Reaction kettle for preparing high-purity cobalt sulfate crystals
By introducing structures such as transfer plates, stirring rods, mounting frames and cleaning rings into the reaction kettle for high-purity cobalt sulfate crystallization preparation, the problems of low reaction efficiency and clogged centrifugal barrels are solved, and more efficient material mixing and in-kettle cleaning are achieved , extends the service life of the equipment.
Patent Information
- Application Number
- CN202421132697.3
- Authority / Receiving Office
- CN · China
- Patent Type
- Utility models(China)
- Current Assignee / Owner
- Filing Date
- 2024-05-23
- Publication Date
- 2025-01-07
- Estimated Expiration
- 2034-05-23
AI Technical Summary
During use, the existing high-purity cobalt sulfate crystal preparation reactor has low reaction efficiency and crystals are easily retained on the wall of the centrifugal cylinder, which leads to difficulty in cleaning and affects subsequent use.
A reactor including a tank body, an evaporation tank, a coolant joint, a centrifugal filter cartridge, a rotary plate, a stirring rod, a reciprocating screw, a mounting frame, a cleaning ring and a strike rod were designed, and the rotation plate and a stirring rod were synchronized. Rotate and reciprocating to achieve full mixing and stirring of materials, and move the mounting frame and cleaning ring to clean the centrifugal filter cartridge to ensure that the materials in the kettle react fully and prevent clogging.
Improve reaction efficiency, ensure the cleaning of the centrifugal filter cartridge, avoid blockage, and extend the service life of the equipment.
Smart Images
Figure CN222305814U_ABST
Abstract
Description
Technical Field
[0001] The utility model relates to the technical field related to the preparation of cobalt sulfate crystals, in particular to a reaction kettle for the preparation of high-purity cobalt sulfate crystals. Background Art
[0002] Cobalt sulfate crystals are usually produced by chemically reacting or heating cobalt metal to produce cobalt oxide, then reacting the cobalt oxide with sulfuric acid to produce a cobalt sulfate solution, and then evaporating and concentrating the resulting solution, cooling and crystallizing it, and centrifuging and dehydrating it to finally obtain cobalt sulfate. The chemical reactions are all completed in a reactor, so a reactor for preparing high-purity cobalt sulfate crystals is used;
[0003] In a reactor for preparing cobalt sulfate based on a continuous process disclosed in publication number CN218307969U, various raw materials are sequentially fed into a plurality of reaction tanks through a feed port in a certain proportion. After the various raw materials are fully reacted in the reaction tanks, the obtained cobalt sulfate solution is fed into a group of evaporation tanks through a pipeline. The evaporation tank heats and evaporates the cobalt sulfate solution, and the steam enters the reaction chamber through the pipeline to increase the temperature in the reaction chamber and accelerate the reaction speed. When the air pressure in the reaction chamber is too high, the gas with a lower temperature is discharged from the exhaust port on the side wall at the bottom of the reaction chamber. When the cobalt sulfate solution in the evaporation tank reaches saturation, the evaporation tank stops heating, and the coolant is transported to the cooling pipeline through the cooling interface to reduce the temperature of the cobalt sulfate solution. As the temperature of the cobalt sulfate solution decreases, the solubility of cobalt sulfate decreases, and part of the cobalt sulfate condenses into solid crystals and precipitates. The precipitated crystals and the remaining cobalt sulfate solution are transported to the centrifugal barrel through a pipeline. Since there is a through hole at the bottom of the centrifugal barrel, the cobalt sulfate solution enters the filter barrel through the through hole, and the cobalt sulfate crystals remain in the centrifugal barrel. The motor is started to drive the centrifugal barrel to rotate for centrifugal dehydration to obtain the required cobalt sulfate, which is then taken out from the material taking door. The splash plate prevents liquid splashing during the centrifugation process. The cobalt sulfate solution in the filter barrel is input into another set of evaporation tanks through a pipeline to continue evaporation and concentration. The extraction rate can be improved by cross-evaporating and concentrating the cobalt sulfate solutions in the two sets of evaporation tanks.
[0004] However, the above scheme still has the following problems during use: when in use, after the reaction materials are placed in a reactor, a cobalt sulfate solution is obtained by self-reaction, and the reaction efficiency is low. After sufficient reaction in the reactor, the obtained cobalt sulfate solution is input into a group of evaporation tanks through pipelines. The evaporation tank heats and evaporates the cobalt sulfate solution, and the centrifugal barrel rotates for centrifugal dehydration to obtain the required cobalt sulfate. During the use of the centrifugal barrel, crystals will remain on the barrel wall. In order to facilitate subsequent use, the centrifugal barrel needs to be cleaned and prevented from being blocked.
[0005] Therefore, we proposed a reaction kettle for preparing high-purity cobalt sulfate crystals in order to solve the above-mentioned problems. Utility Model Content
[0006] The utility model aims to provide a reactor for preparing high-purity cobalt sulfate crystals, so as to solve the problem that the reactor for preparing high-purity cobalt sulfate crystals currently available on the market proposed in the above background technology, when in use, after the reaction materials are placed in the reactor, a cobalt sulfate solution is obtained by self-reaction, and the reaction efficiency is low. After sufficient reaction in the reactor, the obtained cobalt sulfate solution is input into a group of evaporation tanks through pipelines, the evaporation tanks heat and evaporate the cobalt sulfate solution, and the centrifugal barrels rotate to perform centrifugal dehydration to obtain the required cobalt sulfate. During the use of the centrifugal barrel, crystals will remain on the barrel wall. In order to facilitate subsequent use, the centrifugal barrel needs to be cleaned and prevented from blocking.
[0007] To achieve the above-mentioned purpose, the utility model provides the following technical solutions: a reaction kettle for preparing high-purity cobalt sulfate crystals, comprising a tank body, wherein a feed port is symmetrically arranged on the top of the tank body, a partition is installed in the middle of the inner side of the tank body, and an evaporation tank and a coolant joint are symmetrically installed on the inner walls on both sides of the inner side of the tank body and on both sides of the outer side, and a centrifugal filter cartridge is installed on the bottom bearing of the inner side of the tank body;
[0008] The top of the evaporation tank is connected to the upper space of the tank body through a connecting pipe, and the bottom of the tank body is connected to the top of the centrifugal filter cartridge through a connecting pipe;
[0009] The invention also includes: a first motor is installed on the top of the tank body, and an output end of the first motor is connected to a shaft rod, and the shaft rod passes through a bearing and is connected to the inner middle part of the tank body, and a rotating plate is fixed on the outer side of the top of the shaft rod, and a stirring rod is slidably connected to the rotating plate at an equal angle;
[0010] A reciprocating screw is integrally installed at the bottom of the shaft rod, and a mounting frame is threadedly connected to the outer side of the reciprocating screw rod, and a cleaning ring is fixed to the bottom of the mounting frame, and the cleaning ring is sleeved on the outer side of the centrifugal filter cylinder. At the same time, the bottom of the centrifugal filter cylinder is connected to the output end of the second motor, and the second motor is installed at the inner bottom of the tank body.
[0011] Preferably, the shaft drives the rotating plate to form a synchronous rotation structure, and the rotating plate is arranged as a flower-shaped structure, and the stirring rod on the rotating plate is arranged as a rectangular structure, and stirring blades are arranged at the bottom of the stirring rod, and a first spring is installed between the stirring rod and the rotating plate.
[0012] Preferably, the top of the stirring rod intermittently misaligns and conflicts with the protrusion, and the protrusion is set to a hemispherical structure, and the protrusion is installed at an equal angle on the inner top of the tank body, and the stirring rod forms a vertical sliding structure through the first spring and the protrusion.
[0013] Preferably, a lever is hinged at an equal angle on the inner top of the tank body, and a first torsion spring is installed at the hinge between the lever and the tank body, and the outer side of the lever abuts against the edge of the rotating plate, and the lever forms an opening and closing rotating structure through the rotating plate and the first torsion spring.
[0014] Preferably, the mounting frame is configured as an inverted "U"-shaped structure, and the top of the mounting frame is slidably connected to the outside of the limiting rod, and the limiting rod is symmetrically installed on the bottom of the partition, and the first magnetic blocks are evenly spaced on the outside of the limiting rod.
[0015] Preferably, the mounting frame drives the cleaning ring to form an up and down moving structure, and a knocking rod is symmetrically hinged on the outer side of the cleaning ring, and a second torsion spring is installed at the hinge between the knocking rod and the cleaning ring, and a pull rope is installed at the hinge of the knocking rod.
[0016] Preferably, the top of the pull rope is connected to the second magnetic block, and the second magnetic block is slidably connected to both sides of the mounting frame through a second spring, and the magnetic poles of the second magnetic block are opposite to those of the first magnetic block, and the knocking rod forms a rotating knocking structure through the second torsion spring, the first magnetic block and the second magnetic block.
[0017] Compared with the prior art, the reactor for preparing high-purity cobalt sulfate crystals of the utility model has the following beneficial effects: when in use, the reactants can be fully mixed and stirred, thereby improving the reaction effect, and the centrifugal filter cartridge can be cleaned and prevented from being blocked, thereby avoiding affecting the subsequent continuous use. The specific contents are as follows:
[0018] 1. Through the arrangement of the rotating plate and the stirring rod, the materials can be fully contacted by circumferential rotation and up and down sliding, thereby improving the reaction efficiency. After the rotating plate rotates, the stirring plate is driven to rotate, and the stirring rod intermittently contacts the protrusion during rotation, thereby compressing the first spring and moving downward. After being dislocated with the protrusion, the first spring drives the stirring rod to move upward and reset, thereby making the stirring rod move up and down, further improving the mixing effect of the materials;
[0019] Furthermore, when the rotating plate rotates, its outer side will intermittently push the lever, causing the lever to rotate, thereby reversing the first torsion spring, and causing the lever to open and close and swing, thereby further improving the full reaction efficiency of the material;
[0020] 2. Through the setting of the mounting frame and the cleaning ring, some residual materials on the centrifugal filter cartridge can be cleaned. After the reciprocating screw rotates, it will drive the mounting frame to move up and down on the limit rod. After the mounting frame moves, it will drive the cleaning ring at the bottom to move synchronously, thereby cleaning the centrifugal filter cartridge to prevent blockage and affect subsequent use;
[0021] 3. Through the setting of the knocking rod, the cleaning ring can clean itself while cleaning the centrifugal filter cartridge, thereby maintaining the cleaning effect of the cleaning ring;
[0022] Furthermore, when the mounting frame moves, the second magnetic block intermittently adsorbs with the first magnetic block, and the second magnetic block compresses the second spring to slide. After the second magnetic block slides, it will pull the pull rope, and the pull rope will drive the knocking rod to rotate, thereby reversing the second torsion spring. When the first magnetic block and the second magnetic block are misaligned, the second spring drives the second magnetic block to reset, and the pull rope is relaxed. The second torsion spring will drive the knocking rod to rotate, thereby hitting the cleaning ring, causing it to vibrate, and then shaking off its own cleaning residues, thereby achieving a self-cleaning effect. BRIEF DESCRIPTION OF THE DRAWINGS
[0023] Figure 1 This is a schematic diagram of the overall front section structure of the utility model;
[0024] Figure 2 For this utility model Figure 1 The enlarged structural diagram at A in the middle;
[0025] Figure 3 This is a schematic diagram of the three-dimensional structure of the connection between the rotating plate, the shaft rod and the stirring rod of the utility model;
[0026] Figure 4 For this utility model Figure 1 The enlarged structural diagram at B in the middle;
[0027] Figure 5 This is a schematic diagram of the three-dimensional structure of the mounting frame, cleaning ring, limit rod and reciprocating screw rod of the utility model;
[0028] Figure 6 For this utility model Figure 1 The enlarged structural diagram at C in the middle;
[0029] Figure 7 It is a schematic diagram of the three-dimensional structure of the knocking rod, the pull rope and the second torsion spring connected in the utility model.
[0030] In the figure: 1. tank body; 2. feed port; 3. first motor; 4. shaft; 5. partition; 6. rotating plate; 7. stirring rod; 8. first spring; 9. lever; 10. first torsion spring; 11. evaporation tank; 12. centrifugal filter cartridge; 13. coolant connector; 14. second motor; 15. reciprocating screw; 16. mounting bracket; 17. cleaning ring; 18. limit rod; 19. first magnetic block; 20. knocking rod; 21. second torsion spring; 22. pull rope; 23. second magnetic block; 24. second spring; 25. bump. DETAILED DESCRIPTION
[0031] The following will be combined with the drawings in the embodiments of the utility model to clearly and completely describe the technical solutions in the embodiments of the utility model. Obviously, the described embodiments are only part of the embodiments of the utility model, not all of the embodiments. Based on the embodiments in the utility model, all other embodiments obtained by ordinary technicians in this field without creative work are within the scope of protection of the utility model.
[0032] Example 1: In order to improve the reaction efficiency of materials during the use of the reactor, the following solution is proposed. Please refer to Figure 1-Figure 3 As shown,
[0033] The invention comprises a tank body 1, and a feed port 2 is symmetrically arranged on the top of the tank body 1, and a partition 5 is installed in the middle of the inner side of the tank body 1, and an evaporation tank 11 and a coolant joint 13 are symmetrically installed on the inner walls on both sides of the inner side of the middle part of the tank body 1 and on both sides of the outer side, and a centrifugal filter cartridge 12 is installed on the bottom bearing of the inner side of the middle part of the tank body 1, and the top of the evaporation tank 11 is communicated with the upper space of the tank body 1 through a connecting pipe, and the bottom of the tank body 1 is communicated with the top of the centrifugal filter cartridge 12 through a connecting pipe. First, the process of preparing crystals is briefly introduced, and the required reactants are put into the interior of the tank body 1 through the feed port 2, and the interior of the tank body 1 is divided into two upper and lower spaces on the partition 5. After the materials are fully reacted, the obtained cobalt sulfate solution is input into a group of evaporation tanks 11 through the connecting pipe, and the evaporation tank 11 heats and evaporates the cobalt sulfate solution. When the cobalt sulfate solution in the evaporation tank 11 reaches saturation, the evaporation tank 11 stops heating, and the coolant is transported to the cooling pipeline through the coolant joint 13 to reduce the temperature of the cobalt sulfate solution. As the temperature of the cobalt sulfate solution decreases, the solubility of the cobalt sulfate decreases, and part of the cobalt sulfate condenses into solid crystals and precipitates; the precipitated crystals and the remaining cobalt sulfate solution are transported to the centrifugal filter drum 12 through the connecting pipe, and the second motor 14 is started, and the second motor 14 drives the centrifugal filter drum 12 to rotate for centrifugal dehydration to obtain the required cobalt sulfate;
[0034] Please refer to Figure 1-Figure 3As shown, a first motor 3 is installed on the top of the tank body 1, and the output end of the first motor 3 is connected to a shaft rod 4, and the shaft rod 4 passes through a bearing and is connected to the inner middle part of the tank body 1, and a rotating plate 6 is fixed to the top outer side of the shaft rod 4, and a stirring rod 7 is slidably connected to the rotating plate 6 at an equal angle, and the shaft rod 4 drives the rotating plate 6 to form a synchronous rotation structure, and the rotating plate 6 is set to a flower-shaped structure, and the stirring rod 7 on the rotating plate 6 is set to a rectangular structure, and a stirring blade is set at the bottom of the stirring rod 7, and a first spring 8 is installed between the stirring rod 7 and the rotating plate 6, and the top of the stirring rod 7 intermittently misaligns and conflicts with the protrusion 25, and the protrusion 25 is set to a hemispherical structure, and The protrusion 25 is installed at an equal angle on the inner top of the tank body 1, and the stirring rod 7 forms a vertical sliding structure through the first spring 8 and the protrusion 25. When the material reacts, the first motor 3 on the tank body 1 is started, and the first motor 3 will drive the shaft rod 4 to rotate. After the shaft rod 4 rotates, it will drive the rotating plate 6 to rotate synchronously. After the rotating plate 6 rotates, it will drive the stirring rod 7 to rotate synchronously. When the stirring rod 7 rotates, its top will intermittently conflict with the protrusion 25, thereby compressing the first spring 8 and moving downward. After being misaligned with the protrusion 25, the first spring 8 will drive the stirring rod 7 to move up and reset, so that the stirring rod 7 moves up and down, further improving the mixing effect of the material;
[0035] Please refer to Figure 1-Figure 3 As shown, a lever 9 is hinged at an equal angle on the inner top of the tank body 1, and a first torsion spring 10 is installed at the hinge between the lever 9 and the tank body 1, and the outer side of the lever 9 is in conflict with the edge of the rotating plate 6, and the lever 9 forms an opening and closing rotating structure through the rotating plate 6 and the first torsion spring 10. When the rotating plate 6 rotates, its outer side will intermittently push the lever 9 to rotate, thereby reversing the first torsion spring 10, and then causing the lever 9 to swing open and close, thereby further improving the full reaction efficiency of the material.
[0036] Example 2: In order to prevent the centrifugal filter cartridge 12 from being blocked during the crystallization of cobalt sulfate, the following solution is proposed. Figure 1 and Figure 4-Figure 5 As shown,
[0037] A reciprocating screw 15 is integrally mounted on the bottom of the shaft 4, and a mounting bracket 16 is threadedly connected to the outer side of the reciprocating screw 15, and a cleaning ring 17 is fixed to the bottom of the mounting bracket 16, and the cleaning ring 17 is sleeved on the outer side of the centrifugal filter cartridge 12. At the same time, the bottom of the centrifugal filter cartridge 12 is connected to the output end of the second motor 14, and the second motor 14 is mounted on the inner bottom of the tank body 1. The mounting bracket 16 is set to an inverted "U"-shaped structure, and the top of the mounting bracket 16 is slidably connected to the outer side of the limit rod 18, and the limit rod 18 is It is installed at the bottom of the partition 5, and the first magnetic block 19 is installed at equal intervals on the outside of the limit rod 18. When the centrifugal filter cartridge 12 processes the material, part of the material will remain in the centrifugal filter cartridge 12, and the shaft rod 4 will drive the reciprocating screw rod 15 at the bottom to rotate synchronously after the rotation of the shaft rod 4. After the reciprocating screw rod 15 rotates, it will drive the mounting frame 16 to move up and down on the limit rod 18. After the mounting frame 16 moves, it will drive the cleaning ring 17 at the bottom to move synchronously, thereby cleaning the centrifugal filter cartridge 12 to prevent blockage and affect subsequent use;
[0038] Embodiment 3: In order to maintain the cleaning effect of the cleaning ring 17, self-cleaning is required, so the following solution is proposed. Please refer to Figure 1 , Figure 4 and Figure 6-Figure 7 As shown,
[0039] The mounting frame 16 drives the cleaning ring 17 to form an up-and-down moving structure, and the outer side of the cleaning ring 17 is symmetrically hinged with a knocking rod 20, and a second torsion spring 21 is installed at the hinge of the knocking rod 20 and the cleaning ring 17, and a pull rope 22 is installed at the hinge of the knocking rod 20, and the top of the pull rope 22 is connected to the second magnetic block 23, and the second magnetic block 23 is slidably connected to both sides of the mounting frame 16 through the second spring 24, and the second magnetic block 23 is opposite to the magnetic pole of the first magnetic block 19, and the knocking rod 20 forms a rotating knocking structure through the second torsion spring 21, the first magnetic block 19 and the second magnetic block 23. When the mounting frame 16 moves, the second magnetic block 23 will It intermittently adsorbs with the first magnetic block 19, so that the second magnetic block 23 compresses the second spring 24 and slides. After the second magnetic block 23 slides, it will pull the pull rope 22, and the pull rope 22 will drive the knocking rod 20 to rotate, thereby reversing the second torsion spring 21. When the first magnetic block 19 and the second magnetic block 23 are misaligned, the second spring 24 drives the second magnetic block 23 to reset, and the pull rope 22 is relaxed. The second torsion spring 21 will drive the knocking rod 20 to rotate, thereby hitting the cleaning ring 17, causing it to vibrate, and then shake off its own cleaning residues, thereby achieving a self-cleaning effect and maintaining the cleaning effect of the cleaning ring 17.
[0040] The contents not described in detail in this specification belong to the prior art known to professional and technical personnel in this field.
[0041] Although the present invention has been described in detail with reference to the aforementioned embodiments, those skilled in the art may still modify the technical solutions described in the aforementioned embodiments, or make equivalent substitutions for some of the technical features therein. Any modifications, equivalent substitutions, improvements, etc. made within the spirit and principles of the present invention shall be included in the protection scope of the present invention.
Claims
1. A reaction kettle for preparing high-purity cobalt sulfate crystals, comprising a tank body (1), wherein a feed port (2) is symmetrically arranged on the top of the tank body (1), a partition (5) is installed in the middle of the inner side of the tank body (1), and an evaporation tank (11) and a coolant joint (13) are symmetrically installed on the inner walls on both sides of the inner side of the tank body (1) and on both sides of the outer side, and a centrifugal filter cartridge (12) is installed on the bottom bearing of the inner side of the tank body (1); The top of the evaporation tank (11) is connected to the upper space of the tank body (1) through a connecting pipe, and the bottom of the tank body (1) is connected to the top of the centrifugal filter cartridge (12) through a connecting pipe; Features: Also includes: A first motor (3) is installed on the top of the tank body (1), and the output end of the first motor (3) is connected to a shaft (4), and the shaft (4) passes through a bearing and is connected to the inner middle part of the tank body (1), and a rotating plate (6) is fixed to the outer side of the top of the shaft (4), and a stirring rod (7) is slidably connected to the rotating plate (6) at an equal angle; A reciprocating screw (15) is integrally mounted on the bottom of the shaft (4), and a mounting frame (16) is threadedly connected to the outer side of the reciprocating screw (15), and a cleaning ring (17) is fixed to the bottom of the mounting frame (16), and the cleaning ring (17) is sleeved on the outer side of the centrifugal filter cartridge (12), and the bottom of the centrifugal filter cartridge (12) is connected to the output end of the second motor (14), and the second motor (14) is mounted on the inner bottom of the tank body (1).
2. A reaction kettle for preparing high-purity cobalt sulfate crystals according to claim 1, characterized in that: The shaft (4) drives the rotating plate (6) to form a synchronous rotation structure, and the rotating plate (6) is arranged in a flower-shaped structure, and the stirring rod (7) on the rotating plate (6) is arranged in a rectangular structure, and stirring blades are arranged at the bottom of the stirring rod (7), and a first spring (8) is installed between the stirring rod (7) and the rotating plate (6).
3. A reaction kettle for preparing high-purity cobalt sulfate crystals according to claim 2, characterized in that: The top of the stirring rod (7) intermittently displaces and contacts the protrusion (25), and the protrusion (25) is set as a hemispherical structure. The protrusion (25) is installed at an equal angle on the inner top of the tank body (1), and the stirring rod (7) forms a vertical sliding structure through the first spring (8) and the protrusion (25).
4. The reaction kettle for preparing high-purity cobalt sulfate crystals according to claim 1, characterized in that: A lever (9) is hinged at an equal angle on the inner top of the tank body (1), and a first torsion spring (10) is installed at the hinge between the lever (9) and the tank body (1), and the outer side of the lever (9) contacts the edge of the rotating plate (6), and the lever (9) forms an opening and closing rotating structure through the rotating plate (6) and the first torsion spring (10).
5. A reaction kettle for preparing high-purity cobalt sulfate crystals according to claim 1, characterized in that: The mounting frame (16) is configured as an inverted "U"-shaped structure, and the top of the mounting frame (16) is slidably connected to the outside of the limiting rod (18), and the limiting rod (18) is symmetrically mounted on the bottom of the partition (5), and the first magnetic blocks (19) are evenly spaced and mounted on the outside of the limiting rod (18).
6. A reaction kettle for preparing high-purity cobalt sulfate crystals according to claim 1, characterized in that: The mounting frame (16) drives the cleaning ring (17) to form an up-and-down moving structure, and a knocking rod (20) is symmetrically hinged on the outer side of the cleaning ring (17), and a second torsion spring (21) is installed at the hinge between the knocking rod (20) and the cleaning ring (17), and a pull rope (22) is installed at the hinge of the knocking rod (20).
7. A reaction kettle for preparing high-purity cobalt sulfate crystals according to claim 6, characterized in that: The top of the pull rope (22) is connected to the second magnetic block (23), and the second magnetic block (23) is slidably connected to the two sides of the mounting frame (16) through the second spring (24), and the magnetic poles of the second magnetic block (23) and the first magnetic block (19) are opposite, and the knocking rod (20) forms a rotating knocking structure through the second torsion spring (21), the first magnetic block (19) and the second magnetic block (23).