlet; 18. Water pipe; 19. Motor No. 2; 20. Water pump; 21. Water flow pipe; 22. Heat conduction block; 23. Heat conduction box; 24. Cooling box; 25. Heat dissipation plate; 26. Drive shaft; 27. Drive column; 28. Sealing block; 29. ​​Tilting spade; 30. Sealing ring; 31. Heat conduction plate; 32. Fan No. 2; 33. Heat dissipation strip; 34. Sealing strip No. 1; 35. Sealing strip No. 2; 36. Collection box. Detailed Implementation

[0027] This section will describe in detail the specific embodiments of the present utility model. The preferred embodiments of the present utility model are shown in the accompanying drawings. The purpose of the drawings is to supplement the textual description with graphics, so that people can intuitively and vividly understand each technical feature and the overall technical solution of the present utility model, but they should not be construed as limiting the scope of protection of the present utility model.

[0028] Reference Figure 1-6 This utility model discloses a device for determining the oil content of shale oil, comprising a housing 5, a protective shell 3 fixedly connected to the upper end of the housing 5, an insulation layer 14 fixedly connected inside the protective shell 3, a heating base 15 fixedly connected to the bottom of the protective shell 3, a combustion chamber 13 disposed at the upper end of the insulation layer 14, a fixing ring 4 fixedly connected inside the combustion chamber 13, a flipping shovel 29 fixedly connected to the upper end of the fixing ring 4, a transmission column 27 fixedly connected to the lower end of the fixing ring 4, and a detector 9 fixedly connected to the upper end of the housing 5. An air pipe 8 is fixedly connected to the lower end of the air pipe 8, and a collection box 36 is provided at the lower end of the air pipe 8. A water pipe 18 is sealed to the outside of the air pipe 8. A water flow pipe 21 is fixedly connected to the lower end of the water pipe 18. The water flow pipe 21 is sealed to the water pipe 18 and the heat conduction box 23. A heat conduction plate 31 is fixedly connected to one side of the heat conduction box 23. A heat conduction block 22 is fixedly connected inside the heat conduction plate 31. A heat dissipation strip 33 is fixedly connected to the other side of the heat conduction plate 31. A cooling box 24 is provided at the lower end of the heat conduction box 23. A heat dissipation plate 25 is provided inside the cooling box 24.

[0029] Specifically: the protective shell 3 protects the internal insulation layer 14; the lower heating seat 15 heats the combustion chamber 13, which burns materials; the fixing ring 4 is used to fix the operation of the tipper 29 and the lower transmission column 27; the detector 9 detects the gas generated during combustion in the combustion chamber 13; the gas pipe 8 connects the detector 9 and the collection box 36; the outer end of the gas pipe 8 is fitted with a water pipe 18 to reduce the temperature of the gas pipe 8; the water pipe 21 leads the cooling water inside the upper water pipe 18 into the lower heat conduction box 23; the heat conduction plate 31 can conduct the temperature of the internal cooling water to the heat conduction block 22; the heat dissipation strip 33 increases the heat dissipation area; the cooling box 24 can collect the cooling water flowing down from the upper heat conduction box 23; and the heat dissipation plate 25 can better transfer the heat inside the cooling box 24.

[0030] The protective shell 3 has a cover 2 at the top, and a handle 1 is fixedly connected to the top of the cover 2. The bottom of the box 5 is fixedly connected to the base 6. The box 5 has an opening 7 that is movably fitted on one side, and a fan 11 is fixedly connected to the other side of the box 5.

[0031] Specifically: handle 1 can better lift the cover 2, base 6 is for fixing the box 5, opening 7 can take out the internal collection box 36, and fan 11 is for cooling the inside of the box 5.

[0032] A controller 10 is fixedly connected to the upper end of the housing 5.

[0033] Specifically: Controller 10 is used to control the entire instrument.

[0034] Two limiting strips 12 are symmetrically opened on the lower edge of the cover 2. An air pipe 8 is fixedly connected inside the cover 2. An air inlet 17 is fixedly connected to one side of the air pipe 8. A sealing block 28 is provided on the other side of the air pipe 8. An air pipe 8 is fixedly connected to the other side of the sealing block 28. A detector 9 is fixedly connected to the other side of the air pipe 8.

[0035] Specifically: the limiting strip 12 is for the cover 2 to be closed more accurately, the gas pipe 8 inside the cover 2 is for the gas to be discharged from the combustion chamber 13, the sealing block 28 is for the gas to be prevented from leaking, and the gas pipe 8 on one side is for the gas connected inside the cover 2 to the detector 9 for detection.

[0036] A first sealing strip 34 is provided on both sides of the upper edge of the combustion chamber 13, and a second sealing strip 35 is fixedly connected to the outer end of the combustion chamber 13. A first sealing strip 34 is provided at the lower end of the second sealing strip 35.

[0037] Specifically: the first sealing strip 34 can retain the gas in the combustion chamber 13, and the second sealing strip 35 works in conjunction with the first sealing strip 34 to seal the combustion chamber 13 so as not to lose the external temperature.

[0038] A drive shaft 26 is movably mounted on the lower end of the drive column 27, and a No. 1 motor 16 is fixedly connected to the lower end of the drive shaft 26.

[0039] Specifically: The output end of motor 16 is fixedly connected to drive shaft 26, and the rotation of drive shaft 26 can provide power to drive column 27.

[0040] A sealing ring 30 is fixedly connected to the upper end of the heat conduction box 23. A water pipe 21 is fixedly connected inside the sealing ring 30. A heat dissipation strip 33 is fixedly connected to one side of the heat conduction plate 31. A second fan 32 is fixedly connected to the other side of the heat dissipation strip 33.

[0041] Specifically: the sealing ring 30 is used to seal the water pipe 21 to the heat conduction box 23, the heat dissipation strip 33 is used to dissipate heat from the heat conduction plate 31, and the second fan 32 is used to dissipate heat from the heat dissipation strip 33.

[0042] A water pipe 21 is fixedly connected to the upper end of one side of the cooling tank 24, and a water pump 20 is fixedly connected to the upper end of the water pipe 21. A second motor 19 is fixedly connected to the other side of the water pump 20, and a water pipe 21 is fixedly connected to the upper end of the water pump 20.

[0043] Specifically: the water pump 20 draws cooling water from the lower cooling tank 24 through the water flow pipe 21 and delivers it to the upper water pipe 18 connected through the water flow pipe 21.

[0044] Working principle: The material is placed into the combustion chamber 13, and the heating seat 15 at the lower end of the combustion chamber 13 heats it. The stirring spatula 29 inside the combustion chamber 13 slowly stirs the material to make the combustion more even. After combustion, the gas from the combustion chamber 13 enters the detector 9 on one side through the gas pipe 8 inside the cover 2. After passing through the detector 9, the gas is connected to the collection box 36 at the lower end through the gas pipe 8. The water pipe 18 outside the gas pipe 8 is filled with cooling water. The cooling water cools the gas pipe 8, causing the gas inside the gas pipe 8 to condense into water. The water flows through the gas pipe 8. The cooling water flows downward into the collection box 36 below and into the heat conduction box 23 at the lower end. The heat in the cooling water is transferred to the heat conduction plate 31 at the rear through the heat conduction block 22. The heat dissipation bar 33 increases the heat dissipation area of ​​the heat conduction plate 31. The second fan 32 dissipates heat from the heat dissipation bar 33. The cooled water enters the cooling box 24 below for storage. The cooling box 24 is equipped with a heat dissipation plate 25 to continue cooling the cooling water. The water pump 20 at the top of the cooling box 24 transports the cooled water into the water pipe 18 on one side for circulation.

[0045] The embodiments of the present utility model have been described in detail above with reference to the accompanying drawings. However, the present utility model is not limited to the above embodiments. Within the scope of knowledge possessed by those skilled in the art, various changes can be made without departing from the spirit of the present utility model.

Claims

1. A device for determining oil content of shale oil comprising a housing (5) characterised in that: The upper end of the box (5) is fixedly connected with a protective shell (3), the inside of the protective shell (3) is fixedly connected with a heat preservation layer (14), the bottom of the protective shell (3) is fixedly connected with a heating seat (15), the upper end of the heat preservation layer (14) is provided with a combustion chamber (13), the inside of the combustion chamber (13) is fixedly connected with a fixed ring (4), the upper end of the fixed ring (4) is fixedly connected with a turning shovel (29), the lower end of the fixed ring (4) is fixedly connected with a transmission column (27), the upper end of the box (5) is fixedly connected with a detector (9), the lower end of the detector (9) is fixedly connected with an air pipe (8), the lower end of the air pipe (8) is provided with a collection box (36), the outside of the air pipe (8) is sealedly sleeved with a water pipe (18), the lower end of the water pipe (18) is fixedly connected with a water flow pipe (21), the water flow pipe (21) is sealedly connected with the water pipe (18) and a heat conduction box (23), one side of the heat conduction box (23) is fixedly connected with a heat conduction plate (31), the inside of the heat conduction plate (31) is fixedly connected with a heat conduction block (22), the other side of the heat conduction plate (31) is fixedly connected with a heat dissipation strip (33), the lower end of the heat conduction box (23) is provided with a cooling box (24), the inside of the cooling box (24) is provided with a heat dissipation plate (25).

2. The device for determining oil content of shale oil according to claim 1, wherein, The upper end of the protective shell (3) is provided with a cover (2), the upper end of the cover (2) is fixedly connected with a handle (1), the lower end of the box (5) is fixedly connected with a base (6), one side of the box (5) is movably sleeved with an opening and closing opening (7), the other side of the box (5) is fixedly connected with a first fan (11).

3. The device for determining oil content of shale oil according to claim 1, wherein, The upper end of the box (5) is fixedly connected with a controller (10).

4. The device for determining oil content of shale oil of claim 2, wherein, The lower end of the cover (2) is symmetrically provided with two limiting strips (12), the inside of the cover (2) is fixedly connected with an air pipe (8), one side of the air pipe (8) is fixedly connected with an air inlet (17), the other side of the air pipe (8) is provided with a sealing block (28), the other side of the sealing block (28) is fixedly connected with the air pipe (8), the other side of the air pipe (8) is fixedly connected with a detector (9).

5. The device for determining oil content of shale oil of claim 1, wherein, The upper end of the combustion chamber (13) is provided with a first sealing strip (34) on both sides, the outer end of the combustion chamber (13) is fixedly connected with a second sealing strip (35), the lower end of the second sealing strip (35) is provided with a first sealing strip (34).

6. The device for determining oil content of shale oil of claim 1, wherein, The lower end of the transmission column (27) is movably sleeved with a transmission shaft (26), the lower end of the transmission shaft (26) is fixedly connected with a first motor (16).

7. The device for determining oil content of shale oil of claim 1, wherein, The upper end of the heat conduction box (23) is fixedly connected with a sealing ring (30), the inside of the sealing ring (30) is fixedly connected with a water flow pipe (21), one side of the heat conduction plate (31) is fixedly connected with a heat dissipation strip (33), the other side of the heat dissipation strip (33) is fixedly connected with a second fan (32).

8. The device for determining oil content of shale oil of claim 1, wherein, One side of the upper end of the cooling box (24) is fixedly connected with a water flow pipe (21), the upper end of the water flow pipe (21) is fixedly connected with a water pump (20), the other side of the water pump (20) is fixedly connected with a second motor (19), the upper end of the water pump (20) is fixedly connected with a water flow pipe (21).

Citation Information

Patent Citations

  • Device for measuring oil content of oil shale

    CN212228784U