Automatic fraction collecting device for rectifying tower

Abstract

The utility model relates to the technical field of rectifying towers, and provides an automatic fraction collecting device for a rectifying tower, which comprises a kettle body, a sealing cover component is arranged at the top of the kettle body, a rotating mechanism is arranged at the top of the sealing cover component, and a rotating output end of the rotating mechanism penetrates through the sealing cover component to the inside of the kettle body. The output end of the rotating mechanism is fixedly connected with a funnel type rotating disc, the funnel type rotating disc is arranged in an inclined opening shape, and through the arranged funnel type rotating disc, after the rotating mechanism is started, the funnel type rotating disc rotates and stops to a needed position; at the moment, the liquid inlet flange receives materials condensed in the previous reaction and flows into a specific collection bottle needing to enter through the funnel type rotating disc, the funnel type rotating disc is arranged to be in an inclined opening shape, the materials can be guided into one side, and material residues are prevented.

Description

TECHNICAL FIELD

[0001] The utility model relates to rectifying tower technical field, concretely relates to a kind of automatic fraction collection devices for rectifying tower. BACKGROUND

[0002] Rectifying tower fractionation uses gas-liquid equilibrium principle: based on the difference of volatility (or boiling point) of each component in mixture. In rectifying tower, when mixture is heated and vaporized, it enters tower, and gas-liquid contact is carried out on tray (or filler). The content of volatile component in gas phase is higher, and the content of difficult volatile component in liquid phase is higher. With the upward flow of gas phase, the downward flow of liquid phase, on each tray (or each section of filler), heat and mass exchange between gas and liquid phases are carried out, so that multiple partial vaporization and partial condensation are realized.

[0003] After searching, the existing patent (CN219399000U) discloses a chemical rectifying tower waste collecting device, which comprises a rectifying tower body, a support frame, a connecting pipe and a collecting and processing pipeline. The support frame is fixedly connected to the outer wall of the rectifying tower body. The bottom end of the rectifying tower body is fixedly connected to one end of the connecting pipe. The other end of the connecting pipe is fixedly connected to the collecting and processing pipeline. As a further scheme of the utility model, the collecting and processing pipeline comprises a pipeline body, a connecting hole, V-shaped grooves and a homogenizing device. The connecting hole is formed in the top end of the pipeline body. The V-shaped grooves are formed in the inner wall of the pipeline body. An opening is formed in the bottom end of the pipeline body. The homogenizing device is fixedly connected in the opening. As a further scheme of the utility model, the homogenizing device comprises a motor, a rotating shaft, stirring shafts and filter cotton. The output shaft of the motor is fixedly connected to one end of the rotating shaft. The other end of the rotating shaft is fixedly connected to one end of the stirring shaft. The stirring shafts are symmetrically arranged on the other end of the rotating shaft. Each stirring shaft is fixedly connected to filter cotton. As a further scheme of the utility model, the connecting pipe comprises a connecting pipe body, a fixed ring and an activated carbon filter element. The fixed ring is fixedly connected to the inner wall of the connecting pipe body. The activated carbon filter element is fixedly connected to the inner wall of the fixed ring. When the utility model is used, waste liquid generated by the rectifying tower enters the collecting and processing pipeline through the connecting pipe. The collecting and processing pipeline can filter and collect waste liquid. The collecting and processing pipeline can be installed with collecting pipeline at both ends to transport treated waste liquid.

[0004] However, in the above scheme, the collection still needs to be manually collected. However, the adaptability of manual collection is limited. For complex mixtures, especially for components with similar boiling points or long-term continuous fraction collection, manual operation is difficult to maintain high accuracy and stability, and human error is easy to occur, such as too long or too short collection time, resulting in low fraction purity.

[0005] Therefore, the utility model provides an automatic fraction collection device for rectifying tower. UTILITY MODEL CONTENT

[0006] The utility model provides a kind of automatic fraction collection device for rectifying column, solve the adaptability of manual collection in relevant technology is limited.For complex mixture, especially there are multiple components with similar boiling points or need long time continuous collection fraction, manual operation is difficult to maintain high accuracy and stability, prone to human error, such as collection time is too long or too short, leading to fraction purity is not high.

[0007] The technical scheme of the utility model is as follows: an automatic fraction collection device for rectifying column, including kettle body: the top of the kettle body is provided with a cover assembly, the top of the cover assembly is provided with a rotating mechanism, the rotating output end of the rotating mechanism penetrates the cover assembly to the inside of the kettle body, the output end of the rotating mechanism is fixedly connected with a funnel type rotary disc, the funnel type rotary disc is provided in an oblique mouth shape, the center position of the inside bottom surface of the kettle body is fixedly connected with a liquid separation mechanism one, the outside of the liquid separation mechanism one is fixedly connected with a liquid separation mechanism two, the number of the liquid separation mechanism two is provided with multiple, the liquid separation mechanism two and the liquid separation mechanism one are fixedly attached with the inner wall of the kettle body, the bottom of the kettle body is fixedly connected with an output pipeline, the bottom of the output pipeline is provided with a collection bottle, a flange connection assembly is arranged between the output pipeline and the collection bottle, the output pipeline is communicated with the inside of the kettle body, the bottom of the output pipeline is communicated with the inside of the collection bottle, the position of the output pipeline communicated with the inside of the kettle body is located between the two liquid separation mechanism two, the funnel type rotary disc is rotated after the rotating mechanism is started, and stops at the required position, at this time, the liquid flange receives the material condensed from the previous reaction and flows into the specific collection bottle required through the funnel type rotary disc, the funnel type rotary disc is provided in an oblique mouth shape to guide the material to one side, to prevent material residue.

[0008] Preferably, the liquid separation mechanism two is radially distributed outside the liquid separation mechanism one, and the liquid separation mechanism two is away from the funnel type rotary disc.

[0009] Preferably, the cover assembly includes a kettle cover, an upper flange one, a lower flange one and a bolt two, an annular notch is formed in the edge of the top of the kettle cover, the upper flange one is snap-connected inside the annular notch, the lower flange one is fixedly connected to the top of the kettle body, and the bolt two is threadedly connected inside the upper flange one and the lower flange one, so that the kettle cover and the kettle body can be fixed by the upper flange one and the lower flange one.

[0010] Preferably, the bolt two is equidistantly distributed inside the upper flange one and the lower flange one, and the top of the bolt two is limited above the upper flange one.

[0011] Preferably, the rotating mechanism comprises a stepping motor, a shaft coupling, a rotating shaft, a mechanical seal assembly and a support rod, the top of the kettle cover is fixedly connected with the support rod, the top of the support rod is fixedly connected with the stepping motor, the output end of the stepping motor is fixedly connected with the shaft coupling, the other end of the shaft coupling is fixedly connected with the rotating shaft, the rotating shaft penetrates the kettle cover and the mechanical seal assembly, and the rotating shaft can be driven to rotate by starting the stepping motor, so that the rotation of the funnel type rotating disc can be realized.

[0012] Preferably, the mechanical seal assembly is fixed at the central position of the top of the kettle cover, and the rotating shaft penetrates the central position in the inside of the mechanical seal assembly, and the rotating shaft rotates in the inside of the kettle cover and the mechanical seal assembly.

[0013] Preferably, the flange connecting assembly comprises an upper flange two, a bolt one and a lower flange two, the upper flange two is fixed to the bottom of the output pipeline, the inside of the upper flange two is provided with the bolt one penetratingly, the outside of the collecting port is fixedly connected with the lower flange two, and the bolt one penetrates the inside of the upper flange two and is in threaded connection with the lower flange two, so that the kettle body and the collecting bottle can be fixed through the upper flange two and the lower flange two.

[0014] Preferably, the kettle body and the collecting bottle are both made of glass.

[0015] The kettle body and the collecting bottle are both made of glass.

[0016] 1. In the utility model, the funnel type rotating disc is set, rotates after the rotating mechanism is started, stops at the required position, at the moment, the liquid inlet flange receives the material condensed from the previous reaction and flows into the required specific collecting bottle through the funnel type rotating disc, the funnel type rotating disc is in the shape of a bevel, can guide the material to one side, and prevents the material from remaining.

[0017] 2. In the utility model, the upper flange one and the lower flange one are set, the kettle cover and the kettle body can be fixed, the stepping motor is started, the rotating shaft can be driven to rotate, the rotation of the funnel type rotating disc can be realized, and the upper flange two and the lower flange two are set, the kettle body and the collecting bottle can be fixed. ACCURACY OF DRAWINGS

[0018] The utility model will be explained further in detail in connection with the drawings and specific embodiments.

[0019] Figure 1 It is the perspective structural schematic view of the utility model from the top;

[0020] Figure 2 It is the perspective structural schematic view of the utility model from the bottom;

[0021] Figure 3It is the inside structure schematic view of the front view of the utility model;

[0022] Figure 4 It is the inside structure schematic view of the top view of the utility model;

[0023] Figure 5 It is the structure schematic view of the collection bottle of the utility model.

[0024] In the figure: 1, stepper motor;2, coupling;3, rotating shaft;4, machine seal assembly;5, kettle cover;6, liquid inlet flange;7, upper flange one;8, lower flange one;9, funnel type rotary disc;10, kettle body;11, output pipeline;12, liquid separation mechanism one;13, liquid separation mechanism two;14, upper flange two;15, bolt one;16, lower flange two;17, collection port;18, collection bottle;19, support rod;20, bolt two. DETAILED DESCRIPTION

[0025] The technical scheme in the embodiments of the utility model will be clearly and completely described below in conjunction with the embodiments of the utility model, and obviously, the described embodiments are only part of the embodiments of the utility model, not all the embodiments. Based on the embodiments in the utility model, all other embodiments obtained by those skilled in the art without creative labor are involved in the protection scope of the utility model.

[0026] Embodiment 1

[0027] The preferred embodiment of the automatic fraction collection device for rectifying column provided by the utility model is as shown in Figures 1 to 5 As shown: an automatic fraction collection device for rectifying column, including kettle body 10: the top of kettle body 10 is provided with cover assembly, the top of cover assembly is provided with rotating mechanism, the rotating output end of rotating mechanism penetrates cover assembly to the inside of kettle body 10, the output end of rotating mechanism is fixedly connected with funnel type rotary disc 9, funnel type rotary disc 9 is provided with inclined mouth shape, the center position of the bottom surface in kettle body 10 is fixedly connected with liquid separation mechanism one 12, liquid separation mechanism one 12 is fixedly connected with liquid separation mechanism two 13 outside, the number of liquid separation mechanism two 13 is provided with multiple, liquid separation mechanism two 13 and liquid separation mechanism one 12 are fixedly combined with the inner wall of kettle body 10, the bottom of kettle body 10 is fixedly connected with output pipeline 11, the bottom of output pipeline 11 is provided with collection bottle 18, flange connection assembly is arranged between output pipeline 11 and collection bottle 18, output pipeline 11 communicates with the inside of kettle body 10, the bottom of output pipeline 11 communicates with the inside of collection bottle 18, the position of output pipeline 11 communicating with the inside of kettle body 10 is located between two liquid separation mechanism two 13.

[0028] It should be noted that the existing collection device still has certain deficiencies, which can only be manually collected, and the adaptability of manual collection is limited. For complex mixtures, especially for components with multiple boiling points close to each other or for long-term continuous collection of fractions, manual operation is difficult to maintain high accuracy and stability, and human error is prone to occur, such as too long or too short collection time, resulting in low purity of the fraction.

[0029] In the embodiment, the funnel-shaped rotating disc 9 is rotated after the rotating mechanism is started, and stops at the required position. At this time, the liquid inlet flange 6 receives the material condensed from the previous reaction and flows into the specific collection bottle 18 through the funnel-shaped rotating disc 9. The funnel-shaped rotating disc 9 is provided in a beveled shape to guide the material to one side and prevent material residue.

[0030] In a further preferred embodiment of the utility model, the liquid separation mechanism two 13 is radially and equidistantly distributed outside the liquid separation mechanism one 12, and the liquid separation mechanism two 13 is away from the funnel-shaped rotating disc 9.

[0031] In a further preferred embodiment of the utility model, the cover assembly includes the kettle cover 5, the upper flange one 7, the lower flange one 8 and the bolt two 20, the edge of the top of the kettle cover 5 is provided with an annular notch, the upper flange one 7 is clamped and connected inside the annular notch, the top of the kettle body 10 is fixedly connected with the lower flange one 8, and the inside of the upper flange one 7 and the lower flange one 8 is screw-connected with the bolt two 20.

[0032] In the embodiment, the upper flange one 7 and the lower flange one 8 can fix the kettle cover 5 and the kettle body 10.

[0033] In a further preferred embodiment of the utility model, the bolt two 20 is equidistantly distributed inside the upper flange one 7 and the lower flange one 8, and the top of the bolt two 20 is limited above the upper flange one 7.

[0034] Embodiment 2

[0035] On the basis of embodiment 1, the preferred embodiment of the automatic fraction collection device for rectifying column provided by the utility model is as follows Figures 1 to 5 As shown in the figure, the rotating mechanism includes the step motor 1, the shaft coupling 2, the rotating shaft 3, the machine seal assembly 4 and the support rod 19, the top of the kettle cover 5 is fixedly connected with the support rod 19, the top of the support rod 19 is fixedly connected with the step motor 1, the output end of the step motor 1 is fixedly connected with the shaft coupling 2, the other end of the shaft coupling 2 is fixedly connected with the rotating shaft 3, and the rotating shaft 3 penetrates through the kettle cover 5 and the machine seal assembly 4.

[0036] In the embodiment, the step motor 1 can drive the rotating shaft 3 to rotate, so as to realize the rotation of the funnel-shaped rotating disc 9.

[0037] The machine seal assembly 4 is fixed at the central position of the top of the kettle cover 5, the rotating shaft 3 penetrates the central position inside the machine seal assembly 4, and the rotating shaft 3 rotates inside the kettle cover 5 and the machine seal assembly 4.

[0038] In the further preferred embodiment of the utility model, the flange connecting assembly comprises an upper flange two 14, a bolt one 15 and a lower flange two 16, the upper flange two 14 is fixed at the bottom of the output pipeline 11, the bolt one 15 is arranged through the inside of the upper flange two 14, the lower flange two 16 is fixedly connected to the outside of the collecting opening 17, and the bolt one 15 penetrates the inside of the upper flange two 14 and is in threaded connection with the lower flange two 16.

[0039] In the embodiment, the upper flange two 14 and the lower flange two 16 can fix the kettle body 10 and the collecting bottle 18.

[0040] In the further preferred embodiment of the utility model, the kettle body 10 and the collecting bottle 18 are both made of glass.

[0041] The utility model further has the advantages that the kettle cover 6 is provided with the rotating shaft 3, the rotating shaft 3 is provided with the funnel type rotary disc 9, the funnel type rotary disc 9 is provided with the collecting opening 17, the collecting opening 17 is provided with the step motor 1, the step motor 1 is provided with the collecting device, and the kettle cover 6 is provided with the temperature sensor and the liquid level sensor.

[0042] The above are only the preferred embodiments of the utility model, and do not limit the utility model, and any modification, equivalent replacement, improvement, etc. within the spirit and principle of the utility model should be included in the protection scope of the utility model.

Claims

1. An automatic fraction collection device for a distillation column, characterized in that, The vessel includes a vessel body (10): a capping assembly is provided on the top of the vessel body (10), a rotating mechanism is provided on the top of the capping assembly, the rotating output end of the rotating mechanism passes through the capping assembly to the interior of the vessel body (10), and a funnel-shaped rotating disk (9) is fixedly connected to the output end of the rotating mechanism. The funnel-shaped rotating disk (9) is shaped with an oblique opening. A liquid-separating mechanism one (12) is fixedly connected to the center of the bottom surface inside the vessel body (10), and a liquid-separating mechanism two (13) is fixedly connected to the outside of the liquid-separating mechanism one (12). Multiple liquid-separating mechanisms two (13) are provided. (13) and the first liquid-separating mechanism (12) are both fixed to the inner wall of the vessel body (10). The bottom of the vessel body (10) is fixedly connected to an output pipe (11). A collection bottle (18) is provided at the bottom of the output pipe (11). A flange connection assembly is provided between the output pipe (11) and the collection bottle (18). The output pipe (11) is connected to the inside of the vessel body (10). The bottom of the output pipe (11) is connected to the inside of the collection bottle (18). The position where the output pipe (11) is connected to the inside of the vessel body (10) is located between the two second liquid-separating mechanisms (13).

2. The automatic fraction collection device for a distillation column according to claim 1, characterized in that, The second liquid-separating mechanism (13) is radially and equidistantly distributed outside the first liquid-separating mechanism (12), and the second liquid-separating mechanism (13) is far away from the funnel-shaped rotating disk (9).

3. The automatic fraction collection device for a distillation column according to claim 1, characterized in that, The sealing assembly includes a lid (5), an upper flange (7), a lower flange (8), and bolts (20). The lid (5) has an annular notch at the top edge, and the upper flange (7) is engaged with the inside of the annular notch. The lower flange (8) is fixedly connected to the top of the vessel body (10), and bolts (20) are threadedly connected to the inside of the upper flange (7) and the lower flange (8).

4. An automatic fraction collection device for a distillation column according to claim 3, characterized in that, The bolts 2 (20) are equidistantly distributed inside the upper flange 1 (7) and the lower flange 1 (8), with the top of the bolts 2 (20) restricted above the upper flange 1 (7).

5. An automatic fraction collection device for a distillation column according to claim 3, characterized in that, The rotating mechanism includes a stepper motor (1), a coupling (2), a rotating shaft (3), a mechanical seal assembly (4), and a support rod (19). The top of the vessel cover (5) is fixedly connected to the support rod (19), the top of the support rod (19) is fixedly connected to the stepper motor (1), the output end of the stepper motor (1) is fixedly connected to the coupling (2), the other end of the coupling (2) is fixedly connected to the rotating shaft (3), and the rotating shaft (3) passes through the vessel cover (5) and the mechanical seal assembly (4).

6. An automatic fraction collection device for a distillation column according to claim 5, characterized in that, The mechanical seal assembly (4) is fixed at the center of the top of the vessel lid (5), and the rotating shaft (3) passes through the center of the interior of the mechanical seal assembly (4). The rotating shaft (3) rotates inside the vessel lid (5) and the mechanical seal assembly (4).

7. An automatic fraction collection device for a distillation column according to claim 1, characterized in that, The flange connection assembly includes an upper flange (14), a bolt (15), and a lower flange (16). The upper flange (14) is fixed to the bottom of the output pipe (11). The bolt (15) is installed through the interior of the upper flange (14). The lower flange (16) is fixedly connected to the exterior of the collection port (17). The bolt (15) penetrates the interior of the upper flange (14) and is threadedly connected to the lower flange (16).

8. An automatic fraction collection device for a distillation column according to claim 1, characterized in that, Both the vessel body (10) and the collection bottle (18) are made of glass.

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