Multi-stage concentration and separation device in chlorophyll extraction process

Abstract

The utility model relates to the technical field of chlorophyll extraction, in particular to a multistage concentration and separation device in a chlorophyll extraction process, which comprises an extraction and separation tank, a first heating shell is welded on the surface of the extraction and separation tank, and a crushing component is arranged at the top of the extraction and separation tank. And the two sides of the rear side of the first heating shell are connected with an ethanol tank and a water storage tank through bolts correspondingly. According to the utility model, crushed chips are added into the extraction and separation tank, then high-concentration ethanol is added into the extraction and separation tank, water in the hot water tank is heated through the heater, the second electromagnetic valve and the first electromagnetic valve are controlled to be opened, and then the water in the hot water tank is pumped out through the third water pump and is injected into the first heating shell; water bath heating is conducted on the interior of the extraction and separation tank through hot water in the first heating shell, a first electromagnetic valve and a second electromagnetic valve are closed, a third electromagnetic valve and a fourth electromagnetic valve are opened, and hot water in the hot water tank is pumped into the second heating shell through a third water pump.

Description

Technical Field

[0001] This utility model relates to the field of chlorophyll extraction technology, specifically to a multi-stage concentration and separation device in the chlorophyll extraction process. Background Technology

[0002] Chlorophyll is needed in chemical experiments. To prepare chlorophyll, it is usually necessary to concentrate and separate it during the extraction process, which requires the use of a concentration and separation device.

[0003] A search revealed that the announcement number is CN218653071U, and the name is "A Chlorophyll Extraction Device, including a support base." Research and analysis showed that although it has the advantage of preventing filter paper from falling off during the transfer process and affecting the experimental results, thereby improving the stability of the experiment and the reliability of the experimental data, it also has the following disadvantages to a certain extent.

[0004] During use, this device can only perform single-stage concentration and separation of chlorophyll. The residue after extraction usually contains a lot of chlorophyll, resulting in low extraction efficiency and low chlorophyll concentration, which is not convenient for experiments. In order to solve the above technical problems, we designed a multi-stage concentration and separation device for chlorophyll extraction. Utility Model Content

[0005] The purpose of this invention is to provide a multi-stage concentration and separation device for chlorophyll extraction, which has the advantages of multi-stage concentration and separation. It solves the problem that the device can only perform single-stage concentration and separation of chlorophyll during use, and the residue after extraction usually contains a lot of chlorophyll, resulting in low extraction efficiency and low chlorophyll concentration after extraction, which is not convenient for experiments.

[0006] To achieve the above objectives, this utility model provides the following technical solution: a multi-stage concentration and separation device for chlorophyll extraction, comprising an extraction and separation tank, a first heating shell welded to the surface of the extraction and separation tank, a crushing component disposed on the top of the extraction and separation tank, an ethanol tank and a water storage tank respectively bolted to the rear sides of the first heating shell, a first water pump bolted to the rear side of the ethanol tank, a second water pump bolted to the rear side of the water storage tank, a mixing component disposed on the top of the ethanol tank, and a first solenoid valve connected to the right side of the first heating shell via a pipe. A hot water tank is connected to the right side of the valve. A heater is installed through the top of the hot water tank. A third water pump is bolted to the top of the hot water tank. The pump's suction pipe is connected to the hot water tank via a pipe. The pump's outlet pipe is connected to a second solenoid valve and a third solenoid valve via pipes. A fourth water pump is bolted to the top of the hot water tank. A fourth solenoid valve is connected to the right side of the hot water tank via a pipe. A second heating shell is connected to the right side of the fourth solenoid valve via a pipe. A concentration tank is welded into the inner cavity of the second heating shell. An air pump is bolted to the top of the concentration tank.

[0007] Preferably, the crushing assembly includes a crushing shell, the top of the extraction and separation tank is connected to the crushing shell, the top of the crushing shell is bolted to a first motor, the drive shaft of the first motor is bolted to a wall-breaking rod, both sides of the crushing shell are bolted to electric telescopic rods, the front side of the electric telescopic rod is bolted to a baffle, and the rear side of the baffle extends into the inner cavity of the crushing shell.

[0008] Preferably, the top of the crushing shell is connected to a feeding pipe, and the top of the feeding pipe is threaded with a first pipe cap.

[0009] Preferably, the mixing assembly includes a mixing tank, the bottom of which is bolted to an ethanol tank and a water storage tank respectively. A second motor is bolted to the right side of the mixing tank, and a stirring rod is bolted to the drive shaft of the second motor. An ethanol concentration detector is bolted to the bottom of the right side of the mixing tank. The pump pipe of the first water pump is connected to the ethanol tank through a pipe, and the pump pipe of the second water pump is connected to the water storage tank through a pipe. The rear side of the mixing tank is connected to the first water pump and the second water pump through pipes respectively. A fifth solenoid valve is connected to the bottom of the mixing tank, and the bottom of the fifth solenoid valve is connected to the extraction and separation tank through a pipe.

[0010] Preferably, the top of the ethanol tank is connected to a first liquid filling pipe, and the top of the first liquid filling pipe is threaded with a second pipe cap; the top of the water storage tank is connected to a second liquid filling pipe, and the top of the second liquid filling pipe is threaded with a third pipe cap.

[0011] Preferably, a support frame is welded to the surface of the first heating shell, a fourth tube cap is threaded onto the bottom of the extraction and separation tank, a vacuum gauge is installed on the top of the concentration tank, and a drain valve is connected to the right side of the concentration tank.

[0012] Preferably, the pumping pipe of the fourth water pump extends through a pipe to the inner cavity of the extraction and separation tank and is connected to a filter shell; the outlet pipe of the fourth water pump is connected to the concentration tank through a pipe; a temperature controller is installed on the top of the hot water tank; the right side of the third solenoid valve is connected to the second heating shell through a pipe; a water inlet pipe is connected to the top of the hot water tank; a fifth pipe cap is threaded on the top of the water inlet pipe; a drain pipe is connected to the front of the hot water tank; a sixth pipe cap is threaded on the front of the drain pipe.

[0013] Compared with the prior art, the beneficial effects of this utility model are as follows:

[0014] 1. This utility model involves adding crushed debris into an extraction and separation tank, then adding high-concentration ethanol into the extraction and separation tank. A heater heats the water in a hot water tank. The second and first solenoid valves are opened, and a third water pump draws water from the hot water tank and injects it into a first heating shell. The hot water in the first heating shell heats the extraction and separation tank, promoting the chlorophyll in the debris to dissolve in the high-concentration ethanol. After a period of dissolution, a fourth water pump draws the ethanol concentrate from the extraction and separation tank into a concentration tank. Then, medium-concentration ethanol is added to the extraction and separation tank to dissolve some of the slightly more polar small molecule impurities in the debris, releasing and extracting the chlorophyll that has fused with them. The fourth water pump then draws the ethanol concentrate from the extraction and separation tank into a concentration tank. Finally, low-concentration ethanol is added to the extraction and separation tank to remove water-soluble impurities such as pectin from the debris, facilitating the extraction of chlorophyll. The fourth water pump then draws the ethanol concentrate from the extraction and separation tank into a concentration tank.

[0015] 2. In this invention, the first and second solenoid valves are closed, while the third and fourth solenoid valves are opened. Hot water from the hot water tank is drawn into the second heating shell by the third water pump. The hot water in the second heating shell heats the solution in the concentration tank in a water bath. The concentration tank is evacuated by a vacuum pump to create a low-pressure state. When the pressure is low, the boiling point of the liquid in the concentration tank decreases, and the hot water in the second heating shell boils and concentrates the liquid in the concentration tank. Attached Figure Description

[0016] Figure 1 This is an isometric view of the structure of this utility model;

[0017] Figure 2 This is a perspective view of the crushing shell and baffle of this utility model;

[0018] Figure 3 This is a perspective view of the ethanol tank and the fifth solenoid valve of this utility model;

[0019] Figure 4 This is a perspective view of the extraction and separation tank and the first heating shell of this utility model;

[0020] Figure 5 This is a perspective view of the fourth water pump of this utility model;

[0021] Figure 6 This is a perspective view of the second heating shell and the concentration tank of this utility model.

[0022] In the diagram: 1. Extraction and separation tank; 2. First heating shell; 3. Crushing shell; 4. First motor; 5. Breaking rod; 6. Electric telescopic rod; 7. Baffle; 8. Ethanol tank; 9. Water tank; 10. First water pump; 11. Second water pump; 12. Stirring tank; 13. Second motor; 14. Stirring rod; 15. Ethanol concentration detector; 16. First solenoid valve; 17. Hot water tank; 18. Second solenoid valve; 19. Third water pump; 20. Third solenoid valve; 21. Heater; 22. Fourth water pump; 23. Fourth solenoid valve; 24. Second heating shell; 25. Concentration tank; 26. Vacuum pump; 27. Vacuum gauge; 28. Crushing assembly; 29. ​​Blending assembly; 30. Fifth solenoid valve. Detailed Implementation

[0023] Please see Figures 1-6 A multi-stage concentration and separation device for chlorophyll extraction includes an extraction and separation tank 1. A first heating shell 2 is welded to the surface of the extraction and separation tank 1. A crushing component 28 is installed on the top of the extraction and separation tank 1. An ethanol tank 8 and a water storage tank 9 are bolted to the rear sides of the first heating shell 2, respectively. A first water pump 10 is bolted to the rear side of the ethanol tank 8, and a second water pump 11 is bolted to the rear side of the water storage tank 9. A mixing component 29 is installed on the top of the ethanol tank 8. A first solenoid valve 16 is connected to the right side of the first heating shell 2 via a pipe. A hot water tank 17 is connected to the right side of the first solenoid valve 16. A heater 21 is installed through the top of the hot water tank 17. A third water pump 19 is bolted to the top of the hot water tank 17. The water pump 19's suction pipe is connected to the hot water tank 17 through a pipe. The water pump 19's outlet pipe is connected to the second solenoid valve 18 and the third solenoid valve 20 through pipes. A fourth water pump 22 is bolted to the top of the hot water tank 17. A fourth solenoid valve 23 is connected to the right side of the hot water tank 17 through a pipe. A second heating shell 24 is connected to the right side of the fourth solenoid valve 23 through a pipe. A concentration tank 25 is welded into the inner cavity of the second heating shell 24. A vacuum pump 26 is bolted to the top of the concentration tank 25.

[0024] Please see Figure 1 and Figure 2The crushing component 28 includes a crushing shell 3. By setting the crushing component 28, it is easy to crush the raw materials and extract chlorophyll from the raw materials. The top of the extraction separation tank 1 is connected to the crushing shell 3. The top of the crushing shell 3 is bolted to a first motor 4. The drive shaft of the first motor 4 is bolted to a wall-breaking rod 5. Both sides of the crushing shell 3 are bolted to electric telescopic rods 6. The front side of the electric telescopic rod 6 is bolted to a baffle 7. The rear side of the baffle 7 extends into the inner cavity of the crushing shell 3.

[0025] Please see Figure 1 and Figure 2 The top of the crushing shell 3 is connected to a feeding pipe. By setting the feeding pipe, it is easy to add raw materials into the crushing shell 3 and to crush the raw materials. The top of the feeding pipe is threaded with a first pipe cap.

[0026] Please see Figure 1 and Figure 3 The mixing component 29 includes a mixing tank 12. By setting the mixing component 29, it is easy to adjust the ethanol concentration and add ethanol of different concentrations to the extraction separation tank 1. The bottom of the mixing tank 12 is connected to the ethanol tank 8 and the water storage tank 9 by bolts. The right side of the mixing tank 12 is connected to the second motor 13 by bolts. The drive shaft of the second motor 13 is connected to the stirring rod 14 by bolts. The bottom of the right side of the mixing tank 12 is connected to the ethanol concentration detector 15 by bolts. The water pump pipe of the first water pump 10 is connected to the ethanol tank 8 by a pipe. The water pump pipe of the second water pump 11 is connected to the water storage tank 9 by a pipe. The rear side of the mixing tank 12 is connected to the first water pump 10 and the second water pump 11 by pipes. The bottom of the mixing tank 12 is connected to the fifth solenoid valve 30. The bottom of the fifth solenoid valve 30 is connected to the extraction separation tank 1 by a pipe.

[0027] Please see Figure 1 and Figure 3 The top of the ethanol tank 8 is connected to a first liquid addition pipe, and the top of the first liquid addition pipe is threaded with a second pipe cap. The top of the water storage tank 9 is connected to a second liquid addition pipe. By setting the first liquid addition pipe and the second liquid addition pipe, it is convenient to add ethanol to the ethanol tank 8 and dilution water to the water storage tank 9 respectively. The top of the second liquid addition pipe is threaded with a third pipe cap. By setting the second pipe cap and the third pipe cap, it is convenient to seal the first liquid addition pipe and the second liquid addition pipe respectively.

[0028] Please see Figure 1A support frame is welded to the surface of the first heating shell 2. The support frame can be used to support the extraction separation tank 1 and the first heating shell 2, and can help the device to remain stable. The bottom of the extraction separation tank 1 is threaded with a fourth tube cover. A vacuum gauge 27 is installed on the top of the concentration tank 25. The vacuum gauge 27 can be used to detect the vacuum condition inside the concentration tank 25. A drain valve can be used to drain the concentrated liquid inside the concentration tank 25. A drain valve is connected to the right side of the concentration tank 25.

[0029] Please see Figure 1 , Figure 4 and Figure 5 The suction pipe of the fourth water pump 22 extends into the inner cavity of the extraction and separation tank 1 through a pipeline and is connected to a filter shell. By setting the filter shell, it can play a filtering role and effectively prevent residue from being sucked into the fourth water pump 22. The discharge pipe of the fourth water pump 22 is connected to the concentration tank 25 through a pipeline. A temperature controller is installed on the top of the hot water tank 17. By setting the temperature controller, it is easy to detect and control the temperature of the hot water in the hot water tank 17 and maintain the temperature of the water in the hot water tank 17. The right side of the third solenoid valve 20 is connected to the second heating shell 24 through a pipeline. The top of the hot water tank 17 is connected to a water inlet pipe, and the top of the water inlet pipe is threaded with a fifth pipe cap. The front side of the hot water tank 17 is connected to a drain pipe, and the front side of the drain pipe is threaded with a sixth pipe cap.

[0030] The ethanol concentration detector 15 is model TBD5-EMC1000, an electromagnetic liquid ethanol concentration meter.

[0031] The vacuum gauge 27, model YZ, has both pressure and vacuum measurement functions.

[0032] In use, the device is controlled by an external controller. The raw material to be processed is added into the crushing shell 3. The drive shaft of the first motor 4 drives the wall-breaking rod 5 to rotate, crushing the raw material. Then, the electric telescopic rod 6 moves back and forth, causing the baffle 7 to move forward and backward, adding the crushed raw material from the crushing shell 3 into the extraction and separation tank 1. The first water pump 10 extracts high-concentration ethanol from the ethanol tank 8 and injects it into the mixing tank 12. The second water pump 11 extracts water from the water storage tank 9 and injects it into the mixing tank 12. The drive shaft of the second motor 13 drives the stirring rod 14 to stir the mixing tank 12. The liquid in tank 12 is stirred and mixed, while the ethanol concentration in the mixing tank 12 is monitored by the ethanol concentration detector 15. After the ethanol is adjusted to a suitable concentration, the fifth solenoid valve 30 is opened to add ethanol into the extraction separation tank 1. 95% ethanol is added into the extraction separation tank 1. The water in the hot water tank 17 is heated by the heater 21. The second solenoid valve 18 and the first solenoid valve 16 are opened by controlling the heater. Then, the water in the hot water tank 17 is drawn out by the third water pump 19 and injected into the first heating shell 2. The hot water in the first heating shell 2 provides a water bath heating for the extraction separation tank 1, promoting the extraction of debris in the extraction separation tank 1. Chlorophyll is dissolved in high-concentration ethanol. After a period of time, the ethanol concentrate in extraction tank 1 is pumped into concentration tank 25 by the fourth water pump 22. Then, 70% ethanol is added to extraction tank 1 to dissolve some slightly polar small molecule impurities in the debris, releasing the chlorophyll that has been fused with it. Then, the ethanol concentrate in extraction tank 1 is pumped into concentration tank 25 by the fourth water pump 22. Finally, 40% ethanol is added to extraction tank 1 to remove water-soluble impurities such as pectin in the debris, facilitating the extraction of chlorophyll. Then, the ethanol concentrate is pumped into concentration tank 25 by the fourth water pump. 22. Ethanol from the extraction and separation tank 1 is pumped into the concentration tank 25. The first solenoid valve 16 and the second solenoid valve 18 are closed, and the third solenoid valve 20 and the fourth solenoid valve 23 are opened. Hot water from the hot water tank 17 is pumped into the second heating shell 24 by the third water pump 19. The solution in the concentration tank 25 is heated by the hot water in the second heating shell 24. The concentration tank 25 is evacuated by the vacuum pump 26 to create a low-pressure state. When the pressure is low, the boiling point of the liquid in the concentration tank 25 decreases. The liquid in the concentration tank 25 is then boiled and concentrated by the hot water in the second heating shell 24.

[0033] In summary, this multi-stage concentration and separation device for chlorophyll extraction, through the concentration tank 25, the vacuum pump 26, the vacuum gauge 27, the crushing component 28, the mixing component 29, and the fifth solenoid valve 30, solves the problems that the device can only perform single-stage concentration and separation of chlorophyll during use, and that the residue after extraction usually contains a large amount of chlorophyll, resulting in low extraction efficiency and low chlorophyll concentration after extraction, which is inconvenient for experiments.

Claims

1. A multi-stage concentration and separation device for chlorophyll extraction, comprising an extraction and separation tank (1), characterized in that: The extraction and separation tank (1) is welded with a first heating shell (2). A crushing component (28) is provided on the top of the extraction and separation tank (1). An ethanol tank (8) and a water storage tank (9) are respectively bolted to the two sides of the rear side of the first heating shell (2). A first water pump (10) is bolted to the rear side of the ethanol tank (8). A second water pump (11) is bolted to the rear side of the water storage tank (9). A mixing component (29) is provided on the top of the ethanol tank (8). A first solenoid valve (16) is connected to the right side of the first heating shell (2) through a pipe. A hot water tank (17) is connected to the right side of the first solenoid valve (16). A heater (2) is provided through the top of the hot water tank (17). 1) The top of the hot water tank (17) is connected to a third water pump (19) by bolts. The pump pipe of the third water pump (19) is connected to the hot water tank (17) through a pipe. The outlet pipe of the third water pump (19) is connected to the second solenoid valve (18) and the third solenoid valve (20) through pipes respectively. The top of the hot water tank (17) is connected to a fourth water pump (22) by bolts. The right side of the hot water tank (17) is connected to the fourth solenoid valve (23) through a pipe. The right side of the fourth solenoid valve (23) is connected to the second heating shell (24) through a pipe. The inner cavity of the second heating shell (24) is welded with a concentration tank (25). The top of the concentration tank (25) is connected to a vacuum pump (26) by bolts.

2. The multi-stage concentration and separation device for chlorophyll extraction according to claim 1, characterized in that: The crushing assembly (28) includes a crushing shell (3). The top of the extraction separation tank (1) is connected to the crushing shell (3). The top of the crushing shell (3) is connected to a first motor (4) by bolts. The drive shaft of the first motor (4) is connected to a wall-breaking rod (5) by bolts. Both sides of the crushing shell (3) are connected to electric telescopic rods (6) by bolts. The front side of the electric telescopic rod (6) is connected to a baffle (7) by bolts. The rear side of the baffle (7) extends into the inner cavity of the crushing shell (3).

3. The multi-stage concentration and separation device for chlorophyll extraction according to claim 2, characterized in that: The top of the crushing shell (3) is connected to a feeding pipe, and the top of the feeding pipe is threaded with a first pipe cap.

4. The multi-stage concentration and separation device for chlorophyll extraction according to claim 1, characterized in that: The mixing assembly (29) includes a mixing tank (12). The bottom of the mixing tank (12) is connected to the ethanol tank (8) and the water storage tank (9) by bolts. The right side of the mixing tank (12) is connected to a second motor (13) by bolts. The drive shaft of the second motor (13) is connected to a stirring rod (14) by bolts. The bottom right side of the mixing tank (12) is connected to an ethanol concentration detector (15) by bolts. The pump pipe of the first water pump (10) is connected to the ethanol tank (8) by a pipe. The pump pipe of the second water pump (11) is connected to the water storage tank (9) by a pipe. The rear side of the mixing tank (12) is connected to the first water pump (10) and the second water pump (11) by pipes. The bottom of the mixing tank (12) is connected to a fifth solenoid valve (30). The bottom of the fifth solenoid valve (30) is connected to the extraction separation tank (1) by a pipe.

5. The multi-stage concentration and separation device for chlorophyll extraction according to claim 1, characterized in that: The top of the ethanol tank (8) is connected to a first liquid filling pipe, and the top of the first liquid filling pipe is threaded with a second pipe cap. The top of the water storage tank (9) is connected to a second liquid filling pipe, and the top of the second liquid filling pipe is threaded with a third pipe cap.

6. The multi-stage concentration and separation device for chlorophyll extraction according to claim 1, characterized in that: The surface of the first heating shell (2) is welded with a support frame, the bottom of the extraction separation tank (1) is threaded with a fourth tube cover, the top of the concentration tank (25) is equipped with a vacuum gauge (27), and the right side of the concentration tank (25) is connected to a drain valve.

7. The multi-stage concentration and separation device for chlorophyll extraction according to claim 1, characterized in that: The pumping pipe of the fourth water pump (22) extends through a pipe to the inner cavity of the extraction separation tank (1) and is connected to a filter shell. The outlet pipe of the fourth water pump (22) is connected to the concentration tank (25) through a pipe. A temperature controller is installed on the top of the hot water tank (17). The right side of the third solenoid valve (20) is connected to the second heating shell (24) through a pipe. A water filling pipe is connected to the top of the hot water tank (17). A fifth pipe cap is threaded on the top of the water filling pipe. A drain pipe is connected to the front side of the hot water tank (17). A sixth pipe cap is threaded on the front side of the drain pipe.

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