High-efficiency extraction device and extraction process for Yuxiang reactant
By designing an efficient smoke reactant extraction device, including extraction tank, stirring and cooling system, combined with concentration and enzymatic treatment, the problems of uneven extraction and insufficient aroma in the prior art are solved, and the aroma enhancement of high-quality cigarettes is achieved .
Patent Information
- Application Number
- CN202411222305.7
- Authority / Receiving Office
- CN · China
- Patent Type
- Applications(China)
- Current Assignee / Owner
- Filing Date
- 2024-09-02
- Publication Date
- 2024-12-17
- Estimated Expiration
- Not applicable · inactive patent
AI Technical Summary
In the prior art, the Yusy Reactant Extraction Device is not convenient for uniform and efficient heating and cooling and temperature control, resulting in limited extracted aroma compounds, which cannot effectively improve the quality of cigarettes, and traditional processes are difficult to meet the needs of high-quality cigarettes.
An efficient extraction device including extraction tank, filter plate, reciprocating lifting assembly, stirring assembly, heater and cooling cooling assembly was designed. Automatic control is achieved through the PLC controller, combining the concentration tank and enzymatic treatment, and the extraction process is optimized to Increase spice concentration.
It realizes the extraction of Yusmok reactants with distinct sensory characteristics and concentrated fragrance ingredients, which improves the quality and aroma explosiveness of cigarettes and meets the needs of high-quality cigarettes.
Smart Images

Figure CN119138641A_ABST
Abstract
Description
Technical Field
[0001] The invention relates to the technical field of processing and extracting tobacco flavors, and in particular to a high-efficiency extraction device and extraction process for Henan tobacco reactants. Background Art
[0002] Tobacco extract is one of the most important raw materials for flavoring Chinese cigarettes. It is used in huge quantities and has the function of strengthening the characteristic aroma of tobacco and improving the sensory quality of cigarettes. Henan tobacco reactant (i.e. Henan tobacco extract) is an extract from Henan tobacco leaves, which has typical strong aroma characteristics. Adding it to cigarettes can further highlight the roasted sweet aroma and strong aroma, enhance the explosiveness and strength of smoke, and increase the concentration and permeability of smoke. It accounts for a large proportion in the flavoring of products of various cigarette industrial enterprises. By rationally utilizing Henan tobacco extract, cigarette industrial enterprises can alleviate the contradiction of insufficient supply of high-quality tobacco leaf raw materials in Henan to a certain extent.
[0003] However, due to the limitation of non-fine processing, the Henan tobacco extract currently used in cigarette processing is mainly obtained by traditional extraction devices and extraction processes, which is not convenient for uniform and efficient heating reaction, nor is it convenient for fast and efficient cooling and temperature control. In addition, the aroma compounds contained in this Henan tobacco extract are limited, which cannot effectively highlight the style of cigarettes and bring some negative effects to cigarettes. With the continuous development of cigarette formula design and cigarette processing, it cannot meet the needs of high-quality cigarette development to a large extent. Therefore, a Henan tobacco reactant efficient extraction device and extraction process are proposed. Summary of the invention
[0004] In order to overcome the technical defects in the prior art and effectively solve the technical problems in the background technology, the present invention provides the following technical solutions:
[0005] A highly efficient extraction device for reactants from Henan smoke, comprising an extraction tank, a filter screen plate fixedly mounted in the middle of the inner side wall of the extraction tank, a fixed plate fixedly mounted on the upper end of the outer side of the extraction tank, a reciprocating lifting assembly fixedly mounted on the upper surface of the fixed plate, a tank cover corresponding to the upper end opening of the extraction tank fixedly mounted on the inner side end of the reciprocating lifting assembly, a stirring assembly located between the inner side wall of the extraction tank and the upper surface of the filter screen plate fixedly mounted at the center of the bottom of the tank cover, a heater fixedly mounted on the bottom of the extraction tank, and cooling assemblies are respectively arranged on the front, back, left and right sides of the extraction tank;
[0006] The cooling and temperature reduction component comprises a spiral cooling pipe, a water pump 1 and a temporary storage tank, wherein the spiral cooling pipe is fixedly installed at the bottom of the temporary storage tank, the liquid outlet end of the spiral cooling pipe is connected to the liquid inlet end of the temporary storage tank through the water pump 1, and the water pump 1 is fixedly installed on the outside of the temporary storage tank;
[0007] One side of the lower end of the outer side of the extraction tank is fixedly connected to the liquid inlet end of one of the spiral cooling tubes through a liquid outlet pipe 1, the liquid outlet end of one of the temporary storage tanks and the liquid inlet end of the adjacent spiral cooling tube are correspondingly fixedly connected through a connecting pipe, the liquid outlet end on the inner side of the temporary storage tank and the liquid inlet end located below the filter screen in the middle of the extraction tank are correspondingly fixedly connected through a liquid inlet pipe 1, and the lower part of the outer side of the extraction tank and the outer sides of the four temporary storage tanks are respectively fixedly installed with temperature sensors corresponding to their inner cavities.
[0008] As a preferred technical solution of the present invention, the reciprocating lifting assembly includes a fixed frame, a lead screw, a lifting block, a guide rod and a reciprocating motor. The fixed frame is fixedly mounted on the outer side of the upper surface of the fixed plate, the guide rod is fixedly mounted between the top and bottom of the inner walls of the two fixed frames, the lead screw is rotatably connected between the top and bottom of the inner walls of the two fixed frames, the lead screw and the guide rod are parallel to each other, the guide rod is slidably connected to the sliding hole on the side of the lifting block, the lead screw is threadedly connected to the threaded hole on the side of the lifting block, the inner end of the lifting block is fixedly connected to one side of the tank cover, the reciprocating motor is fixedly mounted on the upper surface of the fixed frame, and the output shaft of the fixed frame is fixedly connected to the top end of the lead screw.
[0009] As a preferred technical solution of the present invention, the stirring assembly includes a stirring motor, a stirring shaft and blades, the top end of the stirring shaft is rotatably connected to the center of the bottom of the tank cover through a bearing, the outer side of the stirring shaft is evenly distributed and fixedly installed with blades, the stirring motor is fixedly installed on the upper surface of the tank cover, and the output shaft of the stirring motor is fixedly connected to the top end of the stirring shaft.
[0010] As a preferred technical solution of the present invention, a water pump 2 is fixedly installed on one side of the temporary storage tank close to the extraction tank, and the liquid outlet end inside the temporary storage tank is connected to the outer end of the liquid inlet pipe 1 through the water pump 2, and the inner end of the liquid inlet pipe 1 is connected to the liquid inlet end in the middle of the extraction tank.
[0011] As a preferred technical solution of the present invention, it also includes a concentration tank, the liquid inlet and liquid outlet of the concentration tank are respectively connected to and fixed with water pump three, and are respectively connected to the lower part of the inner cavity of the extraction tank through water pump three and corresponding liquid inlet pipe two and liquid outlet pipe two.
[0012] As a preferred technical solution of the present invention, a PLC controller is fixedly installed on the upper surface of the fixed plate, and the reciprocating motor, stirring motor, temperature sensor, heater, water pump one, water pump two and water pump three are electrically connected to the PLC controller respectively, and the PLC controller is electrically connected to an external power supply.
[0013] A process for extracting a reactant from a smoke from a cigarette, comprising the following steps:
[0014] S1: Weigh a certain mass of tobacco leaf fragments produced in Henan and a solvent, add them into an extraction tank, heat and extract for a period of time, cool and filter after the extraction, and obtain a Henan tobacco extract solution, the solvent is a 10% to 50% ethanol aqueous solution by mass, the amount of solvent added is 6 to 9 times the mass of the tobacco leaf fragments produced in Henan, the extraction temperature is 60 to 100°C, and the extraction time is 5 to 9 hours;
[0015] S2: The extract of the Yu tobacco extract is transferred to a concentration tank, and concentrated under reduced pressure under certain temperature and pressure conditions to remove organic solvents and water in the extract to obtain the prepared Yu tobacco extract. The temperature of the reduced pressure concentration is 45-55°C, the vacuum pressure is 60-90Pa, and the concentration of the prepared Yu tobacco extract is 1.2-1.5g / mL;
[0016] S3: Add the biological enzyme to sterile water and activate it at an appropriate temperature for a period of time. The biological enzyme is composed of protease, amylase, pectinase and galactomannan. The amount of sterile water added is 8 to 16 times the mass of the biological enzyme. The activation temperature is 28 to 45°C and the activation time is 2.5 to 3.5 hours.
[0017] S4: Weigh a certain mass of the prepared Henan tobacco extract, distilled water and activated biological enzyme respectively, adjust the pH, perform enzymolysis treatment under appropriate temperature conditions for a period of time, and after the enzymolysis is completed, heat to inactivate the biological enzyme, and then cool to room temperature. The amount of distilled water added is 6 to 9 times the mass of the prepared Henan tobacco extract, and the amount of activated biological enzyme added is 1.2‰ to 4.5‰ of the mass of the prepared Henan tobacco extract; the pH of the enzymolysis system is 5.5 to 7.3, the enzymolysis temperature is 36 to 54°C, and the enzymolysis time is 3.5 to 5h; the biological enzyme inactivation temperature is 85 to 95°C, and the inactivation time is 25 to 35min;
[0018] S5: adding amino acids and catalysts to the enzymatic hydrolysate of Henan tobacco extract, reacting under certain temperature conditions, cooling the reaction solution to room temperature after the reaction, filtering and concentrating under reduced pressure to obtain the Maillard reaction flavor of Henan tobacco extract, wherein the amino acids are composed of proline, threonine, leucine and tryptophan, and the amount of amino acids added is 4‰ to 8‰ of the mass of the enzymatic hydrolysate of Henan tobacco extract; the catalyst is at least one of citric acid, malic acid, alginic acid and sorbic acid, and the amount of catalyst added is 1.2‰ to 4.5‰ of the mass of the enzymatic hydrolysate of Henan tobacco extract; the reaction temperature is 60 to 120°C, and the reaction time is 5 to 9h; the temperature of reduced pressure concentration is 45 to 55°C, the vacuum pressure is 55 to 90Pa, and the concentration of the Maillard reaction flavor of Henan tobacco extract is 1.2 to 1.5g / mL.
[0019] Compared with the prior art, the present invention has the following beneficial effects:
[0020] 1. Perform extraction and other related operations through the extraction tank. The reciprocating motor drives the screw to rotate, which can drive the lifting block to move up and down, and then drive the tank cover to open and close, which is convenient for adding materials;
[0021] 2. The stirring motor drives the stirring shaft and blades to rotate, so that stirring operation can be performed, which is convenient for rapid and uniform reaction and uniform heating;
[0022] 3. The temperature sensor can detect and feedback the temperature in the extraction tank and the corresponding temporary storage tank; the heater can be used for heating; the PLC controller can be used for automatic control;
[0023] 4. Through the four cooling components, when cooling is needed, cyclic cooling can be performed, and when cooled to a suitable temperature, the liquid is transported back to the extraction tank through the liquid inlet pipe 1 and the water pump 2 for the next operation;
[0024] 5. Concentration operation can be performed through the concentration tank, liquid inlet pipe 2, liquid outlet pipe 2 and water pump 3;
[0025] 6. By using tobacco leaf fragments produced in Henan as raw materials and using the extraction device and extraction process described in the present invention, Henan tobacco reactants with distinct sensory characteristics, clear functional orientations, and concentrated aroma active ingredients can be obtained. BRIEF DESCRIPTION OF THE DRAWINGS
[0026] Figure 1 It is a structural schematic diagram of the present invention.
[0027] Figure 2 It is a schematic structural diagram of the reciprocating lifting assembly and the stirring assembly of the present invention.
[0028] Figure 3 It is a structural schematic diagram of the extraction tank of the present invention.
[0029] Figure 4 It is a top view of the extraction tank of the present invention.
[0030] Figure 5 It is a schematic diagram of the structure of a part of the present invention.
[0031] Figure 6 It is a top view of a part of the present invention.
[0032] Figure 7 It is a bottom view of a part of the present invention.
[0033] Figure 8 It is a side view of the heater of the present invention.
[0034] In the figure: extraction tank 1, tank cover 2, filter screen plate 3, fixed plate 4, reciprocating lifting component 5, fixed frame 51, screw 52, lifting block 53, guide rod 54, reciprocating motor 55, stirring component 6, stirring motor 61, stirring shaft 62, blade 63, temperature sensor 7, heater 8, PLC controller 9, liquid outlet pipe 10, cooling component 11, spiral cooling pipe 111, water pump 1 112, temporary storage tank 113, connecting pipe 12, liquid inlet pipe 1 13, water pump 2 14, concentration tank 15, liquid inlet pipe 2 16, liquid outlet pipe 2 17, water pump 3 18. DETAILED DESCRIPTION
[0035] The following will be combined with the drawings in the embodiments of the present invention to clearly and completely describe the technical solutions in the embodiments of the present invention. Obviously, the described embodiments are only part of the embodiments of the present invention, not all of the embodiments. Based on the embodiments of the present invention, all other embodiments obtained by ordinary technicians in this field without creative work are within the scope of protection of the present invention.
[0036] See also Figure 1-8 The present invention provides a technical solution: a high-efficiency extraction device for Henan smoke reactants, comprising an extraction tank 1, through which extraction and other related operations are performed, a filter screen plate 3 is fixedly installed in the middle of the inner wall of the extraction tank 1, a fixing plate 4 is fixedly installed at the upper end of the outer side of the extraction tank 1, a reciprocating lifting component 5 is fixedly installed on the upper surface of the fixing plate 4, a tank cover 2 corresponding to the upper end opening of the extraction tank 1 is fixedly installed at the inner end of the reciprocating lifting component 5, a stirring component 6 located between the inner wall of the extraction tank 1 and the upper surface of the filter screen plate 3 is fixedly installed at the center of the bottom of the tank cover 2, a heater 8 is fixedly installed at the bottom of the extraction tank 1, and a heating operation can be performed through the heater 8, and cooling components 11 are respectively arranged on the front, back, left and right sides of the extraction tank 1;
[0037] The cooling component 11 comprises a spiral cooling pipe 111, a water pump 112 and a temporary storage tank 113. The spiral cooling pipe 111 is fixedly installed at the bottom of the temporary storage tank 113. The liquid outlet of the spiral cooling pipe 111 is connected to the liquid inlet of the temporary storage tank 113 through the water pump 112. The water pump 112 is fixedly installed on the outside of the temporary storage tank 113.
[0038] One side of the lower end of the outer side of the extraction tank 1 is fixedly connected to the liquid inlet end of one of the spiral cooling tubes 111 through a liquid outlet pipe 10, the liquid outlet end of one of the temporary storage tanks 113 and the liquid inlet end of the adjacent spiral cooling tube 111 are correspondingly fixedly connected through a connecting pipe 12, the liquid outlet end on the inner side of the temporary storage tank 113 and the liquid inlet end of the middle part of the extraction tank 1 located below the filter screen plate 3 are correspondingly fixedly connected through a liquid inlet pipe 13, and the lower part of the outer side of the extraction tank 1 and the outer sides of the four temporary storage tanks 113 are respectively fixedly installed with temperature sensors 7 correspondingly connected to their inner cavities, and the temperature in the extraction tank 1 and the corresponding temporary storage tank 113 can be detected and fed back through the temperature sensor 7.
[0039] Further, such as Figure 2 As shown, the reciprocating lifting assembly 5 includes a fixed frame 51, a lead screw 52, a lifting block 53, a guide rod 54 and a reciprocating motor 55. The fixed frame 51 is fixedly installed on the outer side of the upper surface of the fixed plate 4, the guide rod 54 is fixedly installed between the top and the bottom of the inner walls of the two fixed frames 51, the lead screw 52 is rotatably connected between the top and the bottom of the inner walls of the two fixed frames 51, the lead screw 52 and the guide rod 54 are parallel to each other, the guide rod 54 is slidably connected to the sliding hole on the side of the lifting block 53, the lead screw 52 is threadedly connected to the threaded hole on the side of the lifting block 53, the inner end of the lifting block 53 is fixedly connected to one side of the tank cover 2, the reciprocating motor 55 is fixedly installed on the upper surface of the fixed frame 51, the output shaft of the fixed frame 51 is fixedly connected to the top of the lead screw 52, and the reciprocating motor 55 drives the lead screw 52 to rotate, which can drive the lifting and lowering movement of the lifting block 53, and then drive the lifting, opening and closing of the tank cover 2 to facilitate the addition of materials.
[0040] Further, such as Figure 2 As shown, the stirring assembly 6 includes a stirring motor 61, a stirring shaft 62 and blades 63. The top end of the stirring shaft 62 is rotatably connected to the center of the bottom of the tank cover 2 through a bearing, and the blades 63 are evenly distributed and fixedly installed on the outside of the stirring shaft 62. The stirring motor 61 is fixedly installed on the upper surface of the tank cover 2, and the output shaft of the stirring motor 61 is fixedly connected to the top end of the stirring shaft 62. The stirring motor 61 drives the stirring shaft 62 and the blades 63 to rotate, so that the stirring operation can be performed, which is convenient for rapid and uniform reaction and uniform heating.
[0041] Further, such as Figure 6 As shown, a water pump 2 14 is fixedly installed on one side of the temporary storage tank 113 close to the extraction tank 1, and the liquid outlet end inside the temporary storage tank 113 is connected with the outer end of the liquid inlet pipe 13 through the water pump 2 14, and the inner end of the liquid inlet pipe 13 is connected with the liquid inlet end in the middle of the extraction tank 1. Through the four cooling and cooling components 11, circulating cooling and cooling can be performed when cooling and cooling are required, and when cooled to a suitable temperature, the liquid is transported back to the extraction tank 1 through the liquid inlet pipe 13 and the water pump 2 14 for the next operation.
[0042] Further, such as Figure 1 As shown, it also includes a concentration tank 15, such as Figure 8 As shown, the liquid inlet end and the liquid outlet end of the concentration tank 15 are respectively connected to a fixed water pump 3 18, and are respectively connected to the lower part of the inner cavity of the extraction tank 1 through the water pump 3 18 and the corresponding liquid inlet pipe 2 16 and liquid outlet pipe 2 17. The concentration operation can be performed through the concentration tank 15, the liquid inlet pipe 2 16, the liquid outlet pipe 2 17 and the water pump 3 18.
[0043] Further, such as Figure 3 As shown, a PLC controller 9 is fixedly installed on the upper surface of the fixed plate 4, and the reciprocating motor 55, the stirring motor 61, the temperature sensor 7, the heater 8, the water pump 1 12, the water pump 2 14, the water pump 3 18 and the concentration tank 15 are electrically connected to the PLC controller 9 respectively, and the PLC controller 9 is electrically connected to the external power supply. Automatic control can be performed through the PLC controller 9 (the above-mentioned related equipment used in the present invention are all existing conventional equipment, and their processing operations are all existing mature technologies, and their principles are not further described).
[0044] When using:
[0045] The extraction tank 1 is used for extraction and other related operations. The reciprocating motor 55 drives the screw 52 to rotate, which can drive the lifting block 53 to move up and down, and then drive the tank cover 2 to open and close, which is convenient for adding materials. The stirring motor 61 drives the stirring shaft 62 and the blade 63 to rotate, so as to perform stirring operations, which is convenient for rapid and uniform reaction and uniform heating. The temperature sensor 7 can detect and feedback the temperature in the extraction tank 1 and the corresponding temporary storage tank 113. The heater 8 can perform heating operations. The PLC controller 9 can perform automatic control. The four cooling and cooling components 11 can perform cyclic cooling and cooling when cooling is required, and when cooled to a suitable temperature, it is transported back to the extraction tank 1 through the liquid inlet pipe 13 and the water pump 2 14 for the next step of operation (specifically, the liquid to be cooled in the extraction tank 1 is transported through the liquid outlet pipe 10 and the corresponding water pump 11). 12, output from the extraction tank 1, and transported into the first temporary storage tank 113 through the first spiral cooling tube 111, cooled in the temporary storage tank 113, when the temperature is appropriate, the cooled liquid is transported back to the extraction tank 1 through the liquid inlet pipe 1 13 and the water pump 2 14 corresponding to the first temporary storage tank 113, if the temperature is not appropriate, operate as above, and continue cooling through the next cooling and cooling component 11 until the temperature is appropriate), the concentration operation can be carried out through the concentration tank 15, the liquid inlet pipe 2 16, the liquid outlet pipe 2 17 and the water pump 3 18 (specifically, the liquid to be concentrated in the extraction tank 1 is transported to the concentration tank 15 through the liquid inlet pipe 2 16 and the corresponding water pump 3 18 for corresponding concentration processing (the processing operation is an existing mature technology, and its principle is not further described), and the concentrated liquid is transported back to the extraction tank 1 through the liquid outlet pipe 2 17 and the corresponding water pump 3 18).
[0046] Specifically, the required Yuyan reactant can be obtained by performing the following processing operations through the above device:
[0047] S1: Weigh a certain mass of Henan tobacco leaf fragments and solvent respectively, add them into extraction tank 1, heat and extract for 6 hours, cool and filter after the extraction, and obtain Henan tobacco extract. Specifically, the solvent is 15% ethanol aqueous solution by mass, the amount of solvent added is 7 times the mass of Henan tobacco leaf fragments, and the extraction temperature is 90°C;
[0048] S2: The extract of Yuyan extract is transferred to the concentration tank 15, and concentrated under reduced pressure at a certain temperature of 50° C. and a pressure of 75 Pa to remove the organic solvent and water in the extract, thereby obtaining a preparatory Yuyan extract of about 1.3 g / mL;
[0049] S3: adding the biological enzyme (consisting of protease, amylase, pectinase and galactomannan) to sterile water and activating it at 35°C for 3h. Specifically, the amount of sterile water added is 12 times the mass of the biological enzyme;
[0050] S4: Weigh a certain mass of the prepared Henan tobacco extract, distilled water and activated biological enzyme respectively (specifically, the amount of distilled water added is 7 times the mass of the prepared Henan tobacco extract, and the amount of activated biological enzyme added is 2.5‰ of the mass of the prepared Henan tobacco extract), adjust the pH to 6, and perform enzymolysis at 45°C for 5h. After the enzymolysis is completed, heat to 90°C to inactivate the biological enzyme for 30min, and then cool to room temperature;
[0051] S5: Add amino acids and catalysts to the enzymatic hydrolysate of Henan tobacco extract, react under certain temperature conditions, cool the reaction solution to room temperature after the reaction, filter and concentrate under reduced pressure to obtain the Maillard reaction flavor of Henan tobacco extract. Specifically, the amino acids are composed of proline, threonine, leucine and tryptophan, and the amount of amino acids added is 6‰ of the mass of the enzymatic hydrolysate of Henan tobacco extract; the catalyst is at least one of citric acid, malic acid, alginic acid and sorbic acid, and the amount of catalyst added is 3‰ of the mass of the enzymatic hydrolysate of Henan tobacco extract; the reaction temperature is 100°C, and the reaction time is 7h; the temperature of reduced pressure concentration is 50°C, the vacuum pressure is 70Pa, and the concentration of the Maillard reaction flavor of Henan tobacco extract is 1.3g / mL.
[0052] Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that various changes, modifications, substitutions and variations may be made to the embodiments without departing from the principles and spirit of the present invention, and that the scope of the present invention is defined by the appended claims and their equivalents.
Claims
1. A highly efficient extraction device for Henan tobacco reactants, comprising an extraction tank (1), characterized in that: A filter screen plate (3) is fixedly mounted in the middle of the inner side wall of the extraction tank (1), a fixed plate (4) is fixedly mounted on the upper end of the outer side of the extraction tank (1), a reciprocating lifting component (5) is fixedly mounted on the upper surface of the fixed plate (4), a tank cover (2) corresponding to the upper end opening of the extraction tank (1) is fixedly mounted on the inner side end of the reciprocating lifting component (5), a stirring component (6) located between the inner side wall of the extraction tank (1) and the upper surface of the filter screen plate (3) is fixedly mounted at the center of the bottom of the tank cover (2), a heater (8) is fixedly mounted at the bottom of the extraction tank (1), and cooling components (11) are respectively arranged on the front, back, left and right sides of the extraction tank (1); The cooling component (11) comprises a spiral cooling pipe (111), a water pump (112) and a temporary storage tank (113); the spiral cooling pipe (111) is fixedly mounted on the bottom of the temporary storage tank (113); the liquid outlet of the spiral cooling pipe (111) is connected to the liquid inlet of the temporary storage tank (113) through the water pump (112); and the water pump (112) is fixedly mounted on the outside of the temporary storage tank (113); One side of the lower end of the outer side of the extraction tank (1) is fixedly connected to the liquid inlet end of one of the spiral cooling tubes (111) via a liquid outlet pipe (10); the liquid outlet end of one of the temporary storage tanks (113) and the liquid inlet end of the adjacent spiral cooling tube (111) are correspondingly fixedly connected via a connecting pipe (12); the liquid outlet end on the inner side of the temporary storage tank (113) and the liquid inlet end of the middle part of the extraction tank (1) located below the filter screen plate (3) are correspondingly fixedly connected via a liquid inlet pipe (13); the lower part of the outer side of the extraction tank (1) and the outer sides of the four temporary storage tanks (113) are respectively fixedly mounted with temperature sensors (7) correspondingly connected to their inner cavities.
2. The high-efficiency extraction device for Henan tobacco reactants according to claim 1 is characterized in that: The reciprocating lifting assembly (5) comprises a fixed frame (51), a lead screw (52), a lifting block (53), a guide rod (54) and a reciprocating motor (55). The fixed frame (51) is fixedly mounted on the outer side of the upper surface of the fixed plate (4). The guide rod (54) is fixedly mounted between the top and bottom of the inner walls of the two fixed frames (51). The lead screw (52) is rotatably connected between the top and bottom of the inner walls of the two fixed frames (51). The lead screw (52) and the guide rod (54) are parallel to each other. The guide rod (54) is slidably connected to the sliding hole on the side of the lifting block (53). The lead screw (52) is threadedly connected to the threaded hole on the side of the lifting block (53). The inner side end of the lifting block (53) is fixedly connected to one side of the tank cover (2). The reciprocating motor (55) is fixedly mounted on the upper surface of the fixed frame (51). The output shaft of the fixed frame (51) is fixedly connected to the top of the lead screw (52).
3. The high-efficiency extraction device for Henan smoke reactants according to claim 2 is characterized in that: The stirring assembly (6) comprises a stirring motor (61), a stirring shaft (62) and blades (63); the top end of the stirring shaft (62) is rotatably connected to the center of the bottom of the tank cover (2) via a bearing; blades (63) are evenly distributed and fixedly installed on the outer side of the stirring shaft (62); the stirring motor (61) is fixedly installed on the upper surface of the tank cover (2); and the output shaft of the stirring motor (61) is fixedly connected to the top end of the stirring shaft (62).
4. The high-efficiency extraction device for Henan tobacco reactants according to claim 3 is characterized in that: A water pump 2 (14) is fixedly installed on one side of the temporary storage tank (113) close to the extraction tank (1); the liquid outlet end inside the temporary storage tank (113) is connected to the outer end of the liquid inlet pipe 1 (13) through the water pump 2 (14); and the inner end of the liquid inlet pipe 1 (13) is connected to the liquid inlet end in the middle of the extraction tank (1).
5. The high-efficiency extraction device for Henan tobacco reactants according to claim 4 is characterized in that: It also includes a concentration tank (15), the liquid inlet end and the liquid outlet end of the concentration tank (15) are respectively connected to and fixed with a water pump three (18), and are respectively connected to the lower part of the inner cavity of the extraction tank (1) through the water pump three (18) and the corresponding liquid inlet pipe two (16) and liquid outlet pipe two (17).
6. The high-efficiency extraction device for Henan tobacco reactants according to claim 5 is characterized in that: A PLC controller (9) is fixedly mounted on the upper surface of the fixed plate (4); the reciprocating motor (55), the stirring motor (61), the temperature sensor (7), the heater (8), the water pump 1 (112), the water pump 2 (14) and the water pump 3 (18) are respectively electrically connected to the PLC controller (9); and the PLC controller (9) is electrically connected to an external power supply.
7. The extraction process of the Yuyan reactant according to any one of claims 1 to 6, characterized in that: The following steps are involved: S1: Weigh a certain mass of Henan tobacco leaf fragments and a solvent respectively and add them into an extraction tank (1), heat and extract for a period of time, cool and filter after the extraction is completed, and obtain a Henan tobacco extract solution, the solvent is a 10% to 50% ethanol aqueous solution, the amount of solvent added is 6 to 9 times the mass of the Henan tobacco leaf fragments, the extraction temperature is 60 to 100° C., and the extraction time is 5 to 9 hours; S2: transferring the extract of the Yu tobacco extract to a concentration tank (15), and concentrating under reduced pressure under certain temperature and pressure conditions to remove organic solvents and water in the extract to obtain a prepared Yu tobacco extract, wherein the temperature for the reduced pressure concentration is 45 to 55° C., the vacuum pressure is 60 to 90 Pa, and the concentration of the prepared Yu tobacco extract is 1.2 to 1.5 g / mL; S3: Add the biological enzyme to sterile water and activate it at an appropriate temperature for a period of time. The biological enzyme is composed of protease, amylase, pectinase and galactomannan. The amount of sterile water added is 8 to 16 times the mass of the biological enzyme. The activation temperature is 28 to 45°C and the activation time is 2.5 to 3.5 hours. S4: Weigh a certain mass of the prepared Henan tobacco extract, distilled water and activated biological enzyme respectively, adjust the pH, perform enzymolysis treatment under appropriate temperature conditions for a period of time, and after the enzymolysis is completed, heat to inactivate the biological enzyme, and then cool to room temperature. The amount of distilled water added is 6 to 9 times the mass of the prepared Henan tobacco extract, and the amount of activated biological enzyme added is 1.2‰ to 4.5‰ of the mass of the prepared Henan tobacco extract; the pH of the enzymolysis system is 5.5 to 7.3, the enzymolysis temperature is 36 to 54°C, and the enzymolysis time is 3.5 to 5h; the biological enzyme inactivation temperature is 85 to 95°C, and the inactivation time is 25 to 35min; S5: adding amino acids and catalysts to the enzymatic hydrolysate of Henan tobacco extract, reacting under certain temperature conditions, cooling the reaction solution to room temperature after the reaction, filtering and concentrating under reduced pressure to obtain the Maillard reaction flavor of Henan tobacco extract, wherein the amino acids are composed of proline, threonine, leucine and tryptophan, and the amount of amino acids added is 4‰ to 8‰ of the mass of the enzymatic hydrolysate of Henan tobacco extract; the catalyst is at least one of citric acid, malic acid, alginic acid and sorbic acid, and the amount of catalyst added is 1.2‰ to 4.5‰ of the mass of the enzymatic hydrolysate of Henan tobacco extract; the reaction temperature is 60 to 120°C, and the reaction time is 5 to 9h; the temperature of reduced pressure concentration is 45 to 55°C, the vacuum pressure is 55 to 90Pa, and the concentration of the Maillard reaction flavor of Henan tobacco extract is 1.2 to 1.5g / mL.
