Phosethyl-Al saponification reaction device

Abstract

The utility model discloses a phosethyl-Al saponification reaction device which comprises a kettle body, a reaction cavity is arranged in the kettle body, a stirring device is arranged in the reaction cavity, and the stirring device comprises a stirring shaft driven by an external driving device and two types of stirring blades arranged on the stirring shaft. The first type of stirring blades are fixed stirring blades fixed on the stirring shaft, the second type of stirring blades are movable stirring blades movably arranged on the stirring shaft, a spiral groove is formed in the side wall of the stirring shaft, and the movable stirring blades are provided with limiting columns extending into the spiral groove; the spiral column of the movable stirring blade is located at the highest end of the spiral groove when the driving device drives forwards, and the spiral column of the movable stirring blade is located at the lowest end of the spiral groove when the driving device drives backwards. The two groups of fixed stirring blades and movable stirring blades are arranged to stir materials during stirring, the driving device intermittently rotates forwards and backwards to drive the movable stirring blades to change the height and the horizontal position, and compared with pure fixed blades, the stirring effect is better, the materials are mixed more uniformly, and the stirring efficiency is improved. The saponification reaction is facilitated.

Description

Technical Field

[0001] This utility model relates to chemical reaction apparatus, and more particularly to an apparatus for saponification of aluminum triethylphosphonate. Background Technology

[0002] Aluminum tris(ethyl phosphonate) is a highly effective, broad-spectrum, and low-toxicity organophosphorus systemic fungicide. It exhibits bidirectional systemic activity, being absorbed by crop roots and translocated to the above-ground stems and leaves, as well as absorbed by upper leaves and translocated to basal leaves, thus providing both protective and curative effects. Its broad fungicidal spectrum is effective against diseases caused by pathogenic fungi of the genera *Peronospora* and *Phytophthora* within the Algae and Mycota phylum. It is suitable for a wide range of crops, including various fruits, vegetables, and flowering plants.

[0003] Currently, the process adopted by domestic manufacturers is to use phosphorus trichloride, anhydrous ethanol, ammonia, and solid aluminum sulfate as the main raw materials, which are then processed through esterification, saponification, and metathesis reactions.

[0004] The existing saponification process for preparing aluminum tris(ethyl phosphonate) is complex and time-consuming. Due to poor mixing of raw materials in the saponification device, incomplete saponification and low conversion rate are easily caused. Utility Model Content

[0005] To address the shortcomings of existing reaction devices for aluminum tris(ethyl phosphonate) with poor mixing performance, this invention provides an aluminum tris(ethyl phosphonate) saponification reaction device.

[0006] The technical solution adopted by this utility model to solve the above-mentioned technical problems is as follows:

[0007] A saponification apparatus for aluminum tris(ethylphosphonate) includes a vessel body with a reaction chamber inside. The reaction chamber contains a stirring device, which includes a stirring shaft driven by an external drive and two types of stirring blades mounted on the shaft. The first type of stirring blade is a fixed blade fixed to the stirring shaft, and the second type is a movable blade movably mounted on the stirring shaft. The side wall of the stirring shaft has a spiral groove. The movable blades have limiting posts extending into the spiral grooves. When the drive is in the forward direction, the spiral posts of the movable blades are at the highest end of the spiral grooves; when the drive is in the reverse direction, the spiral posts of the movable blades are at the lowest end of the spiral grooves. This design, by using two sets of fixed and movable stirring blades to stir the material, and by intermittently driving the movable blades in both forward and reverse directions to change their height and horizontal position, achieves better stirring effect and more uniform material mixing compared to purely fixed blades, which is beneficial for the saponification reaction.

[0008] Preferably, the fixed stirring blade includes an annular fixed sleeve, several first stirring rods disposed on the fixed sleeve, and rectangular blades disposed at the outer ends of the first stirring rods. The fixed sleeve is fitted and fixed on the stirring shaft, and several first stirring rods are disposed in an annular array on the fixed sleeve.

[0009] Preferably, the movable stirring blade includes an annular movable sleeve, several stirring rods disposed on the movable sleeve, and L-shaped blades disposed at the outer ends of the second stirring rods. The movable sleeve is fitted onto the stirring shaft and the limiting post is located on the inner wall of the movable sleeve. Several second stirring rods are disposed and distributed in an annular array on the movable sleeve.

[0010] Preferably, the rectangular blade is located at the notch above the L-shaped blade so that the two do not interfere with each other when the L-shaped blade rises.

[0011] Preferably, the second stirring rod passes through the movable sleeve and is fixed to the movable sleeve, and the second stirring rod extends beyond the inner wall of the movable sleeve to form a limiting post that extends into the spiral groove.

[0012] Preferably, the end of the limiting post is equipped with a roller, which is located within the spiral groove. This design uses a roller to move within the spiral groove instead of the limiting post, which reduces wear and increases service life.

[0013] Preferably, the two types of stirring blades are spaced apart along the axial direction of the stirring shaft. The vertical spacing can improve the uniformity of materials at different vertical heights during stirring.

[0014] Preferably, the driving device is a bidirectional motor located at the top of the vessel, and the bidirectional motor is connected to the top of the stirring shaft.

[0015] Preferably, the vessel body includes a tank at the bottom and a detachable lid at the top of the tank. The lid is provided with several feeding pipe joints and a pressure gauge. The side wall of the tank is provided with a partition and a temperature sensor for monitoring the internal temperature of the tank. A set of heating pipes communicating with the internal space of the partition are provided at the partition.

[0016] Preferably, a discharge port is provided at the bottom of the tank, and a ball valve is provided at the discharge port.

[0017] Compared with the prior art, the advantages of this utility model are as follows: This application sets two sets of fixed stirring blades and movable stirring blades to stir the material during stirring, and drives the movable stirring blades to change their height and horizontal position by intermittently rotating forward and reverse by the driving device. Compared with pure fixed blades, the stirring effect is better, the material is mixed more evenly, and it is beneficial to the saponification reaction. Attached Figure Description

[0018] The present invention will be further described in detail below with reference to the accompanying drawings and preferred embodiments. However, those skilled in the art will understand that these drawings are drawn only for the purpose of explaining the preferred embodiments and therefore should not be construed as limiting the scope of the present invention. Furthermore, unless specifically indicated, the drawings are only schematic representations of the composition or structure of the described objects and may contain exaggerated depictions, and the drawings are not necessarily drawn to scale.

[0019] Figure 1 This is a perspective view of the present application;

[0020] Figure 2 This is a cross-sectional view of this application;

[0021] Figure 3 This is a side view of this application;

[0022] Figure 4 This is a schematic diagram of the stirring device in this application;

[0023] Figure 5 This is an exploded view of the stirring device in this application;

[0024] In the diagram: 10, vessel body; 101, tank body; 1011, heating tube; 1012, temperature sensor; 1013, spacer; 1014, ball valve; 102, tank cover; 1021, feeding pipe connector; 1022, pressure gauge; 20, drive device; 30, stirring device; 300, stirring shaft; 301, fixed stirring blade; 3011, first stirring rod; 3012, rectangular blade; 3013, fixed sleeve; 302, movable stirring blade; 3021, second stirring rod; 30211, roller; 3022, movable sleeve; 3023, L-shaped blade. Detailed Implementation

[0025] The preferred embodiments of the present invention will be described in detail below with reference to the accompanying drawings. Those skilled in the art will appreciate that these descriptions are merely descriptive and exemplary and should not be construed as limiting the scope of protection of the present invention.

[0026] It should be noted that similar labels in the following figures indicate similar items; therefore, once an item is defined in one figure, it may not be further defined and explained in subsequent figures.

[0027] This embodiment mainly describes the title of an apparatus for saponifying aluminum tris(ethylphosphonate), as follows:

[0028] Main scheme :

[0029] An apparatus for saponification of aluminum tris(ethylphosphonate), such as Figure 1-5As shown, the device includes a vessel body 10, which contains a reaction chamber. The reaction chamber contains a stirring device 30. The stirring device 30 includes a stirring shaft 300 driven by an external driving device 20 and two types of stirring blades mounted on the stirring shaft 300. The first type of stirring blade is a fixed stirring blade 301 fixed to the stirring shaft 300, and the second type of stirring blade is a movable stirring blade 302 movably mounted on the stirring shaft 300. The side wall of the stirring shaft 300 has a spiral groove. The movable stirring blade 302 has a limiting post extending into the spiral groove. When the driving device 20 drives in the forward direction, the spiral post of the movable stirring blade 302 is located at the highest end of the spiral groove. When the driving device 20 drives in the reverse direction, the spiral post of the movable stirring blade 302 is located at the lowest end of the spiral groove. This solution uses two sets of fixed stirring blades 301 and movable stirring blades 302 to stir the material during stirring. The movable stirring blades 302 are driven by the intermittent forward and reverse rotation of the drive device 20 to change their height and horizontal position. Compared with pure fixed blades, the stirring effect is better and the material is mixed more evenly, which is conducive to the saponification reaction.

[0030] stirring blade section :

[0031] like Figure 2 , 4 As shown in Figure 5, the fixed stirring blade 301 includes an annular fixing sleeve 3013, a plurality of first stirring rods 3011 disposed on the fixing sleeve 3013, and rectangular blades 3012 disposed at the outer end of the first stirring rods 3011. The fixing sleeve 3013 is sleeved and fixed on the stirring shaft 300. A plurality of first stirring rods 3011 are disposed and distributed in an annular array on the fixing sleeve 3013.

[0032] Preferably, the movable stirring blade 302 includes an annular movable sleeve 3022, a plurality of stirring rods disposed on the movable sleeve 3022, and an L-shaped blade 3023 disposed on the outer end of the second stirring rod 3021. The movable sleeve 3022 is sleeved on the stirring shaft 300 and the limiting post is located on the inner wall of the movable sleeve 3022. A plurality of second stirring rods 3021 are disposed and distributed in an annular array on the movable sleeve 3022.

[0033] Preferably, the rectangular blade 3012 is located at the notch above the L-shaped blade 3023 so that the two do not interfere with each other when the L-shaped blade 3023 rises.

[0034] Preferably, the second stirring rod 3021 passes through the movable sleeve 3022 and is fixed on the movable sleeve 3022, and the second stirring rod 3021 extends beyond the inner wall of the movable sleeve 3022 to form a limiting post that extends into the spiral groove.

[0035] Preferably, the end of the limiting post is provided with a roller 30211, which is located within the spiral groove. This design uses the roller 30211 to travel within the spiral groove instead of the limiting post, which can reduce wear and increase service life.

[0036] Preferably, the two types of stirring blades are spaced apart along the axial direction of the stirring shaft 300. The vertical spacing can improve the uniformity of materials at different vertical heights during stirring.

[0037] Driver section :

[0038] like Figure 1 and 2 As shown, the drive device 20 is a bidirectional motor located at the top of the vessel body 10, and the bidirectional motor is connected to the top of the stirring shaft 300.

[0039] Tank body :

[0040] like Figure 2 and 3 As shown, the vessel body 10 includes a tank body 101 at the bottom and a tank cover 102 that is detachably disposed on the top of the tank body 101. The tank cover 102 is provided with several feeding pipe joints 1021 and pressure gauges 1022. The side wall of the tank body 101 is provided with a partition sleeve 1013 and a temperature sensor 1012 for monitoring the internal temperature of the tank body 101. A set of heating pipes 1011 communicating with the internal space of the partition sleeve 1013 is provided at the partition sleeve 1013.

[0041] Preferably, the bottom of the tank 101 is provided with a discharge port, and a ball valve 1014 is provided at the discharge port.

[0042] The title provided above provides a detailed description of the present utility model. Specific examples have been used to illustrate the principles and implementation methods of the present utility model. The description of the above embodiments is only for the purpose of helping to understand the present utility model and its core ideas. It should be noted that for those skilled in the art, several improvements and modifications can be made to the present utility model without departing from the principles of the present utility model, and these improvements and modifications also fall within the protection scope of the claims of the present utility model.

Claims

1. A device for saponification of aluminum triethylphosphinate, comprising a kettle body, a reaction cavity is arranged in the kettle body, characterized in that, The reaction cavity is provided with a stirring device, which comprises a stirring shaft driven by an external driving device and two types of stirring blades arranged on the stirring shaft.

2. The apparatus for saponification reaction of aluminum trisethylphosphinate according to claim 1, characterized in that, The fixed stirring blades comprise a circular ring-shaped fixed sleeve, a plurality of first stirring rods arranged on the fixed sleeve, and rectangular blades arranged at the outer end of the first stirring rods.

3. The apparatus for saponification reaction of aluminum trisethylphosphinate according to claim 2, characterized in that, The movable stirring blades comprise a circular ring-shaped movable sleeve, a plurality of second stirring rods arranged on the movable sleeve, and L-shaped blades arranged at the outer end of the second stirring rods.

4. The apparatus for saponification reaction of aluminum trisethylphosphinate according to claim 3, characterized in that, The rectangular blades are located above the gap of the L-shaped blades, so that the L-shaped blades do not interfere with each other when they are raised.

5. The apparatus for saponification reaction of aluminum triethylphosphinate according to claim 4, characterized in that, The second stirring rods penetrate the movable sleeve and are fixed to the movable sleeve, and the second stirring rods protrude beyond the inner wall of the movable sleeve to form a limiting column that protrudes into the spiral groove.

6. The apparatus for saponification of aluminum triethylphosphinate according to claim 5, characterized in that, The end of the limiting column is provided with a roller, which is located in the spiral groove.

7. The apparatus for saponification of aluminum trisethylphosphonate according to any one of claims 1 to 5, characterized in that, The two types of stirring blades are arranged along the axial direction of the stirring shaft.

8. The apparatus for saponification of aluminum triethylphosphinate according to claim 1, characterized in that, The driving device is a bidirectional motor arranged at the top of the kettle body, and the bidirectional motor is in transmission connection with the top end of the stirring shaft.

9. The apparatus for saponification of aluminum triethylphosphinate according to claim 1, characterized in that, The kettle body comprises a tank body at the bottom and a tank cover detachably arranged at the top of the tank body, a plurality of charging pipe joints and pressure gauges are arranged on the tank cover, a temperature sensor for monitoring the temperature inside the tank body is arranged on the side wall of the tank body, and a group of heating pipes in communication with the inner space of the spacer sleeve are arranged at the spacer sleeve.

10. The apparatus for saponification of aluminum triethylphosphinate according to claim 9, characterized in that, The bottom of the tank body is provided with a discharge port, and the discharge port is provided with a ball valve.

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