Atomized liquid based on acidic electrolyzed water, preparation method and method for preparing acidic electrolyzed water

Abstract

The present invention discloses a kind of atomized liquid based on acidic electrolyzed water, preparation method and acidic electrolyzed water preparation method, by electrolyzing salt electrolyte (potassium carbonate) solution, adjusting electrolysis time and electrolysis pressure, producing acidic electrolyzed water with pH value of 2-5 at anode; adding acidic electrolyzed water when allocating electronic atomized liquid, adjusting atomized liquid pH value, reducing pH value of atomized liquid system, weakening irritation and burr sense caused by nicotine, more compliant, better comfort, while acidic electrolyzed water is colorless and tasteless water, will not bring peculiar smell and the addition of water, will not only make mist more compliant, but also bring comfortable moist feeling, user's suction experience is better, less irritation. The manufacturing process is simple, time-consuming, low cost investment, economic and environmental protection; adding atomized liquid is simple to operate, and the quality of atomized liquid, suction experience and comfort can be improved.

Description

Technical Field

[0001] The invention belongs to the technical field of manufacturing tobacco substitutes among human daily necessities, and specifically relates to an atomizing liquid based on acid electrolyzed water, a preparation method and a method for preparing acid electrolyzed water. Background Art

[0002] Nebulizer liquid is a liquid used for atomization inhalation therapy. Depending on the type of inhaled liquid, it has the effects of humidifying the airway, controlling infection, improving ventilation, expectoration and antitussive, etc. Nebulizer inhalation therapy is to use a nebulizer to disperse the liquid medicine into fine droplets, which are inhaled into the respiratory tract through the nose or mouth to achieve the purpose of preventing and treating diseases.

[0003] The nebulizer liquid requires that the active ingredients are water-soluble, non-irritating, non-toxic, and do not cause allergic reactions; the pH value is close to neutral and can adapt to the colloidal osmotic pressure of tissues; and it has good nebulization effect and stability.

[0004] Traditional tobacco has a significant impact on the human body, the environment and the surrounding people. With the development of social culture, economy and residents' living standards, atomizer liquid is further developed and expanded to its application functions as a tobacco substitute.

[0005] Atomizer liquids used as tobacco substitutes usually need to have a certain degree of mist wetness and softness, and be non-irritating, so as to meet the user's requirements for the smoking experience. Atomizer liquids in the prior art usually only focus on the adjustment of taste and aroma, and have no effective means of controlling the pH value and softness of the mist. Therefore, there are defects such as strong irritation, insufficient mist wetness, and insufficient softness. Summary of the invention

[0006] In order to solve the above-mentioned problems existing in the prior art, the purpose of the present invention is to provide an atomized liquid based on acidic electrolyzed water, a preparation method and an acidic electrolyzed water preparation method, wherein the pH value of the atomized liquid is reduced by acidic electrolyzed water, the mist has sufficient wetness and good softness, which can improve the user's suction experience and reduce irritation.

[0007] The technical solution adopted by the present invention is:

[0008] An atomized liquid based on acidic electrolyzed water includes the following components:

[0009] pH adjusting agent, nicotine salt, a first atomizing agent, and a second atomizing agent;

[0010] The proportions of each component by weight are as follows:

[0011]

[0012] The pH regulator is acidic electrolyzed water.

[0013] The first atomizer is propylene glycol.

[0014] The second atomizing agent is glycerol.

[0015] The pH value of the acidic electrolyzed water is 2-5.

[0016] A method for preparing acidic electrolyzed water for the above-mentioned atomized liquid based on acidic electrolyzed water comprises the following steps:

[0017] A1, using food grade potassium carbonate as raw material;

[0018] A2, the electrolysis equipment uses an electrolytic water generator;

[0019] A3, adjust and set the electrolysis time of the electrolyzed water generator;

[0020] A4, electrolyzing food-grade potassium carbonate and collecting acidic electrolyzed water produced by the anode of the electrolyzed water generator;

[0021] A5, membrane filtration, to obtain acidic electrolyzed water with a pH value of 2 to 5.

[0022] A method for preparing the above-mentioned atomized liquid based on acidic electrolyzed water comprises the following steps:

[0023] S1, preparing acidic electrolyzed water;

[0024] S2, weighing 1 to 10 portions of nicotine salt;

[0025] S3, measure 1 to 3 parts of acidic electrolyzed water;

[0026] S4, mixing nicotine salt and acidic electrolyzed water and stirring them evenly;

[0027] S5, adding 50-70 parts of propylene glycol;

[0028] S6, adding 30 to 40 parts of propylene glycol;

[0029] S7, mixing and stirring uniformly to obtain an atomized liquid.

[0030] Furthermore, in step S2, 1 g, 3 g, 5 g or 8 g of nicotine salt is weighed.

[0031] Furthermore, in step S3, 1 g, 1.5 g, 2 g or 2.5 g of acidic electrolyzed water is measured.

[0032] Further, in step S5, 50 g, 55 g, 60 g or 65 g of propylene glycol is weighed;

[0033] Furthermore, in step S6, 30 g, 32 g, 36 g or 40 g of propylene glycol is weighed.

[0034] Finally, the sensory evaluation step is also used for verification, which includes the following:

[0035] S8, sampling the atomized liquid obtained in step S7, and measuring the pH value of the sample;

[0036] S9, organize sensory evaluation team;

[0037] S10, each member of the sensory evaluation team smoked the sample using the lung inhalation method, taking 10 puffs, with 10 seconds between each puff; the sensory evaluation items included five items: throat hit, off-flavor, irritation, smoothness and headiness;

[0038] S11, after an interval of 20 minutes, conduct sensory evaluation of the next sample.

[0039] The beneficial effects of the present invention are:

[0040] A kind of atomizing liquid based on acidic electrolyzed water, preparation method and acidic electrolyzed water preparation method, by electrolyzing salt electrolyte (potassium carbonate) solution, adjusting electrolysis time and electrolysis pressure, acidic electrolyzed water with pH value of 2-5 is produced at the anode; acidic electrolyzed water is added when preparing electronic atomizing liquid, and the pH value of the atomizing liquid is adjusted to reduce the pH value of the atomizing liquid system, reduce the irritation and burr feeling caused by nicotine, and make it smoother and more comfortable. At the same time, acidic electrolyzed water is colorless and odorless water, which will not bring peculiar smell, and the addition of water will not only make the mist smoother, but also bring a comfortable moist feeling, so that the user's suction experience is better and less irritating. The production and manufacturing process is simple, time-consuming, low-cost, economical and environmentally friendly; adding it to the atomizing liquid is simple to operate, and can improve the quality of the atomizing liquid, the suction experience and the comfort. DETAILED DESCRIPTION

[0041] The technical solution of the present invention will be clearly and completely described below in conjunction with the specific embodiments of the present invention. Obviously, the described embodiments are only part of the embodiments of the present invention, not all of the embodiments. All other embodiments obtained by ordinary technicians in this field without creative work are within the scope of protection of the present invention.

[0042] The present invention provides an atomized liquid based on acidic electrolyzed water, a preparation method and an acidic electrolyzed water preparation method. The overall planning scheme is: to provide a new method for preparing an atomized liquid; to make the mist smoother by appropriately lowering the pH value of the atomized liquid, thereby improving the consumer's inhalation experience.

[0043] Acidic electrolyzed water is an acidic water with a pH of 2-5 produced at the anode by electrolyzing a salt electrolyte (potassium carbonate) solution, adjusting the electrolysis time and electrolysis pressure. Its acidic characteristics can be added when preparing electronic atomization liquid to adjust the pH of the atomization liquid, lower the pH of the atomization liquid system, reduce the irritation and burr feeling caused by nicotine, and make it smoother and more comfortable. At the same time, acidic electrolyzed water is colorless and odorless, and will not bring odor. The addition of water will not only make the mist smoother, but also bring a comfortable moist feeling. It makes consumers have a better smoking experience and less irritation.

[0044] 1. Acidic electrolyzed water has acidic characteristics. It is added to the atomizing liquid to adjust the pH of the atomizing liquid and moderately reduce the pH value of the atomizing liquid system, making the mist smoother and moister, and the suction experience better and more comfortable;

[0045] 2. The addition of acidic electrolyzed water will not bring odor or irritation, and it is simple to prepare and low in cost. It is easy to add to the atomized liquid and can improve the quality of the atomized liquid.

[0046] The acidic electrolyzed water produced by electrolyzing potassium carbonate at the anode is added to nicotine salt, propylene glycol, and glycerol to prepare the electronic cigarette atomization liquid. The prepared atomization liquid has no odor, no irritation, is more moist, smooth, and has a better smoking experience. Thus, a preparation method for adding acidic electrolyzed water to nicotine salt atomization liquid to obtain a highly soft new atomization liquid is provided.

[0047] The specific technical solutions are as follows:

[0048] 1. An atomized liquid based on acidic electrolyzed water, comprising the following components:

[0049] pH regulator, nicotine salt, first atomizer and second atomizer; the first atomizer mainly acts as a heat preservation agent, so that the mist is sufficiently moist, the atomization effect is gentler and the atomization effect is good; the second atomizer mainly acts as a lubricant, so that the atomization effect is smoother;

[0050] The proportions of each component by weight are as follows:

[0051]

[0052] Acidic electrolyzed water is used as the pH adjuster.

[0053] The first atomizer, i.e., the moisturizer, is propylene glycol.

[0054] The second atomizer, i.e. the lubricant, is glycerol.

[0055] The pH value of acidic electrolyzed water is 2-5.

[0056] 2. A method for preparing the acidic electrolyzed water for the above-mentioned atomized liquid based on acidic electrolyzed water, comprising the following steps:

[0057] A1, using food grade potassium carbonate as raw material;

[0058] A2, the electrolysis equipment uses an electrolytic water generator;

[0059] A3, adjust and set the electrolysis time of the electrolyzed water generator;

[0060] A4, electrolyze food-grade potassium carbonate and collect the acidic electrolyzed water produced by the anode of the electrolyzed water generator; the chemical expression is:

[0061] Anode: 2H2O→4H + +O2↑+4e - ;

[0062] A5, membrane filtration, obtaining acidic electrolyzed water with a pH value of 2 to 5;

[0063] After being filtered through activated carbon adsorption, it is electrolyzed by an electrolytic water generator.

[0064] 3. A method for preparing the above-mentioned atomized liquid based on acidic electrolyzed water comprises the following steps:

[0065] S1, preparing acidic electrolyzed water;

[0066] S2, weighing 1 to 10 portions of nicotine salt;

[0067] S3, measure 1 to 3 parts of acidic electrolyzed water;

[0068] S4, mixing nicotine salt and acidic electrolyzed water and stirring them uniformly; stirring them by a magnetic stirrer for 3 to 4 hours at room temperature;

[0069] S5, adding 50-70 parts of propylene glycol;

[0070] S6, adding 30 to 40 parts of propylene glycol;

[0071] S7, mixing and stirring uniformly to obtain an atomized liquid.

[0072] Furthermore, in step S2, 1 g, 3 g, 5 g or 8 g of nicotine salt is weighed.

[0073] Furthermore, in step S3, 1 g, 1.5 g, 2 g or 2.5 g of acidic electrolyzed water is measured.

[0074] Further, in step S5, 50 g, 55 g, 60 g or 65 g of propylene glycol is weighed;

[0075] Furthermore, in step S6, 30 g, 32 g, 36 g or 40 g of propylene glycol is weighed.

[0076] Finally, the sensory evaluation step is also used for verification, which includes the following:

[0077] S8, sampling the atomized liquid obtained in step S7, and measuring the pH value of the sample;

[0078] S9, organize sensory evaluation team;

[0079] S10, each member of the sensory evaluation team smoked the sample using the lung inhalation method, taking 10 puffs, with 10 seconds between each puff; the sensory evaluation items included five items: throat hit, off-flavor, irritation, smoothness and headiness;

[0080] S11, after an interval of 20 minutes, conduct sensory evaluation of the next sample.

[0081] Embodiment 1:

[0082] Firstly, food-grade potassium carbonate is used, the electrolysis time is adjusted, and electrolysis is performed by an electrolytic water generator, and alkaline electrolytic water with a pH value of 2 is obtained after membrane filtration for standby use;

[0083] Then weigh 5g of nicotine salt and measure 1g of acidic electrolyzed water.

[0084] Mix nicotine salt and acidic electrolyzed water and stir evenly;

[0085] Then add 59g of propylene glycol and 35g of glycerol in sequence.

[0086] Finally, stir and mix evenly to obtain a small batch sample 1 of about 100 g of atomized liquid based on acidic electrolyzed water.

[0087] Embodiment 2:

[0088] Firstly, food-grade potassium carbonate is used, the electrolysis time is adjusted, and electrolysis is performed by an electrolytic water generator, and alkaline electrolytic water with a pH value of 3 is obtained after membrane filtration for standby use;

[0089] Then weigh 8 g of nicotine salt and measure 2 g of acidic electrolyzed water.

[0090] Mix nicotine salt and acidic electrolyzed water and stir evenly;

[0091] Then add 58g of propylene glycol and 32g of glycerol in sequence.

[0092] Finally, the mixture was stirred and mixed evenly to obtain a small batch sample 2 of about 100 g of atomized liquid based on acidic electrolyzed water.

[0093] Embodiment three:

[0094] Firstly, food-grade potassium carbonate is used, the electrolysis time is adjusted, and electrolysis is performed by an electrolytic water generator, and alkaline electrolytic water with a pH value of 4 is obtained after membrane filtration for standby use;

[0095] Then weigh 10g of nicotine salt and measure 3g of acidic electrolyzed water.

[0096] Mix nicotine salt and acidic electrolyzed water and stir evenly;

[0097] Then add 57g of propylene glycol and 30g of glycerol in sequence.

[0098] Finally, the mixture was stirred and mixed evenly to obtain a small batch sample 3 of about 100 g of atomized liquid based on acidic electrolyzed water.

[0099] Embodiment 4:

[0100] Firstly, food-grade potassium carbonate is used, the electrolysis time is adjusted, and electrolysis is performed by an electrolytic water generator, and alkaline electrolytic water with a pH value of 5 is obtained after membrane filtration for standby use;

[0101] Then weigh 10g of nicotine salt and 0g of acidic electrolyzed water.

[0102] Mix nicotine salt and acidic electrolyzed water and stir evenly;

[0103] Then add 60g of propylene glycol and 30g of glycerol in sequence.

[0104] Finally, the mixture was stirred and mixed evenly to obtain a small batch sample 4 of about 100 g of atomized liquid based on acidic electrolyzed water.

[0105] Example 5: pH value test of atomized liquid based on acidic electrolyzed water;

[0106] The atomized liquid samples of Examples 1 to 4 were taken, and the pH values ​​of the samples of Examples 1 to 4 were tested. The test results are shown in Appendix 1.

[0107] From the test results of the pH value of the atomized liquid samples of Examples 1 to 4, the addition of acidic electrolyzed water reduces the pH value of the atomized liquid. Compared with the electronic atomized liquid without the addition of acidic electrolyzed water, the pH is significantly reduced, the irritation caused by nicotine is reduced, and the mist is smoother.

[0108] Example 6: Sensory evaluation and verification of atomized liquid based on acidic electrolyzed water;

[0109] Take the atomized liquid samples of Examples 1 to 4;

[0110] Organize 20 smoking technicians to form a sensory evaluation team, use atomizers to perform sensory evaluation on the atomized liquid samples of Examples 1 to 4; and give sensory evaluations in an anonymous scoring manner. Among them, each smoking technician uses the lung inhalation method to take 10 puffs of each e-liquid, with an interval of 10 seconds between each puff, and the interval between inhaling different e-liquids is not less than 20 minutes to avoid mutual influence. The sensory evaluation items include 5 items: throat hit, off-flavor, irritation, smoothness, and head feeling. The results are shown in Table 2.

[0111] From the test results: 1. Adding acidic electrolyzed water to the atomizing liquid reduces the pH value of the atomizing liquid system, which can improve the softness of the mist and remove odor; 2. When the amount of acidic electrolyzed water added increases, its softness is enhanced. When the added amount is 2% or more, the mist is the softest and the inhalation experience is good; 3. Using acidic electrolyzed water to add to the atomizing liquid not only reduces the pH value of the system and increases the flexibility of the mist, but also the addition of water makes the mist more moist and more comfortable.

[0112] The present invention is not limited to the above-mentioned optional implementation modes. Anyone can derive other various forms of products under the inspiration of the present invention. However, no matter what changes are made in the shape or structure, all technical solutions that fall within the scope defined by the claims of the present invention fall within the protection scope of the present invention.

[0113] Table 1: pH test results of samples of Examples 1 to 4

[0114] Example Nicotine salt Propylene glycol Glycerol Acidic electrolyzed water pH 1 5 59 35 1 4.17 2 8 58 32 2 4.15 3 10 57 30 3 4.13 4 10 60 30 0 4.60

[0115] Table 2 Sensory evaluation results

[0116] Example Sensory evaluation results 1 Moderate throat hit, no odor, no irritation, smooth, quick onset 2 Moderate throat hit, no odor, no irritation, very smooth, quick to get high 3 Moderate throat hit, no odor, no irritation, very smooth, quick to get high 4 Moderate throat hit, slightly peculiar smell, slightly irritating, relatively smooth, quick to get high

Claims

1. An atomized liquid based on acidic electrolyzed water, characterized in that: Includes the following components: pH adjusting agent, nicotine salt, a first atomizing agent, and a second atomizing agent; The proportions of each component by weight are as follows: The pH regulator is acidic electrolyzed water; The first atomizer is propylene glycol; the second atomizer is glycerol; The acidic electrolyzed water is prepared by the following steps: A1, using food grade potassium carbonate as raw material; A2, the electrolysis equipment uses an electrolytic water generator; A3, adjust and set the electrolysis time of the electrolyzed water generator; A4, electrolyzing food-grade potassium carbonate and collecting acidic electrolyzed water produced by the anode of the electrolyzed water generator; A5, membrane filtration, obtaining acidic electrolyzed water with a pH value of 2 to 5; The steps for preparing the atomized liquid based on acidic electrolyzed water are as follows: S1, preparing acidic electrolyzed water; S2, weighing 1 to 10 portions of nicotine salt; S3, measure 1 to 3 parts of acidic electrolyzed water; S4, mixing nicotine salt and acidic electrolyzed water and stirring them evenly; S5, adding 50 to 70 parts of propylene glycol; S6, adding 30 to 40 parts of propylene glycol; S7, mixing and stirring uniformly to obtain an atomized liquid.

2. A method for preparing acidic electrolyzed water for the atomized liquid based on acidic electrolyzed water according to claim 1, characterized in that: The following steps are included: A1, using food grade potassium carbonate as raw material; A2, the electrolysis equipment uses an electrolytic water generator; A3, adjust and set the electrolysis time of the electrolyzed water generator; A4, electrolyzing food-grade potassium carbonate and collecting acidic electrolyzed water produced by the anode of the electrolyzed water generator; A5, membrane filtration, to obtain acidic electrolyzed water with a pH value of 2 to 5.

3. A method for preparing an atomized liquid based on acidic electrolyzed water according to claim 1, characterized in that: The following steps are included: S1, preparing acidic electrolyzed water; S2, weighing 1 to 10 portions of nicotine salt; S3, measure 1 to 3 parts of acidic electrolyzed water; S4, mixing nicotine salt and acidic electrolyzed water and stirring them evenly; S5, adding 50 to 70 parts of propylene glycol; S6, adding 30 to 40 parts of propylene glycol; S7, mixing and stirring uniformly to obtain an atomized liquid.

4. The method for preparing the atomized liquid based on acidic electrolyzed water according to claim 3, characterized in that: In step S2, 1 g, 3 g, 5 g or 8 g of nicotine salt is weighed.

5. The method for preparing the atomized liquid based on acidic electrolyzed water according to claim 3, characterized in that: In step S3, 1 g, 1.5 g, 2 g or 2.5 g of acidic electrolyzed water is measured.

6. The method for preparing the atomized liquid based on acidic electrolyzed water according to claim 3, characterized in that: In the step S5, 50 g, 55 g, 60 g or 65 g of propylene glycol is weighed; In the step S6, 30 g, 32 g, 36 g or 40 g of propylene glycol is weighed.

7. The method for preparing an atomized liquid based on acidic electrolyzed water according to claim 3, characterized in that: It also includes sensory evaluation verification steps, including the following: S8, sampling the atomized liquid obtained in step S7, and measuring the pH value of the sample; S9, organize sensory evaluation team; S10, each member of the sensory evaluation team smoked the sample using the lung inhalation method, taking 10 puffs, with 10 seconds between each puff; the sensory evaluation items included five items: throat hit, off-flavor, irritation, smoothness and headiness; S11, after an interval of 20 minutes, conduct sensory evaluation of the next sample.

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