Foamed ceramic filter sheet prepared from chemical zirconium and preparation method of foamed ceramic filter sheet

Through the combination of chemical zirconium and acrylate polymerizer and high-temperature firing technology, foam ceramic filters with high melting point and high hardness were prepared, which solved the stability and impurities of traditional ceramic filters in high-temperature and high-pressure environments, and improved the Filtration efficiency and purity, suitable for high-end fields.

CN119158338APending Publication Date: 2024-12-20JINAN GAOYI NEW MATERIALS CO LTD
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Patent Information

Application Number
CN202411370696.7
Authority / Receiving Office
CN · China
Patent Type
Applications(China)
Current Assignee / Owner
Filing Date
2024-09-29
Publication Date
2024-12-20

AI Technical Summary

Technical Problem

Foam ceramic filters prepared by traditional zirconia have many impurities, low strength, and are not suitable for high-temperature and high-pressure environments. In the filtration process of high-temperature alloys, impurities may be brought into the purity and performance of the alloy, limiting their application in aerospace and other fields.

Method used

Use chemical zirconium and acrylate polymerizer to mix, stir, dry and fire at high temperature to form a liquid sponge on the porous sponge, forming a foam ceramic filter with high melting point and high hardness, with excellent physical and chemical properties and good filtration efficiency.

Benefits of technology

It improves the corrosion resistance and filtration efficiency of foam ceramic filters, reduces environmental pollution and harmful gas emissions, broadens its application range, and ensures stable working and filtration quality in high-temperature environments.

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Abstract

The invention belongs to the technical field of ceramic filters, and particularly relates to a foamed ceramic filter prepared from chemical zirconium and a preparation method thereof, the foamed ceramic filter comprises a ceramic filter, and the ceramic filter is provided with filter holes; the chemical zirconium is used as a main raw material, so that the prepared foamed ceramic filter has excellent physical and chemical properties such as high melting point, high hardness and corrosion resistance, the filter can stably work for a long time in a high-temperature and high-corrosivity environment, and the application range of the filter is widened.
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Description

Technical Field

[0001] The invention belongs to the technical field of ceramic filter discs, and specifically refers to a foam ceramic filter disc prepared from chemical zirconium and a preparation method thereof. Background Art

[0002] As a porous material, ceramic filter is widely used in the field of filtration and separation of liquids and gases. It intercepts and removes impurities through micropores and mesoporous structures.

[0003] Traditionally, most foam ceramic filters on the market are made from zirconium oxide as the main raw material. However, this preparation method has significant drawbacks: due to process limitations, the foam ceramic filters produced often contain more impurities, resulting in low product purity; at the same time, the presence of impurities also reduces the overall strength of the filter, making it vulnerable to damage in extreme environments such as high temperature and high pressure. More importantly, during the filtration process of high-temperature alloy solutions, these impurities may be brought into the alloy, seriously affecting the purity and performance of the high-temperature alloy, limiting its application and development in high-end fields such as aerospace and energy. Summary of the invention

[0004] In order to solve the above problems, the present invention proposes a foam ceramic filter sheet prepared by chemical zirconium and a preparation method thereof.

[0005] The technical solution adopted by the present invention is as follows: The present invention provides a foam ceramic filter prepared by chemical zirconium, comprising a ceramic filter, and the ceramic filter is provided with filter holes.

[0006] This scheme also discloses a method for preparing a foam ceramic filter sheet using chemical zirconium, which mainly comprises the following steps:

[0007] S1. The organic polymerizing agent and the chemical zirconium are mixed and stirred to form a flowing liquid having fluidity and adhesion;

[0008] S2. Immersing the porous sponge in the flowing liquid so that the flowing liquid is evenly hung on the porous sponge to form a liquid sponge;

[0009] S3. Dry the liquid sponge with a high temperature furnace;

[0010] S4. Maintain a vacuum reducing atmosphere in a high temperature furnace for high temperature sintering and molding.

[0011] Furthermore, the ratio of the organic polymerizing agent to the chemical zirconium is 4:6.

[0012] Furthermore, the organic polymerizing agent is an acrylate polymerizing agent.

[0013] The beneficial effects achieved by the present invention using the above structure are as follows:

[0014] (1) Using chemical zirconium as the main raw material, the prepared foam ceramic filter has excellent physical and chemical properties such as high melting point, high hardness, and corrosion resistance, which enables the filter to work stably for a long time in a high temperature and highly corrosive environment, thereby broadening its application range.

[0015] (2) The filtration efficiency is improved by evenly mounting a flowing liquid containing chemical zirconium on a porous sponge and solidifying it into a porous ceramic filter in a subsequent step. At the same time, the microporous structure of the ceramic material can effectively block impurities and ensure the filtration quality.

[0016] (3) The use of acrylic polymerizers as organic components has low toxicity and good environmental compatibility, which is beneficial to reducing environmental pollution during the production process. At the same time, maintaining a vacuum reducing atmosphere during high-temperature firing helps reduce the emission of harmful gases. BRIEF DESCRIPTION OF THE DRAWINGS

[0017] In order to more clearly illustrate the technical solution of the present invention, the accompanying drawings required for use in the description will be briefly introduced below. Obviously, the accompanying drawings in the following description are only some embodiments of the present invention. For ordinary technicians in this field, other accompanying drawings can be obtained based on these accompanying drawings without paying creative work.

[0018] Figure 1 This is a schematic diagram of the structure of a foam ceramic filter prepared by chemical zirconium in the present invention.

[0019] Among them, 1. Ceramic filter, 2. Filter hole. DETAILED DESCRIPTION

[0020] In order to make the purpose, features and advantages of the present invention more obvious and easy to understand, the technical scheme of the present invention will be clearly and completely described below in conjunction with the drawings in this specific embodiment. Obviously, the embodiments described below are only part of the embodiments of the present invention, not all of them. Based on the embodiments in this patent, all other embodiments obtained by ordinary technicians in this field without creative work are within the scope of protection of this patent.

[0021] like Figure 1 As shown, the present invention proposes a foam ceramic filter sheet prepared by chemical zirconium, comprising a ceramic filter sheet 1, wherein the ceramic filter sheet 1 is provided with filter holes 2.

[0022] A method for preparing a foam ceramic filter sheet using chemical zirconium comprises the following steps:

[0023] S1. The organic polymerizing agent and the chemical zirconium are mixed and stirred to form a flowing liquid having fluidity and adhesion;

[0024] S2. Immersing the porous sponge in the flowing liquid so that the flowing liquid is evenly hung on the porous sponge to form a liquid sponge;

[0025] S3. Dry the liquid sponge with a high temperature furnace;

[0026] S4. Maintain a vacuum reducing atmosphere in a high temperature furnace for high temperature sintering and molding.

[0027] The ratio of organic polymerizer to chemical zirconium is 4:6.

[0028] The organic polymerizing agent is an acrylate polymerizing agent.

[0029] It can be seen from the above embodiments that the beneficial effects of the present invention are:

[0030] By using chemical zirconium as the main raw material, the prepared foam ceramic filter has excellent physical and chemical properties such as high melting point, high hardness, and corrosion resistance, so that the filter can work stably for a long time in a high-temperature and highly corrosive environment, thereby broadening its application range; by evenly mounting a flowing liquid containing chemical zirconium on a porous sponge and solidifying it into a ceramic filter with a porous structure in a subsequent step, the filtration efficiency is improved. At the same time, the microporous structure of the ceramic material can effectively block impurities and ensure the filtration quality; using an acrylic polymerizer as an organic component, it has low toxicity and good environmental compatibility, which is beneficial to reducing environmental pollution in the production process. At the same time, maintaining a vacuum reducing atmosphere during high-temperature firing helps reduce the emission of harmful gases.

[0031] The above description of the disclosed embodiments enables one skilled in the art to implement or use the present invention. Various modifications to these embodiments will be apparent to one skilled in the art, and the general principles defined herein may be implemented in other embodiments without departing from the spirit or scope of the present invention. Therefore, the present invention will not be limited to the embodiments shown herein, but rather to the widest scope consistent with the principles and novel features disclosed herein.

Claims

1. A foam ceramic filter prepared from chemical zirconium, characterized in that: It comprises a ceramic filter plate (1), wherein the ceramic filter plate (1) is provided with filter holes (2).

2. A method for preparing a foam ceramic filter sheet using chemical zirconium, characterized in that: The method for preparing a foam ceramic filter sheet using chemical zirconium according to claim 1 comprises the following steps: S1. The organic polymerizing agent and the chemical zirconium are mixed and stirred to form a flowing liquid having fluidity and adhesion; S2. Immersing the porous sponge in the flowing liquid so that the flowing liquid is evenly hung on the porous sponge to form a liquid sponge; S3. Dry the liquid sponge with a high temperature furnace; S4. Maintain a vacuum reducing atmosphere in a high temperature furnace for high temperature sintering and molding.

3. The method for preparing a foam ceramic filter sheet using chemical zirconium according to claim 2, characterized in that: The ratio of the organic polymerizing agent to the chemical zirconium is 4:

6.

4. The method for preparing a foam ceramic filter sheet using chemical zirconium according to claim 2, characterized in that: The organic polymerizing agent is an acrylate polymerizing agent.