Catalyst gas modification production device

By introducing an intermittent atmosphere rotary kiln and an inert gas conveying system into the catalyst gas modification production unit, the problem of limited catalyst loading was solved, and uniform contact and heating of the catalyst and inert gas were achieved, thereby improving modification efficiency and safety.

CN224086761UActive Publication Date: 2026-04-07YUEYANG JUCHENG CHEM CO LTD
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Patent Information

Authority / Receiving Office
CN · China
Patent Type
Utility models(China)
Current Assignee / Owner
Filing Date
2025-02-05
Publication Date
2026-04-07

AI Technical Summary

Technical Problem

Traditional catalyst gas modification production equipment has a limited catalyst loading capacity, which results in the bottom catalyst not being able to fully react with the inert gas, uneven heating, and the inability to achieve large-scale catalyst gas modification, leading to low modification efficiency.

Method used

An intermittent atmosphere rotary kiln combined with an inert gas conveying device is adopted. The catalyst is tumbled by a rotating disc, and a turning plate and nozzles are set in the kiln to increase the contact area and efficiency between the catalyst and the inert gas. Temperature is monitored by thermocouples, and a micro pressure gauge and pressure relief valve are installed in the exhaust pipe to ensure stability and safety. The shell is equipped with a heat insulation layer and cooling exhaust vents to control temperature and heat.

Benefits of technology

This method achieves uniform contact between the catalyst and the inert gas, resulting in uniform heating, increased catalyst loading and modification reaction effect, ensured the stability and safety of the modification process, and improved modification efficiency.

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Abstract

The utility model discloses a catalyst gas modification production device, which relates to the technical field of catalyst gas modification and comprises a shell, rotating discs are respectively arranged at two ends of the shell, an intermittent atmosphere rotary kiln is transversely arranged in the shell in a penetrating manner, and two ends of the intermittent atmosphere rotary kiln are respectively arranged on the rotating discs at two ends; an exhaust pipe is arranged at the other end of the intermittent atmosphere rotary kiln; and the inert gas conveying device is communicated with the gas inlet pipe. Compared with an existing vertical gas modification production device, the device has the advantages that a catalyst can continuously roll in the intermittent atmosphere rotary kiln and is in full contact with inert gas, so that the contact area and efficiency of the catalyst and the inert gas are effectively increased, and uniform heating and reaction of the catalyst are realized; and the device can effectively improve the loading capacity of the catalyst, avoids the situation that the catalyst pressed at the bottom cannot be fully heated and react, and effectively improves the modification reaction effect and efficiency of the catalyst.
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Description

TECHNICAL FIELD

[0001] The utility model relates to catalyst gas modification technical field, concretely relates to a catalyst gas modification production device. BACKGROUND

[0002] Catalyst gas modification has a wide application prospect in modern industry, and its main purpose is to improve its catalytic activity, selectivity, stability and other properties by changing the surface properties and structure of the catalyst, so as to optimize the chemical reaction process, improve production efficiency, reduce cost and meet environmental protection requirements.

[0003] In the related art, the traditional catalyst gas modification production device is usually vertically arranged, but the loading capacity of the device for loading catalyst is limited, and if the loading capacity of the catalyst is large, the catalyst accumulated in the middle and bottom cannot be fully reacted with inert gas, and the heating is uneven, so that the gas modification operation of a large amount of catalyst cannot be realized, and the catalyst needs to be modified in batches, which reduces the catalyst modification efficiency.

[0004] Therefore, there is an urgent need for a catalyst gas modification production device that can meet the larger loading capacity of the catalyst and improve the catalyst modification reaction effect. UTILITY MODEL CONTENT

[0005] The utility model aims at providing a catalyst gas modification production device to solve at least one aspect of the problems and defects in the above background technology.

[0006] To achieve the above-mentioned purpose, the utility model provides the following technical scheme:

[0007] A catalyst gas modification production device, comprising a shell, the shell is provided with a rotating disc at both ends,

[0008] The shell is provided with an intermittent atmosphere rotary kiln transversely, and the both ends of the intermittent atmosphere rotary kiln are arranged on the rotating discs at both ends;

[0009] The intermittent atmosphere rotary kiln is provided with an air inlet pipe at one end and an air outlet pipe at the other end;

[0010] An inert gas conveying device, which is in communication with the air inlet pipe.

[0011] The catalyst gas modification production device according to the present scheme has at least the following technical effects:

[0012] By setting the intermittent atmosphere rotary kiln in the catalyst gas modification production device, and the intermittent atmosphere rotary kiln rotates through the rotating disc, and the inert gas conveying device is used to convey the inert gas into the intermittent atmosphere rotary kiln, the catalyst in the intermittent atmosphere rotary kiln can be modified; compared with the existing vertical gas modification production device, the catalyst can rotate with the intermittent atmosphere rotary kiln, so that the catalyst can continuously tumble in the intermittent atmosphere rotary kiln, and fully contact with the inert gas, thereby effectively increasing the contact area and efficiency of the catalyst and the inert gas, so that the catalyst is uniformly heated and reacted; and the device can effectively improve the loading capacity of the catalyst, and avoid that the catalyst loaded at the bottom cannot be fully heated and reacted when the loading capacity of the catalyst in the vertical gas modification production device is large, thereby effectively improving the catalyst modification reaction effect and efficiency.

[0013] As a further scheme of the present application, the gas inlet pipe extends into the intermittent atmosphere rotary kiln, and a plurality of nozzles are arranged at the free end of the gas inlet pipe.

[0014] Since the gas inlet pipe extends into the intermittent atmosphere rotary kiln, and a plurality of nozzles are arranged at the free end of the gas inlet pipe, the inert gas can be uniformly sprayed into each area in the intermittent atmosphere rotary kiln, so that the inert gas is uniformly distributed in the whole kiln, and the concentration of the inert gas in some areas in the kiln is prevented from being too high or too low, thereby ensuring that the catalyst and the inert gas are more uniformly contacted, and the modification effect of the catalyst is improved.

[0015] As a further scheme of the present application, a plurality of material turning plates are uniformly arranged along the inner side wall of the intermittent atmosphere rotary kiln in the circumferential direction.

[0016] By uniformly arranging a plurality of material turning plates along the inner side wall of the intermittent atmosphere rotary kiln in the circumferential direction, the material turning plates are driven to rotate when the intermittent atmosphere rotary kiln rotates, so that the material turning plates continuously turn the catalyst in the intermittent atmosphere rotary kiln, thereby ensuring that the catalyst can be fully contacted with the inert gas, and the combination reaction of the catalyst and the inert gas is ensured, and the modification effect of the catalyst is improved.

[0017] As a further scheme of the present application, the free end of the material turning plate is provided with a bending portion.

[0018] Since the free end of the material turning plate is provided with a bending portion, the catalyst can be turned to a higher height through the bending portion of the free end of the material turning plate in the process of turning the catalyst, the falling time of the catalyst is increased, the catalyst can be better contacted with the inert gas, the combination reaction of the catalyst and the inert gas is further ensured, and the modification effect of the catalyst is improved.

[0019] As a further scheme of the present application, the intermittent atmosphere rotary kiln is provided with a temperature measuring thermocouple at one end close to the exhaust pipe.

[0020] By setting the temperature measuring thermocouple on one end of the intermittent atmosphere rotary kiln close to the exhaust pipe, the temperature in the intermittent atmosphere rotary kiln can be monitored in real time, and the heating system can be adjusted according to accurate temperature data, so that the temperature in the kiln is kept within a predetermined process range, the catalyst is uniformly heated in the kiln, local overheating or insufficient heating of the catalyst is avoided, and the catalyst modification effect is ensured.

[0021] As a further scheme of the utility model: the exhaust pipe is provided with a micro-pressure gauge.

[0022] Because the micro-pressure gauge is arranged on the exhaust pipe, the pressure in the exhaust pipe and the flow of gas in the exhaust pipe can be monitored in real time, so that the gas flow is ensured, and blockage or uneven gas flow is prevented; and the resistance problem in the gas flow can be found and solved in time, so that the stability and efficiency of the catalyst modification process are ensured.

[0023] As a further scheme of the utility model: the exhaust pipe is provided with a pressure relief valve.

[0024] By arranging the pressure relief valve on the exhaust pipe, when the pressure in the exhaust pipe exceeds the set value, the excess pressure in the kiln can be released by opening the pressure relief valve, so that the intermittent atmosphere rotary kiln is prevented from being damaged due to overpressure, the pressure stability in the intermittent atmosphere rotary kiln is ensured, and the safety and reliability of the catalyst modification process are effectively improved.

[0025] As a further scheme of the utility model: a heat preservation layer is arranged along the inner side wall of the shell.

[0026] Because the heat preservation layer is arranged along the inner side wall of the shell, the heat transfer from the inside of the intermittent atmosphere rotary kiln to the outside can be effectively reduced, the heat loss is reduced, the energy utilization efficiency is improved, the uniformity of the temperature in the shell is maintained, the temperature fluctuation is reduced, and the catalyst modification process is ensured to be carried out under stable temperature conditions.

[0027] As a further scheme of the utility model: cooling exhaust ports are arranged at both ends of the top of the shell.

[0028] By arranging the cooling exhaust ports at both ends of the top of the shell, uniform cooling of the inside of the shell can be achieved, the cooling efficiency is improved, the pressure rise in the intermittent atmosphere rotary kiln due to heat accumulation is prevented, and by promoting air circulation, the excess heat in the inside of the shell can be reduced, and the heat consistency and stability of the catalyst modification process are ensured. BRIEF DESCRIPTION OF DRAWINGS

[0029] In order to facilitate those skilled in the art to understand, the utility model will be further described below in combination with the drawings.

[0030] Figure 1It is a kind of catalyst gas modification production device main view structure schematic diagram;

[0031] Figure 2 It is a kind of catalyst gas modification production device side view partial structure schematic diagram.

[0032] Reference signs:

[0033] 1, shell;2, rotating disc;3, intermittent atmosphere rotary kiln;31, air inlet pipe;311, nozzle;32, exhaust pipe;33, turning plate;331, bending part;4, inert gas conveying device;5, temperature measuring thermocouple;6, micro-pressure gauge;7, pressure relief valve;8, heat preservation layer;9, cooling exhaust port. DETAILED DESCRIPTION

[0034] The embodiments of the present application are described in detail below, and examples of the embodiments are shown in the drawings, wherein the same or similar reference signs represent the same or similar elements or elements having the same or similar functions throughout. The embodiments described below by referring to the drawings are exemplary and are only used to explain the present application, and cannot be understood as a limitation of the present application.

[0035] In the description of the present application, it should be understood that, if the orientation description, such as the orientation or position relationship indicated by up, down, front, back, left, right, etc. is based on the orientation or position relationship shown in the drawings, and is only for the convenience of describing the present application and simplifying the description, and therefore cannot be understood as a limitation of the present application.

[0036] In the description of the present application, the meaning of several is one or more, and the meaning of multiple is more than two, greater than, less than, more than, etc. are not included in the number, and above, below, etc. are included in the number. If it is described as first, second, it is only used to distinguish the technical features for the purpose, and cannot be understood as indicating or implying the relative importance or implicitly indicating the number of indicated technical features or implicitly indicating the sequence of indicated technical features.

[0037] In the description of the present application, unless otherwise explicitly limited, the words such as setting, installing, connecting, etc. should be understood in a broad sense, and the person skilled in the art can reasonably determine the specific meaning of the above words in the present application according to the specific content of the technical scheme.

[0038] In order to make the purpose, technical scheme and advantages of the utility model clearer and more apparent, the utility model will be further described in detail below in combination with the drawings and examples. It should be understood that the specific examples described herein are only used to explain the utility model and are not used to limit the utility model, that is, the described examples are only a part of the examples of the utility model, but not all the examples. The components of the utility model examples described and shown in the drawings herein can be arranged and designed in various different configurations.

[0039] Therefore, the following detailed description of the embodiments of the utility model provided in the drawings is not intended to limit the scope of the claimed utility model, but only represents selected embodiments of the utility model. Based on the embodiments of the utility model, all other embodiments obtained by those skilled in the art without creative labor are within the scope of protection of the utility model.

[0040] As Figure 1 and Figure 2 The utility model example shows a kind of catalyst gas modification production device, including shell 1, shell 1 two ends are respectively provided with rotary disc 2, shell 1 is transversely provided with intermittent atmosphere rotary kiln 3, intermittent atmosphere rotary kiln 3 two ends are respectively arranged on two end rotary disc 2;Intermittent atmosphere rotary kiln 3 one end is provided with air inlet pipe 31, the other end is provided with exhaust pipe 32;Inert gas conveying device 4, inert gas conveying device 4 is communicated with air inlet pipe 31.

[0041] Specifically, by being provided with intermittent atmosphere rotary kiln 3 in catalyst gas modification production device, and intermittent atmosphere rotary kiln 3 is rotated by rotary disc 2, while using inert gas conveying device 4 to inert gas is conveyed to intermittent atmosphere rotary kiln 3, catalyst in intermittent atmosphere rotary kiln 3 can be modified operation;Compared with the prior vertical gas modification production device, catalyst can be rotated with intermittent atmosphere rotary kiln 3 in intermittent atmosphere rotary kiln 3, so that catalyst is constantly tumbled in intermittent atmosphere rotary kiln 3, and fully contact with inert gas, effectively increase the contact area and efficiency of catalyst and inert gas, so as to realize the uniform heating and reaction of catalyst;And the device can effectively improve the loading capacity of catalyst, avoid the catalyst loaded in the bottom of vertical gas modification production device when catalyst loading capacity is large, cannot be heated and reacted fully, effectively improve catalyst modification reaction effect and efficiency.

[0042] As Figure 1 Indicated, air inlet pipe 31 extends to intermittent atmosphere rotary kiln 3, and the free end of air inlet pipe 31 is provided with a plurality of nozzles 311.

[0043] Specifically, since the air inlet pipe 31 extends into the intermittent atmosphere rotary kiln 3, the free end of the air inlet pipe 31 is provided with a plurality of nozzles 311, which can uniformly spray inert gas into each area inside the intermittent atmosphere rotary kiln 3, ensuring that the inert gas is uniformly distributed throughout the kiln, avoiding excessive or insufficient concentration of inert gas in some areas of the kiln, thereby ensuring more uniform contact between the catalyst and the inert gas and improving the modification effect of the catalyst.

[0044] As shown in Figure 2 , a plurality of material turning plates 33 are uniformly arranged along the circumference of the inner side wall of the intermittent atmosphere rotary kiln 3.

[0045] Specifically, by uniformly arranging a plurality of material turning plates 33 along the circumference of the inner side wall of the intermittent atmosphere rotary kiln 3, the intermittent atmosphere rotary kiln 3 drives the material turning plates 33 to rotate when it rotates, causing the material turning plates 33 to continuously turn the catalyst inside the intermittent atmosphere rotary kiln 3, so that the catalyst can be fully contacted with the inert gas, ensuring the combination reaction of the catalyst and the inert gas and improving the modification effect of the catalyst.

[0046] Further, the free end of the material turning plate 33 is provided with a bending portion 331.

[0047] Specifically, since the free end of the material turning plate 33 is provided with a bending portion 331, the material turning plate 33 can turn the catalyst to a higher height during the turning process through the bending portion 331 at the free end of the material turning plate 33, increasing the falling time of the catalyst and allowing the catalyst to better contact with the inert gas, further ensuring the combination reaction of the catalyst and the inert gas and improving the modification effect of the catalyst.

[0048] As shown in Figure 1 , the intermittent atmosphere rotary kiln 3 is provided with a temperature measuring thermocouple 5 near one end of the exhaust pipe 32.

[0049] Specifically, by arranging the temperature measuring thermocouple 5 near one end of the exhaust pipe 32 of the intermittent atmosphere rotary kiln 3, the temperature inside the intermittent atmosphere rotary kiln 3 can be monitored in real time, and the heating system can be adjusted according to accurate temperature data to ensure that the temperature inside the kiln remains within the predetermined process range, allowing the catalyst to be uniformly heated in the kiln and avoiding local overheating or insufficient heating of the catalyst, thereby ensuring the modification effect of the catalyst.

[0050] As shown in Figure 1 , a micro-pressure gauge 6 is arranged on the exhaust pipe 32.

[0051] Specifically, since the micro-pressure gauge 6 is arranged on the exhaust pipe, the pressure inside the exhaust pipe 32 and the flow of gas in the exhaust pipe 32 can be monitored in real time, ensuring smooth gas flow and preventing blockage or uneven gas flow; and the resistance problem in the gas flow can be discovered and solved in a timely manner, ensuring the stability and efficiency of the catalyst modification process.

[0052] Further, the exhaust pipe 32 is provided with a pressure relief valve 7.

[0053] Specifically, by providing the pressure relief valve 7 on the exhaust pipe 32, when the pressure in the exhaust pipe 32 exceeds the set value, the excess pressure in the kiln can be released by opening the pressure relief valve 7, preventing the intermittent atmosphere rotary kiln 3 from being damaged due to overpressure, ensuring the pressure stability in the intermittent atmosphere rotary kiln 3, and effectively improving the safety and reliability of the catalyst modification process.

[0054] According to the embodiment of the utility model, the heat preservation layer 8 is arranged along the inner side wall of the shell 1.

[0055] Specifically, since the heat preservation layer 8 is arranged along the inner side wall of the shell 1, the heat transfer from the inside of the intermittent atmosphere rotary kiln 3 to the outside can be effectively reduced, the heat loss is reduced, the energy utilization efficiency is improved, the uniformity of the internal temperature of the shell 1 is maintained, the temperature fluctuation is reduced, and the catalyst modification process is ensured to be carried out under stable temperature conditions.

[0056] Further, the shell 1 is provided with cooling exhaust ports 9 at both ends of the top.

[0057] Specifically, by providing the cooling exhaust ports 9 at both ends of the top of the shell 1, uniform cooling of the inside of the shell 1 can be achieved, the cooling efficiency is improved, the pressure rise in the intermittent atmosphere rotary kiln 3 due to heat accumulation is prevented, and by promoting air circulation, the excess heat in the inside of the shell 1 can be reduced, ensuring the heat consistency and stability of the catalyst modification process.

[0058] The sample was tested by the catalyst gas modification production device, and the results are shown in Table 1:

[0059] Table 1

[0060]

[0061]

[0062] The test was carried out by the catalyst gas modification production device, and the experimental results showed that the stability of temperature control, the optimization of process parameters, the rationality of gas flow and the reliability of equipment operation all reached the expected target.

[0063] The above content is only an example and description of the structure of the utility model, and those skilled in the art can make various modifications or supplements or use similar ways to replace the described specific embodiments, as long as they do not deviate from the structure of the utility model or exceed the scope defined by the present claims, which shall belong to the protection scope of the utility model.

Claims

1. A catalyst gas modification production apparatus, comprising a shell (1), wherein rotating disks (2) are respectively disposed at both ends of the shell (1), characterized in that, An intermittent atmosphere rotary kiln (3) is transversely arranged inside the shell (1), and the two ends of the intermittent atmosphere rotary kiln (3) are respectively arranged on the two end rotating disks (2); The intermittent atmosphere rotary kiln (3) is provided with an air inlet pipe (31) at one end and an exhaust pipe (32) at the other end. An inert gas delivery device (4) is connected to the inlet pipe (31); A number of turning plates (33) are evenly arranged along the inner sidewall of the intermittent atmosphere rotary kiln (3), and the free end of the turning plate (33) is provided with a bent part (331).

2. The catalyst gas modification production apparatus according to claim 1, characterized in that, The air inlet pipe (31) extends into the intermittent atmosphere rotary kiln (3), and a number of nozzles (311) are provided at the free end of the air inlet pipe (31).

3. The catalyst gas modification production apparatus according to claim 1, characterized in that, A thermocouple (5) is provided at one end of the intermittent atmosphere rotary kiln (3) near the exhaust pipe (32).

4. The catalyst gas modification production apparatus according to claim 1, characterized in that, A micro pressure gauge (6) is installed on the exhaust pipe (32).

5. The catalyst gas modification production apparatus according to claim 4, characterized in that, The exhaust pipe (32) is equipped with a pressure relief valve (7).

6. The catalyst gas modification production apparatus according to any one of claims 1 to 5, characterized in that, A heat insulation layer (8) is provided along the inner sidewall of the shell (1).

7. The catalyst gas modification production apparatus according to claim 6, characterized in that, Cooling exhaust vents (9) are provided at both ends of the top of the housing (1).