A condenser system for insecticide workshop and its implementation method
By using titanium wrapping and round hole graphite condensers in the condenser system, combined with hoop smashing components and sealing gaskets, the corrosion, leakage and poor cooling effects of amine kettles, chlorination kettles and vacuum tanks are solved. Achieve longer service life, higher vacuum and lower energy consumption.
Patent Information
- Application Number
- CN202211254421.8
- Authority / Receiving Office
- CN · China
- Patent Type
- Patents(China)
- Current Assignee / Owner
- Filing Date
- 2022-10-13
- Publication Date
- 2024-12-13
- Estimated Expiration
- 2042-10-13
AI Technical Summary
In the existing condenser system, the amine kettle has serious corrosion, and the chlorination kettle has run, leak, drip and leakage. The cooling effect and vacuum degree of the secondary crystallization vacuum tank are poor, and it is difficult to disassemble and has poor sealing performance. Safety hazards and high energy consumption problems.
Using titanium wrap-on type condenser and round hole graphite condenser, combined with hoop assembly and sealing gasket, improve the design of amine kettle, chlorination kettle and vacuum tank, extend service life, improve cooling effect and vacuum degree, and enhance sealing , easy to disassemble and assemble.
Extend the service life of the amine-transferred condenser, reduce leakage in the chlorinated condenser, improve the cooling effect and vacuum degree of the secondary crystallization vacuum tank, reduce the frequency of water replacement, reduce freezing consumption, and improve product quality and safety. sex.
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Figure CN115531906B_ABST
Abstract
Description
Technical Field
[0001] The invention relates to the technical field of condenser systems, and in particular to a condenser system for an insecticide workshop and an implementation method thereof. Background Art
[0002] Chongdan is an organic nephrite poison insecticide with the characteristics of high efficiency, low toxicity and broad spectrum. It is made from raw materials such as allyl chloride and dimethylamine through amination, acidification, dehydration, chlorination, sulfonation, crystallization, separation and other processes to obtain the finished mother liquor of Chongdan, which requires the use of condenser equipment.
[0003] In the existing technology, the amine steaming kettle uses a 40m2 (primary circulating water, primary cold brine) carbon steel tube condenser, which is severely corroded and can no longer be used; the chlorination kettle uses 3 groups of glass condensers (2 groups of circulating water, 1 group of cold brine), which have serious running, bubbling, dripping and leakage during use, and chlorine leakage alarms often occur. The glass material also poses a safety risk; the secondary crystallization vacuum pool uses a 40m2 modified polypropylene graphite condenser, which has poor cooling effect, poor vacuum effect, and frequent water changes in the vacuum pool.
[0004] Secondly, when the air conditioner is installed, the installation site is difficult to disassemble, and the sealing performance of the connection is poor and prone to water leakage. Summary of the invention
[0005] The purpose of the present invention is to provide a condenser system for a single insecticide workshop and an implementation method thereof, so as to extend the service life of an amine vaporizing condenser, save energy and reduce consumption, reduce the running, bubbling, dripping and leakage of a chlorination condenser, eliminate potential safety hazards, improve the cooling effect of a secondary crystallization vacuum pool, increase the vacuum degree, enhance the concentration effect, reduce the frequency of water changes, ensure the sealing inside the inlet head covering shell, prevent leakage, and facilitate disassembly and assembly by means of a hoop smashing assembly, thereby improving practicality, so as to solve the problems raised in the above-mentioned background technology.
[0006] To achieve the above object, the present invention provides the following technical solutions:
[0007] A condenser system for a single insecticide workshop, comprising an amine evaporation kettle, a chlorination kettle and a vacuum tank, wherein both the amine evaporation kettle and the vacuum tank are provided with a titanium winding condenser;
[0008] The titanium wound condenser comprises a shell, an inlet head, an outlet head, a connecting flange, an inlet pipe, an outlet pipe, a heat exchange medium inlet and a heat exchange medium outlet. One end of the shell is connected to the outlet head through a connecting flange, one end of the inlet head is connected to the inlet pipe, one end of the outlet head is connected to the outlet pipe, and the side ends of the shell are respectively provided with a heat exchange medium inlet and a heat exchange medium outlet;
[0009] The chlorination kettle is provided with a round-hole graphite condenser;
[0010] The circular hole graphite condenser comprises a shell, a tube box, a fixed tube sheet, an outer head cover, a floating head, a floating tube sheet, a hook ring, an anti-collision plate and a baffle, a tube box is arranged at one end of the shell, a fixed tube sheet is installed on the inner wall of one end of the shell, an outer head cover is arranged at the other end of the shell, a floating tube sheet is installed on the inner wall of the other end of the shell, a floating head is connected to the side end of the floating tube sheet, a tube box is arranged at one end of the shell, a fixed tube sheet is installed on the inner wall of one end of the shell, an outer head cover is connected at the other end of the shell, a floating head is arranged inside the outer head cover, the outer head cover and the shell are connected by a hook ring, a floating tube sheet is installed on the inner wall of the other end of the shell, and the fixed tube sheet and the floating tube sheet are connected by a tube bundle;
[0011] The amine steaming kettle and the vacuum tank are connected to the titanium winding condenser through a docking device, and the chlorination kettle is connected to the round-hole graphite condenser through a connecting component.
[0012] Furthermore, a partition plate is extended between the fixed tube sheet and the floating tube sheet. The fixed tube sheet divides the tube box into two parts through the partition plate, and the floating head of the floating tube sheet is divided into two spaces through the partition plate. An anti-collision plate is provided on the outer side of the tube bundle. The tube bundle is fitted with the inner wall of the shell through the anti-collision plate, and multiple groups of baffles are provided on the tube bundle.
[0013] Furthermore, the docking device includes a hoop smashing assembly, a condensate recovery pipe, a covering shell, an access pipe and an air injection pipe. The hoop smashing assembly is connected to the top of the covering shell, and the hoop smashing assembly is connected to the bottom end of the shell of the titanium wrapped condenser. The access pipe is connected to the bottom of the covering shell, and the access pipe penetrates the covering shell and is connected to the air injection pipe. A condensate recovery pipe is arranged at the side end of the access pipe, and the condensate recovery pipe is installed at the bottom end of the covering shell.
[0014] Furthermore, the hoop smashing assembly includes a left hoop half ring, a right hoop half ring, a left mounting half ring, a right mounting half ring and an external sleeve ring. The left hoop half ring and the right hoop half ring are sleeved on the outside of the shell, and locking plates are respectively connected to the two ends of the left hoop half ring and the right hoop half ring. The locking plates of the left hoop half ring and the right hoop half ring are locked by bolts. The left mounting half ring is connected to the bottom of the left hoop half ring, and the right mounting half ring is connected to the bottom of the right hoop half ring. The external sleeve ring movably covers the left mounting half ring and the right mounting half ring.
[0015] Furthermore, an internal thread is provided on the inner wall of the external sleeve ring, and an external thread is provided on the outer side walls of the left mounting half ring and the right mounting half ring. The external sleeve ring is movably locked with the left mounting half ring and the right mounting half ring through the thread. An umbrella-mounted rubber sleeve is provided on the inner wall of the external sleeve ring, and a through hole is provided at the bottom end of the umbrella-mounted rubber sleeve. After the hoop smashing assembly is installed, the umbrella-mounted rubber sleeve is covered and arranged at the bottom end of the shell.
[0016] Furthermore, the bottom end of the gas injection pipe is fixed on the covering shell, and the upper end of the gas injection pipe is arranged in the titanium wound condenser. The upper end of the covering shell is connected to the hoop assembly through an internal bearing, and the access pipes of the two sets of docking devices are respectively connected to the amine steaming kettle and the vacuum tank.
[0017] Furthermore, the connecting assembly includes a locking ring, a fixing ring, a docking ring, an inner rubber hose and a sealing gasket. The fixing ring is sleeved on the feed pipe of the round hole graphite condenser. One end of the docking ring is connected to the chlorination kettle through a pipe. The locking ring is sleeved on the surface of the docking ring. The inner end of the docking ring is provided with an inner rubber hose, and the extension of the inner rubber hose is inserted into the fixing ring.
[0018] Furthermore, threads are provided on the surfaces of the fixing ring and the docking ring, the inner wall of the locking ring is locked at the connection between the fixing ring and the docking ring through threads, and the fixing ring and the docking ring are press-fitted and connected by a sealing gasket.
[0019] The present invention provides another technical solution: an implementation method of a condenser system for a single insecticide workshop, comprising the following steps:
[0020] Step 1: The steam generated by the amine steaming kettle and the vacuum tank is transported to the titanium wound condenser through the access pipe and the gas injection pipe. The two ends of the shell are provided with wound pipes for condensation. The steam enters the wound pipes, and the heat exchange medium inlet is injected with the medium for heat exchange. The heat exchange medium outlet draws out the medium after heat exchange, so that the steam in the shell is quickly condensed, and then the condensed gas is discharged through the outlet pipe;
[0021] Step 2: The steam generated by the chlorination kettle is discharged into the round-hole graphite condenser through a pipeline, and condensed when passing through the tube bundle. Water circulates in the shell at the upper end of the partition plate, and the inside of the shell at the lower end of the partition plate is cold salt water. The gas and liquid are separated after condensation and discharged from the upper and lower outlets of the floating head respectively;
[0022] Step 3: When the titanium wound condenser condenses, the condensed water flows down the wound pipe under the action of gravity, flows into the covering shell, and is then discharged from the condensed water recovery pipe.
[0023] Furthermore, with respect to step three, when the titanium wrapped condenser is installed, the left hoop half ring and the right hoop half ring are wrapped around the surface of the titanium wrapped condenser, and when the left installation half ring and the right installation half ring are pressed together, the external sleeve ring is rotated and threadedly screwed onto the outside of the left installation half ring and the right installation half ring.
[0024] Compared with the prior art, the present invention has the following beneficial effects:
[0025] 1. The insecticide single workshop condenser system and its implementation method proposed by the present invention replace the traditional amine evaporation kettle with a 12m2 titanium winding condenser, which prolongs the service life of the amine evaporation condenser, saves energy and reduces consumption, replaces the traditional chlorination kettle with a set of 10m2 round hole graphite condensers, reduces the running, bubbling, dripping and leakage of the chlorination condenser, and eliminates safety hazards, and replaces the vacuum pool with a 100m2 spirally wound tube titanium condenser to improve the cooling effect of the secondary crystallization vacuum pool, improve the vacuum degree, enhance the concentration effect, and reduce the frequency of water change. Due to the good cooling effect of the titanium condenser, the brine flow rate is only half of the previous one, which greatly reduces the refrigeration consumption and the chlorination process. After the replacement of the first condenser, there was basically no leakage, bubbling, dripping or leaking on site, and there has never been an alarm for chlorine leakage from the condenser. The on-site environment has been greatly improved, greatly reducing the workload and maintenance costs of the mechanics. After the secondary crystallization condenser was replaced, the water temperature in the vacuum pool was significantly lower than before, and the vacuum degree was basically stable at above -0.08Mpa. The dehydration time for each batch of materials was shortened by about 1 hour compared with before, saving steam consumption. The frequency of water change in the vacuum pool was significantly lower than before, from once every 2 days to once every 3 days, reducing the discharge of wastewater. Due to the high vacuum degree, the concentration temperature was reduced, the product quality was improved, and the average content of secondary powder was increased by one point.
[0026] 2. The insecticide single workshop condenser system and its implementation method proposed by the present invention, the upper end of the coating shell is connected to the hoop assembly through an internal bearing, and the access pipes of the two sets of docking devices are respectively connected to the amine steaming kettle and the vacuum tank. When the titanium wound condenser condenses, the condensed water flows down along the wound pipe under the action of gravity, flows into the coating shell, and is then discharged from the condensed water recovery pipe. The air injection pipe is inserted and arranged in the inlet head. When the condensed water refluxes, it directly flows into the coating shell along the inlet head to prevent the condensed water from refluxing. To improve the collection efficiency, the umbrella-mounted rubber sleeve is set at the bottom of the shell. When the titanium wrapped condenser is installed, the left hoop half ring and the right hoop half ring are covered on the surface of the titanium wrapped condenser. When the left installation half ring and the right installation half ring are pressed together, the external sleeve ring is rotated and screwed on the outside of the left installation half ring and the right installation half ring. When the external sleeve ring is twisted upward, it drives the umbrella-mounted rubber sleeve to move upward, and the umbrella-mounted rubber sleeve is covered on the outside of the inlet head to ensure the sealing of the inlet head covering shell to prevent leakage. The hoop smashing assembly is convenient for disassembly and assembly, thereby improving practicality.
[0027] 3. The insecticide single-workshop condenser system and implementation method thereof proposed in the present invention have threads on the surfaces of the fixing ring and the docking ring, the inner wall of the locking ring is locked at the connection between the fixing ring and the docking ring by threads, the fixing ring and the docking ring are press-fitted together by a sealing gasket, when connected to the round-hole graphite condenser, the fixing ring and the docking ring are aligned, the locking ring locks the connection between the fixing ring and the docking ring, the internal rubber hose insertion installation ensures the sealing, and ensures the sealing of the connection while facilitating disassembly and assembly. BRIEF DESCRIPTION OF THE DRAWINGS
[0028] Figure 1 It is a schematic diagram of the overall structure of the present invention;
[0029] Figure 2 It is a schematic diagram of the structure of the titanium wound condenser of the present invention;
[0030] Figure 3 It is a cross-sectional view of the structure of the circular hole graphite condenser of the present invention;
[0031] Figure 4 It is a schematic diagram of the structure of the docking device of the present invention;
[0032] Figure 5 It is an exploded view of the docking device structure of the present invention;
[0033] Figure 6 It is a cross-sectional view of the connection structure between the docking device of the present invention and the titanium winding condenser;
[0034] Figure 7 It is a schematic diagram of the structure of the connection assembly of the present invention;
[0035] Figure 8 It is a schematic diagram of the structure of the present invention and an exploded diagram of the structure.
[0036] In the figure: 1, amine steaming kettle; 2, chlorination kettle; 3, vacuum tank; 4, titanium wound condenser; 41, shell; 42, inlet head; 43, outlet head; 44, connecting flange; 45, inlet pipe; 46, outlet pipe; 47, heat exchange medium inlet; 48, heat exchange medium outlet; 5, round hole graphite condenser; 51, shell; 52, tube box; 53, fixed tube sheet; 531, tube bundle; 532, partition plate; 54, outer head cover; 55, floating head; 56, floating tube sheet; 57, hook ring; 58, anti- Punch plate; 59, baffle; 6, docking device; 61, hoop smashing assembly; 611, left hoop half ring; 6111, locking plate; 612, right hoop half ring; 613, left mounting half ring; 614, right mounting half ring; 615, external sleeve ring; 6151, umbrella-mounted rubber sleeve; 62, condensate recovery pipe; 63, covering shell; 631, internal bearing; 64, access pipeline; 65, gas injection pipe; 7, connection assembly; 71, locking ring; 72, fixing ring; 73, docking ring; 74, inner rubber hose; 75, sealing gasket. DETAILED DESCRIPTION
[0037] The following will be combined with the drawings in the embodiments of the present invention to clearly and completely describe the technical solutions in the embodiments of the present invention. Obviously, the described embodiments are only part of the embodiments of the present invention, not all of the embodiments. Based on the embodiments of the present invention, all other embodiments obtained by ordinary technicians in this field without creative work are within the scope of protection of the present invention.
[0038] In order to solve the existing carbon steel tube condenser, the corrosion is serious, the glass condenser has serious leakage, chlorine leakage alarm often occurs, and the glass material also has safety risks; the modified polypropylene graphite condenser has poor cooling effect, poor vacuum effect, and frequent water changes in the vacuum tank, please refer to Figure 1-Figure 3 , this embodiment provides the following technical solutions:
[0039] A condenser system for a single insecticide workshop and an implementation method thereof include an amine steaming kettle 1, a chlorination kettle 2 and a vacuum tank 3. The amine steaming kettle 1 and the vacuum tank 3 are both provided with a titanium wound condenser 4. The titanium wound condenser 4 includes a shell 41, an inlet head 42, an outlet head 43, a connecting flange 44, an inlet pipe 45, an outlet pipe 46, a heat exchange medium inlet 47 and a heat exchange medium outlet 48. One end of the shell 41 is connected to the outlet head 43 through the connecting flange 44, one end of the inlet head 42 is connected to the inlet pipe 45, and one end of the outlet head 43 is connected to the inlet pipe 45. An outlet pipe 46 is connected, and a heat exchange medium inlet 47 and a heat exchange medium outlet 48 are respectively provided at the side ends of the shell 41. The steam generated by the amine steaming kettle 1 and the vacuum pool 3 is transported to the titanium wound condenser 4 through the access pipe 64 and the gas injection pipe 65. Wrapped pipes for condensation are provided at both ends of the shell 41. Steam enters the wrapped pipes, and the heat exchange medium inlet 47 injects the medium for heat exchange. The heat exchange medium outlet 48 extracts the medium after heat exchange, so that the steam in the shell 41 is quickly condensed, and the condensed gas is discharged through the outlet pipe 46.
[0040] A round-hole graphite condenser 5 is provided on the chlorination kettle 2;
[0041] The round hole graphite condenser 5 comprises a shell 51, a tube box 52, a fixed tube sheet 53, an outer head cover 54, a floating head 55, a floating tube sheet 56, a hook ring 57, an anti-collision plate 58 and a baffle 59. The tube box 52 is arranged at one end of the shell 51, the fixed tube sheet 53 is installed on the inner wall of one end of the shell 51, the outer head cover 54 is arranged at the other end of the shell 51, the floating tube sheet 56 is installed on the inner wall of the other end of the shell 51, and the floating head 55 is connected to the side end of the floating tube sheet 56. The tube box 52 is arranged at one end of the shell 51, the fixed tube sheet 53 is installed on the inner wall of one end of the shell 51, the outer head cover 54 is connected at the other end of the shell 51, and the floating head 55 is arranged inside the outer head cover 54. The outer head cover 54 and the shell 51 are press-fitted and connected by the hook ring 57. The inner wall of the other end of the shell 51 is A floating tube sheet 56 is installed, and the fixed tube sheet 53 and the floating tube sheet 56 are connected by a tube bundle 531. The amine steaming kettle 1 and the vacuum pool 3 are connected to the titanium winding condenser 4 through a docking device 6, and the chlorination kettle 2 is connected to the round-hole graphite condenser 5 through a connecting component 7. A partition plate 532 is extended between the fixed tube sheet 53 and the floating tube sheet 56. The fixed tube sheet 53 divides the inside of the tube box 52 into two parts through the partition plate 532. The floating tube sheet 56 is divided into two spaces in the floating head 55 through the partition plate 532. The outer side of the tube bundle 531 is covered with an anti-collision plate 58. The tube bundle 531 is attached to the inner wall of the shell 51 through the anti-collision plate 58. A plurality of baffles 59 are arranged on the tube bundle 531. The steam generated by the chlorination kettle 2 is discharged to the round-hole graphite condenser through a pipeline. In the ink condenser 5, condensation is carried out when passing through the tube bundle 531. Water circulates in the shell 51 at the upper end of the partition plate 532, and the interior of the shell 51 at the lower end of the partition plate 532 is cold brine. The gas and liquid after condensation are separated and discharged from the upper and lower outlets of the floating head 55 respectively. The traditional amine evaporation kettle 1 is replaced with a 12m2 titanium wound condenser 4 to extend the service life of the amine evaporation condenser, save energy and reduce consumption. The traditional chlorination kettle 2 is replaced with a set of 10m2 round hole graphite condensers 5 to reduce the running, bubbling, dripping and leakage of the chlorination condenser and eliminate safety hazards. The vacuum pool 3 is replaced with a 100m2 spirally wound tube titanium condenser to improve the cooling effect of the secondary crystallization vacuum pool 3, improve the vacuum degree, enhance the concentration effect, and reduce the frequency of water replacement. Due to the cooling of the titanium condenser The effect is good. The brine flow rate is only half of the previous one, which greatly reduces the refrigeration consumption. After the condenser of the chlorination section is replaced, there is basically no leakage, bubbling, dripping or leaking on site, and there has never been an alarm for chlorine leakage from the condenser. The on-site environment has been greatly improved, greatly reducing the workload and maintenance costs of the mechanics. After the condenser is replaced for secondary crystallization, the water temperature of vacuum pool 3 is significantly lower than before, and the vacuum degree is basically stable at above -0.08Mpa. The dehydration time of each batch of materials is shortened by about 1 hour compared with before, saving steam consumption. The frequency of water change in vacuum pool 3 is significantly lower than before, from once every 2 days to once every 3 days, reducing the discharge of wastewater. Due to the high vacuum degree, the concentration temperature is reduced, the product quality is improved, and the average content of secondary powder is increased by one point.
[0042] In order to solve the existing problem that the installation location of the air conditioner is difficult to disassemble and the sealing performance of the connection is poor and it is easy to leak, please refer to Figure 4-Figure 6 , this embodiment provides the following technical solutions:
[0043] The docking device 6 includes a hoop smashing assembly 61, a condensate recovery pipe 62, a covering shell 63, an access pipe 64 and an air injection pipe 65. The upper part of the covering shell 63 is connected to the hoop smashing assembly 61, and the hoop smashing assembly 61 is connected to the bottom end of the shell 41 of the titanium wound condenser 4. The lower part of the covering shell 63 is connected to the access pipe 64, and the access pipe 64 penetrates the covering shell 63 and is connected to the air injection pipe 65. The condensate recovery pipe 62 is arranged at the side end of the access pipe 64, and the condensate recovery pipe 62 is installed at the bottom end of the covering shell 63. The bottom end of the air injection pipe 65 is fixed on the covering shell 63, and the upper end of the air injection pipe 65 is fixed to the upper end of the covering shell 63. It is arranged in the titanium wound condenser 4, and the upper end of the sheathing shell 63 is connected to the hoop assembly 61 through the internal bearing 631. The access pipes 64 of the two sets of docking devices 6 are respectively connected to the amine distillation kettle 1 and the vacuum tank 3. When the titanium wound condenser 4 condenses, the condensed water flows down along the wound pipe under the action of gravity, flows into the sheathing shell 63, and is then discharged by the condensed water recovery pipe 62. The gas injection pipe 65 is inserted and arranged in the inlet head 42. When the condensed water refluxes, it directly flows into the sheathing shell 63 along the inlet head 42 to prevent the condensed water from reflux and improve the collection efficiency.
[0044] The hoop assembly 61 includes a left hoop half ring 611, a right hoop half ring 612, a left installation half ring 613, a right installation half ring 614 and an external sleeve ring 615. The left hoop half ring 611 and the right hoop half ring 612 are sleeved on the outside of the shell 41. The two ends of the left hoop half ring 611 and the right hoop half ring 612 are respectively connected with locking plates 6111. The locking plates 6111 of the left hoop half ring 611 and the right hoop half ring 612 are locked by bolts. The left installation half ring 613 is connected to the bottom of the left hoop half ring 611, and the right installation half ring 614 is connected to the bottom of the right hoop half ring 612. The external sleeve ring 615 is movably covered on the left installation half ring 613 and the right installation half ring 614. An internal thread is provided on the inner wall of the external sleeve ring 615, and an external thread is provided on the outer side walls of the left installation half ring 613 and the right installation half ring 614. The external sleeve ring 615 is connected to the left installation half ring 613 and the right installation half ring 614 through threads. The ring 613 and the right mounting half ring 614 are movably locked, and an umbrella-mounted rubber sleeve 6151 is arranged on the inner wall of the external sleeve ring 615, and a through hole is opened at the bottom end of the umbrella-mounted rubber sleeve 6151. After the hoop smashing assembly 61 is installed, the umbrella-mounted rubber sleeve 6151 is covered and arranged on the bottom end of the shell 41. When the titanium material wrapped condenser 4 is installed, the left hoop half ring 611 and the right hoop half ring 612 are covered on the surface of the titanium material wrapped condenser 4. When the left mounting half ring 613 and the right mounting half ring 614 are pressed together, the external sleeve ring 615 is rotated and screwed on the outside of the left mounting half ring 613 and the right mounting half ring 614. When the external sleeve ring 615 is twisted upward, the umbrella-mounted rubber sleeve 6151 is driven to move upward, and the umbrella-mounted rubber sleeve 6151 is covered on the outside of the inlet head 42, so as to ensure the sealing inside the covering shell 63 of the inlet head 42 and prevent leakage. Moreover, the hoop smashing assembly 61 is used to facilitate disassembly and assembly, thereby improving practicality.
[0045] See also Figure 7-Figure 8 The connecting assembly 7 includes a locking ring 71, a fixing ring 72, a docking ring 73, an inner rubber tube 74 and a sealing gasket 75. The fixing ring 72 is sleeved on the feed pipe of the round-hole graphite condenser 5. One end of the docking ring 73 is connected to the chlorination kettle 2 through a pipeline. The locking ring 71 is sleeved on the surface of the docking ring 73. The inner end of the docking ring 73 is provided with an inner rubber tube 74. The extension of the inner rubber tube 74 is inserted and arranged in the fixing ring 72. The surfaces of the fixing ring 72 and the docking ring 73 are both provided with threads. The inner wall of the locking ring 71 is locked at the connection between the fixing ring 72 and the docking ring 73 through threads. The fixing ring 72 and the docking ring 73 are press-fitted and connected by the sealing gasket 75. When connected to the round-hole graphite condenser 5, the fixing ring 72 and the docking ring 73 are aligned, and the locking ring 71 locks the connection between the fixing ring 72 and the docking ring 73. The insertion installation of the inner rubber tube 74 ensures the sealing performance, which ensures the sealing performance of the connection while facilitating disassembly and assembly.
[0046] A method for implementing a condenser system for a single insecticide workshop comprises the following steps:
[0047] Step 1: The steam generated by the amine steaming kettle 1 and the vacuum tank 3 is transported to the titanium wound condenser 4 through the access pipe 64 and the gas injection pipe 65. The two ends of the shell 41 are provided with wound pipes for condensation. The steam enters the wound pipes, and the heat exchange medium inlet 47 injects the medium for heat exchange. The heat exchange medium outlet 48 extracts the medium after heat exchange, so that the steam in the shell 41 is quickly condensed, and then the condensed gas is discharged through the outlet pipe 46;
[0048] Step 2: The steam generated by the chlorination kettle 2 is discharged into the round-hole graphite condenser 5 through a pipeline, and condensed when passing through the tube bundle 531. Water circulates in the shell 51 at the upper end of the partition plate 532, and the inside of the shell 51 at the lower end of the partition plate 532 is cold salt water. The gas and liquid are separated after condensation and discharged from the upper and lower outlets of the floating head 55 respectively;
[0049] Step 3: When the titanium wound condenser 4 condenses, the condensed water flows down along the wound pipe under the action of gravity, flows into the covering shell 63, and is then discharged from the condensed water recovery pipe 62.
[0050] In summary, the insecticide single workshop condenser system and implementation method proposed in the present invention replace the traditional amine evaporation kettle 1 with a 12m2 titanium wound condenser 4, thereby extending the service life of the amine evaporation condenser and saving energy and reducing consumption; replace the traditional chlorination kettle 2 with a set of 10m2 round hole graphite condensers 5, thereby reducing the running, bubbling, dripping and leakage of the chlorination condenser and eliminating safety hazards; replace the vacuum pool 3 with a 100m2 spirally wound tube titanium condenser, thereby improving the cooling effect of the secondary crystallization vacuum pool 3, improving the vacuum degree, enhancing the concentration effect, and reducing the frequency of water changes; due to the good cooling effect of the titanium condenser, the brine flow rate is only half of the previous one, which greatly reduces The refrigeration consumption was reduced. After the condenser of the chlorination section was replaced, there was basically no leakage, bubbling, dripping or leaking on site, and there was never any chlorine leakage alarm of the condenser. The on-site environment was greatly improved, which greatly reduced the workload and maintenance costs of the mechanics. After the condenser was replaced for secondary crystallization, the water temperature of vacuum pool 3 was significantly lower than before, and the vacuum degree was basically stable at above -0.08Mpa. The dehydration time of each batch of materials was shortened by about 1 hour compared with before, saving steam consumption. The frequency of water change in vacuum pool 3 was significantly reduced from once every 2 days to once every 3 days, reducing the discharge of wastewater. Due to the high vacuum degree, the concentration temperature was reduced, the product quality was improved, and the secondary The average powder content is increased by one point. When the titanium wound condenser 4 condenses, the condensed water flows down the wound pipe under the action of gravity, flows into the covering shell 63, and is discharged by the condensed water recovery pipe 62. The gas injection pipe 65 is inserted into the inlet head 42. When the condensed water flows back, it directly flows into the covering shell 63 along the inlet head 42 to prevent the condensed water from flowing back and improve the collection efficiency. The umbrella-mounted rubber sleeve 6151 is covered at the bottom of the shell 41. When the titanium wound condenser 4 is installed, the left hoop half ring 611 and the right hoop half ring 612 are covered on the surface of the titanium wound condenser 4. When the left installation half ring 613 and the right installation half ring 614 are pressed together The external sleeve ring 615 is rotated and screwed on the outside of the left mounting half ring 613 and the right mounting half ring 614. When the external sleeve ring 615 is screwed upward, the umbrella-mounted rubber sleeve 6151 is driven to move upward. The umbrella-mounted rubber sleeve 6151 is covered on the outside of the inlet head 42 to ensure the sealing of the inlet head 42 covering shell 63 to prevent leakage. The hoop assembly 61 is convenient for disassembly and assembly to improve practicality. When connected to the round-hole graphite condenser 5, the fixing ring 72 and the docking ring 73 are aligned, and the locking ring 71 locks the connection between the fixing ring 72 and the docking ring 73. The insertion installation of the inner rubber tube 74 ensures the sealing, which ensures the sealing of the connection while facilitating disassembly and assembly.
[0051] The above description is only a preferred specific implementation manner of the present invention, but the protection scope of the present invention is not limited thereto. Any technician familiar with the technical field can make equivalent replacements or changes according to the technical scheme and inventive concept of the present invention within the technical scope disclosed by the present invention, which should be covered by the protection scope of the present invention.
Claims
1. A condenser system for insecticide single workshop, Features: The invention comprises an amine steaming kettle (1), a chlorination kettle (2) and a vacuum tank (3), wherein the amine steaming kettle (1) and the vacuum tank (3) are both provided with a titanium wound condenser (4), wherein the titanium wound condenser (4) comprises a shell (41), an inlet head (42), an outlet head (43), a connecting flange (44), an inlet pipe (45), an outlet pipe (46), a heat exchange medium inlet (47) and a heat exchange medium outlet (48), wherein one end of the shell (41) is connected to the outlet head (43) via a connecting flange (44), one end of the inlet head (42) is connected to the inlet pipe (45), one end of the outlet head (43) is connected to the outlet pipe (46), and the side ends of the shell (41) are respectively provided with a heat exchange medium inlet (47) and a heat exchange medium outlet (48). The chlorination kettle (2) is provided with a circular-hole graphite condenser (5), and the circular-hole graphite condenser (5) comprises a shell (51), a tube box (52), a fixed tube sheet (53), an outer head cover (54), a floating head (55), a floating tube sheet (56), a hook ring (57), an anti-collision plate (58) and a baffle (59). One end of the shell (51) is provided with a tube box (52), the inner wall of one end of the shell (51) is provided with a fixed tube sheet (53), the outer head cover (54) is provided at the other end of the shell (51), the floating tube sheet (56) is installed on the inner wall of the other end of the shell (51), and the side end of the floating tube sheet (56) is connected to the floating head (55). One end of the shell (51) is provided with a tube box (52), and the shell (5 1) A fixed tube sheet (53) is installed on the inner wall of one end, an outer head cover (54) is connected to the other end of the outer shell (51), a floating head (55) is arranged inside the outer head cover (54), the outer head cover (54) and the outer shell (51) are pressed and connected by a hook ring (57), a floating tube sheet (56) is installed on the inner wall of the other end of the outer shell (51), the fixed tube sheet (53) and the floating tube sheet (56) are connected by a tube bundle (531), the amine steaming kettle (1) and the vacuum pool (3) are connected to the titanium winding condenser (4) through a docking device (6), and the chlorination kettle (2) is connected to the round hole graphite condenser (5) through a connecting assembly (7), and the docking device (6) includes a hoop assembly (61), a condensate recovery pipe (62), a covering shell (63), An access pipe (64) and an air injection pipe (65) are connected. A hoop assembly (61) is connected to the top of the covering shell (63). The hoop assembly (61) is connected to the bottom end of the shell (41) of the titanium wound condenser (4). An access pipe (64) is connected to the bottom of the covering shell (63). The access pipe (64) penetrates the covering shell (63) and is connected to the air injection pipe (65). A condensate recovery pipe (62) is arranged at the side end of the access pipe (64). The condensate recovery pipe (62) is installed at the bottom end of the covering shell (63). The bottom end of the air injection pipe (65) is fixed on the covering shell (63). The upper end of the air injection pipe (65) is arranged in the titanium wound condenser (4). The upper end of the covering shell (63) is connected to the hoop assembly (61) through an internal bearing (631).The access pipes (64) of the two groups of docking devices (6) are respectively connected to the amine steaming kettle (1) and the vacuum tank (3); the hoop assembly (61) comprises a left hoop half ring (611), a right hoop half ring (612), a left installation half ring (613), a right installation half ring (614) and an external sleeve ring (615); the left hoop half ring (611) and the right hoop half ring (612) are sleeved on the outside of the shell (41); the two ends of the left hoop half ring (611) and the right hoop half ring (612) are respectively connected with locking plates (6111), the locking plates (6111) of the left hoop half ring (611) and the right hoop half ring (612) are locked by bolts, the left hoop half ring (611) is connected with a left mounting half ring (613) below, the right hoop half ring (612) is connected with a right mounting half ring (614) below, an external sleeve ring (615) is movably covered on the left mounting half ring (613) and the right mounting half ring (614), the inner wall of the external sleeve ring (615) is provided with an internal thread, the left mounting half ring (61 3) and the outer side wall of the right mounting half ring (614) are provided with external threads, the external sleeve ring (615) is movably locked with the left mounting half ring (613) and the right mounting half ring (614) through the threads, the inner wall of the external sleeve ring (615) is provided with an umbrella-mounted rubber sleeve (6151), and the bottom end of the umbrella-mounted rubber sleeve (6151) is provided with a through hole. After the hoop assembly (61) is installed, the umbrella-mounted rubber sleeve (6151) is covered and arranged on the bottom end of the shell (41), and the left hoop half ring (611) and the right hoop half ring (61 2) Wrapped on the surface of the titanium wound condenser (4), when the left installation half ring (613) and the right installation half ring (614) are pressed together, the external sleeve ring (615) is screwed on the outside of the left installation half ring (613) and the right installation half ring (614), and when the external sleeve ring (615) is screwed upward, the umbrella-mounted rubber sleeve (6151) is driven to move upward, and the umbrella-mounted rubber sleeve (6151) is wrapped on the outside of the inlet head (42), so as to ensure the sealing performance of the inlet head (42) in the covering shell (63).
2. The insecticide single workshop condenser system according to claim 1, Features: A partition plate (532) is provided between the fixed tube sheet (53) and the floating tube sheet (56), and the fixed tube sheet (53) and the floating tube sheet (56) are divided into two areas by the partition plate (532). An anti-collision plate (58) is provided on the outer side of the tube bundle (531), and the tube bundle (531) is attached to the inner wall of the shell (51) through the anti-collision plate (58). A plurality of baffles (59) are provided on the tube bundle (531).
3. The insecticide workshop condenser system according to claim 2, Features: The connection assembly (7) comprises a locking ring (71), a fixing ring (72), a docking ring (73), an inner rubber tube (74) and a sealing gasket (75); the fixing ring (72) is sleeved on the feed pipe of the round-hole graphite condenser (5); one end of the docking ring (73) is connected to the chlorination kettle (2) through a pipe; the locking ring (71) is sleeved on the surface of the docking ring (73); an inner rubber tube (74) is arranged at the inner end of the docking ring (73); and an extension of the inner rubber tube (74) is inserted and arranged in the fixing ring (72).
4. The insecticide workshop condenser system according to claim 3, Features: The surfaces of the fixing ring (72) and the docking ring (73) are both provided with threads, the inner wall of the locking ring (71) is locked at the connection between the fixing ring (72) and the docking ring (73) through threads, and the fixing ring (72) and the docking ring (73) are press-fitted and connected by a sealing gasket (75).
5. A method for implementing the insecticide workshop condenser system according to claim 4, Features: The steps include: Step 1: The steam generated by the amine steaming kettle (1) and the vacuum tank (3) is transported to the titanium wound condenser (4) through the access pipe (64) and the gas injection pipe (65). Wrapped pipes for condensation are provided at both ends of the shell (41). The steam enters the wrapped pipes, and the heat exchange medium inlet (47) injects the medium for heat exchange. The heat exchange medium outlet (48) draws out the medium after heat exchange, so that the steam in the shell (41) is quickly condensed, and the condensed gas is discharged through the outlet pipe (46); Step 2: The steam generated by the chlorination kettle (2) is discharged into the circular hole graphite condenser (5) through a pipeline, and condensed when passing through the tube bundle (531). Water circulates in the shell (51) at the upper end of the partition plate (532), and cold salt water is inside the shell (51) at the lower end of the partition plate (532). After condensation, the gas and liquid are separated and discharged from the upper and lower outlets of the floating head (55) respectively; Step 3: When the titanium wound condenser (4) condenses, the condensed water flows down the wound pipe under the action of gravity, flows into the covering shell (63), and is then discharged from the condensed water recovery pipe (62).
6. The implementation method of the insecticide workshop condenser system according to claim 5, Features: With respect to step three, when the titanium wound condenser (4) is installed, the left hoop half ring (611) and the right hoop half ring (612) are wrapped around the surface of the titanium wound condenser (4), and when the left mounting half ring (613) and the right mounting half ring (614) are pressed together, the external sleeve ring (615) is screwed and fixed to the outside of the left mounting half ring (613) and the right mounting half ring (614).
Citation Information
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