Reticulate embossment glaze and preparation method thereof
Through the formulation of three-layer glaze and high-temperature firing technology, the problem that existing relief glazes are difficult to achieve complex relief effects is solved, and the mesh relief glaze with low lead and cadmium content and high thermal stability is achieved to meet market demand and meet export requirements. standard.
Patent Information
- Application Number
- CN202411407400.4
- Authority / Receiving Office
- CN · China
- Patent Type
- Applications(China)
- Current Assignee / Owner
- Filing Date
- 2024-10-10
- Publication Date
- 2025-01-10
- Estimated Expiration
- 2044-10-10
AI Technical Summary
The existing relief glaze technology is difficult to achieve complex relief effects, and lead-containing metal glaze is not suitable for export daily porcelain production and cannot meet market demand.
The three-layer glaze formula is adopted, including base glaze, surface glaze and spray point glaze. By controlling the composition and thickness of each glaze, combined with high-temperature firing technology, a mesh-like relief effect is formed, with low lead and cadmium content and thermal stability. High, gentle luster and delicate touch.
The complex embossing effect has been achieved, with low content of lead and cadmium, high thermal stability, warm luster and delicate touch, which meets market demand and meets export quality standards.
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Figure BDA0005077030260000061 
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Abstract
Description
Technical Field
[0001] The invention belongs to the technical field of daily-use stoneware glaze preparation, and particularly relates to a reticulated relief glaze and a preparation method thereof. Background Art
[0002] Daily-use ceramics mainly include fine porcelain, stoneware, fine pottery, and coarse pottery. The main difference lies in the water absorption rate of the finished ceramics. The water absorption rate of stoneware is between 0.5% and 3%, and the firing temperature is between 1160 and 1260 degrees Celsius. Stoneware is mainly decorated with colored glazes. Because the firing temperature is relatively low, it is suitable for the coloring of various inorganic ceramic pigments, so colored glaze stoneware is currently popular in the world. Colored glaze stoneware pursues novelty, novelty, and uniqueness in decoration, and at the same time gives it certain cultural connotations or other aesthetic wills. Colored glaze stoneware truly makes daily-use ceramics artistic and artistic ceramics daily-use.
[0003] The invention patent with patent publication number CN104016722A discloses a reaction glaze with relief effect, including a base glaze and a surface glaze, characterized in that the components of the base glaze and the mass parts of each component are as follows: feldspar: 31 parts to 35 parts; quartz: 20 parts to 23 parts; calcite: 12 parts to 15 parts; Guizhou soil: 4 parts to 5 parts; zinc oxide: 2.5 parts to 5 parts; zirconium silicate: 8 parts to 10 parts; strontium carbonate: 5 parts to 8 parts; the components of the surface glaze and the mass parts of each component are as follows: feldspar: 23 parts to 25 parts; borax: 20 parts to 25 parts; quartz 12 parts to 15 parts; calcite: 15 parts to 18 parts; Guizhou soil 3 parts to 5 parts; zinc oxide: 15 parts to 17 parts; zirconium silicate: 8 parts to 10 parts; titanium oxide 9 parts to 10 parts; color base: 11 parts to 15 parts. This technical solution can make the glaze surface appear concave and convex, with a simple relief effect, but it cannot achieve complex relief effects and has limitations.
[0004] The patent application with the patent publication number CN104909832A discloses a gold metal glaze and its preparation method. The components and mass percentages of the gold metal glaze are as follows: potassium feldspar: 35-40 parts; kaolin: 5-8 parts; quartz: 8-12 parts; high expansion coefficient frit: 3-5 parts; barium carbonate: 4-7 parts; high lead frit: 15-25 parts; vanadium pentoxide: 1-2 parts; manganese dioxide: 10-12 parts; copper oxide: 1-3 parts; talc: 1-2 parts. This patent is a glaze formula. By adding high lead powder, it breaks the traditional lead-free metal glaze mode. It can make the metallic luster of the oxide more stable, but it does not have a relief effect. Because it contains lead, it is not suitable for the production of daily-use porcelain for export, that is, it does not meet the export quality standards.
[0005] In the prior art, the embossed glaze production process requires the use of a special rubber roller or a printing screen with optimized mesh count to print the special glaze on the base glaze and top glaze, and then sinter at high temperature to make the special glaze pattern sink into the ordinary top glaze. In view of the defects of the prior art, it is of great significance to research and develop a mesh-like embossed glaze to meet the current market demand. Summary of the invention
[0006] The technical problem to be solved by the present invention is to provide a mesh relief glaze and a preparation method thereof, so as to obtain a mesh relief glaze with low lead and cadmium content, high thermal stability, warm gloss and delicate touch.
[0007] The content of the present invention includes:
[0008] A net-like relief glaze comprises a base glaze, a surface glaze and a spray glaze, wherein the base glaze comprises the following raw materials in parts by weight: 13-17 parts of 3# frit, 38-42 parts of potassium feldspar, 14-20 parts of quartz, 10-15 parts of calcite, 2-6 parts of barium carbonate, 3-7 parts of calcined talc, 3-7 parts of calcined zinc, 3-7 parts of Guizhou soil, 1-5 parts of zirconium silicate, and 0.1-10 parts of synthetic coloring agent;
[0009] The glaze comprises the following raw materials in parts by weight: 8-15 parts of 2# frit, 38-42 parts of potassium feldspar, 14-20 parts of quartz, 13-17 parts of calcite, 3-7 parts of barium carbonate, 1-3 parts of calcined talc, 3-7 parts of calcined zinc, 8-12 parts of longyan mud, 15-22 parts of zirconium silicate, 3-7 parts of titanium dioxide, 1-3 parts of calcined bone carbon, and 0-10 parts of synthetic coloring agent;
[0010] The spray glaze comprises the following raw materials in parts by weight: 14-18 parts of 3# frit, 38-42 parts of potassium feldspar, 8-12 parts of quartz, 10-14 parts of calcite, 3-7 parts of barium carbonate, 1-3 parts of calcined talc, 3-7 parts of calcined zinc, 8-12 parts of longyan mud and 6-10 parts of vanadium pentoxide.
[0011] In one embodiment, the base glaze includes the following raw materials in parts by weight: 15 parts of 3# frit, 40 parts of potassium feldspar, 16 parts of quartz, 12 parts of calcite, 4 parts of barium carbonate, 5 parts of calcined talc, 5 parts of calcined zinc, 5 parts of Guizhou soil, 3 parts of zirconium silicate, and 7 parts of synthetic colorant;
[0012] The glaze comprises the following raw materials in parts by weight: 10 parts of 2# frit, 40 parts of potassium feldspar, 16 parts of quartz, 15 parts of calcite, 5 parts of barium carbonate, 2 parts of calcined talc, 5 parts of calcined zinc, 10 parts of longyan mud, 20 parts of zirconium silicate, 5 parts of titanium dioxide, 2 parts of calcined bone carbon, and 10 parts of synthetic coloring agent;
[0013] The spray glaze comprises the following raw materials in parts by weight: 16 parts of 3# frit, 40 parts of potassium feldspar, 10 parts of quartz, 12 parts of calcite, 5 parts of barium carbonate, 2 parts of calcined talc, 5 parts of calcined zinc, 10 parts of longyan mud, and 8 parts of vanadium pentoxide.
[0014] Another object of the present invention is to provide a method for preparing the above-mentioned reticulated relief glaze, comprising the following steps:
[0015] (1) preparing a ceramic wet blank and drying it to form a ceramic dry blank;
[0016] (2) Applying a base glaze on the surface of the ceramic blank, spraying a top glaze, and finally spraying a spray point glaze of appropriate size to form a ceramic glaze blank;
[0017] (3) drying the ceramic glaze blank to make the moisture content of the blank less than 1%;
[0018] (4) The dried body is put into a kiln for firing to obtain a mesh-like relief glaze product.
[0019] In one embodiment, the thickness of the base glaze in step (2) is 0.10-0.25 mm.
[0020] In one embodiment, the thickness of the glaze in step (2) is 0.10-0.15 mm.
[0021] In one embodiment, the average particle size of the base glaze and top glaze slurry in step (2) is 40-60 μm.
[0022] In one embodiment, the drying temperature of the ceramic wet blank in step (1) is 100-120° C., and the drying time is 70-90 min.
[0023] In one embodiment, the drying temperature of the ceramic glaze blank in step (3) is 100-120° C., and the drying time is 30-50 min.
[0024] In one embodiment, the sintering atmosphere in step (4) is an oxidizing atmosphere.
[0025] In one embodiment, the sintering temperature in step (4) is 1170-1210°C.
[0026] The compositions of the 2# frit and the 3# frit are:
[0027] <![CDATA[SiO2]]> <![CDATA[Al2O3]]> <![CDATA[B2O3]]> CaO MgO <![CDATA[K2O]]> <![CDATA[Na2O]]> <![CDATA[Li2O]]> 2# Frit 58 7.2 13 6.8 1.5 6.2 7 / 3# Frit 56.2 14 8.1 9.4 / 2 9.5 0.5
[0028] Beneficial effects of the present invention:
[0029] (1) The present invention is presented in the form of three layers of glaze, wherein the base glaze is mainly bright glaze; the surface glaze (middle layer) is mainly bright glaze, which has a certain viscosity and maintains a certain fluidity, and is well combined with the base glaze but has obvious layers, and does not melt or react with each other; then, a uniform coarse dot glaze is sprayed on the two layers of glaze, and the top coarse dot glaze produces a depression, which squeezes the surface glaze (middle layer) glaze to form a mesh, and the base glaze also sinks relatively without exposing the body, forming a net-shaped relief effect, a net-shaped relief glaze with a delicate touch and a warm gloss;
[0030] (2) Adding vanadium pentoxide to the spray glaze formula can enhance the transparency and color layering of the glaze surface. Adding too little will easily lead to unclear relief effect, while adding too much will easily lead to too obvious relief effect and even expose the embryo.
[0031] (3) Adding zirconium silicate to the glaze formula can not only improve the body-glaze separation performance of the ceramic, but also play a role in whitening. Too little addition can easily lead to poor glaze flow and blurred reticulation effect;
[0032] (4) The three-layer glaze of the present invention needs to be added in strict proportion. If a certain component of the glaze formula is added too much or too little, it will affect the relief effect, glaze gloss, texture and other effects of the relief glaze;
[0033] (5) The preparation process of the present invention is simple, the content of lead and cadmium is low, the thermal stability is high, the gloss is warm, and the textured relief glaze with delicate touch is produced. All indicators meet the relevant standard requirements, and the present invention has strong universality and is easy to promote and apply in the industry. The present invention can control the base glaze color and the texture color as needed, which can better meet the design requirements and adapt to customer needs. DETAILED DESCRIPTION
[0034] Example 1
[0035] A formula and preparation method of a reticulated relief glaze, comprising the following steps:
[0036] (1) preparing a ceramic wet blank, drying it at 110°C for 80 minutes to form a ceramic dry blank. Then applying glaze on the surface of the ceramic dry blank to form a ceramic glaze blank; the glaze comprises the following: the base glaze comprises the following components in parts by weight: 15 parts of 3# frit, 40 parts of potassium feldspar, 16 parts of quartz, 12 parts of calcite, 4 parts of barium carbonate, 5 parts of calcined talc, 5 parts of calcined zinc, 5 parts of Guizhou clay, 3 parts of zirconium silicate, 2 parts of vanadium blue, and 5 parts of praseodymium yellow.
[0037] The components of the surface glaze by weight are: 10 parts of 2# frit, 40 parts of potassium feldspar, 16 parts of quartz, 15 parts of calcite, 5 parts of barium carbonate, 2 parts of calcined talc, 5 parts of burned zinc, 10 parts of longyan mud, 20 parts of zirconium silicate, 5 parts of titanium dioxide, 2 parts of calcined bone carbon, and 10 parts of 1519# wrapped red.
[0038] The components of the outermost spray glaze by weight are: 16 parts of 3# frit, 40 parts of potassium feldspar, 10 parts of quartz, 12 parts of calcite, 5 parts of barium carbonate, 2 parts of calcined talc, 5 parts of burned zinc, 10 parts of Longyan mud, and 8 parts of vanadium pentoxide.
[0039] (2) drying the glaze blank at 110°C for 40 minutes to keep the moisture content of the blank below 1%;
[0040] (3) The finished body is put into a kiln and fired at 1200°C in an oxidizing atmosphere. After firing, the product becomes a green-bottomed red-net-patterned embossed stoneware product.
[0041] Example 2
[0042] A formula and preparation method of a reticulated relief glaze, comprising the following steps:
[0043] (1) preparing a ceramic wet blank, drying it at 100°C for 90 minutes to form a ceramic dry blank. Then applying glaze on the surface of the ceramic dry blank to form a ceramic glaze blank; the glaze comprises the following: the base glaze comprises the following components in parts by weight: 15 parts of 3# frit, 40 parts of potassium feldspar, 16 parts of quartz, 12 parts of calcite, 4 parts of barium carbonate, 5 parts of calcined talc, 5 parts of calcined zinc, 5 parts of Guizhou clay, 3 parts of zirconium silicate, 2 parts of vanadium blue, and 5 parts of praseodymium yellow.
[0044] The components of the surface layer glaze by weight are: 12 parts of 2# frit, 40 parts of potassium feldspar, 16 parts of quartz, 15 parts of calcite, 5 parts of barium carbonate, 2 parts of calcined talc, 5 parts of burned zinc, 10 parts of longyan mud, 20 parts of zirconium silicate, 5 parts of titanium dioxide, and 2 parts of calcined bone carbon.
[0045] The components of the outermost spray glaze by weight are: 16 parts of 3# frit, 40 parts of potassium feldspar, 10 parts of quartz, 12 parts of calcite, 5 parts of barium carbonate, 2 parts of calcined talc, 5 parts of burned zinc, 10 parts of Longyan mud, and 8 parts of vanadium pentoxide.
[0046] (2) drying the glaze blank at 100°C for 40 minutes to keep the moisture content of the blank below 1%;
[0047] (3) The green body after the above processing is put into the kiln for firing at 1200℃ in an oxidizing atmosphere. After firing, the product is a green-bottomed white mesh embossed stoneware product.
[0048] Example 3
[0049] A formula and preparation method of a reticulated relief glaze, comprising the following steps:
[0050] (1) preparing a ceramic wet blank, drying it at 110° C. for 80 minutes to form a ceramic dry blank. Then applying glaze on the surface of the ceramic dry blank to form a ceramic glaze blank; the glaze comprises the following: the base glaze comprises the following components in parts by weight: 15 parts of 3# frit, 40 parts of potassium feldspar, 16 parts of quartz, 12 parts of calcite, 4 parts of barium carbonate, 5 parts of calcined talc, 5 parts of calcined zinc, 5 parts of Guizhou soil, 3 parts of zirconium silicate, and 6 parts of orange red.
[0051] The components of the surface layer glaze by weight are: 12 parts of 2# frit, 40 parts of potassium feldspar, 16 parts of quartz, 15 parts of calcite, 5 parts of barium carbonate, 2 parts of calcined talc, 5 parts of burned zinc, 10 parts of longyan mud, 20 parts of zirconium silicate, 5 parts of titanium dioxide, and 2 parts of calcined bone carbon.
[0052] The components of the outermost spray glaze by weight are: 16 parts of 3# frit, 40 parts of potassium feldspar, 10 parts of quartz, 12 parts of calcite, 5 parts of barium carbonate, 2 parts of calcined talc, 5 parts of burned zinc, 10 parts of Longyan mud, and 8 parts of vanadium pentoxide.
[0053] (2) drying the glaze blank at 110°C for 40 minutes to keep the moisture content of the blank below 1%;
[0054] (3) The green body after the above processing is put into the kiln for firing at 1200℃ in an oxidizing atmosphere. After firing, the product is a red-bottomed white mesh embossed stoneware product.
[0055] Example 4
[0056] A formula and preparation method of a reticulated relief glaze, comprising the following steps:
[0057] (1) A ceramic wet blank is prepared and dried at 120°C for 70 minutes to form a ceramic dry blank. Then a glaze is applied on the surface of the ceramic dry blank to form a ceramic glaze blank; the glaze comprises the following: the base glaze comprises the following components in parts by weight: 15 parts of 3# frit, 40 parts of potassium feldspar, 16 parts of quartz, 12 parts of calcite, 4 parts of barium carbonate, 5 parts of calcined talc, 5 parts of calcined zinc, 5 parts of Guizhou soil, 3 parts of zirconium silicate, 5 parts of dark blue, and 0.5 parts of brilliant black.
[0058] The components of the surface layer glaze by weight are: 12 parts of 2# frit, 40 parts of potassium feldspar, 16 parts of quartz, 15 parts of calcite, 5 parts of barium carbonate, 2 parts of calcined talc, 5 parts of burned zinc, 10 parts of longyan mud, 20 parts of zirconium silicate, 5 parts of titanium dioxide, and 2 parts of calcined bone carbon.
[0059] The components of the outermost spray glaze by weight are: 16 parts of 3# frit, 40 parts of potassium feldspar, 10 parts of quartz, 12 parts of calcite, 5 parts of barium carbonate, 2 parts of calcined talc, 5 parts of burned zinc, 10 parts of Longyan mud, and 8 parts of vanadium pentoxide.
[0060] (2) drying the glaze blank at 120°C for 30 minutes to keep the moisture content of the blank below 1%;
[0061] (3) The green body after the above processing is put into the kiln and fired at 1180℃ in an oxidizing atmosphere. After firing, the product is a blue-bottomed white mesh embossed stoneware product.
[0062] Example 5
[0063] A formula and preparation method of a reticulated relief glaze, comprising the following steps:
[0064] (1) A ceramic wet blank is prepared and dried at 110° C. for 80 minutes to form a ceramic dry blank. Then a glaze is applied on the surface of the ceramic dry blank to form a ceramic glaze blank; the glaze comprises the following: the base glaze comprises the following components in parts by weight: 15 parts of 3# frit, 40 parts of potassium feldspar, 16 parts of quartz, 12 parts of calcite, 4 parts of barium carbonate, 5 parts of calcined talc, 5 parts of calcined zinc, 5 parts of Guizhou soil, 3 parts of zirconium silicate, 5 parts of dark blue, and 0.5 parts of brilliant black.
[0065] The components of the surface glaze by weight are: 12 parts of 2# frit, 40 parts of potassium feldspar, 16 parts of quartz, 15 parts of calcite, 5 parts of barium carbonate, 2 parts of calcined talc, 5 parts of calcined zinc, 10 parts of Longyan mud, 20 parts of zirconium silicate, 5 parts of titanium dioxide, 2 parts of calcined bone carbon. 10 parts of 1519# wrapped red.
[0066] The components of the outermost spray glaze by weight are: 16 parts of 3# frit, 40 parts of potassium feldspar, 10 parts of quartz, 12 parts of calcite, 5 parts of barium carbonate, 2 parts of calcined talc, 5 parts of burned zinc, 10 parts of Longyan mud, and 8 parts of vanadium pentoxide.
[0067] (2) drying the glaze blank at 110°C for 40 minutes to keep the moisture content of the blank below 1%;
[0068] (3) The finished body is put into a kiln and fired at 1200°C in an oxidizing atmosphere. After firing, the product becomes a blue-bottomed red-net-shaped embossed stoneware product with an overall purple tint.
[0069] Example 6
[0070] The components of the spray glaze by weight are: 18 parts of 3# frit, 38 parts of potassium feldspar, 12 parts of quartz, 12 parts of calcite, 7 parts of barium carbonate, 2 parts of calcined talc, 3 parts of burned zinc, 12 parts of Longyan mud, and 6 parts of vanadium pentoxide.
[0071] The rest is the same as in Example 1.
[0072] Example 7
[0073] The components of the surface glaze by weight are: 15 parts of 2# frit, 38 parts of potassium feldspar, 14 parts of quartz, 13 parts of calcite, 5 parts of barium carbonate, 3 parts of calcined talc, 5 parts of burned zinc, 12 parts of longyan mud, 18 parts of zirconium silicate, 5 parts of titanium dioxide, 2 parts of calcined bone carbon, and 8 parts of synthetic colorant 5010# package yellow.
[0074] The rest is the same as in Example 1.
[0075] Example 8
[0076] The formula of the base glaze is 13 parts of 3# frit, 42 parts of potassium feldspar, 14 parts of quartz, 12 parts of calcite, 5 parts of barium carbonate, 7 parts of calcined talc, 3 parts of burned zinc, 4 parts of Guizhou soil, 5 parts of zirconium silicate, and 7 parts of synthetic colorant 5010# wrapped yellow.
[0077] The rest is the same as in Example 1.
[0078] Comparative Example 1
[0079] The vanadium pentoxide in the spray glaze formula is reduced to 3 parts, and the rest is the same as in Example 1.
[0080] Comparative Example 2
[0081] The vanadium pentoxide in the spray glaze formula is increased to 18 parts, and the rest is the same as in Example 1.
[0082] Comparative Example 3
[0083] The zirconium silicate content of the glaze layer is reduced to 5 parts, the zinc content is increased to 10 parts, and the rest is the same as in Example 1.
[0084] Comparative Example 4
[0085] Compared with Example 1, no top glaze is used, and the bottom glaze is directly sprayed, that is, the middle glaze layer is reduced. Other aspects are the same as Example 1.
[0086] Comparative Example 5
[0087] The components of the surface glaze by weight are: 5 parts of 2# frit, 35 parts of potassium feldspar, 22 parts of quartz, 10 parts of calcite, 10 parts of barium carbonate, 5 parts of calcined talc, 8 parts of burned zinc, 5 parts of longyan mud, 25 parts of zirconium silicate, 2 parts of titanium dioxide, 5 parts of calcined bone carbon, and 8 parts of synthetic colorant 1519# wrapped red.
[0088] The other base glaze and spray glaze components are the same as those in Example 1, and the preparation method is the same as that in Example 1.
[0089] Comparative Example 6
[0090] The components of the spray glaze by weight are: 8 parts of 3# frit, 45 parts of potassium feldspar, 6 parts of quartz, 16 parts of calcite, 10 parts of barium carbonate, 5 parts of calcined talc, 2 parts of burned zinc, 6 parts of Longyan mud, and 10 parts of vanadium pentoxide.
[0091] The other base glaze and top glaze components are the same as those in Example 1, and the preparation method is the same as that in Example 1.
[0092] The test results are shown in the following table.
[0093] Table 1 Product quality inspection results
[0094]
[0095]
[0096] A person skilled in the art should understand that the discussion of any of the above embodiments is merely illustrative and is not intended to imply that the scope of protection of the present application is limited to these examples. In line with the concept of the present application, the technical features in the above embodiments or different embodiments may be combined, the steps may be implemented in any order, and there are many other variations of different aspects of one or more embodiments of the present application as described above, which are not provided in detail for the sake of simplicity.
[0097] One or more embodiments of the present application are intended to cover all such substitutions, modifications and variations that fall within the broad scope of the present application. Therefore, any omissions, modifications, equivalent substitutions, improvements, etc. made within the spirit and principles of one or more embodiments of the present application should be included in the protection scope of the present application.
Claims
1. A mesh relief glaze, characterized in that: The invention comprises a base glaze, a surface glaze and a spray glaze, wherein the base glaze comprises the following raw materials in parts by weight: 13-17 parts of 3# frit, 38-42 parts of potassium feldspar, 14-20 parts of quartz, 10-15 parts of calcite, 2-6 parts of barium carbonate, 3-7 parts of calcined talc, 3-7 parts of calcined zinc, 3-7 parts of Guizhou soil, 1-5 parts of zirconium silicate and 0.1-10 parts of synthetic colorant; The glaze comprises the following raw materials in parts by weight: 8-15 parts of 2# frit, 38-42 parts of potassium feldspar, 14-20 parts of quartz, 13-17 parts of calcite, 3-7 parts of barium carbonate, 1-3 parts of calcined talc, 3-7 parts of calcined zinc, 8-12 parts of longyan mud, 15-22 parts of zirconium silicate, 3-7 parts of titanium dioxide, 1-3 parts of calcined bone carbon, and 0-10 parts of synthetic coloring agent; The spray glaze comprises the following raw materials in parts by weight: 14-18 parts of 3# frit, 38-42 parts of potassium feldspar, 8-12 parts of quartz, 10-14 parts of calcite, 3-7 parts of barium carbonate, 1-3 parts of calcined talc, 3-7 parts of calcined zinc, 8-12 parts of longyan mud and 6-10 parts of vanadium pentoxide.
2. The reticulated relief glaze according to claim 1, characterized in that: The base glaze comprises the following raw materials in parts by weight: 15 parts of 3# frit, 40 parts of potassium feldspar, 16 parts of quartz, 12 parts of calcite, 4 parts of barium carbonate, 5 parts of calcined talc, 5 parts of calcined zinc, 5 parts of Guizhou soil, 3 parts of zirconium silicate, and 7 parts of synthetic coloring agent; The glaze comprises the following raw materials in parts by weight: 10 parts of 2# frit, 40 parts of potassium feldspar, 16 parts of quartz, 15 parts of calcite, 5 parts of barium carbonate, 2 parts of calcined talc, 5 parts of calcined zinc, 10 parts of longyan mud, 20 parts of zirconium silicate, 5 parts of titanium dioxide, 2 parts of calcined bone carbon, and 10 parts of synthetic coloring agent; The spray glaze comprises the following raw materials in parts by weight: 16 parts of 3# frit, 40 parts of potassium feldspar, 10 parts of quartz, 12 parts of calcite, 5 parts of barium carbonate, 2 parts of calcined talc, 5 parts of calcined zinc, 10 parts of longyan mud, and 8 parts of vanadium pentoxide.
3. A method for preparing a reticulated relief glaze as claimed in claim 1 or 2, characterized in that: The steps include: (1) preparing a ceramic wet blank and drying it to form a ceramic dry blank; (2) Applying a base glaze on the surface of the ceramic blank, spraying a top glaze, and finally spraying a spray point glaze of appropriate size to form a ceramic glaze blank; (3) drying the ceramic glaze blank to make the moisture content of the blank less than 1%; (4) The dried body is put into a kiln for firing to obtain a mesh-like relief glaze product.
4. The method for preparing the reticulated relief glaze according to claim 3, characterized in that: The thickness of the base glaze in step (2) is 0.10-0.25 mm.
5. The method for preparing the reticulated relief glaze according to claim 3, characterized in that: The thickness of the glaze in step (2) is 0.10-0.15 mm.
6. The method for preparing the reticulated relief glaze according to claim 3, characterized in that: The average particle size of the slurry of the base glaze and the top glaze in step (2) is 40-60 μm.
7. The method for preparing the reticulated relief glaze according to claim 3, characterized in that: The drying temperature of the ceramic wet blank in the step (1) is 100-120° C., and the drying time is 70-90 min.
8. The method for preparing the reticulated relief glaze according to claim 3, characterized in that: The drying temperature of the ceramic glaze blank in the step (3) is 100-120° C., and the drying time is 30-50 min.
9. The method for preparing the reticulated relief glaze according to claim 3, characterized in that: The firing atmosphere in the step (4) is an oxidizing atmosphere.
10. The method for preparing the reticulated relief glaze according to any one of claims 3 to 9, characterized in that: The calcination temperature in step (4) is 1170-1210°C.
Citation Information
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