Production process of photosensitive monomer material

Abstract

The invention provides a photosensitive monomer material production technology, and relates to the technical field of photosensitive monomer material production, and the photosensitive monomer material production technology comprises the following steps: S1, solution regulation: firstly taking deionized water and photosensitive resin, diluting the deionized water and the photosensitive resin into a 40-200ml / l working solution during use, then measuring the pH value by using an acidimeter, then regulating the pH value, then taking acrylamide and diacetone acrylamide, and carrying out uniform stirring; compared with a traditional photosensitive monomer material, the photosensitive monomer material has the advantages that the sensitivity / granularity, definition and hierarchy of the obtained photosensitive monomer material can be improved by adding the silver halide emulsion, and the sensitivity / granularity, definition and hierarchy of the obtained photosensitive monomer material can be improved by adding the plasticizer, so that the sensitivity / granularity, definition and hierarchy of the obtained photosensitive monomer material can be improved, and the sensitivity / granularity, definition and hierarchy of the obtained photosensitive monomer material can be improved. The composite material weakens the acting force between polymer molecules, reduces the melting temperature and melt viscosity, improves the molding processability, endows the plastic product with flexibility and other various necessary properties within the use temperature range, and is low in manufacturing cost and suitable for large-scale production of enterprises.

Description

technical field

[0001] The invention relates to the technical field of production of photosensitive monomer materials, in particular to a production process of photosensitive monomer materials. Background technique

[0002] Photosensitive material refers to a semiconductor material with photosensitive properties, so it is also called photoconductive material or photosensitive semiconductor. Commonly used photosensitive materials on copiers are: organic photosensitive drum (OPC), amorphous silicon photosensitive drum, cadmium sulfide photosensitive drum and selenium photosensitive drum. In addition, photosensitive materials are often used in photography. There are many varieties of photosensitive materials, which are generally classified according to their uses, supports and color-sensing properties. Acrylamide-diacetone acrylamide copolymer is a new type of water-soluble that has developed rapidly internationally in recent years. Sexual functional polymer materials, but thi...

Examples

Embodiment 1

[0022] Example 1, please refer to figure 1 , the present invention provides a technical scheme: the production process of the photosensitive monomer material, comprising the following steps:

[0023] S1: Solution adjustment, first take deionized water and photosensitive resin, dilute to 155ml / l working solution when using, then measure pH with acidity meter, then adjust pH, then take acrylamide and diacetone acrylamide, after obtaining the acrylamide and diacetone acrylamide in conditioned deionized water:

[0024] S2: Mixing reaction, then weigh the initiator and add it into the reaction kettle, and gradually increase the temperature of the reaction kettle itself, and keep it for 4 hours. After the maintenance, the initiator is added to the reaction kettle again, and the polymerization operation is carried out for 10 hours to obtain the photosensitive polymer:

[0025] S3: Fine treatment, then add defoaming agent to the reaction kettle, and continuously defoaming the solutio...

Embodiment 2

[0035] Example 2, please refer to figure 1 , the present invention provides a technical scheme: the production process of the photosensitive monomer material, comprising the following steps:

[0036] S1: Solution adjustment, first take deionized water and photosensitive resin, dilute to 120ml / l working solution when using, then measure pH with acidity meter, then adjust pH, then take acrylamide and diacetone acrylamide, after obtaining acrylamide and diacetone acrylamide in conditioned deionized water:

[0037] S2: Mixing reaction, then weigh the initiator and add it to the reaction kettle, and gradually increase the temperature of the reaction kettle itself, and keep it for 3 hours. After the maintenance, the initiator is added to the reaction kettle again, and the polymerization operation is carried out for 8 hours to obtain the photosensitive polymer:

[0038] S3: Fine treatment, then add defoaming agent to the reaction kettle, and continuously defoaming the solution in th...

Embodiment 3

[0048] Example three, please refer to figure 1 , the present invention provides a technical scheme: the production process of the photosensitive monomer material, comprising the following steps:

[0049] S1: Solution adjustment, first take deionized water and photosensitive resin, dilute to 200ml / l working solution when using, then measure pH with acidity meter, then adjust pH, then take acrylamide and diacetone acrylamide, after obtaining the acrylamide and diacetone acrylamide in conditioned deionized water:

[0050] S2: Mixing reaction, then weigh the initiator and add it to the reaction kettle, and gradually increase the temperature of the reaction kettle itself, and keep it for 4 hours. After holding, the initiator is added to the reaction kettle again, and the polymerization operation is carried out for 8 hours to obtain the photosensitive polymer:

[0051] S3: Fine treatment, then add defoaming agent to the reaction kettle, and continuously defoaming the solution in th...

technical field

[0001] The invention relates to the technical field of production of photosensitive monomer materials, in particular to a production process of photosensitive monomer materials. Background technique

[0002] Photosensitive material refers to a semiconductor material with photosensitive properties, so it is also called photoconductive material or photosensitive semiconductor. Commonly used photosensitive materials on copiers are: organic photosensitive drum (OPC), amorphous silicon photosensitive drum, cadmium sulfide photosensitive drum and selenium photosensitive drum. In addition, photosensitive materials are often used in photography. There are many varieties of photosensitive materials, which are generally classified according to their uses, supports and color-sensing properties. Acrylamide-diacetone acrylamide copolymer is a new type of water-soluble that has developed rapidly internationally in recent years. Sexual functional polymer materials, but thi...

Examples

Embodiment 1

[0022] Example 1, please refer to figure 1 , the present invention provides a technical scheme: the production process of the photosensitive monomer material, comprising the following steps:

[0023] S1: Solution adjustment, first take deionized water and photosensitive resin, dilute to 155ml / l working solution when using, then measure pH with acidity meter, then adjust pH, then take acrylamide and diacetone acrylamide, after obtaining the acrylamide and diacetone acrylamide in conditioned deionized water:

[0024] S2: Mixing reaction, then weigh the initiator and add it into the reaction kettle, and gradually increase the temperature of the reaction kettle itself, and keep it for 4 hours. After the maintenance, the initiator is added to the reaction kettle again, and the polymerization operation is carried out for 10 hours to obtain the photosensitive polymer:

[0025] S3: Fine treatment, then add defoaming agent to the reaction kettle, and continuously defoaming the solutio...

Embodiment 2

[0035] Example 2, please refer to figure 1 , the present invention provides a technical scheme: the production process of the photosensitive monomer material, comprising the following steps:

[0036] S1: Solution adjustment, first take deionized water and photosensitive resin, dilute to 120ml / l working solution when using, then measure pH with acidity meter, then adjust pH, then take acrylamide and diacetone acrylamide, after obtaining acrylamide and diacetone acrylamide in conditioned deionized water:

[0037] S2: Mixing reaction, then weigh the initiator and add it to the reaction kettle, and gradually increase the temperature of the reaction kettle itself, and keep it for 3 hours. After the maintenance, the initiator is added to the reaction kettle again, and the polymerization operation is carried out for 8 hours to obtain the photosensitive polymer:

[0038] S3: Fine treatment, then add defoaming agent to the reaction kettle, and continuously defoaming the solution in th...

Embodiment 3

[0048] Example three, please refer to figure 1 , the present invention provides a technical scheme: the production process of the photosensitive monomer material, comprising the following steps:

[0049] S1: Solution adjustment, first take deionized water and photosensitive resin, dilute to 200ml / l working solution when using, then measure pH with acidity meter, then adjust pH, then take acrylamide and diacetone acrylamide, after obtaining the acrylamide and diacetone acrylamide in conditioned deionized water:

[0050] S2: Mixing reaction, then weigh the initiator and add it to the reaction kettle, and gradually increase the temperature of the reaction kettle itself, and keep it for 4 hours. After holding, the initiator is added to the reaction kettle again, and the polymerization operation is carried out for 8 hours to obtain the photosensitive polymer:

[0051] S3: Fine treatment, then add defoaming agent to the reaction kettle, and continuously defoaming the solution in th...

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