The invention discloses a preparation method of high-specific-surface-area, high-dispersion and high-purity nano
calcium carbonate, which comprises the following steps: S1, calcining limestone, digesting the
lime and water in proportion, and screening to remove gravel; s2,
ammonium salt or
ammonia water is added into the obtained
lime slurry, and the
solid content is adjusted; s3, layering the
lime slurry after standing, and then concentrating to obtain concentrated lime
slurry; s4, putting the concentrated lime slurry into a
carbonization tower, and carrying out
carbonization reaction by controlling the temperature, the stirring rate, the
carbon dioxide concentration and the
carbon dioxide flow; s5, when over-
carbonization is achieved, obtaining a nano
calcium carbonate suspension; s6, standing and
settling the suspension, and removing upper-layer water to enable the
solid content to be within a certain range; and S7, adding
stearic acid into the suspension liquid for
surface modification, and carrying out filter pressing,
drying, crushing and sieving on the obtained suspension liquid to obtain the nano
calcium carbonate powder. The method is low in
raw material cost, economical,
environmentally friendly, simple in control step, short in carbonization time, high in production efficiency and convenient for industrialization.