Atomized liquid, compartmented atomizer and electronic atomization device
By storing and atomizing the first and second liquids of low-polarity flavoring substances and high-smoke solvents in separate compartmentalized atomizing devices, the problems of uneven dissolution of low-polarity flavoring substances and insufficient smoke volume in existing atomizing liquids are solved, achieving consistency in taste and improvement in smoke volume.
Patent Information
- Authority / Receiving Office
- CN · China
- Patent Type
- Patents(China)
- Current Assignee / Owner
- Filing Date
- 2024-01-16
- Publication Date
- 2026-04-07
AI Technical Summary
The low-polarity flavoring substances in existing atomizing liquids are difficult to dissolve evenly, resulting in inconsistent taste or burnt flavor. Furthermore, the amount of vapor produced is reduced after solvents such as ethylene glycol and glycerol are replaced, affecting the user experience.
A compartmentalized atomizing device is used to store and atomize the first liquid containing low-polarity flavor substances and the second liquid containing high vapor volume separately. The A-type and C-type solvents with different polarities are used to uniformly dissolve the flavor substances and provide sufficient vapor volume respectively.
It achieves uniform dissolution of low-polarity flavor substances, resulting in a consistent taste after atomization without burning, while providing ample vapor production and enhancing the user experience.
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Abstract
Description
Technical Field
[0001] This application belongs to the field of electronic atomization technology, and particularly relates to an atomizing liquid, a compartmentalized atomizer, and an electronic atomization device. Background Technology
[0002] Electronic atomizers typically contain a rich variety of flavorings and fragrances dissolved in the emulsion, resulting in a diverse range of flavors and distinct tastes. These flavoring substances can vary significantly in polarity, often requiring some low-polarity flavorings to achieve a highly immersive and intense flavor. However, these substances are often difficult to dissolve in solvents containing large amounts of ethylene glycol and glycerol, leading to stratification between the low-polarity flavorings and the solvent. This can result in inconsistent tastes or even a burnt sensation during inhalation. Furthermore, ethylene glycol and glycerol are usually the primary sources of sufficient vapor production. Replacing them with solvents like propylene glycol or ethanol significantly reduces vapor production.
[0003] Therefore, it is necessary to provide an improved atomizing fluid. Summary of the Invention
[0004] In view of this, the main objective of this disclosure is to provide an atomizing liquid that can uniformly dissolve sufficient low-polarity aroma substances, resulting in an improved and consistent flavor after atomization without burning, while also providing a sufficient amount of vapor. A further objective of this application is to provide an atomizer and an electronic atomization device comprising the aforementioned atomizing liquid.
[0005] To achieve the above objectives, this disclosure provides the following technical solution.
[0006] The first aspect of this disclosure provides an atomizing liquid for use in a compartmentalized atomizing device, comprising a first liquid and a second liquid, wherein the first liquid and the second liquid are stored independently in the compartmentalized atomizing device, the first liquid comprising a first solvent and a first solute, and the second liquid comprising a second solvent and a second solute, wherein the first solvent comprises at least a type A solvent, and the second solvent comprises at least a type C solvent, wherein the type A solvent comprises one or more of ethanol, propanol, butanol, and benzyl alcohol, and the type C solvent comprises one or more of water, ethylene glycol, glycerol, and glycerol; wherein the proportion of the total mass of the type A solvent in the second solvent is less than the proportion of the total mass of the type A solvent in the first solvent, or the proportion of the total mass of the type C solvent in the second solvent is greater than the proportion of the total mass of the type C solvent in the first solvent.
[0007] According to one embodiment of this disclosure, the first solvent further includes a type B solvent, which includes one or more of propylene glycol, butanediol, triethyl citrate, triacetin, and caprylic / capric triglycerides, wherein the total mass percentage of the type A solvent and the type B solvent in the first solvent is 60%-98%, preferably 70%-95%, based on the mass percentage in the first liquid; more preferably, the total mass percentage of the type A solvent in the first solvent is 60%-95%, preferably 70%-90%, based on the mass percentage in the first liquid.
[0008] According to one embodiment of this disclosure, the second solvent further comprises a type B solvent, which includes one or more of propylene glycol, butanediol, triethyl citrate, triacetin, and caprylic / capric triglycerides, wherein, by mass percentage in the second liquid, the total mass percentage of the type C solvent and the type B solvent in the second solvent is 60%-95%, preferably 70%-92%, wherein; more preferably, by mass percentage in the second liquid, the total mass percentage of the type C solvent in the second solvent is 20%-60%, preferably 30%-50%.
[0009] According to one embodiment of this disclosure, the proportion of the total mass of substances with a n-octanol-water partition coefficient greater than 0.73 in the first solute is greater than the proportion of the total mass of substances with a n-octanol-water partition coefficient greater than 0.73 in the second solute; or, the proportion of the total mass of substances with a n-octanol-water partition coefficient less than -0.74 in the first solute is less than the proportion of the total mass of substances with a n-octanol-water partition coefficient less than -0.74 in the second solute.
[0010] According to one embodiment of this disclosure, the first solute further includes a substance with an octanol-water partition coefficient greater than or equal to -0.74 and less than or equal to 0.73. The total mass percentage of the substance with an octanol-water partition coefficient greater than or equal to -0.74 in the first solute is 2%-30%, preferably 5%-15%, based on its mass percentage in the first liquid. More preferably, the total mass percentage of the substance with an octanol-water partition coefficient greater than 0.73 in the first solute is 2%-15%, preferably 4%-10%, based on its mass percentage in the first liquid.
[0011] According to one embodiment of this disclosure, the second solute further includes a substance with an octanol-water partition coefficient greater than or equal to -0.74 and less than or equal to 0.73. The total mass percentage of the substance with an octanol-water partition coefficient less than or equal to 0.73 in the second solute is 5%-30%, preferably 8%-20% by mass percentage in the second liquid. More preferably, the total mass percentage of the substance with an octanol-water partition coefficient less than -0.74 in the second solute is 5%-20%, preferably 9%-15% by mass percentage in the second liquid.
[0012] According to one embodiment of this disclosure, the substance with a n-octanol-water partition coefficient greater than 0.73 includes one or more of the following: pinene, limonene, myrcene, caryophyllene, nonanal, decanal, lauryl alcohol, undecyl lactone, rose ether, thujone, camphene, sabinene, phellandrene, terpinene, umbelliferone, limonene, octyl alcohol, terpineol, terpinene, linalool, octanol, neraldehyde, geraniol, nerol, geraniol, perillaldehyde, undecylaldehyde, dodecaaldehyde, and ethane.
[0013] According to one embodiment of this disclosure, the substance with a n-octanol-water partition coefficient less than -0.74 includes one or more of neotame, adventitia, sucralose, acesulfame potassium, glucosylstevioside, aspartame, hesperidin dihydrochalcone, neohesperidin dihydrochalcone, naringin dihydrochalcone, WS-3, WS-5, WS-12, WS-14, WS-23, WS-25, WS-27, menthol, menthyl ether, menthyl ester, nicotinic acid benzoate, nicotinic acid levulinic acid, nicotinic acid tartrate, nicotinic acid citrate, nicotinic acid acetate, and nicotinic acid oxalate.
[0014] A second aspect of this disclosure provides a compartmentalized atomizer comprising an atomizing fluid according to any of the above embodiments.
[0015] A third aspect of this disclosure provides an electronic atomizing device, including a battery assembly and the aforementioned compartmentalized atomizer, wherein the battery assembly is used to power the atomizer.
[0016] In the atomizing liquid disclosed herein, the proportion of the total mass of type A solvent in the second solvent is less than the proportion of the total mass of type A solvent in the first solvent, or the proportion of the total mass of type C solvent in the second solvent is greater than the proportion of the total mass of type C solvent in the first solvent, thereby achieving both uniform dissolution of sufficient low-polarity aroma substances, improved and consistent taste after atomization without burning, and sufficient vapor production.
[0017] In addition to the technical problems solved by this disclosure, the technical features constituting the technical solutions, and the beneficial effects brought about by the technical features of these technical solutions as described above, other technical problems that this disclosure can solve, other technical features contained in the technical solutions, and the beneficial effects brought about by these technical features will be further described in detail in the following specific embodiments. Detailed Implementation
[0018] The technical solution of this disclosure will be clearly and completely described below with reference to specific embodiments. Obviously, the described embodiments are only a part of the embodiments of this disclosure, and not all of them. Based on the embodiments in this disclosure, all other embodiments obtained by those skilled in the art without creative effort are within the scope of protection of this application.
[0019] Throughout this specification, unless otherwise specified, the terminology used herein shall be understood as having the meaning as commonly used in the art. Therefore, unless otherwise defined, all technical and scientific terms used herein have the same meaning as commonly understood by one of ordinary skill in the art. In the event of any conflict, this specification shall prevail.
[0020] It should be noted that, in this disclosure, the term "comprising" or any other variation thereof is intended to cover non-exclusive inclusion, such that a method or apparatus that comprises a list of elements includes not only the elements expressly stated, but also other elements not expressly listed, or elements inherent to implementing the method or apparatus. Without further limitations, an element defined by the phrase "containing..." does not exclude the presence of other related elements in the method or apparatus that includes that element.
[0021] Unless otherwise stated, all percentages or % in this disclosure refer to percentages or mass percentages.
[0022] It should be understood that the phrases "one embodiment" or "some embodiments" used throughout the specification mean that a particular feature, structure, or characteristic related to an embodiment is included in at least one embodiment of this disclosure. Therefore, "in one embodiment" or "in some embodiments" appearing throughout the specification do not necessarily refer to the same embodiment.
[0023] Low-polarity flavor compounds, such as pinene, limonene, myrcene, caryophyllene, nonanal, decanal, lauryl alcohol, gamma-undecyl lactone, and rose ether, or natural extracts containing large amounts of low-polarity flavor compounds, such as sweet orange oil, bitter almond oil, bitter orange oil, cardamom oil, cinnamon oil, and clove oil, have low solubility in solvents such as ethylene glycol and glycerol, affecting the taste. Increasing the content of low-polarity flavor compounds can lead to inconsistent taste due to uneven dispersion, and may even cause burning during atomization. On the other hand, solvents such as ethylene glycol and glycerol are usually the main source of sufficient smoke production. If solvents such as ethanol and propanol are partially replaced by ethylene glycol and glycerol, the smoke production will be significantly reduced. In addition, the use of large amounts of solvents such as ethanol and propanol will lower the flash point of the atomizing liquid, which can easily cause fire safety risks during storage, transportation, and production.
[0024] Therefore, in order to ensure both uniform dissolution of sufficient low-polarity aroma substances, consistent taste after atomization without burning, and sufficient vapor production, the first aspect of this disclosure aims to provide an atomizing liquid for use in a compartmentalized atomizing device. The atomizing liquid comprises a first liquid and a second liquid, wherein the first liquid and the second liquid are stored independently in the compartmentalized atomizing device. The first liquid comprises a first solvent and a first solute, and the second liquid comprises a second solvent and a second solute. The first solvent comprises at least a type A solvent, and the second solvent comprises at least a type C solvent. Type A solvents include one or more of ethanol, propanol, butanol, and benzyl alcohol, and type C solvents include one or more of water, ethylene glycol, glycerol, and glycerol. The proportion of the total mass of type A solvents in the second solvent is less than the proportion of the total mass of type A solvents in the first solvent, or the proportion of the total mass of type C solvents in the second solvent is greater than the proportion of the total mass of type C solvents in the first solvent.
[0025] This disclosure utilizes a compartmentalized atomizing device, designing an atomizing liquid comprising a first liquid and a second liquid. The first liquid, containing a large amount of low-polarity flavorings (such as sweet orange oil, lemon oil, etc.) or low-polarity aroma substances (such as pinene, limonene, myrcene, caryophyllene, nonanol, decanol, lauryl alcohol, and propyl undecyl lactone rose ether, etc.), and the second liquid, containing a solvent capable of producing a large amount of vapor, are atomized separately. The first liquid is a dissolving system with a higher proportion of type A solvents, which have a high ability to dissolve low-polarity aroma substances, thus ensuring the uniform dissolution of a large number of low-polarity aroma substances. The second liquid is a dissolving system with a higher proportion of type C solvents, which can provide sufficient vapor volume and ensure the uniform dissolution of a large number of high-polarity aroma substances. The first and second liquids, stored independently in the compartmentalized atomizing device, mix the vapors after separate atomization, thereby achieving both uniform dissolution of sufficient low-polarity aroma substances, improved and consistent taste after atomization without burning, and sufficient vapor volume.
[0026] Commonly used solvents in atomizing fluids include water, ethanol, ethylene glycol, propanol, propylene glycol, glycerol, butanol, butanediol, benzyl alcohol, triethyl citrate, triacetin, and caprylic / capric triglycerides. According to embodiments of this disclosure, type A solvents include ethanol, propanol, butanol, and benzyl alcohol, while type C solvents include water, ethylene glycol, glycerol, and propylene glycol. By differentiating the solvent polarities of the first and second liquids in the atomizing fluid, the first and second liquids can uniformly dissolve solutes with significantly different polarities, and the second liquid does not need to consider the dissolution of low-polarity solutes, thus including sufficient type C solvents to provide adequate vapor volume.
[0027] The first and / or second solvents disclosed herein further include type B solvents. The type B solvents include one or more of propylene glycol, butanediol, triethyl citrate, triacetin, and caprylic / capric triglycerides. Type B solvents can assist type C or type A solvents in dissolving substances of moderate polarity.
[0028] According to some embodiments of this disclosure, the total mass percentage of the type A solvent and the type B solvent in the first solvent, based on their mass percentage in the first liquid, is 60%-98%, preferably 70%-95%. Exemplarily, the total mass percentage of the type A solvent and the type B solvent in the first solvent is 60%, 65%, 70%, 75%, 80%, 85%, 90%, 95%, or 98%. Within the above ranges, the type A solvent and the type B solvent are more conducive to the uniform dissolution of a larger amount of low-polarity aroma substances in the first solvent.
[0029] In some embodiments, the total mass percentage of the Class A solvent in the first solvent is 60%-95%, preferably 70%-90%, based on its mass percentage in the first liquid. Exemplarily, the total mass percentage of the Class A solvent in the first solvent is 60%, 65%, 70%, 75%, 80%, 85%, 90%, or 95%. Class A solvents within the above ranges further facilitate the uniform dissolution of a greater amount of low-polarity flavoring substances in the first solvent.
[0030] In some embodiments, the total mass percentage of type B solvent in the first solvent is 0%-38%, preferably 5-25%, and more preferably 5-15%, based on its mass percentage in the first liquid. The total mass percentage of type B solvent in the first solvent is 0%, 3%, 5%, 8%, 10%, 12%, 15%, 20%, 25%, 30%, 35%, or 38%.
[0031] According to some embodiments of this disclosure, the total mass percentage of the C-type solvent and the B-type solvent in the second solvent, based on their mass percentage in the second liquid, is 60%-95%, preferably 70%-92%. Exemplarily, the total mass percentage of the C-type solvent and the B-type solvent in the second solvent is 65%, 70%, 75%, 80%, 85%, 90%, 92%, or 95%. Within the above ranges, the C-type solvent and the B-type solvent are more conducive to the uniform dissolution of a larger amount of highly polar flavoring substances in the second solvent.
[0032] In some embodiments, the total mass percentage of the Class C solvent in the second solvent is 20%-60%, preferably 30%-50%, based on its mass percentage in the second liquid. Exemplarily, the total mass percentage of the Class C solvent in the second solvent is 20%, 25%, 30%, 35%, 40%, 45%, 50%, 55%, or 60%. Class C solvents within the above ranges further facilitate the uniform dissolution of a larger amount of highly polar flavoring substances in the second solvent and provide sufficient smoke volume.
[0033] According to a specific embodiment, the mass percentage of glycerol in the second solvent is 20%-60%, preferably 30%-50%, based on its mass percentage in the second liquid. Exemplarily, the mass percentage of glycerol in the second solvent is 0%, 10%, 20%, 30%, 35%, 37%, 40%, 43%, 45%, 50%, or 60%. Glycerol within the above range is more conducive to achieving high vapor production.
[0034] In some embodiments, the total mass percentage of type B solvent in the second solvent is 0%-75%, preferably 30-65%, and more preferably 45-55% by mass percentage in the second liquid. Exemplarily, the total mass percentage of type B solvent in the second solvent is 0%, 10%, 20%, 30%, 35%, 40%, 45%, 47%, 50%, 53%, 55%, 60%, 65%, 70%, or 75%.
[0035] According to some embodiments of this disclosure, the proportion of the total mass of substances with a n-octanol-water partition coefficient greater than 0.73 in the first solute is greater than the proportion of the total mass of substances with a n-octanol-water partition coefficient greater than 0.73 in the second solute; or, the proportion of the total mass of substances with a n-octanol-water partition coefficient less than -0.74 in the first solute is less than the proportion of the total mass of substances with a n-octanol-water partition coefficient less than -0.74 in the second solute. Accurately quantifying the polarity of the solute using the n-octanol-water partition coefficient differentiates the polarity of the solutes in the first and second liquids of the atomized liquid, which facilitates the uniform dissolution of more solutes with significant polarity differences in the first and second liquids.
[0036] The “octanol-water partition coefficient” refers to the standard GB / T 21853-2008 Chemical Partition Coefficient (octanol-water) Shake Flask Method Test, wherein the octanol-water partition coefficient of the analyte is logK = log(analyte concentration in octanol (mol / L) / analyte concentration in water (mol / L)).
[0037] According to some embodiments of this disclosure, the substances with a n-octanol-water partition coefficient greater than 0.73 include one or more of the following: pinene, limonene, myrcene, caryophyllene, nonanal, decanal, lauryl alcohol, undecyl lactone, rose ether, thujone, camphene, sapinene, phellandrene, terpinene, umbelliferone, limonene, octyl alcohol, terpinene, linalool, octanol, neraldehyde, geraniol, nerol, geraniol, perillaldehyde, undecylaldehyde, dodecaaldehyde, and farnesene. The aforementioned substances with a n-octanol-water partition coefficient greater than 0.73 can achieve high flavor fidelity and aroma richness.
[0038] According to some embodiments of this disclosure, the substances with a n-octanol-water partition coefficient less than -0.74 include one or more of neotame, adventitia, sucralose, acesulfame potassium, glucosylstevioside, aspartame, hesperidin dihydrochalcone, neohesperidin dihydrochalcone, naringin dihydrochalcone, WS-3, WS-5, WS-12, WS-14, WS-23, WS-25, WS-27, menthol, menthyl ether, menthyl ester, nicotinic acid benzoate, nicotinic acid levulinic acid, nicotinic acid tartrate, nicotinic acid citrate, nicotinic acid acetate, and nicotinic acid oxalate. The aforementioned substances with a n-octanol-water partition coefficient less than -0.74 can reduce irritation or increase satisfaction, or achieve certain special tastes, such as sweetness and coolness.
[0039] The first and / or second solutes of this disclosure further include substances with an octanol-water partition coefficient greater than or equal to -0.74 and less than or equal to 0.73. Exemplarily, the substances with an octanol-water partition coefficient greater than or equal to -0.74 and less than or equal to 0.73 may be dimethyl glutarate, octanedione, ethylene acetone, ethyl lactate, etc. Such substances can help substances with an octanol-water partition coefficient less than -0.74 or greater than 0.73 to exhibit better odor or flavor.
[0040] According to some embodiments of this disclosure, the total mass percentage of substances in the first solute with an octanol-water partition coefficient greater than or equal to -0.74 is 2%-30%, preferably 5%-15%, based on their mass percentage in the first liquid. Exemplarily, the total mass percentage of substances in the first solvent with an octanol-water partition coefficient greater than or equal to -0.74 is 2%, 3%, 5%, 8%, 10%, 13%, 15%, 17%, 20%, 25%, or 30%. Substances with an octanol-water partition coefficient greater than or equal to -0.74 within the above range are more conducive to the uniform dissolution of such substances in the first solvent.
[0041] According to some embodiments of this disclosure, the total mass percentage of substances in the first solute with an octanol-water partition coefficient greater than 0.73 is 2%-15%, preferably 4%-10%, based on their mass percentage in the first liquid. Exemplarily, the total mass percentage of substances in the first solvent with an octanol-water partition coefficient greater than 0.73 in the first liquid is 2%, 3%, 4%, 6%, 8%, 10%, 13%, or 15%. The presence of substances with an octanol-water partition coefficient greater than 0.73 within the above range further facilitates the uniform dissolution of such substances in the first solvent.
[0042] In some embodiments, the total mass percentage of substances in the first solvent with an octanol-water partition coefficient greater than or equal to -0.74 and less than or equal to 0.73 is 0%-28%, preferably 0-15%, and more preferably 0-5%, based on their mass percentage in the first liquid. Exemplarily, the total mass percentage of such substances in the first solvent is 0%, 0.5%, 1%, 2%, 5%, 10%, 15%, 20%, or 25%.
[0043] According to some embodiments of this disclosure, the total mass percentage of substances in the second solute with an octanol-water partition coefficient less than or equal to 0.73 is 5%-30%, preferably 8%-20%, based on their mass percentage in the second liquid. Exemplarily, the total mass percentage of substances in the second solvent with an octanol-water partition coefficient less than or equal to 0.73 is 5%, 8%, 10%, 13%, 15%, 18%, 20%, 25%, or 30%. Substances with an octanol-water partition coefficient less than or equal to 0.73 within the above ranges are more conducive to the uniform dissolution of such substances in the second solvent.
[0044] According to some embodiments of this disclosure, the total mass percentage of substances with an octanol-water partition coefficient less than -0.74 in the second solute is 5%-20%, preferably 9%-15%, based on their mass percentage in the second liquid. Exemplarily, the total mass percentage of substances with an octanol-water partition coefficient less than -0.74 in the second solvent is 5%, 8%, 10%, 13%, 15%, 18%, or 20%. Substances with an octanol-water partition coefficient less than -0.74 within the above range further facilitate the uniform dissolution of such substances in the second solvent.
[0045] In some embodiments, the total mass percentage of substances in the second solvent with an octanol-water partition coefficient greater than or equal to -0.74 and less than or equal to 0.73 is 0%-25%, preferably 0-15%, and more preferably 0-5%, based on their mass percentage in the second liquid. Exemplarily, the total mass percentage of such substances in the second solvent is 0%, 0.5%, 1%, 2%, 5%, 10%, 15%, 20%, or 25%.
[0046] This disclosure does not particularly limit the preparation methods of the first and second liquids of the atomizing fluid, which generally include the step of mixing the components evenly. According to some embodiments, heating may be performed to accelerate dissolution, for example, heating at about 30°C-50°C for 10-20 minutes.
[0047] A second aspect of this disclosure provides a compartmentalized atomizer. The atomizer includes an atomizing liquid according to any of the above embodiments. Exemplarily, the atomizer has two reservoirs for independently storing a first liquid and a second liquid of the atomizing liquid. Exemplarily, the atomizing component of the atomizer may be a single component with two inlet ports, each fluidly connected to one of the two reservoirs. Exemplarily, the atomizing component may be two components, each with one inlet port, each fluidly connected to one of the two reservoirs. Optionally, the atomizer may also have more than two reservoirs, or other compartmentalized configurations; this disclosure does not impose specific limitations in this regard, as long as the independent storage of the first and second liquids is ensured.
[0048] The atomizing fluid disclosed herein is applicable to various types of atomizing components, such as resistance heating atomizing components, flat ultrasonic atomizing components, vibrating screen hole atomizing components, electrostatic atomizing components, infrared atomizing components, and microwave atomizing components, but is not limited thereto.
[0049] A third aspect of this disclosure provides an electronic atomizing device, including a battery assembly and an atomizer according to any of the above embodiments, wherein the battery assembly is used to power the atomizer.
[0050] The present disclosure will be further described below with reference to specific embodiments. All raw materials involved are obtained through commercial purchase.
[0051] Example
[0052] Examples 1-3 and Comparative Examples 1-3
[0053] According to the formulations shown in Table 1, the components were mixed evenly to obtain the first and second liquids of the atomizing liquids for Examples 1-3, wherein each raw material component is expressed as a percentage by mass. The atomizing liquids of Examples 1-3 and Comparative Examples 1-3 were tested using a compartmentalized electronic atomizing device with two storage chambers. The first and second liquids of Examples 1-3 were stored independently in the two storage chambers of the compartmentalized electronic atomizing device. In Comparative Example 1, the first and second liquids of Example 1 were mixed evenly, then divided into two equal portions by mass, and these two portions were placed in the two storage chambers of the compartmentalized electronic atomizing device respectively; that is, the first and second liquids were not stored independently. In Comparative Example 2, the first liquid from Example 1 was placed simultaneously in the two storage chambers of the compartmentalized electronic atomizing device. In Comparative Example 3, the second liquid from Example 1 was placed simultaneously in the two storage chambers of the compartmentalized electronic atomizing device.
[0054] Table 1. Weight parts of each component in the atomizing liquid of Examples 1-3 and Comparative Examples 1-3
[0055]
[0056]
[0057] As shown in Table 1, the e-liquid in both storage tanks of Examples 1-3 was uniformly clear, meaning that each first solute was uniformly dispersed in its corresponding first solvent, and each second solute was uniformly dispersed in its corresponding second solvent. In Comparative Example 1, the originally uniformly clear first and second liquids from Examples 1 were mixed, resulting in turbidity and stratification, with suspended small droplets appearing.
[0058] Sensory evaluation test
[0059] A panel of six individuals, selected through sensory evaluation, conducted sensory assessments of the atomizing liquids containing Examples 1-3 and Comparative Examples 1-3, using smoke volume, aroma reproduction, aroma intensity, sweetness, and consistency as evaluation indicators. To eliminate differences in electronic atomization devices, three parallel samples were prepared for each example and comparative example. To eliminate mutual influence between samples, the evaluators rinsed their mouths and throats with 200 mL of purified water before evaluating each sample and remained silent until the sweetness of the previous sample had completely dissipated.
[0060] Each person performed a vaping test on each of all the examples and comparative samples, using a holistic cyclical vaping evaluation method. A blind vaping scoring method was employed, and based on the meanings of the four sensory quality evaluation indicators (smoke volume, aroma fidelity, aroma intensity, and sweetness) in Table 2, the average score of all vapers was taken for each item of each vaporizer sample. Furthermore, if more than half of the six sensory personnel indicated poor vaping consistency, off-odors, or a burnt / bitter taste, the sample was considered to have poor vaping consistency or an off-odor. The sensory evaluation results are shown in Table 3.
[0061] Table 2 Scoring Criteria for Sensory Evaluation of Electronic Atomizing Fluids
[0062] Score smoke volume Aroma fidelity Aroma intensity Sweetness 9 adequate very good Very strong Very sweet 8 foot good powerful sweet 7 More adequate better Strong Sweeter 6 Slightly sufficient Slightly better Slightly heavier Slightly sweet 5 middle middle middle middle 4 Slightly Slightly worse Slightly weak Slightly lighter 3 Lighter Poor Weak Lighter 2 light Difference weak light 1 Very light Very bad Very weak Very light
[0063] Table 3 Sensory evaluation of the examples and comparative samples
[0064] sample smoke volume Aroma fidelity Aroma intensity Sweetness consistency Example 1 8.22 8.15 8.22 7.45 Good consistency and no odor Example 2 8.40 8.11 8.09 7.19 Good consistency and no odor Example 3 8.31 8.34 8.18 7.22 Good consistency and no odor Comparative Example 1 8.13 6.77 7.01 6.49 Poor consistency and unpleasant odor Comparative Example 2 1.25 5.08 7.11 1 Odorless Comparative Example 3 8.09 1 1 8.87 Odorless
[0065] Based on the formulation in Table 1 and the data in Table 3, it can be seen that in Example 1, the first liquid only includes substances with a n-octanol-water partition coefficient greater than 0.73, and the second liquid only includes substances with a n-octanol-water partition coefficient less than -0.74. This achieves a rich and reducing aroma, good taste consistency, no off-odors, and sufficient smoke. In Example 2, the first liquid includes a small amount of substances with a n-octanol-water partition coefficient less than -0.74. The total mass percentage of substances with a n-octanol-water partition coefficient greater than 0.73 in the first liquid is greater than that in the second liquid, also achieving good taste and aroma. In Example 3, the total mass percentage of substances with a n-octanol-water partition coefficient less than -0.74 in the first liquid is greater than the total mass percentage of substances with a n-octanol-water partition coefficient greater than 0.73, and the total mass percentage of substances with a n-octanol-water partition coefficient greater than 0.73 in the first liquid is greater than the total mass percentage of substances with a n-octanol-water partition coefficient greater than 0.73 in the second liquid, which can also achieve good taste and aroma.
[0066] In Comparative Example 1, both storage chambers contained a mixture of the first and second liquids from Example 1, resulting in suspended small droplets. These droplets were clustered together, consisting of aroma compounds with similar polarities. As the atomizing liquid was gradually consumed, while the flavor was relatively rich when the small droplet areas were atomized, the limited solvent content meant that the simultaneous evaporation and dissipation of heat by the solvent created localized high-temperature spots, leading to a higher risk of scorching. Since most of the aroma compounds were concentrated in the small droplets, the flavor was not as rich and accurate when the non-small droplet areas of the atomizing liquid were atomized. This random atomization of the small and non-small droplet areas resulted in an inconsistent flavor before and after vaping.
[0067] In Comparative Example 2, both storage chambers contained the first liquid from Example 1. Due to the lack of the second liquid and the absence of Class C solvent, the variety of aroma substances was limited, the aroma reduction was significantly reduced, and the amount of smoke was weak. In Comparative Example 3, both storage chambers contained the second liquid from Example 1. Due to the lack of the first liquid, the variety of aroma substances was limited, especially the lack of aroma substances with a n-octanol-water partition coefficient greater than -0.74, resulting in a very unpleasant sensation.
[0068] The above descriptions are merely some specific embodiments of this disclosure, intended to illustrate this disclosure, and are not intended to limit the scope of protection claimed in this application. Any modifications or substitutions made using the present application specification under the inventive concept of this disclosure, or direct / indirect applications in other related technical fields, are included within the scope of protection claimed in this application.
Claims
1. An atomizing liquid for use in a compartmentalized atomizing device, comprising a first liquid and a second liquid, characterized in that, The first liquid and the second liquid are stored independently in the compartmentalized atomizing device. The first liquid includes a first solvent and a first solute, and the second liquid includes a second solvent and a second solute. The first solvent includes at least a type A solvent and a type C solvent, and the second solvent includes at least a type A solvent and a type C solvent. The type A solvent includes one or more of ethanol, propanol, butanol, and benzyl alcohol, and the type C solvent includes one or more of water, ethylene glycol, glycerol, and glycerol. Wherein, the proportion of the total mass of the type A solvent in the second solvent is less than the proportion of the total mass of the type A solvent in the first solvent, or the proportion of the total mass of the type C solvent in the second solvent is greater than the proportion of the total mass of the type C solvent in the first solvent.
2. The atomizing liquid according to claim 1, characterized in that, The first solvent further includes a type B solvent, which includes one or more of propylene glycol, butanediol, triethyl citrate, triacetyl glycerol, and caprylic / capric glycerol, wherein the total mass percentage of the type A solvent and the type B solvent in the first solvent is 60%-98% by mass percentage in the first liquid.
3. The atomizing liquid according to claim 2, characterized in that, The total mass percentage of the Class A solvent and the Class B solvent in the first solvent is 70%-95% based on the mass percentage in the first liquid.
4. The atomizing liquid according to claim 3, characterized in that, The total mass percentage of the Class A solvent in the first solvent is 60%-95% based on the mass percentage in the first liquid.
5. The atomizing liquid according to claim 4, characterized in that, The total mass percentage of the Class A solvent in the first solvent is 70%-90% based on the mass percentage in the first liquid.
6. The atomizing liquid according to claim 1, characterized in that, The second solvent further includes a type B solvent, which includes one or more of propylene glycol, butanediol, triethyl citrate, triacetyl glycerol, and caprylic / capric glycerol, wherein the total mass percentage of the type C solvent and the type B solvent in the second solvent is 60%-95% by mass percentage in the second solvent.
7. The atomizing liquid according to claim 6, characterized in that, The total mass percentage of the Class C solvent and the Class B solvent in the second solvent is 70%-92% by mass percentage in the second liquid.
8. The atomizing liquid according to claim 7, characterized in that, The total mass percentage of the Class C solvent in the second solvent is 20%-60% based on the mass percentage in the second liquid.
9. The atomizing liquid according to claim 8, characterized in that, The total mass percentage of the Class C solvent in the second solvent is 30%-50% based on the mass percentage in the second liquid.
10. The atomizing liquid according to claim 1, characterized in that, The proportion of the total mass of substances with a n-octanol-water partition coefficient greater than 0.73 in the first solute is greater than the proportion of the total mass of substances with a n-octanol-water partition coefficient greater than 0.73 in the second solute; or, the proportion of the total mass of substances with a n-octanol-water partition coefficient less than -0.74 in the first solute is less than the proportion of the total mass of substances with a n-octanol-water partition coefficient less than -0.74 in the second solute.
11. The atomizing liquid according to claim 10, characterized in that, The first solute further includes substances with a n-octanol-water partition coefficient greater than or equal to -0.74 and less than or equal to 0.
73. The total mass percentage of substances with a n-octanol-water partition coefficient greater than or equal to -0.74 in the first liquid is 2%-30%.
12. The atomizing liquid according to claim 11, characterized in that, The total mass percentage of substances in the first solute with a n-octanol-water partition coefficient greater than or equal to -0.74 is 5%-15% based on the mass percentage in the first liquid.
13. The atomizing liquid according to claim 11 or 12, characterized in that, The total mass percentage of substances in the first solute with a n-octanol-water partition coefficient greater than 0.73 is 2%-15% based on the mass percentage in the first liquid.
14. The atomizing liquid according to claim 13, characterized in that, The total mass percentage of substances in the first solute with a n-octanol-water partition coefficient greater than 0.73 is 4%-10% based on the mass percentage in the first liquid.
15. The atomizing liquid according to claim 10, characterized in that, The second solute further includes substances with a n-octanol-water partition coefficient greater than or equal to -0.74 and less than or equal to 0.73, and the total mass percentage of substances with a n-octanol-water partition coefficient less than or equal to 0.73 in the second liquid is 5%-30%.
16. The atomizing liquid according to claim 15, characterized in that, The total mass percentage of substances in the second solute with a n-octanol-water partition coefficient of less than or equal to 0.73 is 8%-20% by mass percentage in the second liquid.
17. The atomizing liquid according to claim 15 or 16, characterized in that, The total mass percentage of substances in the second solute with a n-octanol-water partition coefficient less than -0.74 is 5%-20% by mass percentage in the second liquid.
18. The atomizing liquid according to claim 17, characterized in that, The total mass percentage of substances in the second solute with a n-octanol-water partition coefficient less than -0.74 is 9%-15% by mass percentage in the second liquid.
19. The atomizing liquid according to claim 10 or claim 11, characterized in that, The substances with a n-octanol-water partition coefficient greater than 0.73 include one or more of the following: pinene, limonene, myrcene, caryophyllene, nonanal, decanal, lauryl alcohol, undecyl lactone, rose ether, thujone, camphene, sabinene, phellandrene, terpinene, umbelliferone, limonene, octyl alcohol, terpineol, linalool, octanol, neraldehyde, geraniol, nerol, geraniol, perillaldehyde, undecylaldehyde, dodecaaldehyde, and ethanoylene.
20. The atomizing liquid according to claim 10 or claim 15, characterized in that, The substances with an octanol-water partition coefficient less than -0.74 include one or more of neotame, adventitia, sucralose, acesulfame potassium, glucosylstevioside, aspartame, hesperidin dihydrochalcone, neohesperidin dihydrochalcone, naringin dihydrochalcone, WS-3, WS-5, WS-12, WS-14, WS-23, WS-25, WS-27, menthol, menthyl ether, menthyl ester, nicotinic acid benzoate, nicotinic acid levulinic acid, nicotinic acid tartrate, nicotinic acid citrate, nicotinic acid acetate, and nicotinic acid oxalate.
21. A compartmentalized atomizer, characterized in that, Includes the atomizing liquid according to any one of claims 1-20.
22. An electronic atomizing device, characterized in that, It includes a battery assembly and a compartmentalized atomizer according to claim 21, wherein the battery assembly is used to power the compartmentalized atomizer.
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