Hair fluffing spray containing silica and preparation method thereof
Through fine stirring and filtration treatment of fine-grained silica and specific formulas, the existing hair fluffy spray large-grained powder clogs pores and poor results are solved, achieving efficient oil absorption and anti-static fluffy effects, and giving aroma to enhance the fragrance. The quality and safety of the product.
Patent Information
- Application Number
- CN202411180633.5
- Authority / Receiving Office
- CN · China
- Patent Type
- Applications(China)
- Current Assignee / Owner
- Filing Date
- 2024-08-27
- Publication Date
- 2025-01-07
- Estimated Expiration
- Not applicable · inactive patent
AI Technical Summary
Existing hair fluffy sprays use large particles of powder, which can easily clog pores and have poor fluffy effects. There is no effective solution yet.
Using fine particles of silica and specific formula raw materials, including polyethylene glycol-32, ethanol, sodium lauryl sulfate, sodium methyl cocoyl taurate, magnesium aluminum silicate and flavor, divided into A The raw materials of phase, phase B, phase C and phase D are finely stirred and filtered to ensure that the mixing uniformity and pH value are within the normal range.
It achieves efficient oil absorption and anti-static effect without clogging pores, making hair fluffy, while giving it a fresh fragrance, improving the purity and safety of the product.
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Figure CN119257957A_ABST
Abstract
Description
Technical Field
[0001] The invention relates to the technical field of hair fluffy spray containing silica, in particular to a hair fluffy spray containing silica and a preparation method thereof. Background Art
[0002] Hair volumizing spray is a beauty product used to increase the volume and fullness of hair. Its main function is to help improve the appearance and texture of hair, making it look more voluminous and fluffy. When the hair is limp, using hair volumizing spray can quickly improve the hairstyle.
[0003] However, existing hair fluffing sprays usually use large-particle powders, which may cause the risk of pore clogging and have an insignificant fluffy effect on hair. Therefore, a hair fluffing spray containing silica and a preparation method thereof are proposed.
[0004] Currently, no effective solution has been proposed for the problems in the related technologies. Summary of the invention
[0005] In view of the problems in the related art, the present invention provides a hair fluffing spray containing silica and a preparation method thereof to overcome the above technical problems existing in the existing related art.
[0006] To this end, the specific technical solution adopted by the present invention is as follows:
[0007] A method for preparing a hair fluffing spray containing silica, the method comprising the following steps:
[0008] S1. Prepare raw materials and preparation tools. The raw materials include water, polyethylene glycol-32, silica, ethanol, sodium laureth sulfate, sodium methyl cocoyl taurate, polyethylene glycol-8, magnesium aluminum silicate and flavor. The preparation tools include containers, digital thermometers, electronic balances, filters, heating plates, pH meters, stirrers and spray bottles.
[0009] S2. Weigh the raw materials in phase A, phase B, phase C and phase D in sequence, add the raw materials in phase A into a container, and use a heating plate to heat and stir;
[0010] S3. After the raw materials in phase A are evenly mixed, the raw materials in phase B are added into the container and mixed and stirred;
[0011] S4, cooling the mixed liquid and performing temperature detection. When the temperature drops to 30°C, add the C phase raw material and stir, and finally add the D phase raw material and continue stirring evenly;
[0012] S5. Filter the successfully prepared raw materials, and perform pH value detection after filtration to verify that the spray pH value is within a normal range.
[0013] As a preferred embodiment, the preparation of raw materials and preparation tools, the raw materials include water, polyethylene glycol-32, silica, ethanol, sodium laureth sulfate, sodium methyl cocoyl taurate, polyethylene glycol-8, magnesium aluminum silicate and flavor, and the preparation tools include a container, an electronic balance, a filter, a heating plate, a pH meter, a stirrer and a spray bottle, and the steps are as follows:
[0014] S11, dividing the prepared raw materials into phase A, phase B, phase C and phase D, wherein phase A includes water and polyethylene glycol-32, phase B is silica, phase C is ethanol, and phase D is sodium laureth sulfate, sodium methyl cocoyl taurate, polyethylene glycol-8, magnesium aluminum silicate and flavor;
[0015] S12: First clean and sterilize the work area, then clean the prepared preparation tools to ensure that the preparation tools are clean and sterile between uses.
[0016] Cleaning and sterilizing work areas and tools can remove potential sources of contamination, such as dust and microorganisms, and reduce the risk of contamination to products, thereby ensuring the purity and safety of the products.
[0017] As a preferred embodiment, the steps of weighing the raw materials in phase A, phase B, phase C and phase D in sequence, adding the raw materials in phase A into a container, and heating and stirring using a heating plate include the following steps:
[0018] S21. Weigh the raw materials in phase A, phase B, phase C, and phase D in sequence using a balance and a measuring cylinder;
[0019] S22, put the raw materials in phase A into the container, turn on the heating plate, heat the raw materials in phase A, and then use a thermometer to detect the temperature of the raw materials in phase A. When the temperature of the raw materials in phase A rises to 45-50° C., use an agitator to start stirring, set the stirring speed to 30 rpm, and stir for 5-10 minutes until the materials are evenly mixed;
[0020] Setting the stirring speed to 30 rpm and the stirring time to 5-10 minutes can ensure that the raw materials are fully mixed, thereby improving the uniformity of the final product.
[0021] As a preferred embodiment, after the raw materials in phase A are mixed uniformly, the raw materials in phase B are put into a container, and the mixing and stirring includes the following steps:
[0022] S31, put the raw materials in phase B into a container, start stirring, set the stirring speed to 30 rpm, and the stirring time to 20-30 minutes. After the stirring is completed, start homogenization once, set the homogenization speed to 8000 rpm, and the homogenization time to 1 minute to mix the materials evenly;
[0023] Homogenization after stirring ensures that all ingredients in the mixture have been preliminarily mixed, and then the homogenization operation is used to improve the uniformity.
[0024] As a preferred embodiment, the mixed liquid is cooled and the temperature is detected. When the temperature drops to 30°C, the C phase raw material is added and stirred, and finally the D phase raw material is added and stirred evenly, which can include the following steps:
[0025] S41, cooling the mixed liquid and using a thermometer to detect the temperature. When the temperature drops to 30°C, adding the C phase raw material and stirring, setting the stirring speed to 20 rpm and the stirring time to 3-5 minutes;
[0026] S42. After the stirring of phase A, phase B and phase C raw materials is completed, continue to add phase D raw materials and stir until the materials are evenly mixed.
[0027] The overall content of the D phase raw material is relatively small, so when mixing and stirring, just mix evenly.
[0028] As a preferred embodiment, the steps of detecting the pH value of the successfully prepared liquid, verifying that the spray pH value is within a normal range, and finally filtering the successfully prepared liquid include:
[0029] S51, using a pH meter to detect the pH value of the liquid to ensure that the pH value is within a normal range. If the pH value is abnormal, the pH value of the liquid is adjusted to make it within a normal range;
[0030] S52. Slowly pour the successfully prepared liquid into the filter to ensure uniform flow rate and prevent the filter from being overloaded or blocked. Meanwhile, observe the flow of liquid during the filtering process. Collect the filtered liquid in a clean container and finally fill the liquid into a spray bottle to complete the production.
[0031] Filtration can remove suspended matter or other impurities from a liquid, thereby improving the purity and clarity of the liquid.
[0032] A hair fluffing spray containing silica, the spray comprising the following ingredients: water, grease adsorbent, antistatic agent, volatile agent, suspension aid, system stabilizer, and fragrance agent;
[0033] The grease adsorbent is 200 silica, the antistatic agent is CARBOWAX TM SENTRY TM Polyethylene Glycol 1450NF Flake Polyethylene Glycol-32 and CARBOWAX TMSENTRYPolyethylene Glycol 400NF polyethylene glycol-8, the volatile agent is ethanol, the suspending aid is magnesium aluminum silicate, the system stabilizer is sodium lauryl polyether sulfate and sodium methyl coconut oil acyl taurate, and the flavoring agent is essence.
[0034] The addition of fragrance agents can give the hair a fresh scent, so the user's hair can smell fresher after using the product.
[0035] The beneficial effects of the present invention are:
[0036] 1. The present invention selects 200 silica as raw material, 200 silica is a high-purity, fine-grained silicon dioxide that is sintered together to form chain aggregates through a high-temperature manufacturing process. The aggregates form larger agglomerates through hydrogen bonds and other weak attractive forces. When the degree of agglomeration increases, it has a stronger oil absorption capacity and does not clog the pores.
[0037] 2. The present invention adopts CARBOWAX TM SENTRY TM Polyethylene Glycol 1450NF Flake is made from polyethylene glycol-32, which is a good moisturizer and antistatic agent. It prevents hair from being charged and makes it easier for hair to be fluffy.
[0038] 3. During the preparation of the present invention, the raw materials are divided into phase A, phase B, phase C and phase D, which can make the raw materials easier to mix. At the same time, the mixing temperature, stirring time and stirring speed are controlled during mixing so that the raw materials can be mixed more evenly. After the raw materials are prepared, the pH value is tested and filtered to ensure the quality of the liquid and guarantee the product effect. BRIEF DESCRIPTION OF THE DRAWINGS
[0039] In order to more clearly illustrate the embodiments of the present invention or the technical solutions in the prior art, the drawings required for use in the embodiments will be briefly introduced below. Obviously, the drawings described below are only some embodiments of the present invention. For ordinary technicians in this field, other drawings can be obtained based on these drawings without paying creative work.
[0040] Figure 1 The present invention is a flow chart of a hair fluffy spray containing silica and a preparation method thereof according to an embodiment of the present invention. DETAILED DESCRIPTION
[0041] To further illustrate each embodiment, the present invention provides drawings, which are part of the disclosure of the present invention and are mainly used to illustrate the embodiments and can be used in conjunction with the relevant descriptions in the specification to explain the operating principles of the embodiments. With reference to these contents, ordinary technicians in the field should be able to understand other possible implementations and advantages of the present invention. The components in the figures are not drawn to scale, and similar component symbols are generally used to represent similar components.
[0042] According to an embodiment of the present invention, a hair fluffing spray containing silica and a preparation method thereof are provided.
[0043] Embodiment 1
[0044] The present invention is further described with reference to the accompanying drawings and specific embodiments. Figure 1 As shown, a method for preparing a hair fluffy spray containing silica according to an embodiment of the present invention comprises the following steps:
[0045] S1. Prepare raw materials and preparation tools. The raw materials include water, polyethylene glycol-32, silica, ethanol, sodium laureth sulfate, sodium methyl cocoyl taurate, polyethylene glycol-8, magnesium aluminum silicate and flavor. The preparation tools include containers, digital thermometers, electronic balances, filters, heating plates, pH meters, stirrers and spray bottles.
[0046] Further, preparing raw materials and preparation tools, the raw materials include water, polyethylene glycol-32, silica, ethanol, sodium laureth sulfate, sodium methyl cocoyl taurate, polyethylene glycol-8, magnesium aluminum silicate and flavor, and the preparation tools include a container, an electronic balance, a filter, a heating plate, a pH meter, a stirrer and a spray bottle, and the following steps are included:
[0047] S11, dividing the prepared raw materials into phase A, phase B, phase C and phase D, wherein phase A includes water and polyethylene glycol-32, phase B is silica, phase C is ethanol, and phase D is sodium laureth sulfate, sodium methyl cocoyl taurate, polyethylene glycol-8, magnesium aluminum silicate and flavor;
[0048] It should be noted that different raw materials require different conditions (such as temperature, pH value, stirring rate, etc.) to achieve the best reaction. Therefore, the raw materials are divided into phase A, phase B, phase C and phase D, so that these conditions can be more accurately controlled during processing, ensuring that each phase can react under the best conditions, thereby improving the quality and consistency of the final product.
[0049] S12; First clean and sterilize the work area, then clean the prepared preparation tools to ensure that the preparation tools are clean and sterile between uses.
[0050] S2. Weigh the raw materials in phase A, phase B, phase C and phase D in sequence, add the raw materials in phase A into a container, and use a heating plate to heat and stir;
[0051] Further, weighing the raw materials in phase A, phase B, phase C and phase D in sequence, adding the raw materials in phase A into a container, and heating and stirring using a heating plate include the following steps:
[0052] S21. Weigh the raw materials in phase A, phase B, phase C, and phase D in sequence using a balance and a measuring cylinder;
[0053] S22, put the raw materials in phase A into the container, turn on the heating plate, heat the raw materials in phase A, and then use a thermometer to detect the temperature of the raw materials in phase A. When the temperature of the raw materials in phase A rises to 45-50° C., use an agitator to start stirring, set the stirring speed to 30 rpm, and stir for 5-10 minutes until the materials are evenly mixed;
[0054] It should be noted that by heating at a temperature of 45-50° C. and stirring the phase A raw material with a stirrer, the solubility and mixing uniformity of the raw material can be increased, the stability and physical properties of the product can be improved, and the chemical reaction can be promoted.
[0055] S3. After the raw materials in phase A are evenly mixed, the raw materials in phase B are added into the container and mixed and stirred;
[0056] Further, after the raw materials in phase A are uniformly mixed, the raw materials in phase B are put into a container, and the mixing and stirring includes the following steps:
[0057] S31, put the raw materials in phase B into a container, start stirring, set the stirring speed to 30 rpm, and the stirring time to 20-30 minutes. After the stirring is completed, start homogenization once, set the homogenization speed to 8000 rpm, and the homogenization time to 1 minute to mix the materials evenly;
[0058] It should be noted that homogenization is a physical treatment process that aims to evenly distribute the components or phases of a substance in a mixture. The agitator can mix the substances evenly through mechanical stirring and shear force. At the same time, homogenization also has the function of increasing the contact area of the reactants and changing the fluidity of the mixture.
[0059] S4, cooling the mixed liquid and performing temperature detection. When the temperature drops to 30°C, add the C phase raw material and stir, and finally add the D phase raw material and continue stirring evenly;
[0060] Further, the mixed liquid is cooled and the temperature is detected. When the temperature drops to 30° C., the C phase raw material is added and stirred, and finally the D phase raw material is added and stirred evenly, which may include the following steps:
[0061] S41, cooling the mixed liquid and using a thermometer to detect the temperature. When the temperature drops to 30°C, adding the C phase raw material and stirring, setting the stirring speed to 20 rpm and the stirring time to 3-5 minutes;
[0062] It should be noted that the raw material of phase C is ethanol, so the temperature needs to be lowered. Adding ethanol at a lower temperature and stirring will help the ethanol and the raw material to be better mixed.
[0063] S42. After the stirring of phase A, phase B and phase C raw materials is completed, continue to add phase D raw materials and stir until the materials are evenly mixed.
[0064] S5. Filter the successfully prepared raw materials, and perform pH value testing after filtration to verify that the spray pH value is within the normal range
[0065] Further, the pH value of the successfully prepared liquid is tested to verify that the spray pH value is within the normal range, and finally the successfully prepared liquid is filtered. The specific steps include:
[0066] S51, using a pH meter to detect the pH value of the liquid to ensure that the pH value is within a normal range. If the pH value is abnormal, the pH value of the liquid is adjusted to make it within a normal range;
[0067] S52. Slowly pour the successfully prepared liquid into the filter to ensure uniform flow rate and prevent the filter from being overloaded or blocked. Meanwhile, observe the flow of liquid during the filtering process. Collect the filtered liquid in a clean container and finally fill the liquid into a spray bottle to complete the production.
[0068] It should be noted that pH testing is an important quality control step. pH testing can ensure the stability of the product. When the pH value is not within the normal range, the pH value of the product will be adjusted to restore it to the normal range.
[0069] A hair fluffing spray containing silica, the spray comprising the following ingredients: water, grease adsorbent, antistatic agent, volatile agent, suspension aid, system stabilizer, and fragrance agent;
[0070] Grease absorbent is 200 silica, antistatic agent is CARBOWAX TM SENTRY TM Polyethylene Glycol 1450NF Flake Polyethylene Glycol-32 and CARBOWAX TMSENTRYPolyethylene Glycol 400NF Polyethylene Glycol-8, the volatile agent is ethanol, the suspending aid is magnesium aluminum silicate, the system stabilizer is sodium lauryl polyether sulfate, sodium methyl coconut oil acyl taurate, and the flavoring agent is essence.
[0071] In summary, the present invention adopts 200 silica as raw material, 200 silica is a high-purity, fine-grained silicon dioxide that is sintered together to form chain aggregates through a high-temperature manufacturing process. The aggregates form larger agglomerates through hydrogen bonding and other weak attractive forces. When the degree of agglomeration increases, it has a stronger oil absorption capacity and does not clog pores. The present invention uses CARBOWAX TM SENTRY TM Polyethylene Glycol 1450NF Flake is made of polyethylene glycol-32, which is a good moisturizer and antistatic agent. It makes the hair less likely to be charged, thus making the hair more fluffy. In the preparation process, the raw materials are divided into phase A, phase B, phase C and phase D, which can make the raw materials easier to mix. At the same time, the mixing temperature, stirring time and stirring speed are controlled during mixing, so that the raw materials can be mixed more evenly. After the raw materials are prepared, the pH value is tested and filtered to ensure the quality of the liquid and the product effect.
[0072] Embodiment 2
[0073] Raw material composition and raw material ratio
[0074]
[0075]
[0076] The above description is only a preferred embodiment of the present invention and is not intended to limit the present invention. Any modifications, equivalent substitutions, improvements, etc. made within the spirit and principle of the present invention should be included in the protection scope of the present invention.
Claims
1. A method for preparing a hair fluffy spray containing silica, characterized in that: The specific preparation method comprises the following steps: S1. Prepare raw materials and preparation tools. The raw materials include water, polyethylene glycol-32, silica, ethanol, sodium laureth sulfate, sodium methyl cocoyl taurate, polyethylene glycol-8, magnesium aluminum silicate and flavor. The preparation tools include containers, digital thermometers, electronic balances, filters, heating plates, pH meters, stirrers and spray bottles. S2. Weigh the raw materials in phase A, phase B, phase C and phase D in sequence, add the raw materials in phase A into a container, and use a heating plate to heat and stir; S3. After the raw materials in phase A are evenly mixed, the raw materials in phase B are added into the container and mixed and stirred; S4, cooling the mixed liquid and performing temperature detection. When the temperature drops to 30°C, add the C phase raw material and stir, and finally add the D phase raw material and continue stirring evenly; S5, detecting the pH value of the successfully prepared liquid to verify that the spray pH value is within a normal range, and finally filtering the successfully prepared liquid.
2. The method for preparing a hair fluffy spray containing silica according to claim 1, characterized in that: The preparation of raw materials and preparation tools, the raw materials include water, polyethylene glycol-32, silica, ethanol, sodium laureth sulfate, sodium methyl cocoyl taurate, polyethylene glycol-8, magnesium aluminum silicate and flavor, and the preparation tools include a container, an electronic balance, a filter, a heating plate, a pH meter, a stirrer and a spray bottle, and the following steps are included: S11, dividing the prepared raw materials into phase A, phase B, phase C and phase D, wherein phase A includes water and polyethylene glycol-32, phase B is silica, phase C is ethanol, and phase D is sodium laureth sulfate, sodium methyl cocoyl taurate, polyethylene glycol-8, magnesium aluminum silicate and flavor; S12: First clean and sterilize the work area, then clean the prepared preparation tools to ensure that the preparation tools are clean and sterile between uses.
3. The method for preparing a hair fluffy spray containing silica according to claim 1, characterized in that: The process of weighing the raw materials in phase A, phase B, phase C and phase D in sequence, adding the raw materials in phase A into a container, and heating and stirring using a heating plate comprises the following steps: S21. Weigh the raw materials in phase A, phase B, phase C, and phase D in sequence using a balance and a measuring cylinder; S22. Put the raw materials in phase A into a container, turn on the heating plate to heat the raw materials in phase A, and then use a thermometer to detect the temperature of the raw materials in phase A. When the temperature of the raw materials in phase A rises to 45-50° C., use an agitator to start stirring, set the stirring speed to 30 rpm, and stir for 5-10 minutes until the materials are evenly mixed.
4. The method for preparing a hair fluffy spray containing silica according to claim 1, characterized in that: After the raw materials in phase A are mixed evenly, the raw materials in phase B are put into a container, and the mixing and stirring includes the following steps: S31. Put the raw materials in phase B into a container, start stirring, set the stirring speed to 30 rpm, and the stirring time to 20-30 minutes. After the stirring is completed, start homogenization once, set the homogenization speed to 8000 rpm, and the homogenization time to 1 minute to mix the materials evenly.
5. The method for preparing a hair fluffy spray containing silica according to claim 1, characterized in that: The mixed liquid is cooled and the temperature is detected. When the temperature drops to 30° C., the C phase raw material is added and stirred, and finally the D phase raw material is added and stirred evenly. The steps include: S41, cooling the mixed liquid and using a thermometer to detect the temperature. When the temperature drops to 30°C, adding the C phase raw material and stirring, setting the stirring speed to 20 rpm and the stirring time to 3-5 minutes; S42. After the stirring of phase A, phase B and phase C raw materials is completed, continue to add phase D raw materials and stir until the materials are evenly mixed.
6. The method for preparing a hair fluffy spray containing silica according to claim 1, characterized in that: The specific steps of testing the pH value of the successfully prepared liquid, verifying that the spray pH value is within the normal range, and finally filtering the successfully prepared liquid include: S51, using a pH meter to detect the pH value of the liquid to ensure that the pH value is within a normal range. If the pH value is abnormal, the pH value of the liquid is adjusted to make it within a normal range; S52. Slowly pour the successfully prepared liquid into the filter to ensure uniform flow rate and prevent the filter from being overloaded or blocked. Meanwhile, observe the flow of liquid during the filtering process. Collect the filtered liquid in a clean container and finally fill the liquid into a spray bottle to complete the production.
7. A hair volumizing spray containing silica according to any one of claims 1 to 6, characterized in that: The spray contains the following ingredients: water, grease adsorbent, antistatic agent, volatile agent, suspension aid, system stabilizer, and fragrance agent; The grease adsorbent is 200 silica, the antistatic agent is CARBOWAX TM SENTRY TM Polyethylene Glycol 1450NF Flake Polyethylene Glycol-32 and CARBOWAX TM SENTRYPolyethylene Glycol 400NF polyethylene glycol-8, the volatile agent is ethanol, the suspending aid is magnesium aluminum silicate, the system stabilizer is sodium lauryl polyether sulfate and sodium methyl coconut oil acyl taurate, and the flavoring agent is essence.
Citation Information
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