Sodium chlorite synthesis reactor

By designing the spiral conveying blades and bottom mixed flow blades of the inner and outer runners in the sodium chlorite synthesis reactor, the problems of uneven material mixing and gas leakage are solved, and more efficient material mixing and a safer production process are achieved.

CN222446533UActive Publication Date: 2025-02-11SHANDONG GAOMI GAOYUAN CHEM IND CO LTD

Patent Information

Application Number
CN202420836925.9
Authority / Receiving Office
CN · China
Patent Type
Utility models(China)
Current Assignee / Owner
Filing Date
2024-04-22
Publication Date
2025-02-11
Estimated Expiration
2034-04-22

AI Technical Summary

Technical Problem

The existing sodium chlorite synthesis reactor has the problem of flowing in a fixed direction during the material mixing process, which leads to the inability to fully stir and mix the materials. At the same time, when adding raw materials, it is easy to cause irritating gas leakage, endangering the human body and the environment.

Method used

A sodium chlorite synthesis reactor including a kettle body, a separator and a screw conveying blade was designed. By setting an inner flow channel and an outer flow channel in the kettle body, and setting a screw conveying main blade and secondary blade in the inner flow channel and the outer flow channel respectively, the opposite conversion of the material flow direction is achieved. At the same time, a bottom mixing blade and a rectangular flow guide hole are provided to enhance material mixing uniformity, and a flap valve is provided in the feed barrel to prevent gas leakage.

Benefits of technology

The design of the spiral conveying blade and the bottom mixed flow blade with opposite conversion significantly improves the mixing uniformity of the material and reduces production costs and time. At the same time, the design of the flip valve effectively prevents gas leakage and ensures the safety of the human body and the environment.

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Abstract

A sodium chlorite synthesis reactor relates to the technical field of reaction devices and comprises a kettle body, a separation cylinder is coaxially and fixedly connected in the kettle body, an inner flow channel is formed through an inner cavity of the separation cylinder, an outer flow channel is formed between the outer wall of the separation cylinder and the inner wall of the kettle body, and the upper and lower ends of the inner flow channel and the outer flow channel are communicated with the inner cavity of the kettle body. A spiral conveying main blade is rotationally arranged in the inner flow channel, a spiral conveying auxiliary blade is rotationally arranged in the outer flow channel, the spiral conveying main blade and the spiral conveying auxiliary blade are synchronously and rotationally arranged, and the thread rotating direction of the spiral conveying main blade is opposite to that of the spiral conveying auxiliary blade. According to the utility model, the problems that in the preparation and synthesis process of sodium chlorite in the prior art, various materials inside are limited by the influence of an internal flow mixing component and easily flow in a fixed direction, so that the various materials cannot be fully stirred and mixed quickly; and raw materials need to be continuously added during the period, so that when the materials are added during the period, internal stimulation gas is easy to leak.
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Description

Technical Field

[0001] The utility model relates to the technical field of reaction devices, in particular to a sodium chlorite synthesis reactor. Background Art

[0002] Sodium chlorite is a highly efficient oxidant bleaching agent. It is mainly used in cotton spinning, flax, pulp bleaching, food disinfection, water treatment, sterilization and algae removal, and fish medicine manufacturing. The production of sodium chlorite generally involves the reaction of sodium chloride solution, concentrated sulfuric acid and hydrogen peroxide to produce chlorine dioxide, which is then reacted with chlorine dioxide to produce sodium chlorite. During the reaction of chlorine dioxide, the materials need to be stirred in multiple stages to ensure that the materials react fully. Generally, multiple reactors are required, resulting in high production costs and low production efficiency.

[0003] A patent with publication number CN213699826U is disclosed in the prior art. In this scheme, a feed port and a discharge port are respectively provided on the top and bottom of the reactor, a first reaction chamber and a second reaction chamber arranged below the first reaction chamber are arranged in the reactor, a partition is arranged between the first reaction chamber and the second reaction chamber, the partition is provided with a feed port respectively connected to the first reaction chamber and the second reaction chamber, the feed port is provided with a first valve, the feed port is connected to the first reaction chamber, the discharge port is connected to the second reaction chamber, the discharge port is provided with a second valve, the first reaction chamber and the second reaction chamber are respectively provided with a first stirring blade and a second stirring blade, the top and the bottom of the reactor are respectively provided with a first motor and a second motor, the first motor and the second motor respectively drive the first stirring blade and the second stirring blade to rotate, so as to realize multi-stage reaction of materials, effectively reduce production costs, and have high production efficiency.

[0004] As the existing devices are used, the shortcomings of the technology are gradually exposed, mainly in the following aspects:

[0005] First, during the preparation and synthesis process of the existing sodium chlorite, various materials inside are restricted by the influence of the internal mixing components and tend to flow in a fixed direction, and various materials cannot be quickly and fully stirred and mixed.

[0006] Second, during the preparation and synthesis process of sodium chlorite, raw materials need to be continuously added, which makes it easy for the irritating gas inside to leak out when adding materials, causing harm to the human body or the environment.

[0007] In summary, the prior art obviously has inconveniences and defects in practical use, so it is necessary to improve it. Utility Model Content

[0008] In view of the defects in the prior art, the utility model solves the problem that in the preparation and synthesis process of sodium chlorite in the traditional technology, various materials inside are restricted by the influence of the internal mixing component and are easy to flow in a fixed direction, and various materials cannot be quickly and fully stirred and mixed; and raw materials need to be continuously added during the process, which makes it easy for the internal irritating gas to leak out when adding materials, causing harm to the human body or the environment.

[0009] In order to solve the above problems, the utility model provides the following technical solutions:

[0010] A sodium chlorite synthesis reactor comprises a kettle body, wherein a separation cylinder is coaxially fixedly connected to the kettle body, an inner flow channel is formed through the inner cavity of the separation cylinder, an outer flow channel is formed between the outer wall of the separation cylinder and the inner wall of the kettle body, and the upper and lower ends of the inner flow channel and the outer flow channel are both connected to the inner cavity of the kettle body.

[0011] A main spiral conveying blade is provided for rotation in the inner flow channel, and a secondary spiral conveying blade is provided for rotation in the outer flow channel. The main spiral conveying blade and the secondary spiral conveying blade are arranged to rotate synchronously, and the thread rotation direction of the main spiral conveying blade is opposite to the thread rotation direction of the secondary spiral conveying blade.

[0012] As an optimized solution, the kettle body is internally provided with bottom mixing flow blades which are in frictional contact with the inner bottom surface thereof.

[0013] As an optimized solution, a feed barrel is fixedly connected to the top of the kettle body, and two flap valves are arranged in parallel from top to bottom in the feed barrel.

[0014] As an optimized solution, rectangular guide holes are horizontally opened on the bottom mixed flow blade.

[0015] As an optimized solution, the upper and lower edges of the rectangular guide hole are inclined.

[0016] As an optimized solution, the inner bottom surface of the kettle body is concavely arranged, and the lower end of the bottom mixed flow blade matches the inner bottom surface of the kettle body.

[0017] As an optimized solution, a discharge valve connected to the inner cavity of the kettle body is fixedly connected to the bottom of the kettle body, and the discharge valve is located at the center of the bottom of the kettle body.

[0018] As an optimized solution, a main shaft is vertically rotated in the kettle body, and two bottom mixed flow blades are oppositely arranged, and the inner ends are fixedly connected to the opposite side walls of the main shaft near the lower end.

[0019] As an optimized solution, the inner edge of the main spiral conveying blade is fixedly connected to the main shaft, and the outer edge of the main spiral conveying blade is in frictional contact with the inner wall of the partition cylinder.

[0020] As an optimized solution, the inner edge of the spiral conveying auxiliary blade is in frictional contact with the outer wall of the separating cylinder, the outer edge of the spiral conveying auxiliary blade is in frictional contact with the inner wall of the kettle body, and the upper end of the spiral conveying auxiliary blade is fixed to the main shaft through a connecting rod.

[0021] As an optimized solution, a driving machine is fixedly connected to the outer top of the kettle body, and the output end of the driving machine is fixedly connected to the upper end of the main shaft.

[0022] Compared with the prior art, the beneficial effects of the utility model are:

[0023] The main shaft is driven to rotate by the driving machine, thereby driving the main blade of the spiral conveying and the auxiliary blade of the spiral conveying to rotate. Since the thread rotation direction of the main blade of the spiral conveying is opposite to the thread rotation direction of the auxiliary blade of the spiral conveying, the flow direction of the materials in the inner flow channel and the outer flow channel is reversed, thereby improving the mixing uniformity of the internal materials. The main shaft is controlled by the driving machine to rotate forward and reverse, thereby realizing the conversion of the flow direction of the materials in the inner flow channel and the outer flow channel, thereby improving the mixing uniformity of various materials. The lower end of the main shaft is connected to the bottom mixing blade to realize stirring and mixing of the materials flowing to the bottom. By setting a rectangular guide hole and slanting the upper and lower edges, secondary guide mixing of the materials is realized, thereby greatly improving the mixing uniformity of various materials.

[0024] By arranging two flap valves in parallel from top to bottom on the feed barrel, when adding materials or additives into the kettle body, the two flap valves are opened alternately, which can prevent the internal toxic gas or irritating gas from leaking out and prevent harm to the human body or the environment. BRIEF DESCRIPTION OF THE DRAWINGS

[0025] In order to more clearly illustrate the specific implementation of the utility model or the technical solution in the prior art, the following is a brief introduction to the drawings required for the specific implementation or the prior art description. In all the drawings, similar elements or parts are generally identified by similar reference numerals. In the drawings, each element or part is not necessarily drawn according to the actual scale.

[0026] Figure 1 It is a schematic diagram of the structure of the utility model;

[0027] Figure 2 It is a structural schematic diagram of the utility model.

[0028] In the figure: 1- kettle body; 2- partition cylinder; 3- inner flow channel; 4- outer flow channel; 5- spiral conveying main blade; 6- spiral conveying auxiliary blade; 7- bottom mixing flow blade; 8- rectangular guide hole; 9- main shaft; 10- discharge valve; 11- support rod; 12- connecting rod; 13- driving machine; 14- feeding cylinder; 15- flap valve. DETAILED DESCRIPTION

[0029] The following embodiments of the technical solution of the utility model are described in detail in conjunction with the accompanying drawings. The following embodiments are only used to more clearly illustrate the technical solution of the utility model, and are therefore only used as examples, and cannot be used to limit the protection scope of the utility model.

[0030] like Figure 1 and Figure 2 As shown, the sodium chlorite synthesis reactor comprises a kettle body 1, a separation cylinder 2 is coaxially fixedly connected in the kettle body 1, and an inner flow channel 3 is formed through the inner cavity of the separation cylinder 2, and an outer flow channel 4 is formed between the outer wall of the separation cylinder 2 and the inner wall of the kettle body 1, and the upper and lower ends of the inner flow channel 3 and the outer flow channel 4 are both connected to the inner cavity of the kettle body 1.

[0031] A spiral conveying main blade 5 is rotated in the inner flow channel 3, and a spiral conveying auxiliary blade 6 is rotated in the outer flow channel 4. The spiral conveying main blade 5 and the spiral conveying auxiliary blade 6 are rotated synchronously, and the thread rotation direction of the spiral conveying main blade 5 is opposite to that of the spiral conveying auxiliary blade 6.

[0032] Two support rods 11 are respectively fixed to the lower end of the separation cylinder 2 , and the support rods 11 are fixed to the inner wall of the kettle body 1 to fix the separation cylinder 2 .

[0033] A bottom mixing flow blade 7 is rotatably provided inside the kettle body 1 and is in frictional contact with the inner bottom surface thereof.

[0034] A feed barrel 14 is fixedly connected to the top of the kettle body 1 , and two flap valves 15 are arranged in parallel from top to bottom in the feed barrel 14 .

[0035] A rectangular flow guide hole 8 is horizontally opened on the bottom mixed flow blade 7 .

[0036] The upper and lower edges of the rectangular guide hole 8 are arranged inclined.

[0037] The inner bottom surface of the kettle body 1 is concavely arranged, and the lower end of the bottom mixed flow blade 7 matches the inner bottom surface of the kettle body 1 .

[0038] A discharge valve 10 communicating with the inner cavity of the kettle body 1 is fixedly connected to the bottom of the kettle body 1 . The discharge valve 10 is located at the center of the bottom of the kettle body 1 .

[0039] A main shaft 9 is vertically rotatably arranged in the kettle body 1, and two bottom mixed flow blades 7 are oppositely arranged, and the inner ends are fixedly connected to the opposite side walls of the main shaft 9 near the lower end.

[0040] The inner edge of the main spiral conveying blade 5 is fixedly connected to the main shaft 9 , and the outer edge of the main spiral conveying blade is in frictional contact with the inner wall of the partition cylinder 2 .

[0041] The inner edge of the spiral conveying auxiliary blade 6 is in frictional contact with the outer wall of the separation tube 2 , the outer edge of the spiral conveying auxiliary blade 6 is in frictional contact with the inner wall of the kettle body 1 , and the upper end of the spiral conveying auxiliary blade 6 is fixedly connected to the main shaft 9 through a connecting rod 12 .

[0042] A driving machine 13 is fixedly connected to the outer top of the kettle body 1 , and an output end of the driving machine 13 is fixedly connected to the upper end of the main shaft 9 .

[0043] The kettle body 1 is also provided with other pipe openings, such as pressure balance holes, inspection holes and other structures, which are common in daily life and do not belong to the innovation of this solution, so they are not described in detail here.

[0044] The working principle of this device is:

[0045] The main shaft 9 is driven to rotate by the driving machine 13, and then the main spiral conveying blade 5 and the secondary spiral conveying blade 6 are driven to rotate. Since the thread rotation direction of the main spiral conveying blade 5 is opposite to the thread rotation direction of the secondary spiral conveying blade 6, the flow direction of the materials in the inner flow channel 3 and the outer flow channel 4 is reversed, and the mixing uniformity of the internal materials is improved. The main shaft 9 is controlled by the driving machine 13 to rotate forward and reverse, so as to realize the conversion of the flow direction of the materials in the inner flow channel 3 and the outer flow channel 4, and improve the mixing uniformity of various materials; wherein the lower end of the main shaft 9 is connected to the bottom mixing blade 7, so as to realize the stirring and mixing of the materials flowing to the bottom, and by setting the rectangular guide hole 8, and the upper and lower edges are inclined, the materials are secondary guided and mixed, which greatly improves the mixing uniformity of various materials;

[0046] By arranging two flap valves 15 in parallel from top to bottom on the feed barrel 14, when adding materials or additives into the kettle body 1, the two flap valves 15 are opened alternately to prevent the internal toxic gas or irritating gas from leaking out and preventing harm to the human body or the environment.

[0047] Finally, it should be noted that the above embodiments are only used to illustrate the technical solution of the utility model, rather than to limit it. Although the utility model has been described in detail with reference to the aforementioned embodiments, those skilled in the art should understand that they can still modify the technical solutions described in the aforementioned embodiments, or replace some or all of the technical features therein by equivalents. These modifications or replacements do not make the essence of the corresponding technical solutions deviate from the scope of the technical solutions of the embodiments of the utility model, and they should all be included in the scope of the claims and specification of the utility model.

Claims

1. Sodium chlorite synthesis reactor, characterized in that: The invention comprises a kettle body (1), wherein a separation cylinder (2) is coaxially fixedly connected inside the kettle body (1), an inner flow channel (3) is formed through the inner cavity of the separation cylinder (2), an outer flow channel (4) is formed between the outer wall of the separation cylinder (2) and the inner wall of the kettle body (1), and the upper and lower ends of the inner flow channel (3) and the outer flow channel (4) are both connected to the inner cavity of the kettle body (1). A main spiral conveying blade (5) is rotatably arranged in the inner flow channel (3), and a secondary spiral conveying blade (6) is rotatably arranged in the outer flow channel (4). The main spiral conveying blade (5) and the secondary spiral conveying blade (6) are arranged to rotate synchronously, and the thread rotation direction of the main spiral conveying blade (5) is opposite to the thread rotation direction of the secondary spiral conveying blade (6).

2. The sodium chlorite synthesis reactor according to claim 1, wherein: The kettle body (1) is internally provided with a bottom mixing flow blade (7) which is in frictional contact with the inner bottom surface thereof and is rotatably provided therein.

3. The sodium chlorite synthesis reactor according to claim 2, characterized in that: A feed cylinder (14) is fixedly connected to the top of the kettle body (1), and two flap valves (15) are arranged in parallel from top to bottom in the feed cylinder (14).

4. The sodium chlorite synthesis reactor according to claim 3, characterized in that: A rectangular flow guide hole (8) is horizontally opened on the bottom mixed flow blade (7), and the upper and lower edges of the rectangular flow guide hole (8) are inclined.

5. The sodium chlorite synthesis reactor according to claim 4, characterized in that: The inner bottom surface of the kettle body (1) is arranged in a concave manner, and the lower end of the bottom mixed flow blade (7) matches the inner bottom surface of the kettle body (1).

6. The sodium chlorite synthesis reactor according to claim 5, characterized in that: The bottom of the kettle body (1) is fixedly connected with a discharge valve (10) communicating with the inner cavity thereof, and the discharge valve (10) is located at the center of the bottom of the kettle body (1).

7. The sodium chlorite synthesis reactor according to claim 6, characterized in that: A main shaft (9) is vertically rotatably arranged in the kettle body (1), and two bottom mixed flow blades (7) are arranged opposite to each other, and the inner ends are fixedly connected to the opposite side walls of the main shaft (9) near the lower end.

8. The sodium chlorite synthesis reactor according to claim 7, characterized in that: The inner edge of the main spiral conveying blade (5) is fixedly connected to the main shaft (9), and the outer edge of the main spiral conveying blade is in frictional contact with the inner wall of the separation cylinder (2).

9. The sodium chlorite synthesis reactor according to claim 8, characterized in that: The inner edge of the spiral conveying auxiliary blade (6) is in frictional contact with the outer wall of the separation cylinder (2), the outer edge of the spiral conveying auxiliary blade (6) is in frictional contact with the inner wall of the kettle body (1), and the upper end of the spiral conveying auxiliary blade (6) is fixedly connected to the main shaft (9) through a connecting rod (12).

10. The sodium chlorite synthesis reactor according to claim 9, characterized in that: A driving machine (13) is fixedly connected to the outer top of the kettle body (1), and the output end of the driving machine (13) is fixedly connected to the upper end of the main shaft (9).

Citation Information

Patent Citations

  • Multi-stage reaction kettle for sodium chlorite production

    CN213699826U

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