Hydrothermal synthesis workstation

Abstract

The utility model relates to a hydro-thermal synthesis workstation, and belongs to the technical field of experimental equipment. The hydro-thermal synthesis workstation comprises a material storage module, a heating module, a drying module, a driving module and an operation module; wherein the drying module comprises a plurality of gas conveying pipes and a gas collecting pipe, the gas conveying pipes are connected with the gas collecting pipe, and the gas collecting pipe can rotate around the axis of the gas collecting pipe to drive pipe openings of the gas conveying pipes to face reagent bottles so as to blow in dry gas; the driving module comprises an X-axis moving guide rail, a Y-axis moving guide rail and a Z-axis moving guide rail which are connected in sequence; the operation module is connected to the Z-axis moving guide rail, can move among the other modules under the action of the driving module, and is used for clamping reagent bottles and taking or putting raw materials into the reagent bottles. The drying module promotes liquid in the reagent bottle to be evaporated quickly, and the drying process and the drying canceling process are switched freely through rotation of the gas collecting pipe. The driving module drives the reagent bottles to move freely through the operation module, and the automation degree is improved.

Description

Technical Field

[0001] The present application relates to the technical field of experimental equipment, and in particular to a hydrothermal synthesis workstation. Background Art

[0002] With the continuous deepening of new material research, the demand for efficient and precise hydrothermal synthesis technology is growing. Traditional hydrothermal synthesis processes mostly rely on manual operation, which is not only time-consuming and inefficient, but also has great limitations in high-throughput experiments and precise control. Therefore, the development of an automated, high-throughput hydrothermal synthesis workstation is crucial to improving synthesis efficiency and quality. In recent years, automation and intelligent technologies have been increasingly used in the field of chemical synthesis, such as automated pipetting, precise temperature control, and high-precision actuators. The development of these technologies has greatly improved experimental efficiency and the repeatability of results, while reducing the possibility of human error. However, there is still a lack of rapid drying to obtain samples and the overall degree of automation. Utility Model Content

[0003] Based on this, it is necessary to provide a hydrothermal synthesis workstation to improve the degree of automation and quickly dry to obtain samples.

[0004] A hydrothermal synthesis workstation comprises a material storage module, a heating module, a drying module, a driving module and an operating module; the material storage module has a material storage station for storing reagent bottles; the heating module is used to heat the reagent bottles; the drying module comprises a plurality of gas pipes and a gas collecting pipe, the plurality of gas pipes are arranged at intervals along the axial direction of the gas collecting pipe, each of the gas pipes is connected to the gas collecting pipe, the gas collecting pipe can rotate around its own axis to drive the pipe mouth of the gas pipe toward the reagent bottle, and the gas pipe can blow dry gas into the heated reagent bottle; the driving module comprises an X-axis movable guide rail, a Y-axis movable guide rail and a Z-axis movable guide rail connected in sequence; the operating module is connected to the Z-axis movable guide rail, the operating module can flow and move between the material storage module, the heating module and the drying module under the action of the driving module, and the operating module is used to clamp the reagent bottle and take or put raw materials in the reagent bottle.

[0005] It is understandable that a storage module is provided to centrally place reagent bottles. The drive assembly controls the operating module through the X-axis moving guide rail, the Y-axis moving guide rail and the Z-axis moving guide rail. The reagent bottle is clamped by the operating module and transferred to each different module. The operating module can also add raw materials to the reagent bottle or take the raw materials in the reagent bottle so as to mix the raw materials and form a chemical reaction. The heating module can heat the reagent bottle to meet the temperature conditions required for the chemical reaction. The drying module blows dry gas into the reagent bottle through the gas collecting pipe and the gas supply pipe to promote the rapid evaporation of the liquid in the reagent bottle, so as to quickly obtain the required sample, and through the rotation of the gas collecting pipe, the drying process and the process of canceling the drying process can be switched freely and easily. The drive module is connected to the operating module to drive the reagent bottle to flow freely in other modules, which improves the overall automation of the hydrothermal synthesis workstation and can meet the needs of high-throughput and high-efficiency hydrothermal synthesis.

[0006] In one embodiment, the drying module further includes a drying drive and a drying transmission assembly, wherein the drying transmission assembly is connected between the drying drive and the air collecting pipe, and the drying transmission assembly drives the air collecting pipe to rotate under the action of the drying drive.

[0007] It can be understood that the drying drive member can provide a power source, and the drying transmission assembly transmits the power to the air collecting pipe to rotate the air collecting pipe, thereby improving the degree of automation.

[0008] In one embodiment, the drying transmission assembly includes a driving gear and a driven gear, which are meshed and transmitted, the driving gear is connected to the drying drive member, and the driven gear is connected to the air collecting pipe.

[0009] It can be understood that the transmission of power through gear transmission is smoother and more efficient.

[0010] In one embodiment, the hydrothermal synthesis workstation further includes a shaking module, wherein the shaking module has a shaking station for placing the reagent bottle, and the shaking module can drive the reagent bottle to shake.

[0011] It can be understood that the shaking module is provided to shake the reagent bottle to promote uniform mixing of the raw materials in the reagent bottle, which is beneficial to accelerate the reaction rate.

[0012] In one embodiment, the shaking module also includes a shaking drive, a shaking transmission mechanism and a shaking table. The shaking transmission mechanism is connected between the shaking drive and the shaking table. The shaking transmission mechanism drives the shaking table to shake under the action of the shaking drive. The shaking table is constructed with a plurality of shaking stations arranged at intervals.

[0013] It can be understood that the shaking driving member provides a power source for the shaking of the shaking table, and the shaking transmission mechanism transmits the power of the shaking driving member to the shaking table to make the shaking table shake.

[0014] In one embodiment, the vibration transmission mechanism includes a transmission assembly, a first transmission belt and multiple transmission shafts, the multiple transmission shafts are circumferentially arranged around the axis of the vibration table and connected to the vibration table, the first transmission belt is tensioned between the multiple transmission shafts, the transmission shaft is also transmission-connected to the vibration transmission assembly, the vibration transmission assembly is connected to the vibration drive member, and can drive the multiple transmission shafts to rotate; wherein each of the transmission shafts includes a first shaft section and a second shaft section, the first shaft section and the second shaft section are connected and eccentrically arranged, the first shaft section is connected to the vibration transmission assembly, and the second shaft section is connected to the vibration table.

[0015] It can be understood that the vibration transmission assembly transmits power smoothly to the transmission shaft, and the multiple transmission shafts can be rotated synchronously through the first transmission belt. Since the first shaft section and the second shaft section of the transmission shaft are eccentrically arranged, the second shaft section rotates around the axis of the first shaft section. Since the multiple transmission shafts are arranged circumferentially around the vibration table, the synchronous rotation of the multiple transmission shafts can drive the vibration table to swing.

[0016] In one embodiment, the vibration transmission assembly includes a driving pulley, a driven pulley and a second transmission belt, the driving pulley is connected to the vibration driving member, the second transmission belt is tensioned between the driving pulley and the driven pulley, and the driven pulley is in transmission connection with one of the transmission shafts.

[0017] It is understandable that, with such an arrangement, the driving pulley transmits power to the driven pulley through the second transmission belt, so that the driven pulley drives the transmission shaft to rotate, thereby realizing power transmission.

[0018] In one embodiment, the reagent bottle includes a bottle body and a cover body, and the hydrothermal synthesis workstation also includes a capping module; the capping module has a second gripping clamp, which is used to clamp the bottle body and cooperate with the operating module to clamp the cover body and rotate it relative to the bottle body; or, the capping module has a second gripping clamp and a third gripping clamp arranged at intervals, the second gripping clamp is used to clamp the bottle body, and the third gripping clamp is used to clamp the cover body and rotate it relative to the bottle body.

[0019] It is understandable that the automatic screwing of the cap body relative to the bottle body can be realized by setting the cap screwing module, thereby improving the degree of automation. The second gripping clamp cooperates with the first gripping clamp or the second gripping clamp cooperates with the third gripping clamp, which is easy to operate.

[0020] In one embodiment, the operation module includes a first gripper, which is at least used to grip the reagent bottle; and / or the operation module includes a pipette, which is used to absorb raw materials in the reagent bottle or add raw materials to the reagent bottle.

[0021] It can be understood that the first gripper is provided to facilitate the movement of the reagent bottle, and the pipette is provided to facilitate the addition and mixing of raw materials to promote the chemical reaction.

[0022] In one embodiment, the Z-axis moving guide rail also includes a chain and a Z-axis driver; the Z-axis driver is connected to and drives the operating module to move along the Z-axis; one end of the chain is connected to the Z-axis driver, and the other end is connected to the end of the operating module away from the storage module along the Z-axis direction; the chain has a wiring space along its own axis, and the circuit of the operating module is passed through the wiring space and is electrically connected to the Z-axis driver.

[0023] It can be understood that the Z-axis drive can provide power for the movement of the operating module in the Z-axis direction, and the wiring space is set through the chain to protect the line and prevent the line from being entangled. The chain can bend or straighten following the movement of the operating module without affecting the movement of the operating module. BRIEF DESCRIPTION OF THE DRAWINGS

[0024] In order to more clearly illustrate the technical solutions in the embodiments of the present application or the conventional technology, the drawings required for use in the embodiments or the conventional technology descriptions are briefly introduced below. Obviously, the drawings described below are only some embodiments of the present application. For ordinary technicians in this field, other drawings can be obtained based on these drawings without creative work.

[0025] Figure 1 A schematic diagram of the structure of the hydrothermal synthesis workstation provided for this application;

[0026] Figure 2 This is a schematic diagram of the structure of the drying module in the hydrothermal synthesis workstation provided in this application;

[0027] Figure 3 A schematic diagram of the structure of the shaking module in the hydrothermal synthesis workstation provided in this application;

[0028] Figure 4 A cross-sectional view of a shaking module in a hydrothermal synthesis workstation provided in the present application;

[0029] Figure 5 This is a schematic diagram of the structure of the transmission shaft of the shaking module in the hydrothermal synthesis workstation provided in this application;

[0030] Figure 6A schematic diagram of the structure of the first gripper in the hydrothermal synthesis workstation provided in this application;

[0031] Figure 7 This is a schematic diagram of the structure of the pipette and the tip in the hydrothermal synthesis workstation provided in this application.

[0032] Reference numerals: 100, hydrothermal synthesis workstation; 10, material storage module; 11, reagent bottle; 12, pipette tip; 20, heating module; 30, drying module; 31, gas delivery pipe; 32, gas collecting pipe; 40, driving module; 41, X-axis moving guide rail; 42, Y-axis moving guide rail; 43, Z-axis moving guide rail; 431, Z-axis driver; 432, chain; 51, first gripper; 52, pipette; 60, shaking module; 61. Vibration drive member; 62. Vibration transmission mechanism; 621. Vibration transmission assembly; 6211. Active pulley; 6212. Driven pulley; 6213. Second transmission belt; 622. Transmission shaft; 6221. First shaft section; 6222. Second shaft section; 623. Bearing seat; 624. Bearing; 63. Vibration table; 70. Capping module; 71. Second gripper; 80. Housing; 81. Interface; 82. Start / stop switch. DETAILED DESCRIPTION

[0033] In order to make the above-mentioned purposes, features and advantages of the present application more obvious and easy to understand, the specific implementation methods of the present application are described in detail below in conjunction with the accompanying drawings. In the following description, many specific details are set forth to facilitate a full understanding of the present application. However, the present application can be implemented in many other ways different from those described herein, and those skilled in the art can make similar improvements without violating the connotation of the present application, so the present application is not limited by the specific embodiments disclosed below.

[0034] It should be noted that when a component is referred to as being "fixed to" or "disposed on" another component, it may be directly on the other component or there may also be a central component. When a component is considered to be "connected to" another component, it may be directly connected to the other component or there may be a central component at the same time. The terms "vertical", "horizontal", "upper", "lower", "left", "right" and similar expressions used in the specification of this application are for illustrative purposes only and do not represent the only implementation method.

[0035] In addition, the terms "first" and "second" are used for descriptive purposes only and should not be understood as indicating or implying relative importance or implicitly indicating the number of the indicated technical features. Therefore, the features defined as "first" and "second" may explicitly or implicitly include at least one of the features. In the description of this application, the meaning of "plurality" is at least two, such as two, three, etc., unless otherwise clearly and specifically defined.

[0036] In the present application, unless otherwise clearly specified and limited, a first feature being “above” or “below” a second feature may mean that the first feature is directly in contact with the second feature, or the first feature and the second feature are indirectly in contact through an intermediate medium. Moreover, a first feature being “above”, “above” or “above” a second feature may mean that the first feature is directly above or obliquely above the second feature, or simply means that the first feature is higher in level than the second feature. A first feature being “below”, “below” or “below” a second feature may mean that the first feature is directly below or obliquely below the second feature, or simply means that the first feature is lower in level than the second feature.

[0037] Unless otherwise defined, all technical and scientific terms used in the specification of this application have the same meaning as those commonly understood by those skilled in the art to which this application belongs. The terms used in the specification of this application are only for the purpose of describing specific embodiments and are not intended to limit this application. The term "and / or" used in the specification of this application includes any and all combinations of one or more related listed items.

[0038] See also Figures 1 to 7 The present application provides a hydrothermal synthesis workstation 100, which includes a material storage module 10, a heating module 20, a drying module 30, a driving module 40 and an operating module; the material storage module 10 has a material storage station for storing a reagent bottle 11; the heating module 20 is used to heat the reagent bottle 11; the drying module 30 includes a plurality of gas pipes 31 and a gas collecting pipe 32, the plurality of gas pipes 31 are arranged at intervals along the axial direction of the gas collecting pipe 32, each gas pipe 31 is connected to the gas collecting pipe 32, and the gas collecting pipe 32 can rotate around its own axis The driving module 40 drives the nozzle of the gas pipe 31 toward the reagent bottle 11, and the gas pipe 31 can blow dry gas into the heated reagent bottle 11; the driving module 40 includes an X-axis movable guide rail 41, a Y-axis movable guide rail 42 and a Z-axis movable guide rail 43 connected in sequence; the operating module is connected to the Z-axis movable guide rail 43, and the operating module can flow and move between the material storage module 10, the heating module 20 and the drying module 30 under the action of the driving module 40, and the operating module is used to clamp the reagent bottle 11 and take or put the raw material in the reagent bottle 11.

[0039] In this way, the material storage module 10 is provided with a material storage station for the stable placement of the reagent bottle 11. A plurality of material storage stations arranged at intervals can be provided to centrally place a plurality of reagent bottles 11, so as to facilitate centralized taking and more convenient operation. Among them, the operating module can take the reagent bottle 11, and can also take out the raw materials in the reagent bottle 11, add them to another reagent bottle 11, mix them and produce a reaction. The driving module 40 is connected to the operating module to control the operating module to circulate in other modules. Specifically, the driving module 40 controls the operation module to move to realize the taking and adding of the raw materials. After the raw materials in the reagent bottle 11 are mixed, the driving module 40 can control it to move to the heating module 20 for heating, so that the temperature is increased to reach the reaction conditions. After the heating is completed, the driving module 40 continues to drive the operating module to move the reagent bottle 11 to the drying module 30. At this time, the gas collecting pipe 32 rotates so that the nozzle of the gas supply pipe 31 faces the bottle mouth of the reagent bottle 11, and then the drying gas is input to the reagent bottle 11. The drying gas can promote the rapid evaporation of the liquid in the reagent bottle 11 to quickly obtain the sample. After drying is completed, the gas collecting pipe 32 rotates in the reverse direction to facilitate the removal of the reagent bottle 11 .

[0040] In summary, it is precisely because of the setting of each module that different functions can be realized clearly and reasonably. The driving module 40 can realize free movement in three dimensions of X-axis, Y-axis and Z-axis, improve the degree of automation, and the setting of the drying module 30 speeds up the process of obtaining samples. The cooperation of the driving module 40, the operating module and the drying module 30 is conducive to automatic and rapid drying to obtain samples, so as to meet the needs of high-throughput and high-efficiency hydrothermal synthesis.

[0041] In a specific embodiment, the reagent bottle 11 includes a bottle body and a bottle cap, and a plurality of material storage stations are provided, and the material storage station can place the bottle body or the cap.

[0042] like Figure 7 As shown, in a specific embodiment, the operation module includes a pipette 52, and the pipette 52 is used to absorb the raw materials in the reagent bottle 11 or add raw materials to the reagent bottle 11, so as to realize the transfer of raw materials and mix different raw materials to produce reactions. In a more specific embodiment, the material storage module 10 also includes a suction head 12, and the suction head 12 can be placed on the material storage station. The pipette 52 is first assembled with the suction head 12, and then the raw materials are absorbed. The suction head 12 is usually a disposable item, and multiple pipettes can be provided to facilitate the replacement of the pipette 52, which is conducive to reducing pollution and ensuring the normal progress of the reaction.

[0043] like Figure 6 As shown, in some embodiments, the operation module includes a first gripper 51 , which is at least used to grip the reagent bottle 11 , and driven by the driving module 40 , can move the reagent bottle 11 to other modules.

[0044] In a specific embodiment, the Z-axis moving guide rail 43 also includes a Z-axis driver 431. Along the X-axis direction, the first gripper 51 and the pipette 52 are arranged on both sides of the Z-axis driver 431, and the Z-axis driver 431 can respectively drive the first gripper 51 and the pipette 52 to move along the Z-axis direction.

[0045] like Figure 1 As shown, in a further embodiment, the Z-axis moving guide rail 43 also includes a chain 432; one end of the chain 432 is connected to the Z-axis driver 431, and the other end is connected to the end of the operating module away from the storage module 10 along the Z-axis direction. The chain 432 has a wiring space along its own axis, and the line of the operating module is arranged in the wiring space and is electrically connected to the Z-axis driver 431. In this way, the chain 432 can be bent or straightened according to the movement of the operating module along the Z-axis. For example, when the operating module moves downward along the Z-axis, the end of the chain 432 connected to the operating module will be bent downward accordingly; and when the operating module moves upward along the Z-axis, the end of the chain 432 connected to the operating module will be straightened upward accordingly. This setting can adapt to the movement of the operating module and will not interfere with the movement of the operating module. Further, a wiring space is provided inside the chain 432, which is convenient for placing the line between the operating module and the Z-axis driver 431 in the wiring space, which is conducive to protecting the line, so that there will be no entanglement between the lines, and avoid interfering with the movement of the operating module.

[0046] like Figure 1 As shown, in a specific embodiment, the heating module 20 is provided with a heating platform, on which a plurality of heating stations arranged at intervals are constructed, and the reagent bottle 11 is placed on the heating station for heating.

[0047] like Figure 1 As shown, in an optional embodiment, the hydrothermal synthesis workstation 100 also includes a shaking module 60, which has a shaking station for placing the reagent bottle 11. The shaking module 60 can drive the reagent bottle 11 to shake, thereby promoting the different raw materials in the reagent bottle 11 to be mixed evenly, which is beneficial to accelerate the reaction rate and promote the progress of the reaction.

[0048] like Figure 3 and Figure 4 As shown, in a further embodiment, the shaking module 60 further includes a shaking drive 61, a shaking transmission mechanism 62 and a shaking table 63, wherein the shaking transmission mechanism 62 is connected between the shaking drive 61 and the shaking table 63, and the shaking transmission mechanism 62 drives the shaking table 63 to shake under the action of the shaking drive 61, and the shaking table 63 is configured with a plurality of shaking stations arranged at intervals. In this way, the shaking station can place the corresponding reagent bottle 11, the shaking drive 61 provides a power source for shaking, and the shaking transmission mechanism 62 transmits power to the shaking table 63, so that the shaking table 63 shakes.

[0049] like Figure 4 and Figure 5 As shown, in a specific embodiment, the vibration transmission mechanism 62 includes a vibration transmission component 621, a first transmission belt and multiple transmission shafts 622, the multiple transmission shafts 622 are circumferentially arranged around the axis of the vibration table 63 and connected to the vibration table 63, the first transmission belt is tensioned between the multiple transmission shafts 622, the transmission shafts 622 are also transmission-connected to the vibration transmission component 621, the vibration transmission component 621 is connected to the vibration drive member 61, and can drive the multiple transmission shafts 622 to rotate; wherein each transmission shaft 622 includes a first shaft section 6221 and a second shaft section 6222, the first shaft section 6221 and the second shaft section 6222 are connected and eccentrically arranged, the first shaft section 6221 is connected to the vibration transmission component 621, and the second shaft section 6222 is connected to the vibration table 63.

[0050] In this way, the shaking transmission assembly 621 transmits the power of the shaking drive member 61 to the transmission shaft 622, and driven by the first transmission belt, the first shaft segments 6221 in the plurality of transmission shafts 622 rotate synchronously. Since the second shaft segment 6222 is eccentrically arranged relative to the first shaft segment 6221, the second shaft segment 6222 rotates around the axis of the first shaft segment 6221. Since the transmission shaft 622 is circumferentially arranged around the axis of the shaking table 63, the shaking table 63 is shaken and swayed under the joint action of the plurality of second shaft segments 6222.

[0051] In a specific embodiment, three transmission shafts 622 are provided, and the three transmission shafts 622 are staggered along the X-axis and the Y-axis to form a circle, so that the vibration table 63 can swing and sway circumferentially under the eccentricity of the second shaft section 6222 relative to the first shaft section 6221. In other embodiments, four, five, etc. transmission shafts 622 can also be provided, as long as the vibration table 63 can swing and sway circumferentially.

[0052] like Figure 4As shown, in a specific embodiment, the vibration transmission assembly 621 includes a driving pulley 6211, a driven pulley 6212 and a second transmission belt 6213. The driving pulley 6211 is connected to the vibration driving member 61. The second transmission belt 6213 is tightened between the driving pulley 6211 and the driven pulley 6212. The driven pulley 6212 is in transmission connection with one of the transmission shafts 622. In this way, the vibration driving member 61 drives the driving pulley 6211 to rotate, and the driving pulley 6211 drives the driven pulley 6212 to rotate through the second transmission belt 6213. Then, the synchronous rotation of multiple transmission shafts 622 is realized through the first transmission belt, and the vibration platform 63 is driven to swing and shake together. In a specific embodiment, each transmission shaft 622 is connected to a driven pulley 6212, the driving pulley 6211 is connected to one of the driven pulleys 6212 through a second transmission belt 6213, and a first transmission belt is tensioned between multiple driven pulleys 6212 to achieve synchronous rotation of multiple driven pulleys 6212, thereby achieving synchronous rotation of multiple transmission shafts 622.

[0053] like Figure 3 and Figure 4 As shown, in a specific embodiment, the vibration transmission mechanism 62 includes a bearing seat 623, the bearing seat 623 is provided with a mounting hole, a bearing 624 is installed in the mounting hole, each transmission shaft 622 is installed in the mounting hole and passes through the bearing 624, and the bearing 624 is arranged to promote the stable rotation of the transmission shaft 622 and avoid direct contact with the bearing seat 623.

[0054] like Figure 1 As shown, in an optional embodiment, the hydrothermal synthesis workstation 100 also includes a capping module 70; the capping module 70 has a second gripper 71, the second gripper 71 is used to clamp the bottle body, and cooperate with the operating module to clamp the cover body to rotate relative to the bottle body, that is, the operating module moves the bottle body into the second gripper 71, the second gripper 71 clamps the bottle body, and the operating module continues to move the cover body to the bottle mouth of the bottle body, and drives the cover body to rotate relative to the bottle body to achieve the tightening of the cover body. In this process, the second gripper 71 clamps the bottle body to prevent the bottle body from rotating, so that the operating module can smoothly drive the cover body to rotate. In a specific embodiment, the first gripper 51 in the operating module clamps the bottle body and the cover body, and the first gripper 51 can rotate around the axis to achieve the rotation of the cover body.

[0055] In another optional embodiment, the capping module 70 has a second gripper 71 and a third gripper which are arranged at intervals, the second gripper 71 is used to clamp the bottle body, and the third gripper is used to clamp the cap body and rotate relative to the bottle body. In this way, the operating module moves the bottle body into the second gripper 71, the second gripper 71 clamps the bottle body, the operating module continues to move the cap body to the bottle mouth of the bottle body, and then the third gripper clamps the cap body and drives the cap body to rotate, so that the cap body rotates relative to the bottle body.

[0056] In a specific embodiment, the second gripper 71 and / or the third gripper can be configured as a pneumatic gripper, and the hydrothermal synthesis workstation 100 further includes a gas pressure regulating valve connected to the pneumatic gripper to control the clamping force of the pneumatic gripper. At the same time, the pneumatic gripper can also be connected to a dry gas source in the drying module 30 to control the output pressure of the dry gas.

[0057] In an optional embodiment, the drying module 30 further includes a drying drive and a drying transmission assembly, wherein the drying transmission assembly is connected between the drying drive and the gas collecting pipe 32, and the drying transmission assembly drives the gas collecting pipe 32 to rotate under the action of the drying drive, and the drying drive provides power for the rotation of the gas collecting pipe 32, and the drying transmission assembly transmits the power, which is conducive to realizing the automation of the rotation of the gas collecting pipe 32. In a specific embodiment, the drying gas can be an inert gas such as nitrogen.

[0058] In a specific embodiment, the drying transmission assembly includes a driving gear and a driven gear, which are meshed and transmitted. The driving gear is connected to the drying drive member, and the driven gear is connected to the air collecting pipe 32. Power transmission is achieved through gear transmission, which is reliable and stable.

[0059] like Figure 1 As shown, in a possible embodiment, along the X-axis direction, the storage module 10, the heating module 20, the shaking module 60 and the drying module 30 are arranged in sequence to conform to the reaction process, shorten the moving path of the driving module 40, improve the overall efficiency, and facilitate precise control. Further, along the X-axis direction, the shaking module 60 overlaps with the capping module 70, and along the Y-axis direction, the shaking module 60 and the capping module 70 are arranged at intervals to reduce the size along the X-axis, so as to facilitate shaking after the capping, and avoid liquid splashing during shaking. Further, along the Z-axis direction, the driving module 40 is located above the storage module 10, the heating module 20, the shaking module 60, the capping module 70 and the drying module 30, so as to facilitate circulation in each module.

[0060] like Figure 1 As shown, in a specific embodiment, the hydrothermal synthesis workstation 100 also includes a shell 80, and the shell 80 is configured with an installation space, and the material storage module 10, the heating module 20, the shaking module 60, the capping module 70, the drying module 30 and the driving module 40 are all located in the installation space.

[0061] In a specific embodiment, the hydrothermal synthesis workstation 100 further includes a fan, which is installed at the bottom of the heating module 20 and the drying module 30 to dissipate heat for the drying drive components in the heating module 20 and the drying module 30 and extend their service life.

[0062] like Figure 1As shown, in a specific embodiment, an interface 81 is installed on the shell 80 to facilitate external power supply, and a start-stop switch 82 is also provided on the shell 80 to control the start and stop of the entire hydrothermal synthesis workstation 100.

[0063] In the present application, the hydrothermal synthesis workstation 100 includes a controller, which is connected to a fan, an air pressure regulating valve, and various modules to control the smooth progress of the entire workflow. The specific control content is a technology well known to those skilled in the art, so it will not be repeated here.

[0064] The technical features of the above-described embodiments may be arbitrarily combined. To make the description concise, not all possible combinations of the technical features in the above-described embodiments are described. However, as long as there is no contradiction in the combination of these technical features, they should be considered to be within the scope of this specification.

[0065] The above-described embodiments only express several implementation methods of the present application, and the descriptions thereof are relatively specific and detailed, but they cannot be understood as limiting the scope of the patent application. It should be pointed out that, for a person of ordinary skill in the art, several variations and improvements can be made without departing from the concept of the present application, and these all belong to the protection scope of the present application. Therefore, the scope of patent protection of the present application shall be subject to the attached claims.

Claims

1. A hydrothermal synthesis workstation, characterized in that: include: A material storage module (10) having a material storage station for storing reagent bottles (11); A heating module (20), used for heating the reagent bottle (11); The drying module (30) comprises a plurality of gas pipes (31) and a gas collecting pipe (32), wherein the plurality of gas pipes (31) are arranged at intervals along the axial direction of the gas collecting pipe (32), each of the gas pipes (31) is connected to the gas collecting pipe (32), and the gas collecting pipe (32) can rotate around its own axis to drive the pipe opening of the gas pipe (31) toward the reagent bottle (11), and the gas pipe (31) can blow dry gas into the heated reagent bottle (11); A driving module (40) comprising an X-axis moving guide rail (41), a Y-axis moving guide rail (42) and a Z-axis moving guide rail (43) which are connected in sequence; An operating module is connected to the Z-axis movable guide rail (43). The operating module can be moved between the material storage module (10), the heating module (20) and the drying module (30) under the action of the driving module (40). The operating module is used to clamp the reagent bottle (11) and take or put the raw material in the reagent bottle (11).

2. The hydrothermal synthesis workstation according to claim 1, characterized in that: The drying module (30) further comprises a drying drive member and a drying transmission assembly, wherein the drying transmission assembly is connected between the drying drive member and the air collecting pipe (32), and the drying transmission assembly drives the air collecting pipe (32) to rotate under the action of the drying drive member.

3. The hydrothermal synthesis workstation according to claim 2, characterized in that: The drying transmission assembly comprises a driving gear and a driven gear, which are meshed and transmitted, the driving gear is connected to the drying drive member, and the driven gear is connected to the air collecting pipe (32).

4. The hydrothermal synthesis workstation according to claim 1, characterized in that: The hydrothermal synthesis workstation further comprises a shaking module (60), wherein the shaking module (60) has a shaking station for placing the reagent bottle (11), and the shaking module (60) can drive the reagent bottle (11) to shake.

5. The hydrothermal synthesis workstation according to claim 4, characterized in that: The shaking module (60) further comprises a shaking driving member (61), a shaking transmission mechanism (62) and a shaking table (63); the shaking transmission mechanism (62) is connected between the shaking driving member (61) and the shaking table (63); the shaking transmission mechanism (62) drives the shaking table (63) to shake under the action of the shaking driving member (61); and the shaking table (63) is constructed with a plurality of shaking stations arranged at intervals.

6. The hydrothermal synthesis workstation according to claim 5, characterized in that: The shaking transmission mechanism (62) comprises a shaking transmission assembly (621), a first transmission belt and a plurality of transmission shafts (622); the plurality of transmission shafts (622) are circumferentially arranged around the axis of the shaking platform (63) and connected to the shaking platform (63); the first transmission belt is tensioned between the plurality of transmission shafts (622); the transmission shafts (622) are also connected to the shaking transmission assembly (621); the shaking transmission assembly (621) is connected to the shaking driving member (61) and can drive the plurality of transmission shafts (622) to rotate; Wherein, each of the transmission shafts (622) comprises a first shaft section (6221) and a second shaft section (6222), the first shaft section (6221) and the second shaft section (6222) are connected and eccentrically arranged, the first shaft section (6221) is connected to the shaking transmission assembly (621), and the second shaft section (6222) is connected to the shaking table (63).

7. The hydrothermal synthesis workstation according to claim 6, characterized in that: The vibration transmission assembly (621) includes a driving pulley (6211), a driven pulley (6212) and a second transmission belt (6213), wherein the driving pulley (6211) is connected to the vibration drive member (61), the second transmission belt (6213) is tensioned between the driving pulley (6211) and the driven pulley (6212), and the driven pulley (6212) is in transmission connection with one of the transmission shafts (622).

8. The hydrothermal synthesis workstation according to claim 1, characterized in that: The reagent bottle (11) comprises a bottle body and a cover body, and the hydrothermal synthesis workstation further comprises a capping module (70); The capping module (70) comprises a second gripping clamp (71), the second gripping clamp (71) is used to clamp the bottle body and cooperate with the operating module to clamp the cap body and rotate relative to the bottle body; or, the capping module (70) comprises a second gripping clamp (71) and a third gripping clamp arranged at intervals, the second gripping clamp (71) is used to clamp the bottle body, and the third gripping clamp is used to clamp the cap body and rotate relative to the bottle body.

9. The hydrothermal synthesis workstation according to any one of claims 1 to 8, characterized in that: The operation module comprises a first gripper (51), the first gripper (51) being at least used to grip the reagent bottle (11); and / or the operation module comprises a pipette (52), the pipette (52) being used to absorb raw materials in the reagent bottle (11) or to add raw materials to the reagent bottle (11).

10. The hydrothermal synthesis workstation according to any one of claims 1 to 8, characterized in that: The Z-axis moving guide rail (43) further comprises a chain (432) and a Z-axis driver (431); the Z-axis driver (431) is connected to and drives the operating module to move along the Z-axis; one end of the chain (432) is connected to the Z-axis driver (431), and the other end is connected to the end of the operating module away from the storage module (10) along the Z-axis direction; The chain (432) has a wiring space along its own axis, and the circuit of the operating module passes through the wiring space and is electrically connected to the Z-axis driver (431).

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