Total reflection X-ray fluorescence spectrometer
By adopting a slidingly snap-in compartment door assembly and fixing mechanism in a total reflective X-ray fluorescence spectrometer, combining balls, guide components, limiting plates, and removable bottom plates and lifting plates, the problem of the inability to balance the convenience and accuracy of the stage design in the prior art is solved, and efficient and accurate sample analysis and good equipment maintenance are achieved.
Patent Information
- Application Number
- CN202411956252.1
- Authority / Receiving Office
- CN · China
- Patent Type
- Applications(China)
- Current Assignee / Owner
- Filing Date
- 2024-12-28
- Publication Date
- 2025-02-25
AI Technical Summary
The stage design of existing total reflective X-ray fluorescence spectrometers cannot balance the convenience and accuracy well, especially in the face of sample analysis tasks with diverse and high-precision needs, and the samples are prone to contamination of the stage, resulting in inconvenience in cleaning and protection, affecting the detection results.
A total reflective X-ray fluorescence spectrometer is designed, using a slidingly snap-in compartment door assembly and fixing mechanism to improve the smoothness and stability of sample placement through ball and guide assembly, and through an adjustable limiting plate, a removable bottom plate and a lifting plate, it is convenient to adapt to samples of different specifications and perform cleaning and maintenance.
It improves the smoothness and stability of sample placement, enhances the adaptability to samples of different specifications, facilitates cleaning and maintenance, and improves the accuracy and applicability of test results.
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Figure CN119510470A_ABST
Abstract
Description
Technical Field
[0001] The invention relates to the field of total reflection X-ray fluorescence spectrometers, in particular to a total reflection X-ray fluorescence spectrometer. Background Art
[0002] Total reflection X-ray fluorescence spectrometer (TXRF) adopts total reflection X-ray fluorescence technology, uses monochromatic light and total reflection optical elements, and excites sample fluorescence through total reflection beam, reduces the absorption and scattering of sample matrix, thereby significantly enhancing fluorescence yield and reducing background noise. It has higher sensitivity and is suitable for trace element analysis. Most existing total reflection X-ray fluorescence spectrometers use fixed or manually adjustable stage designs to place samples to be tested. Among them, although the fixed stage has a simple and stable structure, it is not flexible enough when dealing with samples of different shapes and sizes; and although the manual adjustment type can adapt to more diverse samples, it is inconvenient to adjust and has the problem of inconvenient operation.
[0003] Moreover, the stage design of most total reflection X-ray fluorescence spectrometers on the market today cannot strike a good balance between convenience and accuracy, especially when faced with diverse, high-precision sample analysis tasks. Moreover, when used for a long time, samples can easily contaminate the stage, making it difficult to clean and protect, affecting the test results and making it inconvenient to use. Summary of the invention
[0004] To this end, the present invention provides a total reflection X-ray fluorescence spectrometer to solve the above problems.
[0005] The present invention provides the following technical solution: a total reflection X-ray fluorescence spectrometer, comprising a spectrometer body, a slot is provided on one side of the spectrometer body, and a door assembly for sealing the slot is slidably engaged on one side of the slot on the spectrometer body, a fixing mechanism for fixing the sample during detection is fixedly installed on the inner side of the slot inside the spectrometer body, a carrying mechanism for carrying the sample is plugged into the interior of the fixing mechanism, an external sample slide is engaged with the carrying mechanism, and when in use, the external slide with the sample is engaged with the carrying mechanism, and the door assembly is opened to expose the slot position, thereby facilitating the insertion of the carrying mechanism with the sample into the interior of the fixing mechanism, and then the door assembly is closed, and detection is performed through the spectrometer body.
[0006] As a preferred solution of the present invention, the compartment door assembly includes a sealing plate for sealing the slot, and slide rails are fixedly installed on the upper and lower ends of the sealing plate, and the slide rails are slidably engaged with the inner side of the spectrometer body, and a reset spring is fixedly installed on one end of the slide rail, and a compartment door wrench is fixedly installed on one side of the sealing plate. When releasing the seal of the slot, the compartment door wrench is pulled to make the sealing plate slide on the spectrometer body through the slide rail, so that the reset spring is compressed, and then the sealing plate moves to one side of the slot to release the seal of the slot. When the compartment door wrench is released, the reset spring is stretched, so that the sealing plate seals the slot.
[0007] As a preferred solution of the present invention, the fixing mechanism includes a fixing cylinder, which is fixedly installed in the position of the slot inside the spectrometer body, and a chamfer is provided on the inner side of one end of the fixing cylinder, a notch is provided on one side of the upper end of the fixing cylinder, the lower side of the end of the fixing cylinder where the chamfer is provided is a concave structure, and a guide component is fixedly installed inside the concave structure, blind holes of a trapezoidal structure are provided in an array at the lower end of the interior of the fixing cylinder, and a support spring is fixedly installed inside the blind hole, a lower gasket is fixedly installed on the upper end of the support spring, a ball is placed on the lower gasket, an upper gasket is fixedly installed on the upper end of the blind hole, and the upper end of the ball extends to the The outer part of the upper surface of the upper gasket is facilitated by the guide assembly and the chamfer to facilitate the insertion of the carrier mechanism into the interior of the fixed cylinder, and the ball is used to improve the smoothness during insertion. After being inserted into place, the support spring supports the lower gasket so that the upper end of the ball protrudes from the upper surface of the upper gasket and engages with the carrier mechanism, thereby improving the stability after insertion. Through the notch, after the carrier mechanism carries the sample and fixes it, the glass slide with the sample is located at the position of the notch, the laser emitting unit inside the spectrometer body irradiates through the notch position, and the laser detector detects the light reflected by the sample at the notch position.
[0008] As a preferred solution of the present invention, the guide assembly includes a mounting plate, the mounting plate is fixedly mounted on the fixed cylinder, and an axle is fixedly mounted inside the mounting plate, a swing frame is rotatably mounted on the axle, a roller is rotatably mounted on the other end of the swing frame, and a torsion spring is fixedly mounted in an array between the axle and the swing frame, and the torsion spring is conveniently applied to the swing frame and the roller through the torsion spring, so that when the carrier mechanism is plugged in, the roller provides a lifting force to the carrier mechanism, and when the roller rotates, it is convenient to guide the carrier mechanism into the interior of the fixed cylinder.
[0009] As a preferred solution of the present invention, the loading mechanism includes a loading plate, and one end of the loading plate is turned to form a handle, and the lower side of the handle is provided with an anti-slip groove, which makes it easy to take the loading plate and avoids being unable to pull it out from the inside of the fixed tube, thereby improving the convenience of operation. A cleaning sponge with an annular structure is embedded and installed on the end of the loading plate opposite to the handle, and the outer side of the cleaning sponge contacts the inner side of the fixed tube, so that when taking and placing the loading mechanism, the cleaning sponge wipes the inside of the fixed tube, thereby avoiding long-term use, which causes the sample to contaminate the inside of the fixed mechanism. The loading plate is also provided with a placement groove with a convex structure, and the lower end of the inner part of the placement groove is fixed with a screw. The bottom plate is easy to disassemble and clean, and a lifting plate is elastically installed on the upper end of the bottom plate to support the bottom of the glass slide when placing a glass slide with a sample, and the upper end of the sample carrier plate is provided with inverted T-shaped slide grooves on both sides of the placement groove, and the inner sliding card of the slide groove is provided with a limit plate with a convex structure, and the limit screw is threadedly connected to the limit plate, and the lower end of the limit screw is pressed against the upper surface of the slide groove, and the position of the limit plate in the slide groove is adjusted to facilitate the adjustment of the distance between the limit plates, so as to facilitate the upper limit of glass slides of different specifications, improve the applicability during use, and through the limit screw, after the adjustment is completed, it is convenient to fix the limit plate.
[0010] As a preferred solution of the present invention, arc grooves are evenly formed on the lower surface of the bottom plate and the lower surface of the carrier plate, and the arc grooves correspond to the positions of the balls. After the carrier mechanism is placed in place, the upper end of the balls is clamped in the inside of the arc grooves, thereby improving the stability during detection. When the carrier mechanism is taken out, the support spring is compressed, and the balls move downward, so that the arc grooves are separated from the balls. A lifting spring is evenly fixed on the upper surface of the bottom plate, and the upper end of the lifting spring is fixedly installed. A connecting block with a convex structure is made of rubber material. The lower surface of the lifting plate is evenly provided with connecting grooves that match the connecting block. The connecting block is plugged into the inside of the connecting groove. Through the connecting groove and the connecting block, it is convenient to separate the lifting plate from the bottom plate, facilitate the installation of auxiliary components, and facilitate the replacement of auxiliary components. Through the lifting spring, the lifting plate applies a limiting force to the bottom of the sample glass slide, which is convenient for clamping the sample glass slide between the lifting plate and the limiting plate.
[0011] As a preferred solution of the present invention, a square groove is provided at the lower end of the lifting plate, and through holes are provided on both sides of the upper end of the lifting plate, the through holes are connected with the square groove, and an auxiliary component is fixedly installed inside the square groove. The middle position of the auxiliary component passes through the through hole and covers the upper surface of the lifting plate, so as to facilitate the coating of the upper surface of the lifting plate by the auxiliary component, thereby reducing the influence of contamination on the upper surface of the lifting plate on the sample detection results during long-term use.
[0012] As a preferred solution of the present invention, the auxiliary component includes a mounting frame, the middle position of the mounting frame is fixedly installed inside the square groove by external screws, and the two ends of the mounting frame are rotatably mounted with a film-releasing roller and a film-collecting roller, the film-releasing roller is wrapped with an isolation film, and one end of the isolation film passes through the through hole and extends to the position of the film-collecting roller and is adhesively connected to the film-collecting roller. The mounting frame is convenient for installing and replacing the auxiliary component. After the isolation film on the film-releasing roller is used up, the auxiliary component is replaced, and one end of the isolation film is a viscose structure, and the end of the isolation film with viscose passes through the through hole, covers the upper surface of the lifting plate, and then adheres to the film-collecting roller and is wrapped around the film-collecting roller, so that the isolation film covering the upper surface of the lifting plate can be replaced each time it is used to avoid contamination.
[0013] As a preferred solution of the present invention, the end positions of the film-releasing roller and the film-collecting roller are fixedly installed with linkage wheels, and a linkage belt is sleeved between the linkage wheels. Through the linkage wheel and the linkage belt, the film-releasing roller and the film-collecting roller rotate synchronously, thereby achieving synchronous film releasing and film collecting of the isolation film, avoiding the isolation film from becoming loose, and facilitating use.
[0014] The beneficial effects of the present invention are as follows: 1. The present invention facilitates the insertion of the carrier mechanism into the fixing mechanism through the ball bearings and the guide assembly, thereby improving the smoothness when placing the sample, and fixes the carrier mechanism through the ball bearings, thereby improving the stability after placement.
[0015] 2. The present invention facilitates the placement and fixation of samples of different sizes by adjusting the distance between the limiting plates, thereby improving the adaptability when carrying samples. The detachable bottom plate and lifting plate facilitate the disassembly and cleaning of the mechanism supporting the sample slide, thereby facilitating operation.
[0016] 3. The present invention uses auxiliary components to move the isolation film when placing the sample glass slide, thereby improving the cleanliness of the bottom support of the sample glass slide and improving the detection results. The cleaning sponge can be used to wipe and clean the inside of the fixing mechanism when the loading mechanism is pulled out and inserted, further improving the test accuracy.
[0017] 4. The present invention can greatly improve the adaptability to sample slides and the convenience of operation, and is suitable for efficient and accurate analysis of samples of various specifications. BRIEF DESCRIPTION OF THE DRAWINGS
[0018] The present invention will be further described below in conjunction with the accompanying drawings.
[0019] Figure 1 It is the overall structure diagram of the present invention; Figure 2 is a structural diagram of a door assembly of the present invention; Figure 3 It is a structural diagram of the fixing mechanism and the object-carrying mechanism of the present invention when they are plugged together; Figure 4 It is an exploded schematic diagram of the fixing mechanism in the present invention; Figure 5 It is a partial structural diagram of the guide component in the present invention; Figure 6 It is an exploded structural diagram of the object-carrying mechanism in the present invention; Figure 7 It is an exploded structural diagram of the object-carrying mechanism of the present invention from another angle; Figure 8 It is a structural diagram of the auxiliary components in the present invention.
[0020] Legend: 1. Spectrometer body; 2. Slot; 3. Door assembly; 31. Sealing plate; 32. Slide rail; 33. Reset spring; 34. Door wrench; 4. Fixing mechanism; 41. Fixing cylinder; 42. Chamfer; 43. Notch; 44. Guide assembly; 441. Mounting plate; 442. Shaft; 443. Swing frame; 444. Roller; 445. Torsion spring; 45. Blind hole; 46. Support spring; 47. Lower gasket; 48. Ball; 49. Upper gasket; 5. Loading mechanism; 51. Loading plate; 52. Handle; 53, anti-slip groove; 54, cleaning sponge; 55, placement groove; 56, bottom plate; 57, lifting plate; 58, slide groove; 59, limit plate; 510, limit screw; 511, arc groove; 512, lifting spring; 513, connecting block; 514, connecting groove; 515, square groove; 516, through hole; 517, auxiliary component; 5171, mounting frame; 5172, film placing roller; 5173, film collecting roller; 5174, isolation film; 5175, linkage wheel; 5176, linkage belt. DETAILED DESCRIPTION
[0021] The following will be combined with the drawings in the embodiments of the present invention to clearly and completely describe the technical solutions in the embodiments of the present invention. Obviously, the described embodiments are only part of the embodiments of the present invention, not all of the embodiments. Based on the embodiments of the present invention, all other embodiments obtained by ordinary technicians in this field without creative work are within the scope of protection of the present invention.
[0022] Specific examples are given below.
[0023] like Figure 1 and Figure 3 As shown, a total reflection X-ray fluorescence spectrometer comprises a spectrometer body 1, a slot 2 is provided on one side of the spectrometer body 1, and a door assembly 3 for sealing the slot 2 is slidably engaged with the spectrometer body 1 on one side of the slot 2, a fixing mechanism 4 for fixing the sample during detection is fixedly installed on the inner side of the slot 2 inside the spectrometer body 1, a carrying mechanism 5 for carrying the sample is plugged into the fixing mechanism 4, an external sample slide is engaged with the carrying mechanism 5, when in use, the external slide with the sample is engaged with the carrying mechanism 5, and the door assembly 3 is opened to expose the slot 2, so as to facilitate the insertion of the carrying mechanism 5 with the sample into the fixing mechanism 4, and then the door assembly 3 is closed, and detection is performed through the spectrometer body 1.
[0024] like Figure 2 As shown, the door assembly 3 includes a sealing plate 31 for sealing the slot 2, and the upper and lower ends of the sealing plate 31 are fixedly installed with slide rails 32, and the slide rails 32 are slidably engaged with the inner side of the spectrometer body 1, and a reset spring 33 is fixedly installed at one end of the slide rail 32, and a door wrench 34 is fixedly installed on one side of the sealing plate 31. When releasing the seal of the slot 2, the door wrench 34 is pulled to make the sealing plate 31 slide on the spectrometer body 1 through the slide rail 32, so that the reset spring 33 is compressed, and then the sealing plate 31 moves to one side of the slot 2 to release the seal of the slot 2. When the door wrench 34 is released, the reset spring 33 is stretched, so that the sealing plate 31 seals the slot 2.
[0025] like Figure 4 and Figure 5As shown, the fixing mechanism 4 includes a fixing cylinder 41, which is fixedly installed in the position of the slot 2 inside the spectrometer body 1, and a chamfer 42 is provided on the inner side of one end of the fixing cylinder 41, and a notch 43 is provided on one side of the upper end of the fixing cylinder 41, and the lower side of the end of the fixing cylinder 41 where the chamfer 42 is provided is a concave structure, and a guide assembly 44 is fixedly installed inside the concave structure, and blind holes 45 of a trapezoidal structure are provided in an array at the lower end of the interior of the fixing cylinder 41, and a support spring 46 is fixedly installed inside the blind hole 45, and a lower gasket 47 is fixedly installed on the upper end of the support spring 46, and a ball 48 is placed on the lower gasket 47, and an upper gasket 49 is fixedly installed on the upper end of the blind hole 45, and the upper end of the ball 48 It extends to the outside of the upper surface of the upper gasket 49, through the guide assembly 44 and the chamfer 42, so as to facilitate the insertion of the carrier mechanism 5 into the interior of the fixed cylinder 41, and through the ball 48, the smoothness during insertion is improved, and after being inserted into place, the support of the lower gasket 47 by the support spring 46 makes the upper end of the ball 48 protrude from the upper surface of the upper gasket 49 and engage with the carrier mechanism 5, thereby improving the stability after insertion, and through the notch 43, after the carrier mechanism 5 carries the sample and is fixed, the glass slide with the sample is located at the position of the notch 43, the laser emitting unit inside the spectrometer body 1 irradiates through the position of the notch 43, and the laser detector detects the light reflected by the sample at the position of the notch 43.
[0026] like Figure 4 and Figure 5 As shown, the guide assembly 44 includes a mounting plate 441, which is fixedly mounted on the fixed cylinder 41, and a shaft 442 is fixedly mounted inside the mounting plate 441, a swing frame 443 is rotatably mounted on the shaft 442, a roller 444 is rotatably mounted on the other end of the swing frame 443, and a torsion spring 445 is fixedly mounted in an array between the shaft 442 and the swing frame 443, and the torsion spring 445 is conveniently applied to the swing frame 443 and the roller 444 through the torsion spring 445, so that when the carrier mechanism 5 is plugged in, the roller 444 provides a lifting force to the carrier mechanism 5, and when the roller 444 rotates, it is convenient to guide the carrier mechanism 5 into the interior of the fixed cylinder 41.
[0027] like Figure 6 and Figure 7As shown, the loading mechanism 5 includes a loading plate 51, and one end of the loading plate 51 is turned to form a handle 52, and the lower side of the handle 52 is provided with an anti-slip groove 53, so as to facilitate the taking of the loading plate 51 and avoid the inability to pull it out from the inside of the fixed cylinder 41, thereby improving the convenience of operation. The end of the loading plate 51 opposite to the handle 52 is inlaid with a cleaning sponge 54 with an annular structure, and the outer side of the cleaning sponge 54 contacts the inner side of the fixed cylinder 41, so that when the loading mechanism 5 is taken and placed, the cleaning sponge 54 wipes the inside of the fixed cylinder 41, so as to avoid long-term use, which causes the sample to contaminate the inside of the fixed mechanism 4. The loading plate 51 is also provided with a placement groove 55 with a convex structure, and the lower end of the inner part of the placement groove 55 is fixed with a bottom plate by screws. The bottom plate 56 is convenient for disassembling and cleaning. A lifting plate 57 is elastically installed on the upper end of the bottom plate 56 to support the bottom of the glass slide when placing the glass slide with the sample. The upper end of the sample carrier plate 51 is located on both sides of the placement groove 55 and is provided with an inverted T-shaped slide groove 58. The inner sliding card of the slide groove 58 is provided with a convex-shaped limit plate 59. The limit plate 59 is threadedly connected with a limit screw 510, and the lower end of the limit screw 510 is pressed tightly against the upper surface of the slide groove 58. By adjusting the position of the limit plate 59 in the slide groove 58, the distance between the limit plates 59 can be adjusted, which is convenient for limiting the upper position of glass slides of different specifications, thereby improving the applicability during use. After the adjustment is completed, the limit screw 510 is used to facilitate The limiting plate 59 is fixed, and the lower surface of the bottom plate 56 and the lower surface of the loading plate 51 are evenly provided with arc grooves 511, and the arc grooves 511 correspond to the positions of the ball bearings 48. After the loading mechanism 5 is placed in place, the upper end of the ball bearings 48 is clamped in the arc grooves 511, thereby improving the stability during detection. When the loading mechanism 5 is taken out, the support spring 46 is compressed, and the ball bearings 48 move downward, so that the arc grooves 511 are separated from the ball bearings 48. The upper surface of the bottom plate 56 is evenly fixed with a lifting spring 512, and the upper end of the lifting spring 512 is fixedly installed with a connecting block 513 with a convex structure. The connecting block 513 is made of rubber material, and the lower surface of the lifting plate 57 is evenly provided with connecting grooves 514 that match the connecting block 513. The block 513 is plugged into the inside of the connecting groove 514. Through the connecting groove 514 and the connecting block 513, it is convenient to separate the lifting plate 57 from the bottom plate 56, to facilitate the installation of the auxiliary component 517, and to facilitate the replacement of the auxiliary component 517. Through the lifting spring 512, the lifting plate 57 applies a limiting force to the bottom of the sample glass slide, so that the sample glass slide is clamped between the lifting plate 57 and the limiting plate 59. A square groove 515 is provided at the lower end of the lifting plate 57, and through holes 516 are provided on both sides of the upper end of the lifting plate 57. The through holes 516 are connected to the square groove 515. The auxiliary component 517 is fixedly installed inside the square groove 515. The middle position of the auxiliary component 517 passes through the through hole 516 and covers the upper surface of the lifting plate 57.It is convenient to coat the upper surface of the lifting plate 57 through the auxiliary component 517, so as to reduce the influence of the contamination on the upper surface of the lifting plate 57 on the sample detection result during long-term use.
[0028] like Figure 7 and Figure 8 As shown, the auxiliary component 517 includes a mounting frame 5171, the middle position of the mounting frame 5171 is fixedly installed in the square groove 515 by external screws, and the two ends of the mounting frame 5171 are rotatably mounted with a film-laying roller 5172 and a film-collecting roller 5173, respectively. The film-laying roller 5172 is wound with an isolation film 5174, and one end of the isolation film 5174 passes through the through hole 516 and extends to the position of the film-collecting roller 5173 and is adhesively connected to the film-collecting roller 5173. The mounting frame 5171 is convenient for installing and replacing the auxiliary component 517. After the isolation film 5174 on the film-laying roller 5172 is used up, the auxiliary component 517 is replaced, and one end of the isolation film 5174 is a viscose structure. The end with adhesive 74 passes through the through hole 516, covers the upper surface of the lifting plate 57, and then adheres to the film collection roller 5173 and is wrapped around the film collection roller 5173, so that the isolation film 5174 covering the upper surface of the lifting plate 57 can be replaced each time it is used to avoid contamination. The end positions of the film-releasing roller 5172 and the film-collecting roller 5173 are fixedly installed with interlocking wheels 5175, and a interlocking belt 5176 is sleeved between the interlocking wheels 5175. Through the interlocking wheels 5175 and the interlocking belt 5176, the film-releasing roller 5172 and the film collection roller 5173 can rotate synchronously, thereby achieving synchronous film releasing and film collection of the isolation film 5174, avoiding the isolation film 5174 from being loosened, and facilitating use.
[0029] The above shows and describes the basic principles, main features and advantages of the present invention. Those skilled in the art should understand that the present invention is not limited to the above embodiments. The above embodiments and descriptions are only for explaining the principles of the present invention. Without departing from the spirit and scope of the present invention, the present invention may have various changes and improvements, which fall within the scope of the present invention. The scope of protection of the present invention is defined by the attached claims and their equivalents.
Claims
1. A total reflection X-ray fluorescence spectrometer, characterized in that: The spectrometer comprises a main body (1), a slot (2) is provided on one side of the main body (1), and a door assembly (3) for sealing the slot (2) is slidably engaged with the main body (1) of the spectrometer and located on one side of the slot (2); a fixing mechanism (4) for fixing a sample during detection is fixedly installed inside the main body (1) and located on the inner side of the slot (2); a loading mechanism (5) for carrying the sample is plugged into the interior of the fixing mechanism (4); and an external sample slide is engaged with the loading mechanism (5).
2. A total reflection X-ray fluorescence spectrometer according to claim 1, characterized in that: The door assembly (3) comprises a sealing plate (31) for sealing the slot (2); a slide rail (32) is fixedly mounted on the upper and lower ends of the sealing plate (31); the slide rail (32) is slidably engaged with the inner side of the spectrometer body (1); a return spring (33) is fixedly mounted on one end of the slide rail (32); and a door wrench (34) is fixedly mounted on one side of the sealing plate (31).
3. A total reflection X-ray fluorescence spectrometer according to claim 1, characterized in that: The fixing mechanism (4) comprises a fixing cylinder (41), the fixing cylinder (41) being fixedly mounted inside the spectrometer body (1) at a position of the slot (2), and a chamfer (42) is provided on the inner side of one end of the fixing cylinder (41), a notch (43) is provided on one side of the upper end of the fixing cylinder (41), a concave structure is provided on the lower side of the end of the fixing cylinder (41) where the chamfer (42) is provided, and a guide assembly (44) is fixedly mounted inside the concave structure, blind holes (45) of a trapezoidal structure are provided in an array at the lower end of the fixing cylinder (41), and a support spring (46) is fixedly mounted inside the blind hole (45), a lower gasket (47) is fixedly mounted on the upper end of the support spring (46), a ball (48) is placed on the lower gasket (47), an upper gasket (49) is fixedly mounted on the upper end of the blind hole (45), and the upper end of the ball (48) extends to the outside of the upper surface of the upper gasket (49).
4. A total reflection X-ray fluorescence spectrometer according to claim 3, characterized in that: The guide assembly (44) comprises a mounting plate (441), the mounting plate (441) being fixedly mounted on the fixed cylinder (41), and a shaft (442) being fixedly mounted inside the mounting plate (441), a swing frame (443) being rotatably mounted on the shaft (442), a roller (444) being rotatably mounted on the other end of the swing frame (443), and a torsion spring (445) being fixedly mounted in an array between the shaft (442) and the swing frame (443).
5. A total reflection X-ray fluorescence spectrometer according to claim 3, characterized in that: The object-carrying mechanism (5) comprises an object-carrying plate (51), and one end of the object-carrying plate (51) is turned to form a handle (52), and a non-slip groove (53) is provided on the lower side of the handle (52). A cleaning sponge (54) with an annular structure is embedded and installed on the end of the object-carrying plate (51) opposite to the handle (52), and the outer side of the cleaning sponge (54) contacts the inner side of the fixing tube (41). The object-carrying plate (51) is also provided with a placement groove (55) with a convex structure, and the placement groove (55) ) is fixedly mounted with a bottom plate (56) at the inner lower end thereof by screws, a lifting plate (57) is elastically mounted at the upper end of the bottom plate (56), and an inverted T-shaped slide groove (58) is provided on both sides of the upper end of the loading plate (51) located at the placement groove (55), a convex-shaped limit plate (59) is slidably engaged inside the slide groove (58), a limit screw (510) is threadedly connected to the limit plate (59), and the lower end of the limit screw (510) is pressed tightly against the upper surface of the slide groove (58).
6. A total reflection X-ray fluorescence spectrometer according to claim 5, characterized in that: The lower surface of the bottom plate (56) and the lower surface of the loading plate (51) are uniformly provided with arc grooves (511), the arc grooves (511) corresponding to the positions of the balls (48), and the upper surface of the bottom plate (56) is uniformly fixed with a lifting spring (512), the upper end of the lifting spring (512) is fixedly mounted with a connecting block (513) with a convex structure, the connecting block (513) is made of rubber material, and the lower surface of the lifting plate (57) is uniformly provided with connecting grooves (514) matching with the connecting block (513), and the connecting block (513) is plugged into the inside of the connecting groove (514).
7. A total reflection X-ray fluorescence spectrometer according to claim 5, characterized in that: A square groove (515) is provided at the lower end of the lifting plate (57), and through holes (516) are provided on both sides of the upper end of the lifting plate (57), the through holes (516) are connected to the square groove (515), and an auxiliary component (517) is fixedly installed inside the square groove (515), and the middle position of the auxiliary component (517) passes through the through hole (516) and covers the upper surface of the lifting plate (57).
8. A total reflection X-ray fluorescence spectrometer according to claim 7, characterized in that: The auxiliary component (517) comprises a mounting frame (5171), the middle position of the mounting frame (5171) is fixedly mounted inside the square groove (515) by means of external screws, and a film placing roller (5172) and a film collecting roller (5173) are rotatably mounted on both ends of the mounting frame (5171), an isolation film (5174) is wound around the film placing roller (5172), and one end of the isolation film (5174) passes through the through hole (516) and extends to the position of the film collecting roller (5173) to be adhesively connected to the film collecting roller (5173).
9. A total reflection X-ray fluorescence spectrometer according to claim 8, characterized in that: Linking wheels (5175) are fixedly mounted at the end positions of the film placing roller (5172) and the film collecting roller (5173), and a linking belt (5176) is sleeved between the linking wheels (5175).