Continuous glucose production device
By designing a continuous glucose production device and automatically controlling process parameters using pH adjustment components, the error problems caused by manual control of process parameters in the prior art are solved, efficient and stable glucose production is achieved, and product quality is improved.
Patent Information
- Application Number
- CN202421105484.1
- Authority / Receiving Office
- CN · China
- Patent Type
- Utility models(China)
- Current Assignee / Owner
- Filing Date
- 2024-05-20
- Publication Date
- 2025-03-11
- Estimated Expiration
- 2034-05-20
AI Technical Summary
In the prior art, in the acid hydrolyzed glucose production process, process parameters (such as material concentration, pH value, reaction temperature) are mainly controlled by the operator manually, resulting in large human errors, large fluctuations in the purity of the finished product, and high defect rate.
A continuous glucose production device is designed, including a reaction tank, a storage tank, an acid tank and a pH adjustment assembly. The pH adjustment assembly consists of a first metering pump, a second metering pump and a pH tester. The pH value in the reaction tank is monitored in real time through the pH tester, and the flow rate of the material and acid liquid is automatically adjusted through the metering pump to reduce human intervention.
By automatically controlling process parameters, artificial errors are reduced, the purity of finished products is improved, the defective rate is reduced, the product quality is improved, and the product quality is improved. It also has the advantages of high automation, simple operation and low implementation cost.
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Figure CN222593889U_ABST
Abstract
Description
Technical Field
[0001] The present application belongs to the technical field of glucose production, and specifically relates to a continuous glucose production device. Background Art
[0002] In the existing technology, glucose, as an important monosaccharide, is widely used in the food industry, pharmaceutical industry, biochemical industry and energy industry, and currently still has huge application potential.
[0003] In the prior art, the production methods of glucose mainly include enzymatic hydrolysis, acid hydrolysis and microbial fermentation. The enzymatic hydrolysis method is highly efficient, but has strict requirements on the reaction conditions. During mass production, the production cost increases significantly. The acid hydrolysis method is a mature process and is suitable for mass production.
[0004] In the prior art, the production of glucose by acid hydrolysis requires an independent hydrolysis pot. The operator generally operates manually and needs to adjust the concentration and pH of the material. The reaction temperature also needs to be manually controlled by the operator. The reaction endpoint is determined by iodine test color development. The error of human factors is relatively large, the purity of the product produced fluctuates greatly, and the defective rate is high. Improvements are urgently needed. Utility Model Content
[0005] In order to solve the technical problems in the prior art that in the acid hydrolysis glucose production process, process parameters such as material concentration, pH value, reaction temperature, etc. are often manually operated by operators and the degree of reaction is judged by the naked eye, resulting in large errors caused by human factors, large fluctuations in the purity of the finished product, and a high defective rate, a continuous glucose production device is proposed.
[0006] The present application adopts the following scheme, a glucose continuous production device, including a reaction tank, a storage tank arranged on the reaction tank, an acid liquid tank arranged on the reaction tank, and a pH adjustment component arranged between the reaction tank, the storage tank and the acid liquid tank. The pH adjustment component includes a first metering pump arranged between the reaction tank and the storage tank, a second metering pump arranged between the reaction tank and the acid liquid tank, and a pH tester arranged on the reaction tank for testing the pH value of the liquid in the reaction tank.
[0007] Furthermore, the material storage tank is provided with a first weight sensor for measuring the weight of the material liquid therein, and the acid liquid tank is provided with a second weight sensor for measuring the weight of the acid liquid therein.
[0008] Furthermore, the reaction tank is provided with a heat preservation component, and the heat preservation component includes a pressure tank provided on the reaction tank, and a heat exchange tower provided on the pressure tank.
[0009] Furthermore, the heat exchange tower is provided with heat exchange coils along its height direction, and the finished liquid after the reaction in the reaction tank is completed can be transported to the heat exchange tower after passing through the pressure tank and contact the outer surface of the heat exchange coils.
[0010] Furthermore, the reaction tank is also provided with an ejector, and when the feed liquid in the storage tank and the acid liquid in the acid liquid tank are transported to the reaction tank, the ejector is used to eject high-temperature steam to the acid liquid and the feed liquid.
[0011] Furthermore, a plurality of temperature sensors are arranged at intervals on the inner wall of the reaction tank along its height direction.
[0012] Furthermore, a flash tank is provided on the heat exchange tower, and the finished liquid in the pressure tank can be transported to the flash tank after passing through the heat exchange tower, and the flash tank is used to concentrate the finished liquid.
[0013] Furthermore, the flash tank is provided with an elution tower, and the elution tower is provided with an elution component along its height direction. The concentrated finished product liquid can be transported to the elution tower and eluted through the elution component.
[0014] Furthermore, the elution component includes a first activated carbon layer, a bentonite layer, and a second activated carbon layer stacked in sequence along the height direction of the elution tower, the thickness of the first activated carbon layer is greater than the thickness of the second activated carbon layer, and the particle size of the activated carbon in the first activated carbon layer is greater than the particle size of the activated carbon in the second activated carbon layer.
[0015] Compared with the prior art, this application has the following beneficial effects:
[0016] The present application provides a glucose continuous production device, comprising a reaction tank, a material storage tank arranged on the reaction tank, an acid liquid tank arranged on the reaction tank, and a pH adjustment component arranged among the reaction tank, the material storage tank and the acid liquid tank, wherein the pH adjustment component comprises a first metering pump located between the reaction tank and the material storage tank, a second metering pump located between the reaction tank and the acid liquid tank, and a pH tester located on the reaction tank, the pH tester is used to reflect the reaction degree in the reaction tank in real time, and the flow rates of the material liquid and the acid liquid transported into the reaction tank are adjusted by the first metering pump and the second metering pump respectively, without the need for manual control by an operator, and without the need for the operator to visually judge the reaction end point in the reaction tank through iodine test paper, thereby reducing human errors, reducing the purity fluctuation of the finished product, and improving product quality, and having the advantages of high degree of automation, efficient and simple operation, low implementation cost, and easy promotion and implementation. BRIEF DESCRIPTION OF THE DRAWINGS
[0017] In order to more clearly illustrate the technical solutions in the embodiments of the present application, the following briefly introduces the drawings required for describing the embodiments.
[0018] Figure 1 It is a structural schematic diagram of a glucose continuous production device of the present application.
[0019] Figure 2 This application Figure 1 A partial enlarged view of point A in the middle. DETAILED DESCRIPTION
[0020] Combined with Figure 1-2 As shown, the technical scheme is further described, a glucose continuous production device includes a reaction tank 1, a storage tank 2 arranged on the reaction tank 1, an acid liquid tank 3 arranged on the reaction tank 1, and a pH adjustment component 4 arranged between the reaction tank 1, the storage tank 2 and the acid liquid tank 3, the pH adjustment component 4 includes a first metering pump 40 arranged between the reaction tank 1 and the storage tank 2, a second metering pump 41 arranged between the reaction tank 1 and the acid liquid tank 3, and a pH tester 42 arranged on the reaction tank 1 for testing the pH value of the liquid in the reaction tank 1.
[0021] The present application provides a glucose continuous production device, comprising a reaction tank, a material storage tank arranged on the reaction tank, an acid liquid tank arranged on the reaction tank, and a pH adjustment component arranged among the reaction tank, the material storage tank and the acid liquid tank, wherein the pH adjustment component comprises a first metering pump located between the reaction tank and the material storage tank, a second metering pump located between the reaction tank and the acid liquid tank, and a pH tester located on the reaction tank, the pH tester is used to reflect the reaction degree in the reaction tank in real time, and the flow rates of the material liquid and the acid liquid transported into the reaction tank are adjusted by the first metering pump and the second metering pump respectively, without the need for manual control by an operator, and without the need for the operator to visually judge the reaction end point in the reaction tank through iodine test paper, thereby reducing human errors, reducing the purity fluctuation of the finished product, and improving product quality, and having the advantages of high degree of automation, efficient and simple operation, low implementation cost, and easy promotion and implementation.
[0022] During the implementation of this embodiment, the material storage tank 2 is provided with a first weight sensor for measuring the weight of the material liquid therein, and the acid liquid tank 3 is provided with a second weight sensor for measuring the weight of the acid liquid therein.
[0023] During the actual implementation process, the pH tester, the first metering pump and the second metering pump are proportionally controlled by PLC. When the pH value measured by the pH tester is higher than its preset value, the second metering pump starts and adds acid to the reaction tank, so that the pH value in the reaction tank is reduced to the preset value of the pH tester; when the pH value measured by the pH tester is lower than its preset value, the first metering pump starts and adds feed liquid to the reaction tank, so that the pH value in the reaction tank rises to the preset value of the pH tester; the first metering pump and the second metering pump can record the flow rate of feed liquid or acid liquid input into the reaction tank and the start and shutdown time, and then measure the replenishment amount of feed liquid and acid liquid, and then calibrate with the weight sensed by the first weight sensor and the second sensor, without the need for manual control by the operator, and without the need for the operator to judge the reaction end point in the reaction tank by naked eyes through iodine test paper, thereby reducing human errors, reducing the purity fluctuation of the finished product, and improving product quality. It has the advantages of high degree of automation, efficient and simple operation, low implementation cost, and easy promotion and implementation.
[0024] During the actual implementation process, the pH tester is also equipped with a buzzer. When the pH tester detects that the pH value is 10% higher than the preset value, the buzzer starts to ensure the reaction pH value of the reaction tank during the actual reaction process. There is no need for manual control by the operator, and there is no need for the operator to use iodine test paper to visually judge the reaction end point in the reaction tank. This reduces human errors, reduces fluctuations in the purity of finished products, and improves product quality. It has the advantages of high degree of automation, efficient and simple operation, low implementation cost, and is easy to promote and implement.
[0025] During the implementation of this embodiment, a heat preservation assembly 5 is provided on the reaction tank 1 , and the heat preservation assembly 5 includes a pressure tank 50 provided on the reaction tank 1 , and a heat exchange tower 51 provided on the pressure tank 50 .
[0026] During the implementation of this embodiment, a heat exchange coil 52 is provided in the heat exchange tower 51 along its height direction. The finished liquid after the reaction in the reaction tank 1 is completed can be transported to the heat exchange tower 51 after passing through the pressure tank 50 and contact the outer surface of the heat exchange coil 52.
[0027] During the implementation of this embodiment, the reaction tank 1 is further provided with an ejector 6. When the feed liquid in the storage tank 2 and the acid liquid in the acid liquid tank 3 are transported to the reaction tank 1, the ejector 6 is used to eject high-temperature steam to the acid liquid and the feed liquid.
[0028] In the actual implementation process, high-temperature steam is sprayed into the feed liquid and acid liquid through an ejector, which can instantly raise the temperature of both to the reaction temperature without the need for continuous heating, thereby improving heating efficiency and speeding up the production process. It has the advantages of easy operation and continuous production.
[0029] During the implementation of this embodiment, a plurality of temperature sensors are arranged at intervals on the inner wall of the reaction tank 1 along its height direction.
[0030] During the actual implementation process, a transparent window is protruding from the side wall of the reaction tank, and the transparent window allows the operator to observe the reaction conditions in the reaction tank.
[0031] During the implementation of this embodiment, a flash tank 7 is provided on the heat exchange tower 51. The finished liquid in the pressure tank 50 can be transported to the flash tank 7 after passing through the heat exchange tower 51. The flash tank 7 is used to concentrate the finished liquid.
[0032] In the actual implementation process, while the heat exchange tower is keeping the finished liquid in the pressure tank warm, the excess heat can be used in the flash tank to concentrate the finished liquid. By recovering heat energy and cooling the flash tank, continuous production can be achieved.
[0033] During the implementation of this embodiment, an elution tower 8 is provided on the flash tank 7, and an elution component 9 is provided inside the elution tower 8 along its height direction. The concentrated finished liquid can be transported to the elution tower 8 and eluted through the elution component 9.
[0034] During the implementation of this embodiment, the elution component 9 includes a first activated carbon layer 90, a bentonite layer 91, and a second activated carbon layer 92 stacked in sequence along the height direction of the elution tower 8. The thickness of the first activated carbon layer 90 is greater than the thickness of the second activated carbon layer 92, and the particle size of the activated carbon in the first activated carbon layer 90 is greater than the particle size of the activated carbon in the second activated carbon layer 92.
[0035] The present application provides a glucose continuous production device, comprising a reaction tank, a material storage tank arranged on the reaction tank, an acid liquid tank arranged on the reaction tank, and a pH adjustment component arranged among the reaction tank, the material storage tank and the acid liquid tank, wherein the pH adjustment component comprises a first metering pump located between the reaction tank and the material storage tank, a second metering pump located between the reaction tank and the acid liquid tank, and a pH tester located on the reaction tank, the pH tester is used to reflect the reaction degree in the reaction tank in real time, and the flow rates of the material liquid and the acid liquid transported into the reaction tank are adjusted by the first metering pump and the second metering pump respectively, without the need for manual control by an operator, and without the need for the operator to visually judge the reaction end point in the reaction tank through iodine test paper, thereby reducing human errors, reducing the purity fluctuation of the finished product, and improving product quality, and having the advantages of high degree of automation, efficient and simple operation, low implementation cost, and easy promotion and implementation.
[0036] The above are only embodiments of the present invention and are not intended to limit the present invention. Any modifications, equivalent substitutions and improvements made within the spirit and principles of the present invention should be included in the protection scope of the present invention.
Claims
1. A continuous glucose production device, characterized in that: The invention comprises a reaction tank (1), a material storage tank (2) arranged on the reaction tank (1), an acid liquid tank (3) arranged on the reaction tank (1), and a pH adjustment component (4) arranged between the reaction tank (1), the material storage tank (2) and the acid liquid tank (3), wherein the pH adjustment component (4) comprises a first metering pump (40) arranged between the reaction tank (1) and the material storage tank (2), a second metering pump (41) arranged between the reaction tank (1) and the acid liquid tank (3), and a pH tester (42) arranged on the reaction tank (1) for testing the pH value of the liquid in the reaction tank (1).
2. A glucose continuous production device according to claim 1, characterized in that: The material storage tank (2) is provided with a first weight sensor for measuring the weight of the material liquid therein, and the acid liquid tank (3) is provided with a second weight sensor for measuring the weight of the acid liquid therein.
3. A glucose continuous production device according to claim 1, characterized in that: The reaction tank (1) is provided with a heat-insulating assembly (5), wherein the heat-insulating assembly (5) comprises a pressure tank (50) provided on the reaction tank (1), and a heat exchange tower (51) provided on the pressure tank (50).
4. A glucose continuous production device according to claim 3, characterized in that: The heat exchange tower (51) is provided with a heat exchange coil (52) along its height direction. The finished liquid after the reaction in the reaction tank (1) is completed can be transported to the heat exchange tower (51) after passing through the pressure tank (50) and contact the outer surface of the heat exchange coil (52).
5. A glucose continuous production device according to claim 1, characterized in that: The reaction tank (1) is also provided with an ejector (6), and when the feed liquid in the storage tank (2) and the acid liquid in the acid liquid tank (3) are transported to the reaction tank (1), the ejector (6) is used to eject high-temperature steam toward the acid liquid and the feed liquid.
6. A glucose continuous production device according to claim 1, characterized in that: A plurality of temperature sensors are arranged at intervals on the inner wall of the reaction tank (1) along its height direction.
7. A glucose continuous production device according to claim 3, characterized in that: The heat exchange tower (51) is provided with a flash tank (7), and the finished liquid in the pressure tank (50) can be transported to the flash tank (7) after passing through the heat exchange tower (51). The flash tank (7) is used to concentrate the finished liquid.
8. A glucose continuous production device according to claim 7, characterized in that: The flash tank (7) is provided with an elution tower (8), and an elution component (9) is provided inside the elution tower (8) along its height direction. The concentrated finished product liquid can be transported to the elution tower (8) and eluted through the elution component (9).
9. A glucose continuous production device according to claim 8, characterized in that: The elution component (9) comprises a first activated carbon layer (90), a bentonite layer (91), and a second activated carbon layer (92) which are stacked in sequence along the height direction of the elution tower (8); the thickness of the first activated carbon layer (90) is greater than the thickness of the second activated carbon layer (92); and the particle size of the activated carbon in the first activated carbon layer (90) is greater than the particle size of the activated carbon in the second activated carbon layer (92).