Magnetic photo-thermal response sponge treatment equipment

Abstract

The utility model discloses a magnetic photo-thermal response sponge treatment equipment, including workbench, first motor and ultrasonic cell disruptor, the right end of workbench top is provided with constant temperature drying box, the middle end of workbench top is provided with first container, the output end of first motor is fixedly equipped with adjusting screw, and the output end of first motor is fixedly equipped with ultrasonic cell disruptor. And the middle end of the adjusting screw rod is in threaded connection with a moving plate, an electric push rod is fixedly installed on the surface of the moving plate, and an amplitude-change pole is fixedly installed between the lower end of the ultrasonic cell crusher and the output end of the electric push rod through a wire. According to the magnetic photo-thermal response sponge preparation device, a plurality of complex steps required by preparation of the magnetic photo-thermal response sponge are effectively integrated and simplified above the workbench, so that personnel can complete the preparation process of the magnetic photo-thermal response sponge only through simple operation, and the efficiency of preparation and production operation is effectively improved; meanwhile, the use cost required by preparation is reduced.

Description

Technical Field

[0001] This utility model relates to the field of polymer composite material preparation technology, specifically a magnetic photothermal responsive sponge processing device. Background Technology

[0002] Magnetic photothermal responsive sponge is a porous material made by combining magnetic nanoparticles with photothermal materials. It has both magnetic responsiveness and photothermal conversion capabilities. Its core features include: magnetic drive: it can achieve directional movement or remote control through an external magnetic field, making it suitable for complex environments; photothermal effect: it heats up rapidly under light, reducing the fluidity of high-viscosity liquids and improving adsorption efficiency; superhydrophobic / oleophilic: after surface modification, it can achieve selective adsorption of oil and water, making it suitable for oil stain treatment.

[0003] Currently, the preparation of magnetic photothermal responsive sponges involves multiple complex steps and a long reaction time, and the operation is quite cumbersome, resulting in low production efficiency and a significant increase in personnel costs. Utility Model Content

[0004] The purpose of this invention is to provide a magnetic photothermal responsive sponge processing device, which integrates and simplifies many complex steps, effectively improving the efficiency of the preparation and production process, and reducing personnel costs.

[0005] To achieve the above objectives, this utility model provides the following technical solution: a magnetic photothermal responsive sponge processing device, comprising a workbench, a first motor, and an ultrasonic cell disruptor. A constant temperature drying oven is placed at the right end of the top of the workbench, and a first container is placed at the middle end of the top of the workbench. An adjusting screw is fixedly installed at the output end of the first motor, and a moving plate is threadedly connected to the middle end of the adjusting screw. An electric push rod is fixedly installed on the surface of the moving plate. An amplitude transformer is fixedly installed between the lower end of the ultrasonic cell disruptor and the output end of the electric push rod via a wire. A constant temperature chamber is placed at the left end of the top of the workbench. A limiting seat is fixedly connected to the bottom of the inner cavity of the constant temperature chamber. A second container is placed in the inner cavity of the limiting seat. A rotating shaft is movably connected to the middle end of the bottom of the second container via a bearing. A square hole is opened at the bottom of the rotating shaft, and a stirring plate is fixedly connected to the top of the rotating shaft. A second motor is fixedly installed at the bottom of the outer surface of the constant temperature chamber. A square rotating rod is fixedly installed at the output end of the second motor, and the upper end of the square rotating rod is movably connected to the surface of the square hole.

[0006] As a preferred embodiment, a fixed frame is fixedly connected to the top of the workbench and located behind the first container. The bottom of the ultrasonic cell disruptor is fixedly installed on the top of the fixed frame. The left side of the first motor is fixedly installed on the right end of the back of the fixed frame. A support plate is movably connected to the left side of the adjusting screw via a bearing. The surface of the support plate is fixedly connected to the left end of the back of the fixed frame. A guide slide is movably connected to the middle of the moving plate. The upper end of the guide slide is fixedly connected to the surface of the fixed frame.

[0007] As a preferred embodiment, an annular positioning frame is fixedly connected to the middle of the top of the workbench, and the surface of the first container is placed in the inner cavity of the annular positioning frame. There are two of both the first container and the annular positioning frame.

[0008] As a preferred embodiment, the outer surface of the second container is covered with a rubber sleeve, the bottom of the rubber sleeve has an insertion hole, and the top of the limiting seat is fixedly connected with an insertion block.

[0009] As a preferred embodiment, there are four sockets and four plug blocks, and the surface of the plug block is movably connected to the surface of the socket.

[0010] As a preferred embodiment, a perfluoroether rubber sealing ring is fixedly installed at the middle of the bottom of the second container, and the lower end of the rotating shaft contacts the surface of the perfluoroether rubber sealing ring.

[0011] As a preferred embodiment, the front surface of the constant temperature chamber is movably connected to a first sealing door via a hinge, and the front surface of the constant temperature drying chamber is movably connected to a second sealing door via a hinge.

[0012] Compared with the prior art, the beneficial effects of this utility model are as follows:

[0013] 1. This utility model effectively integrates and simplifies the multiple complex steps required for the preparation of magnetic photothermal responsive sponge above the workbench, allowing personnel to complete the preparation process of magnetic photothermal responsive sponge with only simple operations, effectively improving the efficiency of the preparation and production operation, while reducing the cost of preparation.

[0014] 2. This utility model, through the setting of the fixed frame, can support the first motor and the ultrasonic cell disruptor. At the same time, through the setting of the support plate, it can support the left side of the adjusting screw and the left end of the fixed frame, so as to prevent the adjusting screw from tilting due to force. Through the setting of the guide slide, the purpose of supporting and guiding the moving plate is achieved, so as to prevent the moving plate from tilting due to force.

[0015] 3. This utility model, through the setting of the annular positioning frame, can limit the surrounding area of ​​the first container to prevent displacement of the first container during use. Through the setting of the rubber sleeve, the insertion hole and the insertion block, the rubber sleeve can be tightly fitted on the surface of the second container, and under the action of the insertion hole and the insertion block, the rubber sleeve and the second container can be limited to a certain extent, preventing the second container from rotating during the stirring process. Through the setting of the perfluoroether rubber sealing ring, the sealing performance between the rotating shaft and the second container is effectively improved. Attached Figure Description

[0016] Figure 1 This is a perspective view of the present utility model;

[0017] Figure 2 This is a partial structural diagram of the fixing frame of this utility model viewed from below;

[0018] Figure 3 This is a partial structural diagram of the back of the fixing frame of this utility model;

[0019] Figure 4 This is a partial cross-sectional view of the constant temperature chamber of this utility model;

[0020] Figure 5 This utility model Figure 4 A magnified view of section A in the image.

[0021] In the diagram: 1. Workbench; 2. Annular positioning frame; 3. First container; 4. Constant temperature chamber; 5. Ultrasonic cell disruptor; 6. Fixing frame; 7. Amplitude rod; 8. Constant temperature drying oven; 9. Guide slide rod; 10. Moving plate; 11. Electric push rod; 12. First motor; 13. Adjusting screw; 14. Support plate; 15. Rubber sleeve; 16. Insertion hole; 17. Insertion block; 18. Limiting seat; 19. Second motor; 20. Second container; 21. Square rotating rod; 22. Perfluoroether rubber sealing ring; 23. Square hole; 24. Stirring plate; 25. Rotating shaft. Detailed Implementation

[0022] The technical solutions of the present utility model will be clearly and completely described below with reference to the accompanying drawings of the embodiments. Obviously, the described embodiments are only some embodiments of the present utility model, and not all embodiments. Based on the embodiments of the present utility model, all other embodiments obtained by those of ordinary skill in the art without creative effort are within the protection scope of the present utility model.

[0023] Secondly, the term "an embodiment" or "embodiment" as used herein refers to a specific feature, structure, or characteristic that may be included in at least one implementation of the present invention. The phrase "in one embodiment" appearing in different places in this specification does not necessarily refer to the same embodiment, nor is it a single or selective embodiment that excludes other embodiments.

[0024] Example 1:

[0025] Please see Figures 1-5 As shown, this utility model provides a magnetic photothermal responsive sponge processing device, including a workbench 1, a first motor 12, and an ultrasonic cell disruptor 5. A constant temperature drying oven 8 is placed at the right end of the top of the workbench 1, and a first container 3 is placed at the middle end of the top of the workbench 1. An adjusting screw 13 is fixedly installed at the output end of the first motor 12, and a moving plate 10 is threadedly connected to the middle end of the adjusting screw 13. An electric push rod 11 is fixedly installed on the surface of the moving plate 10. A variable frequency drive is fixedly installed between the lower end of the ultrasonic cell disruptor 5 and the output end of the electric push rod 11 via a wire. A constant temperature chamber 4 is placed on the left end of the top of the workbench 1 and the boom 7. A limit seat 18 is fixedly connected to the bottom of the inner cavity of the constant temperature chamber 4. A second container 20 is placed in the inner cavity of the limit seat 18. A rotating shaft 25 is movably connected to the middle of the bottom of the second container 20 through a bearing. A square hole 23 is opened at the bottom of the rotating shaft 25. A stirring plate 24 is fixedly connected to the top of the rotating shaft 25. A second motor 19 is fixedly installed at the bottom of the outer surface of the constant temperature chamber 4. A square rotating rod 21 is fixedly installed at the output end of the second motor 19. The upper end of the square rotating rod 21 is movably connected to the surface of the square hole 23.

[0026] In this technical solution, by effectively integrating and simplifying the multiple complex steps required for the preparation of magnetic photothermal responsive sponge above the workbench 1, personnel can complete the preparation process of magnetic photothermal responsive sponge with only simple operations, which effectively improves the efficiency of the preparation and production operation, while reducing the cost of preparation.

[0027] Example 2:

[0028] Based on Embodiment 1, this utility model is as follows: Figures 1-3 As shown, a fixed frame 6 is fixedly connected to the top of the workbench 1 and behind the first container 3. The bottom of the ultrasonic cell disruptor 5 is fixedly installed on the top of the fixed frame 6. The left side of the first motor 12 is fixedly installed on the right end of the back of the fixed frame 6. The left side of the adjusting screw 13 is movably connected to the support plate 14 through the bearing. The surface of the support plate 14 is fixedly connected to the left end of the back of the fixed frame 6. The middle end of the moving plate 10 is movably connected to the guide slide rod 9. The upper end of the guide slide rod 9 is fixedly connected to the surface of the fixed frame 6.

[0029] In this technical solution, the fixed frame 6 can support the first motor 12 and the ultrasonic cell disruptor 5, while the support plate 14 can support the left side of the adjusting screw 13 and the left end of the fixed frame 6, thus preventing the adjusting screw 13 from tilting due to force. The guide slide rod 9 can support and guide the moving plate 10, thus preventing the moving plate 10 from tilting due to force.

[0030] Example 3:

[0031] Based on Embodiment 1, this utility model is as follows: Figure 1 , Figure 4 and Figure 5 As shown, a ring-shaped positioning frame 2 is fixedly connected to the middle of the top of the workbench 1. The surface of the first container 3 is placed in the inner cavity of the ring-shaped positioning frame 2. There are two of each of the first container 3 and the ring-shaped positioning frame 2. A rubber sleeve 15 is fitted on the outer surface of the second container 20. An insertion hole 16 is opened at the bottom of the rubber sleeve 15. An insertion block 17 is fixedly connected to the top of the limiting seat 18. There are four of each of the insertion holes 16 and the insertion blocks 17. The surface of the insertion block 17 is movably connected to the surface of the insertion hole 16. A perfluoroether rubber sealing ring 22 is fixedly installed at the middle of the bottom of the second container 20. The lower end of the rotating shaft 25 contacts the surface of the perfluoroether rubber sealing ring 22. The front surface of the constant temperature chamber 4 is movably connected to the first sealing door through a hinge. The front surface of the constant temperature drying chamber 8 is movably connected to the second sealing door through a hinge.

[0032] In this technical solution, the annular positioning frame 2 can limit the surrounding area of ​​the first container 3 to prevent displacement of the first container 3 during use. The rubber sleeve 15, the insertion hole 16 and the insertion block 17 can tightly fit the rubber sleeve 15 on the surface of the second container 20. Under the action of the insertion hole 16 and the insertion block 17, the rubber sleeve 15 and the second container 20 can be limited to a certain extent to prevent the second container 20 from rotating during stirring. The perfluoroether rubber sealing ring 22 effectively improves the sealing performance between the rotating shaft 25 and the second container 20.

[0033] The working principle of this invention is as follows: First, 150 ml of 1.0 M hydrochloric acid and 3.78 g of aniline are weighed and added to the second container 20. A clean polyurethane sponge block is then immersed in the solution. Next, 20 ml of 0.25 M ammonium persulfate oxidant is slowly added. While the temperature inside the constant temperature chamber 4 is set at 0-5℃, the second motor 19 is started via an external PLC controller, driving the square rotating rod 21, square hole 23, rotating shaft 25, and stirring plate 24 to stir at 450 rpm for 3 hours. Afterward, the polyurethane sponge block is removed and placed inside a constant temperature drying oven 8, where it is dried at 70℃ for 4 hours. Next, 200 mg of multi-walled carbon nanotubes and 200 ml of ethanol solution were weighed and added to the first container 3 located on the left. Then, the first motor 12 was started by the external PLC controller, which drove the adjusting screw 13 to rotate. The rotation of the adjusting screw 13 drove the moving plate 10, the electric push rod 11, and the amplitude rod 7 to move to the left until the amplitude rod 7 was above the first container 3 on the left. Then, by manipulating the electric push rod 11 to extend, the amplitude rod 7 was pushed into the first container 3. Under the action of the ultrasonic cell disruptor 5, the amplitude rod 7 was able to undergo ultrasonic vibration in the first container 3 for 5 minutes, so that the multi-walled carbon nanotubes could be subjected to ultrasonic vibration. A uniform dispersion and mixing can be achieved between the polyurethane foam and the ethanol solution. The dried and pre-modified polyurethane sponge is then immersed in the solution. The mixture is then subjected to continuous operation for 25 minutes using an ultrasonic cell disruptor 5 and an amplitude transformer 7, which anchors multi-walled carbon nanotubes onto the framework of the polyurethane sponge block. The polyurethane sponge block is then removed and placed back into a constant-temperature drying oven 8 at 70°C for 4 hours. Next, 1.5g of PDMS, 0.15g of curing agent, 1.5g of iron oxide, and 150g of n-hexane are weighed and mixed to form a suspension, which is then added to the first container 3 on the right. Finally, the dried and pre-modified polyurethane sponge is immersed in the solution. The polyurethane sponge block is placed in the suspension, and the first motor 12 is started to drive the adjusting screw 13 to rotate in another direction, which in turn drives the moving plate 10, the electric push rod 11 and the amplitude rod 7 after cleaning to move to the right, so that the amplitude rod 7 can be positioned above the first container 3 on the right. Under the extension of the electric push rod 11, the amplitude rod 7 can be inserted into the first container 3. Through the operation of the ultrasonic cell disruptor 5 and the amplitude rod 7, the polyurethane sponge block is ultrasonically soaked for 45 minutes. After that, the polyurethane sponge block is taken out again and placed inside the constant temperature drying oven 8 for drying and curing at 70°C for 4 hours to obtain the magnetic photothermal responsive sponge.

[0034] Finally, it should be noted that the above embodiments are only used to illustrate the technical solutions of this utility model, and are not intended to limit the scope of protection of this utility model. Although this utility model has been described in detail with reference to preferred embodiments, those skilled in the art should understand that modifications or equivalent substitutions can be made to the technical solutions of this utility model without departing from the essence and scope of the technical solutions of this utility model.

Claims

1. A magnetic photothermal response sponge treatment device, comprising a workbench (1), a first motor (12) and an ultrasonic cell disruptor (5), characterized in that: The right end of the top of the workbench (1) is placed with a constant temperature drying box (8), the middle end of the top of the workbench (1) is placed with a first container (3), the output end of the first motor (12) is fixedly installed with an adjusting screw rod (13), the middle end of the adjusting screw rod (13) is threadedly connected with a moving plate (10), the surface of the moving plate (10) is fixedly installed with an electric push rod (11), the lower end of the ultrasonic cell disruptor (5) is fixedly installed between the output end of the electric push rod (11) and the wire with a variable amplitude rod (7), the left end of the top of the workbench (1) is placed with a constant temperature box (4), the bottom of the inner cavity of the constant temperature box (4) is fixedly connected with a limiting seat (18), the inner cavity of the limiting seat (18) is placed with a second container (20), the middle end of the bottom of the second container (20) is movably connected with a rotating shaft (25) through a bearing, the bottom of the rotating shaft (25) is provided with a square hole (23), the top of the rotating shaft (25) is fixedly connected with a stirring disc (24), the bottom of the outer surface of the constant temperature box (4) is fixedly installed with a second motor (19), the output end of the second motor (19) is fixedly installed with a square rotating rod (21), and the upper end of the square rotating rod (21) is movably connected to the surface of the square hole (23).

2. The magnetic photothermally responsive sponge treatment apparatus according to claim 1, wherein: The top of the workbench (1) is fixedly connected with a fixed frame (6) behind the first container (3), the bottom of the ultrasonic cell disruptor (5) is fixedly installed on the top of the fixed frame (6), the left side of the first motor (12) is fixedly installed on the right end of the back of the fixed frame (6), the left side of the adjusting screw rod (13) is movably connected with a support plate (14) through a bearing, the surface of the support plate (14) is fixedly connected to the left end of the back of the fixed frame (6), and the middle end of the moving plate (10) is movably connected with a guide slide rod (9), the upper end of the guide slide rod (9) is fixedly connected to the surface of the fixed frame (6).

3. The magnetic photothermally responsive sponge treatment device of claim 1, wherein: The middle end of the top of the workbench (1) is fixedly connected with an annular positioning frame (2), and the surface of the first container (3) is placed in the inner cavity of the annular positioning frame (2). The number of the first container (3) and the annular positioning frame (2) is two.

4. The magnetic photothermally responsive sponge treatment apparatus of claim 1, wherein: The outer surface of the second container (20) is sleeved with a rubber sleeve (15), the bottom of the rubber sleeve (15) is provided with a jack (16), and the top of the limiting seat (18) is fixedly connected with a plug (17).

5. The magnetic photothermally responsive sponge treatment apparatus of claim 4, wherein: The number of the jack (16) and the plug (17) is four, and the surface of the plug (17) is movably connected to the surface of the jack (16).

6. The magnetic photothermally responsive sponge treatment apparatus of claim 1, wherein: The middle end of the bottom of the second container (20) is fixedly installed with a perfluoroether rubber sealing ring (22), and the lower end of the rotating shaft (25) contacts the surface of the perfluoroether rubber sealing ring (22).

7. The magnetic photothermally responsive sponge treatment device of claim 1, wherein: The front surface of the constant temperature box (4) is movably connected with a first sealing door through a hinge, and the front surface of the constant temperature drying box (8) is movably connected with a second sealing door through a hinge.

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