Preparation method of biochemical product additive

Abstract

The invention relates to the technical field of biochemical products, in particular to a preparation method of a biochemical product additive, which comprises the following steps: S1, preparing attapulgite powder, wormwood and honeysuckle, airing the attapulgite powder, then crushing and grinding, and sieving by an electronic sieve to prepare a first powdery mixture of 200-800 meshes; s2, putting wormwood into a distillation generator, extracting wormwood essential oil, and then preparing wormwood alcohol dew from the wormwood essential oil; s3, putting the honeysuckle flowers into a distillation generator, heating, distilling, condensing and separating to obtain honeysuckle flower distillate; s4, mixing and stirring 90 to 120 parts of the prepared first mixture, 120 to 200 parts of wormwood alcohol distillate, 120 to 200 parts of honeysuckle distillate and 480 to 670 parts of water; s5, bottling and packaging the prepared liquid; and S6, sterilizing and disinfecting the prepared solution, and finally warehousing. The use safety of the additive is ensured.

Description

Technical Field

[0001] The present invention relates to the technical field of biochemical products, and in particular to a method for preparing a biochemical product additive. Background Art

[0002] When preparing biochemical additives, it is often necessary to add some additives. When adding additives, the existing additives may contain silicon oxide, chromium oxide, aluminum oxide, lead, mercury, arsenic, hexavalent chromium, polybrominated biphenyls, and polybrominated ethers, which may cause excessive levels of heavy metal elements and harmful pollutants, seriously affecting the safety of the additives. In order to solve this problem, we proposed a method for preparing biochemical additives. Summary of the invention

[0003] The purpose of the present invention is to solve the shortcomings of the existing technology that the heavy metal elements and harmful pollutants exceed the standard, and propose a preparation method of a biochemical additive.

[0004] In order to achieve the above object, the present invention adopts the following technical solutions: A method for preparing a biochemical additive is designed, comprising the following steps: S1, preparing attapulgite powder, wormwood, and honeysuckle, drying the attapulgite powder, then crushing and grinding it, and sieving it through an electronic sieve to prepare a first mixture in a powdery state of 200-800 meshes; S2, putting the wormwood into a distillation generator to extract the wormwood essential oil, and then using the wormwood essential oil to prepare wormwood alcohol dew; S3, putting honeysuckle into a distillation generator, heating, distilling, condensing, and separating to obtain honeysuckle dew; S4, mixing 90-120 parts of the prepared first mixture, 120-200 parts of wormwood alcohol dew, 120-200 parts of honeysuckle dew, and 480-670 parts of water; S5, bottling and packaging the prepared liquid; S6. Sterilize and disinfect the prepared solution and finally put it into storage.

[0005] Preferably, the preparation of wormwood alcohol dew in step S2 includes the following steps: S21, putting wormwood into a distiller for distillation, the temperature during distillation is 105-110 ° C, the time is 1-2h, and its volatiles are condensed and collected to obtain wormwood essential oil; S22, the obtained wormwood essential oil is put into a distiller, pure water is added at the same time, and a first distillation is performed to obtain a crude liquid, the distillation temperature is 100-106 ° C, and the time is 30-45min, then pure water is added to the crude liquid, and a second distillation is performed, the temperature during distillation is 102-104 ° C, and the time is 60-75min, and condensation obtains wormwood alcohol dew.

[0006] Preferably, when adding purified water, the weight of the purified water added is equal to the weight of the distillate.

[0007] Preferably, in step S4, when stirring and mixing, first mix the wormwood alcohol extract, honeysuckle extract and water, and then add the attapulgite powder to mix. When mixing, stir it with a spiral stirring blade to stir the attapulgite powder that has settled to the bottom, thereby ensuring the mixing effect.

[0008] Preferably, in step S3, dry honeysuckle is prepared and soaked for 30-40 minutes.

[0009] Preferably, the steps of distilling, condensing and separating honeysuckle include: The softened water is added to a steam generator for heating and pressurization to reach a temperature of 110°C and a pressure of 1.2 standard atmospheres; the dried honeysuckle is placed in a distiller, and a small amount of water is added to moisten it. Suizhou pressurizes and seals the distiller, opens the heating and pressurization valve for distillation, and the ratio of water to honeysuckle is 10:1 during distillation. When collecting honeysuckle dew, it needs to be done under sterile and dust-free conditions, and high-temperature disinfection is performed after extraction.

[0010] Preferably, during disinfection and sterilization, the bottled items are placed in a pressure cooker, the temperature in the pressure cooker increases with the increase of steam pressure, and the steam pressure is controlled at 102-103.5 kPa, while the added temperature is controlled at 120-125° C., and the heating time is 20-30 min.

[0011] The invention provides a preparation method for a biochemical additive, which has the beneficial effects of reducing the content of heavy metal elements in the additive and excluding harmful pollutants such as polybrominated biphenyls and polybrominated ethers, thereby avoiding harm to the body and ensuring the safety of the additive. DETAILED DESCRIPTION

[0012] The technical solutions in the embodiments of the present invention will be clearly and completely described below in conjunction with the embodiments of the present invention. Obviously, the described embodiments are only part of the embodiments of the present invention, rather than all the embodiments.

[0013] Embodiment 1: A method for preparing a biochemical additive, comprising the following steps: S1, preparing attapulgite powder, wormwood, and honeysuckle, drying the attapulgite powder, then crushing and grinding the attapulgite powder, and sieving the powder through an electronic sieve to prepare a first mixture in a 200-mesh powder form; S2, putting the wormwood into a distillation generator to extract the wormwood essential oil, and then using the wormwood essential oil to prepare wormwood alcohol dew; S3, putting honeysuckle into a distillation generator, heating, distilling, condensing, and separating to obtain honeysuckle dew; S4, mixing 90 parts of the prepared first mixture, 120 parts of wormwood alcohol dew, 120 parts of honeysuckle dew, and 480 parts of water; S5, bottling and packaging the prepared liquid; S6, sterilize and disinfect the prepared solution, and finally store it in storage; The preparation of wormwood alcohol dew in step S2 includes the following steps: S21, putting wormwood into a distiller for distillation, the temperature during distillation is 105 ° C, the time is 1h, and its volatiles are condensed and collected to obtain wormwood essential oil; S22, the obtained wormwood essential oil is put into a distiller, pure water is added simultaneously, and a first distillation is performed to obtain a thick liquid, and the temperature of the distillation is 100 ° C, and the time is 30 min, and then pure water is added to the thick liquid, and a second distillation is performed, and the temperature during the distillation is 102 ° C, and the time is 75 min, and condensation obtains wormwood alcohol dew.

[0014] When adding purified water, the weight of the purified water added is equal to the weight of the distillate.

[0015] In step S4, when stirring and mixing, first mix the wormwood alcohol extract, honeysuckle extract and water, and then add the attapulgite powder into the mixture. When mixing, stir it with a spiral stirring blade to stir the attapulgite powder that has settled to the bottom, thereby ensuring the mixing effect.

[0016] In step S3, dry honeysuckle is prepared and soaked for 30 minutes.

[0017] The steps of distilling, condensing and separating honeysuckle include: The softened water is added to a steam generator for heating and pressurization to reach a temperature of 110°C and a pressure of 1.2 standard atmospheres; the dried honeysuckle is placed in a distiller, and a small amount of water is added to moisten it. Suizhou pressurizes and seals the distiller, opens the heating and pressurization valve for distillation, and the ratio of water to honeysuckle is 10:1 during distillation. When collecting honeysuckle dew, it needs to be done under sterile and dust-free conditions, and high-temperature disinfection is performed after extraction.

[0018] During disinfection and sterilization, the bottled items are placed in a pressure cooker. The temperature in the pressure cooker increases with the increase of steam pressure. The steam pressure is controlled at 102 kPa, and the added temperature is controlled at 120°C. The heating time is 20 minutes.

[0019] The prepared additive is mixed with other ingredients to prepare wormwood shampoo, which includes the following ingredients: 100 parts of water, 0.5 parts of sodium laureth sulfate, 0.1 parts of ammonium lauryl sulfate, 0.14 parts of ethylene glycol distearate, 0.21 parts of polydimethylsiloxane, 0.35 parts of sodium chloride, 0.7 parts of potassium cocoyl hydrolyzed oat protein, 1 part of acrylic copolymer, 0.9 parts of cocamide MEA, 0.35 parts of sodium methyl cocoyl taurate, 1 part of essence, 2 parts of sodium cocamidopropyl PG-dimethyl ammonium chloride phosphate, 10 parts of glycerin, 15 parts of maleic acid modified castor oil, 4 parts of guar hydroxypropyltrimonium chloride, 0.5 parts of laureth-23, 5 parts of DMDM ​​hydantoin, 3 parts of potassium chloride, 0.19 parts of C12-15 polyether-3, 2 parts of hydrolyzed corn starch, and 3 parts of additives.

[0020] The content of heavy metal elements in the additives in the shampoo is reduced, and the shampoo does not contain harmful pollutants such as polybrominated biphenyls and polybrominated ethers, thus avoiding harm to the body and ensuring the safety of the additives. At the same time, the wormwood alcohol dew contained in the shampoo is volatile and insect repellent, and has a fragrance that is beneficial to the effect of refreshing the mind. At the same time, because the additive contains attapulgite powder, which is a natural silicate mineral matrix with excellent decolorization, adsorption, ion exchange, thermal stability, salt resistance, gelation and high-temperature phase change properties, the attapulgite powder in the shampoo plays the role of oil control, cleaning and antibacterial repair. This natural ingredient can effectively It helps control the oil secretion of the scalp, keeps the scalp clean and healthy, and helps repair the damaged scalp environment and promote the health of the scalp. The addition of attapulgite powder can also enhance the stability of the shampoo, making it more gentle and safe during use, and protect the scalp and hair. At the same time, the additive contains honeysuckle, which has anti-inflammatory and antibacterial properties and can effectively improve scalp problems caused by inflammation and infection, such as skin itching, dandruff and acne. These properties are very beneficial for maintaining scalp health and reducing scalp inflammation and infection. The additive contains wormwood, and the addition of wormwood to the shampoo The hair water has the functions of relieving itching, removing dandruff, protecting hair, promoting hair growth, Improve the scalp environment.

[0021] Embodiment 2: A method for preparing a biochemical additive comprises the following steps: S1, preparing attapulgite powder, wormwood, and honeysuckle, drying the attapulgite powder, then crushing and grinding it, and sieving it through an electronic sieve to prepare a first mixture in the form of 800-mesh powder; S2, putting the wormwood into a distillation generator to extract the wormwood essential oil, and then using the wormwood essential oil to prepare wormwood alcohol dew; S3, putting honeysuckle into a distillation generator, heating, distilling, condensing, and separating to obtain honeysuckle dew; S4, mixing 120 parts of the prepared first mixture, 200 parts of wormwood alcohol dew, 200 parts of honeysuckle dew, and 670 parts of water; S5, bottling and packaging the prepared liquid; S6. Sterilize and disinfect the prepared solution and finally put it into storage.

[0022] The preparation of wormwood alcohol dew in step S2 includes the following steps: S21, put the wormwood into a distiller for distillation, the temperature during distillation is 110 ° C, the time is 2h, and its volatiles are condensed and collected to obtain wormwood essential oil; S22, the obtained wormwood essential oil is put into a distiller, pure water is added simultaneously, and a first distillation is performed to obtain a crude liquid, the temperature of the distillation is 106 ° C, and the time is 45 min, and then pure water is added to the crude liquid, and a second distillation is performed, and the temperature during distillation is 104 ° C, and the time is 75 min, and condensation obtains wormwood alcohol dew.

[0023] When adding purified water, the weight of the purified water added is equal to the weight of the distillate.

[0024] In step S4, when stirring and mixing, first mix the wormwood alcohol extract, honeysuckle extract and water, and then add the attapulgite powder into the mixture. When mixing, stir it with a spiral stirring blade to stir the attapulgite powder that has settled to the bottom, thereby ensuring the mixing effect.

[0025] In step S3, dry honeysuckle is prepared and soaked for 40 minutes.

[0026] The steps of distilling, condensing and separating honeysuckle include: The softened water is added to a steam generator for heating and pressurization to reach a temperature of 110°C and a pressure of 1.2 standard atmospheres; the dried honeysuckle is placed in a distiller, and a small amount of water is added to moisten it. Suizhou pressurizes and seals the distiller, opens the heating and pressurization valve for distillation, and the ratio of water to honeysuckle is 10:1 during distillation. When collecting honeysuckle dew, it needs to be done under sterile and dust-free conditions, and high-temperature disinfection is performed after extraction.

[0027] During disinfection and sterilization, the bottled items are placed in a pressure cooker. The temperature in the pressure cooker increases with the increase of steam pressure. The steam pressure is controlled at 103.5 kPa, and the added temperature is controlled at 125°C. The heating time is 30 minutes.

[0028] The prepared additives are mixed into other ingredients to prepare wormwood shower gel, which includes the following ingredients: 50 parts of water, 2 parts of sodium laureth sulfate, 1 part of ammonium lauryl sulfate, 10 parts of glycerin, 1 part of acrylic acid, 0.2 parts of cocamidopropyl betaine, 0.1 parts of magnesium aluminum silicate, 2 parts of flavor, 3 parts of sodium chloride, 0.5 parts of sodium lauroylamphoacetate, 0.3 parts of DMDM ​​hydantoin, 6 parts of dichlorobenzyl alcohol, 0.4 parts of sodium hydroxide, and 2 parts of additives.

[0029] The content of heavy metal elements in the additives in the shower gel is reduced, and at the same time, it does not contain harmful pollutants such as polybrominated biphenyls and polybrominated ethers, avoiding harm to the body, thereby ensuring the safety of the additive. Since the additive contains attapulgite powder, the attapulgite powder can effectively help maintain the moisture of the skin and reduce skin problems caused by dryness. In addition, the addition of attapulgite powder can also help maintain the acid-base balance of the skin and avoid skin discomfort caused by too high or too low pH value. As an ingredient in shower gel, attapulgite not only provides moisture, but also maintains the acid-base balance of the skin. Balance, thus helping to improve skin condition, making the bathing process more pleasant and comfortable. Because the additive contains wormwood, wormwood is warm in nature and enters the spleen, liver, and kidney meridians. When used externally, it can relieve skin itching and remove moisture to a certain extent, so that the shower gel can maintain the skin, keep the skin moisturized, and avoid dry skin. Because the additive contains honeysuckle, when added to the shower gel, the chlorogenic acid and luteolin components contained in the honeysuckle have good antibacterial and anti-inflammatory effects, and can inhibit the growth and reproduction of a variety of bacteria and fungi, thereby having a certain alleviating effect on skin itching, eczema and other skin disease symptoms.

[0030] The above description is only a preferred specific implementation manner of the present invention, but the protection scope of the present invention is not limited thereto. Any technician familiar with the technical field can make equivalent replacements or changes according to the technical scheme and inventive concept of the present invention within the technical scope disclosed by the present invention, which should be covered by the protection scope of the present invention.

Claims

1. A method for preparing a biochemical additive, characterized in that: The following steps are involved: S1, preparing attapulgite powder, wormwood, and honeysuckle, drying the attapulgite powder, then crushing and grinding it, and sieving it through an electronic sieve to prepare a first mixture in a powdery state of 200-800 meshes; S2, putting the wormwood into a distillation generator to extract the wormwood essential oil, and then using the wormwood essential oil to prepare wormwood alcohol dew; S3, putting honeysuckle into a distillation generator, heating, distilling, condensing, and separating to obtain honeysuckle dew; S4, mixing 90-120 parts of the prepared first mixture, 120-200 parts of wormwood alcohol dew, 120-200 parts of honeysuckle dew, and 480-670 parts of water; S5, bottling and packaging the prepared liquid; S6. Sterilize and disinfect the prepared solution and finally put it into storage.

2. The method for preparing a biochemical additive according to claim 1, characterized in that: The preparation of wormwood alcohol dew in step S2 includes the following steps: S21, putting wormwood into a distiller for distillation, the temperature during distillation is 105-110 ° C, the time is 1-2h, and its volatiles are condensed and collected to obtain wormwood essential oil; S22, the obtained wormwood essential oil is put into a distiller, pure water is added at the same time, and a first distillation is performed to obtain a crude liquid, the distillation temperature is 100-106 ° C, and the time is 30-45min, then pure water is added to the crude liquid, and a second distillation is performed, the temperature during distillation is 102-104 ° C, and the time is 60-75min, and condensation obtains wormwood alcohol dew.

3. The method for preparing a biochemical additive according to claim 2, characterized in that , when adding purified water, the weight of the purified water added should be equal to the weight of the distillate.

4. The method for preparing a biochemical additive according to claim 1, characterized in that: In step S4, when stirring and mixing, first mix the wormwood alcohol extract, honeysuckle extract and water, and then add the attapulgite powder into the mixture. When mixing, stir it with a spiral stirring blade to stir the attapulgite powder that has settled to the bottom, thereby ensuring the mixing effect.

5. The method for preparing a biochemical additive according to claim 1, characterized in that: In step S3, dry honeysuckle is prepared and soaked for 30-40 minutes.

6. The method for preparing a biochemical additive according to claim 5, characterized in that: The steps of distilling, condensing and separating honeysuckle include: The softened water is added to a steam generator for heating and pressurization to reach a temperature of 110°C and a pressure of 1.2 standard atmospheres; the dried honeysuckle is placed in a distiller, and a small amount of water is added to moisten it. Suizhou pressurizes and seals the distiller, opens the heating and pressurization valve for distillation, and the ratio of water to honeysuckle is 10:1 during distillation. When collecting honeysuckle dew, it needs to be done under sterile and dust-free conditions, and high-temperature disinfection is performed after extraction.

7. The method for preparing a biochemical additive according to claim 1, characterized in that: During disinfection and sterilization, the bottled items are placed in a pressure cooker. The temperature in the pressure cooker increases with the increase of steam pressure. The steam pressure is controlled at 102-103.5 kPa. At the same time, the added temperature is controlled at 120-125°C, and the heating time is 20-30 minutes.