Solvent recovery device based on macroporous resin adsorption

By using a flattening mechanism and a adjustment mechanism in the macroporous resin adsorption tank, the macroporous resin is flattened to increase the contact area with high-temperature steam, the problem of insufficient reaction in the prior art resulting in low solvent extraction rate is solved, and more efficient solvent recovery and resin replacement are achieved.

CN222550184UActive Publication Date: 2025-03-04JIANGSU YONGAN CHEM CO LTD
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Patent Information

Application Number
CN202420895694.9
Authority / Receiving Office
CN · China
Patent Type
Utility models(China)
Current Assignee / Owner
Filing Date
2024-04-26
Publication Date
2025-03-04
Estimated Expiration
2034-04-26

AI Technical Summary

Technical Problem

In the existing macroporous resin adsorption tank, the resin is placed in a manner that accumulates, resulting in a low reaction rate between steam and macroporous resin, and insufficient reaction, resulting in a decrease in solvent extraction rate.

Method used

A solvent recovery device based on adsorption of large pore resin is designed, using a flattening mechanism and a adjustment mechanism, which drives the screw and threaded seat to move through the motor, drives the scraper to flatten the large pore resin, increase the contact area with high-temperature steam, and facilitates the replacement of the resin through the adjustment mechanism.

Benefits of technology

By flattening the macroporous resin, the contact area with high-temperature steam is increased, the problem of insufficient reaction is solved, the solvent extraction rate is improved, and the resin replacement and protection is facilitated.

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Abstract

The utility model discloses a solvent recovery device based on macroporous resin adsorption, relates to the technical field of resin solvent recovery, and adopts the technical scheme that a flattening mechanism comprises a plurality of groups of motors, one side of each group of motor is mounted on one side of a shell, and the other side of each group of motor is mounted on the other side of the shell; output shafts of the multiple sets of motors penetrate through one side of the shell and are connected with one end of a screw rod, the other end of the screw rod is installed in the shell through a bearing, the outer surface of the screw rod is in threaded connection with a threaded seat, and the lower portion of a transverse plate is connected with a scraping plate through an adjusting mechanism. The scraper is driven to move, macroporous resin placed above the filter plate is flattened, the contact area of the macroporous resin and high-temperature steam is increased, the macroporous resin can fully react with the high-temperature steam, and therefore the problem that the extraction rate of a solvent is reduced due to the fact that part of the macroporous resin and the high-temperature steam are not fully reacted is solved.
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Description

Technical Field

[0001] The utility model relates to the technical field of resin solvent recovery, and more specifically, to a solvent recovery device based on macroporous resin adsorption. Background Art

[0002] Macroporous resin is a polymer adsorption resin with a special macroporous structure. It is formed by a specific synthesis method to form a large number of pores in the polymer network. The diameter of these pores is generally greater than 2 nanometers, and some can even reach hundreds of nanometers, so they are called "macroporous". Macroporous resins are characterized by high specific surface area and pore volume, which makes them excellent in adsorption performance and can effectively adsorb various molecules, including organic, inorganic and biological macromolecules.

[0003] In some chemical production processes, solvent utilization efficiency and cost control are very important factors. By using macroporous resins to adsorb and recover solvents, production costs can be greatly reduced and environmental pollution can be reduced.

[0004] The existing solvent recovery device for macroporous resin adsorption introduces high-temperature steam into a resin adsorption tank containing macroporous resin. The water vapor in the steam desorbs the substances adsorbed on the macroporous resin again, forming a liquid that flows into a condenser through a pipeline for cooling. The cooled liquid passes through a stratification device to separate the solvent from water, thereby achieving the purpose of solvent recovery. However, in the existing resin adsorption tank, the resins are mostly stacked, resulting in a low reaction rate between the steam added to the resin adsorption tank and the macroporous resin, and may cause a situation where some macroporous resins do not react fully with the high-temperature steam, resulting in a reduced solvent extraction rate.

[0005] Therefore, in order to solve the above technical problems, the present application proposes a solvent recovery device based on macroporous resin adsorption. Utility Model Content

[0006] In view of the shortcomings of the prior art, the purpose of the utility model is to provide a solvent recovery device based on macroporous resin adsorption.

[0007] To achieve the above-mentioned purpose, the utility model provides the following technical solution: a solvent recovery device based on macroporous resin adsorption comprises a workbench and a scraper, and a shell is connected to the top of the workbench;

[0008] A flattening mechanism is arranged inside the shell and is used to flatten the macroporous resin placed inside the shell;

[0009] An adjustment mechanism is arranged inside the housing and is used to adjust the position of the scraper;

[0010] The flattening mechanism includes a motor, and the number of the motors is multiple groups. One side of the multiple groups of motors is installed on one side of the shell, and the output shafts of the multiple groups of motors pass through one side of the shell and are connected to one end of the screw. The other end of the screw is installed in the shell through a bearing. The outer surface of the screw is threadedly connected to a threaded seat, one side of the threaded seat is connected to a cross plate, and the bottom of the cross plate is connected to a scraper through an adjustment mechanism.

[0011] Preferably, a plurality of groups of filter plates are connected inside the shell, and a macroporous resin is placed above the filter plates. The water vapor in the steam causes the adsorbed substances on the macroporous resin to be desorbed again, forming a liquid that passes through the filter plates.

[0012] Preferably, the adjustment mechanism includes bolts, and the bottom of the cross plate is connected to two groups of mounting blocks. One side of the two groups of mounting blocks is provided with threaded holes. One side of the scraper is penetrated by a first through hole and a second through hole. The outer surface of the bolt can penetrate the first through hole or the second through hole and be threadedly connected to the threaded hole. The bolt passes through the first through hole to connect to the mounting block, so that the scraper is at a certain distance from the filter plate to flatten the macroporous resin. The bolt passes through the second through hole to connect to the mounting block, so that the scraper is close to the filter plate to push away the macroporous resin placed on the filter plate.

[0013] Preferably, a gap is formed between one end of the filter plate and the inner wall of the shell, and the pushed macroporous resin falls from the gap to the bottom of the shell, which is convenient for removal.

[0014] Preferably, the inner wall of the shell is connected to multiple groups of baffles to prevent the macroporous resin from moving to the bottom of the screw, thereby avoiding damage to the macroporous resin due to movement of the threaded seat.

[0015] Preferably, the top of the shell is connected to the steam pipe, the bottom of the shell is connected to one end of the first pipe, the other end of the first pipe is connected to the top of the condenser, the bottom of the condenser is connected to one end of the second pipe, the other end of the second pipe is connected to the stratification device, the two sides of the stratification device are symmetrically connected to one end of the third pipe, and the other ends of the two groups of third pipes are respectively connected to the solvent tank and the wastewater tank.

[0016] Preferably, the top of the workbench is connected to a condenser, a layering device, a solvent tank and a waste water tank.

[0017] Preferably, a door is installed at the opening of the shell to facilitate replacement of the macroporous resin inside the shell.

[0018] Compared with the prior art, the utility model has the following beneficial effects:

[0019] 1. By setting up a flattening mechanism, the motor can be controlled to drive the screw to rotate, drive the threaded seat to move, drive the scraper to move, flatten the macroporous resin placed on the filter plate, increase the contact area between the macroporous resin and the high-temperature steam, and enable the macroporous resin to fully react with the high-temperature steam, thereby solving the problem of insufficient reaction between some macroporous resins and high-temperature steam, resulting in a reduced solvent extraction rate.

[0020] 2. By adjusting the mechanism and the gap, the bolt can be passed through the second through hole to thread the threaded block, so that the scraper is close to the filter plate. The scraper is driven to move by the control motor to push the macroporous resin above the filter plate to fall from the gap to the bottom of the shell, which is convenient for replacing the macroporous resin in the shell.

[0021] 3. By setting a baffle, the macroporous resin can be prevented from moving to the bottom of the screw, thereby avoiding damage to the macroporous resin caused by the movement of the threaded seat. BRIEF DESCRIPTION OF THE DRAWINGS

[0022] The drawings described herein are used to provide a further understanding of the present invention and constitute a part of the present application. The illustrative embodiments of the present invention and their descriptions are used to explain the present invention and do not constitute an improper limitation on the present invention. In the drawings:

[0023] Figure 1 It is a structural schematic diagram of the utility model;

[0024] Figure 2 It is a structural schematic diagram of the housing in the utility model;

[0025] Figure 3 It is a structural schematic diagram of the filter plate in the utility model;

[0026] Figure 4 It is a structural schematic diagram of the installation block in the utility model;

[0027] Figure 5 It is a structural schematic diagram of the threaded hole in the utility model;

[0028] 1. Shell; 2. Motor; 3. Door; 4. Workbench; 5. First pipeline; 6. Solvent tank; 7. Stratification device; 8. Wastewater tank; 9. Condenser; 10. Steam pipe; 11. Threaded seat; 12. Baffle; 13. Bearing; 14. Screw; 15. Cross plate; 16. Filter plate; 17. Gap; 18. Mounting block; 19. Bolt; 20. Threaded hole; 21. First through hole; 22. Second through hole; 23. Scraper; 24. Second pipeline. DETAILED DESCRIPTION

[0029] like Figure 1 - Figure 5As shown, the utility model provides a solvent recovery device based on macroporous resin adsorption, comprising a workbench 4 and a scraper 23, and a shell 1 is connected to the top of the workbench 4;

[0030] The flattening mechanism is arranged inside the shell 1 and is used to flatten the macroporous resin placed inside the shell 1;

[0031] An adjustment mechanism, disposed inside the housing 1, for adjusting the position of the scraper 23;

[0032] The flattening mechanism includes a motor 2, and the number of motors 2 is multiple, and one side of the multiple motors 2 is installed on the side of the housing 1. The output shafts of the multiple motors 2 pass through the side of the housing 1 and are connected to one end of a screw 14. The other end of the screw 14 is installed in the housing 1 through a bearing 13. The outer surface of the screw 14 is threadedly connected to a threaded seat 11. One side of the threaded seat 11 is connected to a horizontal plate 15. The bottom of the horizontal plate 15 is connected to a scraper 23 through an adjustment mechanism.

[0033] Multiple groups of filter plates 16 are connected inside the housing 1, and macroporous resin is placed above the filter plates 16;

[0034] The adjustment mechanism includes a bolt 19, and the bottom of the horizontal plate 15 is connected to two groups of mounting blocks 18. The two groups of mounting blocks 18 have threaded holes 20 on one side. The scraper 23 has a first through hole 21 and a second through hole 22 on one side. The outer surface of the bolt 19 can penetrate the first through hole 21 or the second through hole 22 and be threadedly connected to the threaded hole 20.

[0035] The inner wall of the shell 1 is connected to multiple groups of baffles 12;

[0036] The top of the shell 1 is connected to the steam pipe 10, the bottom of the shell 1 is connected to one end of the first pipe 5, the other end of the first pipe 5 is connected to the top of the condenser 9, the bottom of the condenser 9 is connected to one end of the second pipe 24, the other end of the second pipe 24 is connected to the layering device 7, the two sides of the layering device 7 are symmetrically connected to one end of the third pipe, and the other ends of the two sets of third pipes are respectively connected to the solvent tank 6 and the wastewater tank 8;

[0037] The top of the workbench 4 is connected to a condenser 9, a layering device 7, a solvent tank 6 and a waste water tank 8;

[0038] A door 3 is installed at the opening of the housing 1;

[0039] One end of the filter plate 16 forms a gap 17 with the inner wall of the housing 1;

[0040] The macroporous resin is placed above each group of filter plates 16, and the screw 19 is threadedly connected to the threaded hole 20 provided in the mounting block 18 through the first through hole 21, and the scraper 23 is installed below the cross plate 15. At this time, the bottom of the scraper 23 is still a certain distance away from the filter plate 16. The motor 2 is controlled to drive the screw 14 to rotate, drive the threaded seat 11 to move, and drive the scraper 23 to move, so as to flatten the macroporous resin placed on the filter plate 16, increase the contact area between the macroporous resin and the high-temperature steam, and then input the high-temperature steam through the steam pipe 10, and the water vapor in the steam causes the substances adsorbed on the macroporous resin to be desorbed again, forming a liquid that flows into the condenser 9 through the pipeline. Cooling, the cooled liquid passes through the stratification device 7 to separate the solvent and water, the water is transported to the wastewater tank 8, and the solvent is transported to the solvent tank 6. The scraper 23 is installed under the cross plate 15 by threading the bolt 19 through the second through hole 22 to the threaded hole 20 opened in the mounting block 18. At this time, the bottom of the scraper 23 is close to the mounting plate, and the control motor 2 drives the scraper 23 to move, pushing the macroporous resin above the filter plate 16 to fall from the gap 17 to the bottom of the shell 1, so as to facilitate the replacement of the macroporous resin in the shell 1. The baffle 12 can prevent the macroporous resin from moving to the bottom of the screw 14, avoiding the damage of the macroporous resin caused by the movement of the threaded seat 11.

[0041] The above are only preferred embodiments of the present invention and are not intended to limit the present invention in any form. Any ordinary technician in the industry can smoothly implement the present invention as shown in the drawings and described above. However, any equivalent changes, modifications and evolutions made by technicians familiar with the profession without departing from the scope of the technical solution of the present invention using the technical content disclosed above are all equivalent embodiments of the present invention. At the same time, any equivalent changes, modifications and evolutions made to the above embodiments based on the essential technology of the present invention are still within the protection scope of the technical solution of the present invention.

Claims

1. A solvent recovery device based on macroporous resin adsorption, characterized in that: It comprises a workbench (4) and a scraper (23), wherein the top of the workbench (4) is connected to a housing (1); A flattening mechanism is arranged inside the shell (1) and is used to flatten the macroporous resin placed inside the shell (1); An adjustment mechanism, arranged inside the housing (1) and used for adjusting the position of the scraper (23); The flattening mechanism comprises a motor (2), wherein the motor (2) is provided in a plurality of groups, one side of each of the plurality of motors (2) is mounted on one side of a housing (1), the output shafts of each of the plurality of motors (2) pass through one side of the housing (1) and are connected to one end of a screw rod (14), the other end of the screw rod (14) is mounted in the housing (1) via a bearing (13), the outer surface of the screw rod (14) is threadedly connected to a threaded seat (11), one side of the threaded seat (11) is connected to a transverse plate (15), and the bottom of the transverse plate (15) is connected to a scraper (23) via an adjustment mechanism.

2. A solvent recovery device based on macroporous resin adsorption according to claim 1, characterized in that: A plurality of groups of filter plates (16) are connected inside the shell (1), and macroporous resin is placed above the filter plates (16).

3. A solvent recovery device based on macroporous resin adsorption according to claim 2, characterized in that: The adjustment mechanism comprises a bolt (19), the bottom of the horizontal plate (15) is connected to two groups of mounting blocks (18), one side of the two groups of mounting blocks (18) is provided with a threaded hole (20), one side of the scraper (23) is provided with a first through hole (21) and a second through hole (22), and the outer surface of the bolt (19) can penetrate the first through hole (21) or the second through hole (22) to be threadedly connected to the threaded hole (20).

4. A solvent recovery device based on macroporous resin adsorption according to claim 3, characterized in that: One end of the filter plate (16) forms a gap (17) with the inner wall of the housing (1).

5. A solvent recovery device based on macroporous resin adsorption according to claim 4, characterized in that: The inner wall of the shell (1) is connected to a plurality of groups of baffles (12).

6. A solvent recovery device based on macroporous resin adsorption according to claim 5, characterized in that: The top of the shell (1) is connected to a steam pipe (10), the bottom of the shell (1) is connected to one end of a first pipe (5), the other end of the first pipe (5) is connected to the top of a condenser (9), the bottom of the condenser (9) is connected to one end of a second pipe (24), the other end of the second pipe (24) is connected to a stratification device (7), the two sides of the stratification device (7) are symmetrically connected to one end of a third pipe, and the other ends of the two groups of third pipes are respectively connected to a solvent tank (6) and a wastewater tank (8).

7. A solvent recovery device based on macroporous resin adsorption according to claim 6, characterized in that: The top of the workbench (4) is connected to a condenser (9), a layering device (7), a solvent tank (6) and a waste water tank (8).

8. A solvent recovery device based on macroporous resin adsorption according to claim 7, characterized in that: A door (3) is installed at the opening of the shell (1).

Citation Information

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