Novel rectifying tower material extraction device

Abstract

The utility model discloses a novel material extraction device for a rectifying tower, which relates to the technical field of rectifying tower equipment and comprises a rectifying tower body, a condenser is mounted at the top of the rectifying tower body, an electronic thermometer is mounted at the bottom of the condenser, and a condensation discharge pipe is mounted at the bottom of the condenser. The bottom of the condensation discharge pipe is provided with a feed port, the bottom of the feed port is provided with a reflux ratio extractor, the top of the reflux ratio extractor is provided with an electromagnetic controller, and the bottom of the reflux ratio extractor is provided with a magnetic swing pipe orifice. Through the arrangement of the base, the motor, the rotating disc and the material receiving barrels, after the single material receiving barrel is full of materials, the rotating disc is driven by the motor to rotate, the empty material receiving barrel rotates to the bottom of the material receiving pipe, continuous material receiving is achieved, workers do not need to watch beside the material receiving barrel at any time to pay attention to the internal material receiving condition, and the labor intensity of the workers is reduced.

Description

TECHNICAL FIELD

[0001] The utility model relates to rectifying tower equipment technical field, concretely is a new rectifying tower material extraction device. BACKGROUND

[0002] Rectification is a kind of distillation method using the difference of volatility of each component in mixture to separate each component, and the specific operation is to evaporate the material that is easy to evaporate first by heating liquid mixture, then condenses the evaporated gas back to liquid, so as to achieve the purpose of separation, in the rectification process, commonly used equipment includes plate rectifying tower and packing rectifying tower, therefore a new rectifying tower material extraction device is needed, and in the actual production process of enterprise, the overhead of plate rectifying tower and packing rectifying tower are all equipped with condenser, so as to condense the gasified liquid into liquid again, and then distill from the condenser outlet, but when rectifying some materials with similar volatility or more mixed components, direct rectification is often used, and high-purity single component cannot be obtained directly, so in order to obtain purer product, liquid mixture often needs to be rectified for many times, i.e. repeated evaporation and condensation process, and such repeated process needs to spend a lot of labor cost, time cost and fuel cost, in order to solve the above problems, a new rectifying tower material extraction device is needed.

[0003] The application of the existing rectifying tower material extraction device is complicated in rectification and purification process, and the purification effect is poor, and continuous feeding cannot be carried out, therefore a new rectifying tower material extraction device is needed. UTILITY MODEL CONTENT

[0004] Therefore, the utility model aims at providing a new rectifying tower material extraction device to solve the problems that the application of the existing rectifying tower material extraction device is complicated in rectification and purification process, and the purification effect is poor, and continuous feeding cannot be carried out.

[0005] To achieve the above object, the utility model provides the following technical scheme: A novel rectifying tower material production device, including rectifying tower body, the top of rectifying tower body is equipped with condenser, the bottom of condenser is equipped with electronic thermometer, the bottom of condenser is equipped with condensed discharge pipe, the bottom of condensed discharge pipe is equipped with feed inlet, the bottom of feed inlet is equipped with reflux ratio production device, the top of reflux ratio production device is equipped with electromagnetic controller, the bottom of reflux ratio production device is equipped with magnetic force swing pipe mouth, the bottom of magnetic force swing pipe mouth is equipped with reflux pipe, the side wall of reflux ratio production device is equipped with material receiving port, the outer wall of material receiving port is equipped with production pipe, the top of condenser is equipped with vacuum pipeline, the outer wall of vacuum pipeline is equipped with material receiving pipe, the bottom of rectifying tower body is equipped with base, the top of base is equipped with motor, the bottom of motor is equipped with carousel, the top of carousel is equipped with material receiving barrel.

[0006] Preferably, the condenser is flange connected with the rectifying tower body, and the condenser is arranged at an inclination angle of 45 degrees.

[0007] Preferably, the reflux pipe is flange intercepted with the rectifying tower body, and the reflux pipe is designed in a U shape.

[0008] Preferably, the vacuum pipeline is arranged at an inclination angle of 45 degrees, and the material receiving pipe is vertically aligned with the material receiving barrel.

[0009] Preferably, the base is welded with the rectifying tower body, and the material receiving barrels are arranged in a ring array around the central axis of the carousel.

[0010] Compared with the prior art, the utility model has the advantages that:

[0011] 1、The electronic thermometer, the condensed discharge pipe, the feed inlet, the reflux ratio production device, the electromagnetic controller, the magnetic force swing pipe mouth, the reflux pipe, the material receiving port and the production pipe are arranged, a plurality of mixed materials are first heated in the rectifying kettle, then ascend along the rectifying tower body, and are uniformly distributed according to the volatility in the rectifying tower body, the materials with good volatility are distributed in the upper layer of the rectifying tower body, and the materials with poor volatility are distributed in the lower layer of the rectifying tower body, then the materials reach the condenser under the action of vacuum, are converted from gas phase to liquid phase, the liquefaction degree is observed according to the electronic thermometer, then the materials reach the feed inlet from the condensed discharge pipe, the materials enter the material receiving port or the reflux pipe under the control of the electromagnetic controller, if the content of the materials is qualified, the materials enter the production pipe, and if the content is unqualified, the materials enter the reflux pipe again, the rectifying tower body is used for rectification again, and the separation and purification of the mixed materials are repeated until the mixed materials are completely separated and purified, and the electromagnetic controller can be set to different production reflux ratios according to the volatility and the different component numbers of the mixed materials, so that the best separation and purification effect is achieved.

[0012] 2、The utility model discloses a base, motor, carousel and receiving barrel are set up, when the material in single receiving barrel is full, rotates through the motor drive carousel, makes empty receiving barrel rotate to the bottom of receiving pipe, and continuously receives the material, and staff need not always keep watch and guard at the side of receiving barrel and pay attention to the internal receiving condition, reduces the labor intensity of staff. BRIEF DESCRIPTION OF DRAWINGS

[0013] Figure 1 It is the structure schematic diagram of the appearance of the utility model from the front view;

[0014] Figure 2 It is the structure schematic diagram of the appearance of the utility model from the side view;

[0015] Figure 3 It is the structure schematic diagram of the surrounding assembly detail display of the utility model reflux ratio production device;

[0016] Figure 4 It is the structure schematic diagram of the surrounding assembly detail display of the carousel of the utility model.

[0017] In the drawing: 1, rectifying tower body;2, condenser;3, electronic thermometer;4, condensed discharge pipe;5, feed inlet;6, reflux ratio production device;7, electromagnetic controller;8, magnetic force swing pipe orifice;9, reflux pipe;10, receiving port;11, production pipe;12, vacuum pipeline;13, receiving pipe;14, base;15, motor;16, carousel;17, receiving barrel. DETAILED DESCRIPTION

[0018] The technical scheme in the embodiments of the utility model will be described clearly and completely below in combination with the drawings in the embodiments of the utility model. The embodiments described below with reference to the drawings are exemplary and are used only for explaining the utility model, and cannot be understood as limiting the utility model.

[0019] The embodiments of the utility model will be described below according to the overall structure of the utility model.

[0020] Please refer to Figures 1-4The utility model provides a new type of rectifying column material tapping device, including rectifying column body 1, the top of rectifying column body 1 is equipped with condenser 2, the bottom of condenser 2 is equipped with electronic thermometer 3, the bottom of condenser 2 is equipped with condensed discharge pipe 4, the bottom of condensed discharge pipe 4 is equipped with feed inlet 5, the bottom of feed inlet 5 is equipped with reflux ratio sampler 6, the top of reflux ratio sampler 6 is equipped with electromagnetic controller 7, the bottom of reflux ratio sampler 6 is equipped with magnetic force swing pipe mouth 8, the bottom of magnetic force swing pipe mouth 8 is equipped with reflux pipe 9, the sidewall of reflux ratio sampler 6 is equipped with material receiving port 10, the outer wall of material receiving port 10 is equipped with tapping pipe 11, the top of condenser 2 is equipped with vacuum pipeline 12, the outer wall of vacuum pipeline 12 is equipped with material receiving pipe 13, condenser 2 is flanged with rectifying column body 1, condenser 2 is arranged with 45 degree inclination angle, reflux pipe 9 is intercepted with the flange of rectifying column body 1, reflux pipe 9 is designed with U shape, by setting electronic thermometer 3, condensed discharge pipe 4, feed inlet 5, reflux ratio sampler 6, electromagnetic controller 7, magnetic force swing pipe mouth 8, reflux pipe 9, material receiving port 10 and tapping pipe 11, first heat the multiple groups of mixed materials in rectifying kettle, then ascend along rectifying column body 1, and according to the volatility, distribute the materials with good volatility in upper layer of rectifying column body 1, and the materials with poor volatility in lower layer of rectifying column body 1, then with the vacuum effect, the materials reach condenser 2, convert from gas phase to liquid phase, according to electronic thermometer 3, observe the liquefaction degree, then the materials reach feed inlet 5 from condensed discharge pipe 4, then control magnetic force swing pipe mouth 8 by electromagnetic controller 7, thereby control the materials to enter material receiving port 10 or reflux pipe 9, if the content is qualified, then enter material receiving port 10, then enter tapping pipe 11, obtain qualified products, if the content is unqualified, then enter reflux pipe 9, re-enter rectifying column body 1 and rectify again, repeat until all the mixed materials are separated and purified, and according to the volatility and component number of mixed materials, set different tapping reflux ratios of electromagnetic controller 7, achieve the best separation and purification effect.

[0021] Please refer to Figures 1-4 The utility model provides a new type of rectifying column material tapping device, the bottom of rectifying column body 1 is equipped with base 14, the top of base 14 is equipped with motor 15, the bottom of motor 15 is equipped with rotating disc 16, the top of rotating disc 16 is equipped with material receiving barrel 17, vacuum pipeline 12 is arranged with 45 degree inclination angle, material receiving pipe 13 is vertically aligned with material receiving barrel 17, base 14 is welded with rectifying column body 1, material receiving barrel 17 is arranged in annular array distribution with the central axis of rotating disc 16 as the center, by setting base 14, motor 15, rotating disc 16 and material receiving barrel 17, when the material in single material receiving barrel 17 is full, rotate rotating disc 16 by motor 15, make empty material receiving barrel 17 rotate to the bottom of material receiving pipe 13, continuously receive material, do not need staff to monitor the internal material receiving condition beside material receiving barrel 17, reduce the labor intensity of staff.

[0022] Working Principle: In operation, the device is first moved to the desired location. Then, multiple mixtures are heated in a distillation kettle and then rise up the distillation column 1. Based on their volatility, the more volatile materials are evenly distributed in the upper layer of the column 1, while the less volatile materials are in the lower layer. Under vacuum, the materials reach the condenser 2, where they transform from a gaseous phase to a liquid phase. The degree of liquefaction is observed using an electronic thermometer 3. The material then flows from the condenser outlet pipe 4 to the inlet 5. An electromagnetic controller 7 controls the magnetic oscillation port 8, thus controlling the material's entry into the receiving port 10 or the reflux pipe 9. If the material content is within acceptable limits, it flows into the receiving port 10 and then into the collection pipe 11 to obtain a qualified product. If the content is not within acceptable limits... The mixture is then transferred to reflux pipe 9 and re-entered into distillation column 1 for further distillation. This process is repeated until all the mixture is completely separated and purified. Furthermore, the electromagnetic controller 7 can be set to different reflux ratios based on the volatility and composition of the mixture to achieve optimal separation and purification. Once a single receiving hopper 17 is full, the motor 15 drives the turntable 16 to rotate, causing the empty receiving hopper 17 to rotate to the bottom of the receiving pipe 13 for continuous material collection. This eliminates the need for staff to constantly monitor the receiving hopper 17, reducing workload. This completes the operation of the device. Content not described in detail in this manual is considered prior art known to those skilled in the art.

[0023] The terms “center,” “longitudinal,” “lateral,” “front,” “rear,” “left,” “right,” “vertical,” “horizontal,” “top,” “bottom,” “inner,” and “outer,” etc., indicate the orientation or positional relationship based on the orientation or positional relationship shown in the accompanying drawings. They are merely simplified descriptions for the convenience of describing this utility model and do not indicate or imply that the device or element referred to must have a specific orientation, or be constructed and operated in a specific orientation. Therefore, they should not be construed as limiting the scope of protection of this utility model.

[0024] Although the present invention has been described in detail with reference to the foregoing embodiments, those skilled in the art can still modify the technical solutions described in the foregoing embodiments or make equivalent substitutions for some of the technical features. Any modifications, equivalent substitutions, improvements, etc., made within the spirit and principles of the present invention should be included within the protection scope of the present invention.

Claims

1. A novel material take-off device for a rectification column, comprising a rectification column body (1), characterized in that: The top of the rectifying tower body (1) is provided with a condenser (2), the bottom of the condenser (2) is provided with an electronic thermometer (3), the bottom of the condenser (2) is provided with a condensing discharge pipe (4), the bottom of the condensing discharge pipe (4) is provided with a feed inlet (5), the bottom of the feed inlet (5) is provided with a reflux ratio extractor (6), the top of the reflux ratio extractor (6) is provided with an electromagnetic controller (7), the bottom of the reflux ratio extractor (6) is provided with a magnetic swing pipe (8), the bottom of the magnetic swing pipe (8) is provided with a reflux pipe (9), the side wall of the reflux ratio extractor (6) is provided with a receiving port (10), the outer wall of the receiving port (10) is provided with an extraction pipe (11), the top of the condenser (2) is provided with a vacuum pipe (12), the outer wall of the vacuum pipe (12) is provided with a receiving pipe (13), the bottom of the rectifying tower body (1) is provided with a base (14), the top of the base (14) is provided with a motor (15), the bottom of the motor (15) is provided with a turntable (16), the top of the turntable (16) is provided with a receiving barrel (17).

2. A novel distillation column material take-off device according to claim 1, characterized in that: The condenser (2) is flange connected with the rectifying tower body (1), and the condenser (2) is provided at an inclination angle of 45 degrees.

3. A novel material take-off device for distillation column as claimed in claim 1, wherein: The reflux pipe (9) is flange intercepted with the rectifying tower body (1), and the reflux pipe (9) is designed in a U shape.

4. A novel material take-off device for distillation column as claimed in claim 1, wherein: The vacuum pipe (12) is provided at an inclination angle of 45 degrees, and the receiving pipe (13) is vertically aligned with the receiving barrel (17).

5. A novel material take-off device for distillation columns as claimed in claim 1, wherein: The base (14) is welded with the rectifying tower body (1), and the receiving barrel (17) is arranged in a ring array around the central axis of the turntable (16).

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